CN105088757A - Preparation method of printing and dyeing finishing agent used for fabric - Google Patents
Preparation method of printing and dyeing finishing agent used for fabric Download PDFInfo
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- CN105088757A CN105088757A CN201510590491.4A CN201510590491A CN105088757A CN 105088757 A CN105088757 A CN 105088757A CN 201510590491 A CN201510590491 A CN 201510590491A CN 105088757 A CN105088757 A CN 105088757A
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Abstract
The invention discloses a preparation method of a printing and dyeing finishing agent used for fabric. The preparation method includes the steps that 1, sodium sulfate, coconut oil die thanolamide, 3-glyceraldehydes phosphate dehydrogenase, palmitic acid and sodium oleate are taken and added into pure water to prepare a water solution; 2, sulphate of ricinoleic acid butyl ester, polyethylene glycol dilaurate, aluminum oxide, titanium dioxide and p-hydroxyphenylacetyl chloride are added into glycerin, and a glycerin solution is prepared at 40-60 DEG C; 3, the water solution and the glycerin solution are mixed, polysorbate 80 and glycerin monostearate are added, and then the printing and dyeing finishing agent is obtained through stirring. Compared with the prior art, the preparation method is simple in technology and low in cost, and the prepared printing and dyeing finishing agent used for the fabric can obviously improve the tensile property and abrasion resistance of the fabric and be suitable for different kinds of fabric, and is wide in application range and excellent in property.
Description
Technical field
The present invention relates to the preparation method of a kind of fabric printing and dyeing finishing agent, belong to printing and dyeing field of material technology.
Background technology
Arrangement is by physical action or uses chemical agent to improve the outward appearance such as gloss, form of fabric; Improve the wearability of fabric or fabric had refuse water, refuse wet goods characteristic.Textile finishing is on fabric, apply a kind of finishing agent, and it can change the surface property of fabric, thus gives fabric special function.Such as hydrophobic and oil repellent arranges is the finishing agent process fabric with low surface tension, changes the surface characteristic of fiber, makes fabric face not easily by water or oily wetting and spreading, thus reach the object of hydrophobic and oil repellent.Soil resistant finish and soil-releasing finiss are by changing the surface property of fiber or surface state, make fabric not easily attach dirt under dress, service condition, or are easy to by the dirt attached wash and the processing technology of no longer staiing.In dyeing process, multiplex to various printing and dyeing agent, but the injury of existing finishing agent multipair fabric is comparatively large, and the fabric after process cannot meet need of production.
At present, the research of existing a large amount of printing and dyeing finishing agent in prior art, although can strengthen fabric abrasion resistance, stretch resistance, washability etc. all to a certain extent, but also there are some defects, as preparation technology is common process, gained printing and dyeing finishing agent range of application is little, is only suitable for certain fabric; The effect such as ABRASION RESISTANCE, stretch resistance is not satisfactory.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the invention provides the preparation method of a kind of fabric printing and dyeing finishing agent.
Technical scheme: for achieving the above object, the invention provides the preparation method of a kind of fabric printing and dyeing finishing agent, comprises the following steps:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 40-60 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, stir, to obtain final product.
As preferably, in described step (3), stirring condition is: temperature 40-60 DEG C, 3000-5000r/min stir 10-20h.
Preferred as another kind, wherein the weight ratio of each raw material is as follows:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 20-40 part, sodium sulphate 1-9 part, cocounut oil diglycollic amide 10-30 part, alundum (Al2O3) 2-8 part, glyceraldehyde 3-phosphate dehydro-genase 5-15 part, palmitic acid 1-7 part, enuatrol 2-10 part, titanium dioxide 1-5 part, para hydroxybenzene chloroacetic chloride 4-16 part, Tween 80 0.1-0.7 part, glycerin monostearate 0.2-0.6 part.
