CN109090525A - It is a kind of can oxidation resistant health product capsule and preparation method thereof - Google Patents
It is a kind of can oxidation resistant health product capsule and preparation method thereof Download PDFInfo
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- CN109090525A CN109090525A CN201810818756.5A CN201810818756A CN109090525A CN 109090525 A CN109090525 A CN 109090525A CN 201810818756 A CN201810818756 A CN 201810818756A CN 109090525 A CN109090525 A CN 109090525A
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- squid
- black pigment
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- 235000013619 trace mineral Nutrition 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 229910001428 transition metal ion Inorganic materials 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 230000004304 visual acuity Effects 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/10—Products from fruits or vegetables; Preparation or treatment thereof of tuberous or like starch containing root crops
- A23L19/105—Sweet potatoes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
- A23L33/185—Vegetable proteins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
- A23L5/27—Removal of unwanted matter, e.g. deodorisation or detoxification by chemical treatment, by adsorption or by absorption
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Mycology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
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Abstract
The present invention relates to field of health care food, disclose it is a kind of can oxidation resistant health product capsule and preparation method thereof.The health product capsule includes the material composition of following parts by weight: 15 ~ 25 parts of purple sweet potato powder of curing, and 25~35 parts of squid ink black pigment, 20~30 parts of pearl powder, 10~15 parts of propolis, 5~10 parts of soyabean protein powder, 2.5 ~ 5 parts of vitamin Cs, 1 ~ 2.5 part of citric acid.The preparation methods of the oxidation-resisting health-care product is carried out proportion and is uniformly mixed in parts by weight the following steps are included: (1) pulverizes and sieves above-mentioned each raw material；(2) capsule is filled.The squid ink black pigment added in the present invention has carried out defishying, will not return out fishy smell after edible.This health care product has stronger anti-oxidation efficacy, and nutritive value is high, without side-effects, and preparation step is simple, and cost of material is low, good in economic efficiency.
Description
Technical field
The present invention relates to field of health care food more particularly to a kind of oxidation resistant health product capsule of energy and preparation method thereof.
The squid ink black pigment added in the present invention has carried out defishying, will not return out fishy smell after edible.This health care product has relatively strong
Anti-oxidation efficacy, nutritive value is high, without side-effects, and preparation step is simple, and cost of material is low, good in economic efficiency.
Background technique
Squid ink is to claim in the generation of large biological molecule polymer contained in squid prepared Chinese ink, is that known can uniquely protect life
Native endogenous biopolymer of the object from radiation injury.Contain a variety of biologies such as polypeptide fragments, acidic polysaccharose, tyrosinase
Active constituent.With the characteristic for removing free radical and combination genotoxic potential ion (such as some transition metal ions), application potential
It is huge.Squid ink black pigment is a kind of good free radical scavenger, it can effectively remove hydroxyl radical free radical, oxygen radical etc.
Free radical.Squid ink black pigment has effects that anticancer, oxidation resistant, causes the extensive concern of researcher.
Contain indoles and heterocycle ammonia nitrogenous compound in squid ink black pigment, both ingredients have fishy smell.At present in squid
In the extraction process of fish melanin, common preparation method mainly has centrifugal process, sour water solution, basic hydrolysis and enzymatic isolation method, but prepare
Melanin seldom passes through defishying.The product being so prepared has bad smell, is not suitable for processing and produce, especially
The preparation of food, drug and cosmetics etc..
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of oxidation resistant health product capsule of energy and its preparation sides
Method.
The specific technical proposal of the invention is: a kind of oxidation resistant health product capsule of energy, the original including following parts by weight
Expect ingredient: 15~25 parts of purple sweet potato powder of curing, 25~35 parts of squid ink black pigment, 20~30 parts of pearl powder, 10~15 parts of propolis, greatly
5~10 parts of legumin powder, 2.5~5 parts of vitamin Cs, 1~2.5 part of citric acid.
