CN105908525A - Waterproof, oil-proof and stain-proof garment fabric with durability and effect of easily removing stains and preparation method thereof - Google Patents

Waterproof, oil-proof and stain-proof garment fabric with durability and effect of easily removing stains and preparation method thereof Download PDF

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Publication number
CN105908525A
CN105908525A CN201610492506.8A CN201610492506A CN105908525A CN 105908525 A CN105908525 A CN 105908525A CN 201610492506 A CN201610492506 A CN 201610492506A CN 105908525 A CN105908525 A CN 105908525A
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agent
proof
fabric
preparation
finishing agent
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CN201610492506.8A
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Inventor
程飞
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Hefei Yundu Cotton Co Ltd
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Hefei Yundu Cotton Co Ltd
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Priority to CN201610492506.8A priority Critical patent/CN105908525A/en
Publication of CN105908525A publication Critical patent/CN105908525A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M23/00Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/0032Determining dye recipes and dyeing parameters; Colour matching or monitoring
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642Compounds containing nitrogen
    • D06P1/649Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6491(Thio)urea or (cyclic) derivatives
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673Inorganic compounds
    • D06P1/67333Salts or hydroxides
    • D06P1/6735Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/01Stain or soil resistance
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10Repellency against liquids
    • D06M2200/11Oleophobic properties
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10Repellency against liquids
    • D06M2200/12Hydrophobic properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention relates to a waterproof, oil-proof and stain-proof garment fabric with durability and the effect of easily removing stains. The garment fabric is characterized in that the water seepage resistance is not less than 10cmH2O; the oil repellency reaches level five; the effect of easily removing stains is above level four; the water/ethanol solution resistance is not less than level seven; the PH value is 6-7. The garment fabric has the advantages that the fabric surface is provided with a layer of functional polymer film, so the fabric has better waterproof and oil-proof effects and is not easily stained by solid dirt; the dirt is easily washed out in water after the fabric is stained; the fabric not only has the waterproof, oil-proof and stain-proof functions but also has the effect of easily removing stains as the dirt is easily washed out after the fabric is stained.

Description

A kind of durable waterproof, grease proofing, antifouling and easy decontamination garment material and preparation method thereof
Technical field
The present invention relates to a kind of durable waterproof, grease proofing, antifouling and easy decontamination garment material and preparation method thereof, especially The production of industrial enterprise's garment materials such as machine-building, maintenance of equipment, automobile industry can be widely used in.
Background technology
In current society, water, oil are the dirts that the fabrics such as the garment material of people are common in daily life and work Dye thing, the particularly fabric used in the environment that some are special, it is easier to stained by the dirt such as water, oil, such as machinery The industry such as manufacture, maintenance of equipment, automobile industry, this just proposes new performance requirement to textile.And it is Water-proof and oil-proof, antifouling Textile be possible to prevent oiliness pollutant and aqueous stain to stain, and through arrangement after textile change original hardly The style of textile, does not produce fabric damage and spot.In nature, the structural property of super-hydrophobicity plant result in them Self-purification capacity, this ability is referred to as " lotus leaf effect ".
At present, the three anti-protective garments used in a lot of industries all make protective garment with the composite such as nylon, terylene, Although these materials also exist certain Water-proof and oil-proof, antifouling characteristic, it is all to have passed through coating to process due to them, thus Inevitably make that the protective garment made is thick and heavy, ventilative, water vapour permeability is poor, can feel hot and uncomfortable at aspect comfortable and easy to wear, Not only influence whether work task efficiency, and likely jeopardize their healthy.
Summary of the invention
The problem to be solved in the present invention is for above not enough, it is provided that a kind of durable waterproof, grease proofing, antifouling and easy decontamination Garment material, this garment material has Water-proof and oil-proof, an antifouling function, and after staining, dirt is washable removes.
It is a further object of the present invention to provide the preparation method of more than one garment materials, use clothes prepared by the method Fabric Water-proof and oil-proof, antifouling and easy decontamination and good endurance.