Preferred as another kind, wherein the weight ratio of each raw material is as follows:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 25-35 part, sodium sulphate 2-8 part, cocounut oil diglycollic amide 15-25 part, alundum (Al2O3) 4-6 part, glyceraldehyde 3-phosphate dehydro-genase 8-12 part, palmitic acid 3-5 part, enuatrol 4-8 part, titanium dioxide 2-4 part, para hydroxybenzene chloroacetic chloride 8-12 part, Tween 80 0.2-0.6 part, glycerin monostearate 0.3-0.5 part.
Preferred as another kind, wherein the weight ratio of each raw material is as follows:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 30 parts, 5 parts, sodium sulphate, cocounut oil diglycollic amide 20 parts, alundum (Al2O3) 5 parts, glyceraldehyde 3-phosphate dehydro-genase 10 parts, palmitic acid 4 parts, enuatrol 6 parts, titanium dioxide 3 parts, para hydroxybenzene chloroacetic chloride 10 parts, Tween 80 0.4 part, glycerin monostearate 0.4 part.
Preferred as another kind, the weight ratio of the sulfuric ester of described pure water and castor oil acid butyl ester is (100-200): 40.
Preferred as another kind, the weight ratio of the sulfuric ester of described glycerine and castor oil acid butyl ester is (70-90): 40.
Preferred as another kind, described fabric is sodolin, all-silk goods, woolen fabric, dacron or COTTON FABRIC.
Beneficial effect: compared with prior art, preparation method's technique of the present invention is simple, and cost is low, gained fabric printing and dyeing finishing agent can not only significantly improve stretch-proof performance and the anti-wear performance of fabric, and different types of fabric can also be applicable to, applied range, excellent performance.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further described.
Embodiment 1
Prescription:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 20 parts, 1 part, sodium sulphate, cocounut oil diglycollic amide 10 parts, alundum (Al2O3) 2 parts, glyceraldehyde 3-phosphate dehydro-genase 5 parts, palmitic acid 1 part, enuatrol 2 parts, titanium dioxide 1 part, para hydroxybenzene chloroacetic chloride 4 parts, Tween 80 0.1 part, glycerin monostearate 0.2 part, pure water 100 parts, glycerine 70 parts.
Preparation method:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 40 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, 40 DEG C, 3000r/min stirs 10h, to obtain final product.
Embodiment 2
Prescription:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 40 parts, 9 parts, sodium sulphate, cocounut oil diglycollic amide 30 parts, alundum (Al2O3) 8 parts, glyceraldehyde 3-phosphate dehydro-genase 15 parts, palmitic acid 7 parts, enuatrol 2-10 part, titanium dioxide 5 parts, para hydroxybenzene chloroacetic chloride 16 parts, Tween 80 0.7 part, glycerin monostearate 0.6 part, pure water 200 parts, glycerine 90 parts.
Preparation method:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 60 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, 60 DEG C, 5000r/min stirs 20h, to obtain final product.
Embodiment 3
Prescription:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 30 parts, 5 parts, sodium sulphate, cocounut oil diglycollic amide 20 parts, alundum (Al2O3) 5 parts, glyceraldehyde 3-phosphate dehydro-genase 10 parts, palmitic acid 4 parts, enuatrol 6 parts, titanium dioxide 3 parts, para hydroxybenzene chloroacetic chloride 10 parts, Tween 80 0.4 part, glycerin monostearate 0.4 part, pure water 150 parts, glycerine 80 parts.
Preparation method:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 50 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, 50 DEG C, 4000r/min stirs 15h, to obtain final product.
Embodiment 4
Prescription:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 25 parts, 2 parts, sodium sulphate, cocounut oil diglycollic amide 15 parts, alundum (Al2O3) 4 parts, glyceraldehyde 3-phosphate dehydro-genase 8 parts, palmitic acid 3 parts, enuatrol 4 parts, titanium dioxide 2 parts, para hydroxybenzene chloroacetic chloride 8 parts, Tween 80 0.2 part, glycerin monostearate 0.3 part, pure water 120 parts, glycerine 75 parts.