Compared to tablet, capsule is disintegrated the absorption for being faster more conducive to body to nutrient in the gastrointestinal tract.Compared to
Electuary, capsule can preferably cover the taste of various composition in health care product, and it is edible to facilitate people.The present invention is eaten same using medicine
The property in source, using common food materials such as curing purple sweet potato powder, squid ink black pigment, soyabean protein powder, propolis, using between them
With when coordinated, reach oxidation-resisting health-care effect.
Lysine in purple sweet potato powder, copper, manganese, potassium, zinc content be higher than 3~8 times of general sweet potato, especially anticancer matter iodine,
20 times higher than other sweet potato of the content of selenium or more.The content of selenium element is highest in food in purple sweet potato, is had antifatigue, anti-ageing
Always, the effect of enriching blood, referred to as " anticancer king " can repair cardiac muscle, enhance immunity of organisms, remove interior free yl, suppression
The synthesis of DNA and the division of cancer cell and growth in cancer cell processed, the generation of the cancers such as prevention gastric cancer, liver cancer.Contain in purple sweet potato powder
There is a large amount of anthocyanidin, anthocyanidin is natural potent free radical scavenger, and Scavenging ability is ascorbic 20 times,
50 times of vitamin E, and anthocyanidin have small molecule structure, be it is a kind of can through blood-brain barrier remove free radical protection brain
The substance of cell, while can be reduced antibiotic to some harm of human body.Curing purple sweet potato powder is more advantageous to body to nutrient
Absorption.
Squid ink black pigment can antibacterial, anti-oxidant, be a kind of good free radical scavenger, it can effectively remove hydroxyl
Base free radical, the free radicals such as oxygen radical are that the known native endogenous biology for uniquely protecting organisms from radiation injury is poly-
It is fit.
The main component of pearl powder is protein, and 18 kinds of amino acid can be obtained after hydrolysis, and (wherein 7 kinds are amino needed by human
Acid), the calcium carbonate of aragonite structure, 20 various trace elements and vitamin B.With strengthen immunity, supplement calcium, Bao Chunyan
It declines, improves sleep, treatment ulcer, nourishes the liver to improve visual acuity, secondary buck and other effects.
Containing 70 kinds or more of flavone compound in propolis, have antibacterial, anti-inflammatory, antipruritic, anti-oxidant, enhancing is immune,
The multiple functions such as hypoglycemic, reducing blood lipid, antitumor.Quercetin in propolis also has antineoplastic action, and the rutin in propolis is just
It is rutin, the permeability that capillary can be softened, enhance capillary, moreover it is possible to cholesterol is reduced, to the prevention and treatment heart, the cerebrovascular
It hardens helpful.The taurine contained in propolis has tranquilizing and allaying excitement, adjusts central nervous system, enhancing myocardial contraction, promotees
The effect synthesized into nerve cell protein.Propolis and purple sweet potato powder collocation can enhance the effect of the two prevention cardiovascular and cerebrovascular disease.
Soyabean protein powder contains eight kinds of amino acid needed by human, approximate with meat, fish, egg, milk, belongs to complete protein.
It is very useful in terms of heart health, preventing osteoporosis and alleviating Woman climacteric.In numerous vegetable proteins
In matter, soyabean protein powder nutritive value highest is cholesterol-free, normal physiological demand, the prevention painstaking effort of energy effective guarantee human body
The generation of pipe disease and animal protein can be substituted.Soyabean protein powder and purple sweet potato powder collocation nutrition are more comprehensively.
Vitamin C can promote the synthesis of collagen, prevention of arterial hardening, protect other antioxidants, anti-cancer etc..It is abundant
Collagen help to prevent the diffusion of cancer cell, antioxidation, which can resist free radical, prevents cell to the injury of cell
Variation, while vitamin C can block nitrite and secondary amine to form strong carcinogen nitrosamine.When VC abundance, it can be formed with-SH
Free radical is removed in strong anti-oxidant combination, prevents the toxic action of lipid peroxidation and certain chemical substances, liver-protective
The eubolism of detoxification ability and cell.All contain-SH group in squid ink black pigment, pearl powder, propolis and soyabean protein powder,
It can act synergistically with vitamin C, enhance antioxidant effect.