For solving above technical problem, the present invention by the following technical solutions: a kind of durable waterproof, grease proofing, antifouling and Easily decontamination garment material, it is characterised in that: described garment material water permeability resistance energy >=more than 10cmH2O, oil repellency reaches 5 Level, easy clean effect reaches more than 4 grades, water resistant/ethanol solution >=7 grade, pH value 6-7.
Based on above garment material, the present invention provides the preparation method of a kind of garment material, described preparation method to include leaching Padding liquor step, with dyeing liquor to textile dyeing;
Described dyeing liquor includes dyestuff 2-4%(o.w.f), urea 20-50g/L, wetting agent 1-2g/L, glauber salt 30-60g/L, even Stain 1-2g/L and alkaline agent 1-3g/L;
Padding dye liquor when first by dyestuff according to color modulation formula, carry out soluble in water for deployed dyestuff sufficiently Stirring, in making dyestuff completely soluble, then rises to 30 DEG C by water temperature, and heating rate per minute is 1-2 DEG C, and temperature rises to 30 DEG C Time, levelling agent is added in dye liquor, adding water temperature after levelling agent according to the speed of intensification per minute 1 DEG C be by dye liquor intensification To 35 DEG C, then urea, wetting agent, glauber salt are sequentially added into dye liquor.Then by dye liquor temperature according to the liter of 2-3 DEG C per minute Temperature speed rises to 60 DEG C, adds alkaline agent, it is noted that add in three times the when of addition alkaline agent, and every minor tick 2 minutes, add alkali After agent, temperature rising to 80 DEG C, heating rate is 2-3 DEG C.Finally open and make fabric is dyeed.
In actual production, inventor finds the pattern phenomenon using above method can effectively reduce fabric, makes dyeing More uniform, improve water-fastness color fastness and the colorfastness to rubbing of fabric, reduce the infringement to fabric of the various auxiliary agent.
Through analysis of experiments: be sufficiently stirred for and be warming up to 30 DEG C by soluble in water for dyestuff, the dissolving of dyestuff in water can be accelerated Speed, does not the most make dyestuff enliven, and heating rate per minute is 1-2 DEG C, when temperature rises to 30 DEG C, is unlikely to make the too fast destruction of intensification The molecular structure of dyestuff.By water temperature according to the speed of intensification per minute 1 DEG C for dye liquor is warming up to 35 DEG C;Can make in dye liquor The molecule of molecule and levelling agent sufficiently combines, the active degree of the molecule in minimizing dye liquor.By dye liquor temperature according to per minute The heating rate of 2-3 DEG C rises to 60 DEG C of molecules making various auxiliary agent and is combined with dye liquor very smoothly, plays its various auxiliary agents Effect, three additions of alkaline agent are possible to prevent dye liquor reflection acutely, destroy its molecular structure and cause dyeing pattern.Temperature is risen to 80 DEG C, heating rate is 2-3 DEG C/min, after making various auxiliary agent fully combine, by temperature rising to 80 DEG C and make in dye liquor slowly Color molecule is the most active, inside upper dye to fibr tissue, and the most permanent fiber being adsorbed onto fabric In.
Inventor also finds, in process above, application urea, glauber salt and wetting agent can make fabric quickly soak The fiber molecule making the quick fabric of dye molecule merges,
A kind of prioritization scheme, described preparation method also includes padding finishing agent step, dyed fabric is carried out finishing functions;
Described finishing agent includes bleeding agent 2-5g/L, crosslinking agent 10-15g/L, softening agent 10-40g/L, three-proof finishing agent 20- 60g/L and soil-releasing finishing agent 40-50g/L;
First requiring to carry out mixing (ratio of generally mixing with is 10:1) according to technology by three-proof finishing agent and bleeding agent, addition dips Temperature is risen to 40 DEG C by groove, and heating rate is 3-5 DEG C per minute, then by crosslinking agent and soil-releasing finishing agent according to technology require into Row mixing (ratio of generally mixing with is 4:1) adds pressure rolling groove and simultaneously the most also temperature is risen to 60 DEG C, and heating rate is 3-5 per minute DEG C, it is warming up to when 50 DEG C be added thereto by softening agent again, after having carried out process above process, its pick-up controls at 50%-80%, The most again by 80-100 DEG C of drying, drying time is 3-5min.