Preparation method:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 45 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, 45 DEG C, 4000r/min stirs 12h, to obtain final product.
Embodiment 5
Prescription:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 35 parts, 8 parts, sodium sulphate, cocounut oil diglycollic amide 25 parts, alundum (Al2O3) 6 parts, glyceraldehyde 3-phosphate dehydro-genase 12 parts, palmitic acid 5 parts, enuatrol 8 parts, titanium dioxide 4 parts, para hydroxybenzene chloroacetic chloride 12 parts, Tween 80 0.6 part, glycerin monostearate 0.5 part, pure water 180 parts, glycerine 85 parts.
Preparation method:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 55 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, 55 DEG C, 4000r/min stirs 18h, to obtain final product.
Experimental example preparation method's gained printing and dyeing of the present invention finishing agent Performance Detection
Contrasting 1 group is commercially available conventional polyester fabric printing and dyeing finishing agents, is used for finishing of cotton textiles;
Contrasting 2 groups is commercially available conventional polyester fabric printing and dyeing finishing agents, is used for arranging dacron;
Embodiment 3 groups, embodiment 4 groups and embodiment 5 groups are respectively the embodiment of the present invention 3,4 and 5 gained finishing agent, are used for respectively arranging dacron, COTTON FABRIC and sodolin;
Detect the performance of each group of gained fabric according to this area conventional method, testing result is in table 1
The each tissue substance performance test results of table 1
Can be obtained by upper table 1 result, commercially available conventional polyester fabric printing and dyeing finishing agent, the effect of process dacron will obviously be better than processing COTTON FABRIC;
And gained finishing agent of the present invention, be used for process dacron, COTTON FABRIC and sodolin, it can reach substantially suitable effect; And compare contrast 1 group and contrast 2 groups, TENSILE STRENGTH increase rate and ABRASION RESISTANCE increase rate are significantly increased, the fabric stretch-proof performance after process and anti-wear performance excellence.
Claims (8)
1. a fabric preparation method for printing and dyeing finishing agent, is characterized in that, comprise the following steps:
(1) get sodium sulphate, cocounut oil diglycollic amide, glyceraldehyde 3-phosphate dehydro-genase, palmitic acid and enuatrol, join in pure water, make the aqueous solution;
(2) sulfuric ester of castor oil acid butyl ester, polyethylene glycol laurate, alundum (Al2O3), titanium dioxide and para hydroxybenzene chloroacetic chloride, join in glycerine, make glycerite for 40-60 DEG C;
(3) by the above-mentioned aqueous solution and glycerite mixing, add Tween 80 and glycerin monostearate, stir, to obtain final product.
2. the preparation method of fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, in described step (3), stirring condition is: temperature 40-60 DEG C, 3000-5000r/min stir 10-20h.
3. the preparation method of fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, wherein the weight ratio of each raw material is as follows:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 20-40 part, sodium sulphate 1-9 part,
Cocounut oil diglycollic amide 10-30 part, alundum (Al2O3) 2-8 part, glyceraldehyde 3-phosphate dehydro-genase 5-15 part,
Palmitic acid 1-7 part, enuatrol 2-10 part, titanium dioxide 1-5 part, para hydroxybenzene chloroacetic chloride 4-16 part,
Tween 80 0.1-0.7 part, glycerin monostearate 0.2-0.6 part.
4. the preparation method of fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, wherein the weight ratio of each raw material is as follows:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 25-35 part, sodium sulphate 2-8 part,
Cocounut oil diglycollic amide 15-25 part, alundum (Al2O3) 4-6 part, glyceraldehyde 3-phosphate dehydro-genase 8-12 part,
Palmitic acid 3-5 part, enuatrol 4-8 part, titanium dioxide 2-4 part, para hydroxybenzene chloroacetic chloride 8-12 part,
Tween 80 0.2-0.6 part, glycerin monostearate 0.3-0.5 part.