In actual production, it is soft that inventor chances on employing above method gained fabric, ventilative, moisture permeable effect Good, it still can kept functional after 50 washings.
Through analysis of experiments: temperature rises to 40 DEG C, heating rate is 3-5 DEG C per minute can make three-proof finishing agent and bleeding agent Combining of quick and stable, it is possible to make three-proof finishing agent quickly penetrate into fibrous inside and be combined with fiber molecule, by temperature Degree rises to 60 DEG C and makes that three-proof finishing agent and osmotic agent solution molecule are more active adds crosslinking agent and soil-releasing finishing agent, makes Its molecular structure preferably combines, and the pick-up of 50%-80% makes various finishing agent preferably combine with fabric, makes arrangement Each molecule of agent is sufficiently attached to above face liber, through 3-5min80-100 DEG C of drying, quickly evaporates finishing agent Moisture in solution, the molecule retaining its finishing agent is preferably attached to above face liber, plays the persistence of its function.Hand over Connection agent promotes the combination of three-proof finishing agent and soil-releasing finishing agent and face liber molecule, more preferably keeps the function of its fabric.
Further, described three-proof finishing agent is FG-910, and soil-releasing finishing agent is FG-979.In actual production, send out A person of good sense finds that the finishing agent of both the above model is best with the use of effect.
Further, in described padding finishing agent step, pick-up 50%-80%.Find after test: 50%-80% rolls Fiber is made to reach optimal band liquid saturation state under remaining rate.
Further, described fabric through preparing grey cloth, grey cloth and boil, practices, floating, after mercerising entrance pad dye liquor step, then Drying, decatize/bake, wash, soap, wash, dry after enter and pad functional finishing agent step, then through preshrunk, dry, roast Baking, rolling step, obtain Water-proof and oil-proof, antifouling and easy decontamination garment material.
Further, described drying: 80-100 DEG C of time is 3-5min;
Preliminary drying: 100-110 DEG C, the time be 1-2min, to containing tide rate 30%-40%.Finishing agent adheres to uniformly in face liber.
Through test post analysis: 100-110 DEG C, the time be that the preliminary drying of 1-2min makes to exist in fabric a certain amount of moisture and whole Reason agent be both molecule slowly be uniformly adhered in the middle of face liber so that it is be unlikely to that temperature in drying course is too high to be made What the molecule of both was the most uneven is attached in the middle of face liber, causes pattern and migration phenomenon, and temperature is the lowest to be likely to Pattern and migration phenomenon occur, loses time finally to increase the generation of substandard products.Process above condition is optimal selection.
Further, baking temperature be 160-180 DEG C, the time be 1-3min.Through test post analysis: 160-180 DEG C of time Can quickly dry the moisture in fabric for 1-3min, reduce finishing agent and the destruction of fabric molecule, the outward appearance of fabric and The impact of feel, if temperature height fabric can turn to be yellow, the bad meeting of hardening control causes fire, and temperature is the lowest loses time, and is fabric There is damp.The decline of its quality can be caused.
The present invention uses above technical scheme, compared with prior art, has the advantage that by using above-mentioned manufacture work Skill, the product of the present invention is a kind of durable waterproof, grease proofing, antifouling and easy decontamination garment material, and preparation method employing is padded Method, by three-proof finishing agent with soil-releasing finishing agent with bath, applies to fabric, then by drying and baking, is allowed to obtain forever The Water-proof and oil-proof of property, antifouling and decontaminable effect for a long time.Make fabric face form a layer function polymeric membrane, have preferably Water-proof and oil-proof effect, it is not easy to stain solid dirt, and after fabric tarnishes, the most easily by eccysis in water. Not only there are Water-proof and oil-proof, an antifouling function, and dirt is washable after staining removes, there is decontaminable effect, can use widely Production in industrial enterprise's garment materials such as machine-building, maintenance of equipment, automobile industries.
Below in conjunction with embodiment, the present invention is described in detail.
Specific embodiment
Should be appreciated that preferred embodiment described herein is merely to illustrate and explains the present invention, be not intended to limit the present invention.
Embodiment 1, a kind of durable waterproof, grease proofing, antifouling and easy decontamination garment material preparation method, step includes:
Prepare grey cloth → grey cloth boil, practice, float, mercerising → pad dye liquor → drying → decatize or bake → wash → soap → wash → dry → pad functional finishing agent → preshrunk → dry → bake → rolling
A, preparation grey cloth: include grey cloth inspection, turn over cloth, margin to seam;
B, grey cloth boil, practice, float, mercerising: the garment material as raw material is singed, desizing, mercerization finish, remove fabric and spin Slurry during yarn and unnecessary finish;
C, pad dye liquor: with dyeing liquor to textile dyeing, dyeing liquor includes dyestuff 2-4%(o.w.f), urea 20-50g/L, wetting Agent 1-2g/L, glauber salt 30-60g/L, levelling agent 1-2g/L, alkaline agent 1-3g/L;
Padding dye liquor when first by dyestuff according to color modulation formula, carry out soluble in water for deployed dyestuff sufficiently Stirring, in making dyestuff completely soluble, then rises to 30 DEG C by water temperature, and heating rate per minute is 1-2 DEG C, and temperature rises to 30 DEG C Time, levelling agent being added in dye liquor, the molecular chaperones of stabilizing dye can make it more stable be attached in the middle of fabric, adds After levelling agent by water temperature according to the speed of intensification per minute 1 DEG C for dye liquor is warming up to 35 DEG C, then will cry urea, wetting Agent, glauber salt are sequentially added into dye liquor, urea and wetting agent and fabric can be made quickly to soak make the quick fabric of dye molecule Fiber molecule merges, and glauber salt can enable dye molecule preferably be combined with the fiber molecule of fabric.Then by dye liquor temperature Degree rises to 60 DEG C according to the heating rate of 2-3 DEG C per minute, adds alkaline agent, it is noted that add in three times the when of addition alkaline agent Enter, every minor tick 2 minutes, prevent from adding the molecular structure of too fast other auxiliary agent of destruction.Add alkaline agent can make to promote dyestuff more Good anchors at fibrous inside, after adding alkaline agent, temperature rises to 80 DEG C, and heating rate is 2-3 DEG C.Finally open and make fabric Dye.
Through long lot of experiments, after using process above condition, can effectively reduce the pattern phenomenon of fabric, make dye Look more uniform, improves water-fastness color fastness and the colorfastness to rubbing of fabric, reduces the infringement to fabric of the various auxiliary agent.
Dyestuff: Shanghai ten thousand obtains dyestuff Shanghai Wan get Dye Co., Ltd
Urea: urea Shandong alliance Chemical Group
Wetting agent: wetting agent jfc Beijing Jie Ershuan High Seience Technology Co., Ltd.
Glauber salt: anhydrous sodium sulfate Jiangsu south wind Chemical Co., Ltd.
Alkaline agent: sodium carbonate (soda ash) Shandong Hai Hua limited company
Levelling agent: Binzhou auxiliary reagent factory, peregal os-15 Shandong
Pad the fabric after dye liquor, through drying → decatize or bake → wash → soap → wash → dry;
Through test of many times, prescription of its dyeing liquor is: dyestuff 3%(o.w.f), urea 30 g/L, wetting agent 2g/L, glauber salt 40g/L, Levelling agent 1.5g/L, alkaline agent 2g/L are preferred value, and the every technical performance index of product prepared during this formula is optimum;
D, pad functional finish: dyed fabric is carried out finishing functions;
Described finishing agent includes bleeding agent 2-5g/L, crosslinking agent 10-15g/L, softening agent 10-40g/L, three-proof finishing agent 20- 60g/L and soil-releasing finishing agent 40-50g/L;
First requiring to carry out mixing (ratio of generally mixing with is 10:1) according to technology by three-proof finishing agent and bleeding agent, addition dips Temperature is risen to 40 DEG C by groove, and heating rate is 3-5 DEG C per minute, and certain temperature that is blended in of three-proof finishing agent and infiltration affects Under, it is possible to make three-proof finishing agent quickly penetrate into fibrous inside and be combined with fiber molecule, the most first by crosslinking agent and easy decontamination Finishing agent requires to carry out mixing (ratio of generally mixing with is 4:1) according to technology and adds pressure rolling groove and the most also temperature is risen to 60 DEG C, heating rate is 3-5 DEG C per minute, is warming up to when 50 DEG C be added thereto by softening agent again, crosslinking agent can promote three prevent whole Managing the combination of agent and soil-releasing finishing agent and face liber molecule, more preferably keep the function of its fabric, being eventually adding softening agent can So that fabric is more soft improves feel comfort, after having carried out process above process, its pick-up controls at 50%-80%, so After again by 80-100 DEG C of drying, drying time is 3-5min.Finally make fabric soft, ventilative, moisture permeable effect is good, It still can kept functional after 50 washings.