5. the preparation method of fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, wherein the weight ratio of each raw material is as follows:
The sulfuric ester 40 parts of castor oil acid butyl ester, polyethylene glycol laurate 30 parts, 5 parts, sodium sulphate,
Cocounut oil diglycollic amide 20 parts, alundum (Al2O3) 5 parts, glyceraldehyde 3-phosphate dehydro-genase 10 parts,
Palmitic acid 4 parts, enuatrol 6 parts, titanium dioxide 3 parts, para hydroxybenzene chloroacetic chloride 10 parts,
Tween 80 0.4 part, glycerin monostearate 0.4 part.
6. the preparation method of fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, the weight ratio of the sulfuric ester of described pure water and castor oil acid butyl ester is (100-200): 40.
7. the preparation method of fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, the weight ratio of the sulfuric ester of described glycerine and castor oil acid butyl ester is (70-90): 40.
8. fabric printing and dyeing finishing agent according to claim 1, it is characterized in that, described fabric is sodolin, all-silk goods, woolen fabric, dacron or COTTON FABRIC.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510590491.4A CN105088757A (en) | 2015-09-16 | 2015-09-16 | Preparation method of printing and dyeing finishing agent used for fabric |
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| CN201510590491.4A CN105088757A (en) | 2015-09-16 | 2015-09-16 | Preparation method of printing and dyeing finishing agent used for fabric |
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| CN201510590491.4A Pending CN105088757A (en) | 2015-09-16 | 2015-09-16 | Preparation method of printing and dyeing finishing agent used for fabric |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105401438A (en) * | 2015-12-22 | 2016-03-16 | 常熟市博凡针纺织有限公司 | Dyeing and finishing process of knitted fabrics |
| CN106758248A (en) * | 2016-12-16 | 2017-05-31 | 吴江市北厍盛源纺织品助剂厂 | A kind of textile auxiliary for improving cloth abrasion degree and preparation method thereof |
| CN109594334A (en) * | 2018-10-17 | 2019-04-09 | 徐州华奥纺织有限公司 | A kind of fabric printing finishing agent and preparation method thereof |
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| CN103147279A (en) * | 2013-03-26 | 2013-06-12 | 无锡新德印染制品有限公司 | Printing and dyeing finishing agent |
| CN104358121A (en) * | 2014-11-28 | 2015-02-18 | 杨帆 | Pre-dyeing auxiliary agent for finishing full-real-silk textile |
| CN104389163A (en) * | 2014-11-28 | 2015-03-04 | 杨帆 | Printing and dyeing pretreatment aid for woolen fabric finishing |
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2015
- 2015-09-16 CN CN201510590491.4A patent/CN105088757A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103147279A (en) * | 2013-03-26 | 2013-06-12 | 无锡新德印染制品有限公司 | Printing and dyeing finishing agent |
| CN104358121A (en) * | 2014-11-28 | 2015-02-18 | 杨帆 | Pre-dyeing auxiliary agent for finishing full-real-silk textile |
| CN104389163A (en) * | 2014-11-28 | 2015-03-04 | 杨帆 | Printing and dyeing pretreatment aid for woolen fabric finishing |
Non-Patent Citations (1)
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| 王展印 等: "新型纺织印染后整理剂AL—12", 《山西化工》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105401438A (en) * | 2015-12-22 | 2016-03-16 | 常熟市博凡针纺织有限公司 | Dyeing and finishing process of knitted fabrics |
| CN106758248A (en) * | 2016-12-16 | 2017-05-31 | 吴江市北厍盛源纺织品助剂厂 | A kind of textile auxiliary for improving cloth abrasion degree and preparation method thereof |
| CN109594334A (en) * | 2018-10-17 | 2019-04-09 | 徐州华奥纺织有限公司 | A kind of fabric printing finishing agent and preparation method thereof |
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Application publication date: 20151125 |