Through long-term lot of experiments, the formula of finishing agent: bleeding agent 3g/L, crosslinking agent 12g/L, softening agent 30g/L, three Anti-finishing agent 40g/L, soil-releasing finishing agent 45g/L are preferred value, and the every technical performance index of product prepared during this formula is Excellent;
Described three-proof finishing agent is FG-910, and soil-releasing finishing agent is FG-979, FG-910 and FG-979 and other arrangement Agent is Beijing Jie Ershuan High Seience Technology Co., Ltd. and produces;
The technical process of padding finishing agent and process conditions are:
Pad the functional finishing agent of above ratio mixing, control pick-up 70%;Padding finishing agent, uses an immersing and rolling mode, i.e. Soak once, pressure rolling once, then through preshrunk, makes Water-proof and oil-proof, antifouling and easy decontamination garment material;
Pad the fabric after functional finishing agent, dry, dry temperature 80 DEG C, time 2min;
Then bake, baking temperature 150 DEG C, time 2min;
E, rolling
The fabric put in order is carried out clot, prepares durable waterproof, grease proofing, antifouling and easy decontamination garment material.
By using above-mentioned manufacturing process, the product of preparation is a kind of durable waterproof, grease proofing, antifouling and easy decontamination clothes Fabric, preparation method uses the method padded, and by three-proof finishing agent with soil-releasing finishing agent with bath, applies to fabric, then leads to Cross and dry and bake, be allowed to obtain permanent Water-proof and oil-proof, antifouling and decontaminable effect, make fabric face form one layer Functional copolymer membrane, has preferable Water-proof and oil-proof effect, it is not easy to stain solid dirt, and after fabric tarnishes, The most easily by eccysis in water, the product therefore prepared not only has Water-proof and oil-proof, antifouling function, and after staining Dirt is washable to be removed, and has decontaminable effect, can be widely used in the industrial enterprises such as machine-building, maintenance of equipment, automobile industry The production of garment material.
Unless there are specified otherwise, the percentage related to when proportioning is mass percent.
After testing: fabric water permeability resistance energy >=more than the 10cmH2O after arrangement, oil repellency reaches 5 grades, easy clean effect Reaching more than 4 grades, water resistant/ethanol solution >=7 grade, pH value 6-7, formaldehydeless and aromatic amine residue, free from extraneous odour is stingless to skin Swash.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention, Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent. All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's Within protection domain.

Claims (8)

1. a durable waterproof, grease proofing, antifouling and easy decontamination garment material, it is characterised in that: the impervious water of described garment material Performance >=10cmH2O, oil repellency reaches 5 grades, and easy clean effect reaches more than 4 grades, water resistant/ethanol solution >=7 grade, pH value 6- 7。
2. durable waterproof, the preparation method of grease proofing, antifouling and easy decontamination garment material as claimed in claim 1, its feature exists In: described preparation method includes padding dye liquor step, with dyeing liquor to textile dyeing;
Described dyeing liquor includes dyestuff 2-4%(o.w.f), urea 20-50g/L, wetting agent 1-2g/L, glauber salt 30-60g/L, even Stain 1-2g/L and alkaline agent 1-3g/L;
Being sufficiently stirred for soluble in water for dyestuff, then water temperature rises to 30 DEG C, heating rate per minute is 1-2 DEG C, temperature When rising to 30 DEG C, levelling agent is added in dye liquor, add water temperature after levelling agent according to the speed of intensification per minute 1 DEG C for will Dye liquor is warming up to 35 DEG C;
Then urea, wetting agent, glauber salt are sequentially added into dye liquor, then dye liquor temperature is fast according to the intensification of 2-3 DEG C per minute Rate rises to 60 DEG C, adds alkaline agent, and alkaline agent adds in three times, every minor tick 2 minutes, after adding alkaline agent, temperature is risen to 80 DEG C, heating rate is 2-3 DEG C/min, finally starts to dye fabric.
Preparation method the most according to claim 2, it is characterised in that: described preparation method also includes that padding finishing agent walks Suddenly, dyed fabric is carried out finishing functions;
Described finishing agent includes bleeding agent 2-5g/L, crosslinking agent 10-15g/L, softening agent 10-40g/L, three-proof finishing agent 20- 60g/L and soil-releasing finishing agent 40-50g/L;
Three-proof finishing agent and bleeding agent 10:1 by weight being mixed, addition dips groove and temperature rises to 40 DEG C, heating rate For 3-5 DEG C per minute, crosslinking agent and soil-releasing finishing agent 4:1 by weight are added pressure rolling groove, temperature is risen to 60 simultaneously DEG C, heating rate is 3-5 DEG C per minute, is warming up to when 50 DEG C be added thereto by softening agent, after having carried out process above process again Its pick-up controls at 50%-80%, and the most again by 80-100 DEG C of drying, drying time is 3-5min.
Preparation method the most according to claim 2, it is characterised in that: described three-proof finishing agent is FG-910, and easy decontamination is whole Reason agent is FG-979.
Preparation method the most according to claim 4, it is characterised in that: in described padding finishing agent step, pick-up 50%- 80%。
Preparation method the most according to claim 4, it is characterised in that: described fabric through preparing grey cloth, grey cloth and boil, practice, floating, Enter after mercerising and pad dye liquor step, then drying, decatize/bake, wash, soap, wash, dry after enter and pad function Finishing agent step, then through preshrunk, dry, bake, rolling step, obtain Water-proof and oil-proof, antifouling and easy decontamination garment material.
Preparation method the most according to claim 6, it is characterised in that: described drying: 80-100 DEG C of time is 3-5min;
Preliminary drying: 100-110 DEG C, the time be 1-2min, to containing tide rate 30%-40%.
Preparation method the most according to claim 4, it is characterised in that: baking temperature is 160-180 DEG C, the time is 1- 3min。
CN201610492506.8A 2016-06-29 2016-06-29 Waterproof, oil-proof and stain-proof garment fabric with durability and effect of easily removing stains and preparation method thereof Withdrawn CN105908525A (en)

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* Cited by examiner, † Cited by third party
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CN107794769A (en) * 2017-09-28 2018-03-13 张家港市金陵纺织有限公司 A kind of dyeing and finishing technology of mosquito proof waterproof and oilproof uvioresistant color-woven fabric
CN108411513A (en) * 2018-03-09 2018-08-17 宁波市鄞州凤林纺织整理有限公司 A kind of knitting fabric processing technology
CN111455665A (en) * 2020-06-02 2020-07-28 江苏康乃馨织造有限公司 Washable three-prevention breathable down-proof fabric easy to clean and easy to drill and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107794769A (en) * 2017-09-28 2018-03-13 张家港市金陵纺织有限公司 A kind of dyeing and finishing technology of mosquito proof waterproof and oilproof uvioresistant color-woven fabric
CN108411513A (en) * 2018-03-09 2018-08-17 宁波市鄞州凤林纺织整理有限公司 A kind of knitting fabric processing technology
CN111455665A (en) * 2020-06-02 2020-07-28 江苏康乃馨织造有限公司 Washable three-prevention breathable down-proof fabric easy to clean and easy to drill and preparation method thereof

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