Citric acid is edible acids, can eubolism in reinforcement.Citric acid is cooperateed with squid ink black pigment can enhance squid
The effect of heavy metal ion in the pitch-dark pigment complexing removal body of fish.
Preferably, the propolis is to obtain after natural propolis purifies to a kind of one kind as oxidation resistant health product capsule of energy
Pure propolis.It is miscellaneous that the propolis without processing directly obtained from beehive contains honeybee limbs, sawdust, silt, burlap fiber etc.
Matter, form are opaque lumps or clastic, are suitable for external application or are used as fodder strengthening agent.Natural propolis is needed by mentioning
It could be edible to human body after pure, removal impurity and heavy metal ion.
Preferably, the propolis is ground into a kind of one kind as oxidation resistant health product capsule of energy under conditions of 5-15 DEG C
The little particle of 50-100 mesh.Propolis is hard crisp at 5-15 DEG C, is easy to crush, so selection at a lower temperature carries out it
Smashing processing.
Preferably, the pearl powder is that pearl obtains after physical grinding to a kind of one kind as oxidation resistant health product capsule of energy
The pearl powder arrived.Physical grinding does not destroy any substance in pearl, maintains all nutritional ingredients of pearl.
Preferably, the squid is Zhoushan squid to a kind of one kind as oxidation resistant health product capsule of energy.Squid is a kind of
Common marine organisms, especially in this coastal cities in Zhoushan, 1 year consumption of squid is huge, and the yield of squid ink is also very
Greatly.
A kind of one kind as oxidation resistant health product capsule of energy is preferred, the extracting method of the squid ink black pigment are as follows:
Squid prepared Chinese ink is taken, with the fat and protein in enzyme hydrolysis squid prepared Chinese ink, is filtered to remove impurity.Concentration is added in filtrate is
The ethanol solution of 90-98wt% precipitates squid ink black pigment, filters, dry, is then crushed to 50-100 mesh i.e. finished product squid
Pitch-dark pigment.
The present invention is first hydrolyzed the fat in squid prepared Chinese ink with protein with enzyme, and filtering removes impurity.Since squid is pitch-dark
Pigment does not dissolve in ethyl alcohol, therefore the ethanol water that concentration is 90-98wt% is added in filtrate precipitates squid ink black pigment, mistake
After filter, the squid ink black pigment of precipitating is dried, squid ink black pigment is obtained.
A kind of one kind as oxidation resistant health product capsule of energy is preferred, the method for the squid ink black pigment deodorization processing
Are as follows: squid ink black pigment is added to the water dissolution, is added excessive glucose, the mass ratio of squid ink black pigment and glucose is
1-1.3:1 is heated to 60-70 DEG C, and formic acid is added, and the additional amount of formic acid is the 2-5% of squid ink black pigment quality, stirs 2-
4h.Feed liquid after reaction is down to room temperature, the ethanol solution that concentration is 90-98wt%, which is added, precipitates squid ink black pigment, mistake
Filter, the ethanol solution for being 90-98wt% with concentration cleans precipitating repeatedly, dry, pulverize that treated to 50-100 mesh i.e. deodorization
Squid ink black pigment.
Since squid ink black pigment has fishy smell, after user's swallowable capsule, may exist and return taste phenomenon, cause to make
User's experience is bad.In order to solve the problems, such as that there is squid ink black pigment fishy smell and capsule to pass through there may be taste, the present invention is returned
The technique that many experiments demonstration obtains the processing of a squid ink black pigment deodorization.
Specifically: the monomer of squid ink black pigment includes DHI (5,6- dihydroxy indole), DHICA (5,6- dihydroxy indoles
Acid), Cys-Dopa (cysteine DOPA) and dopamine (simultaneously containing indoles and phenylpropyl alcohol thiazine structure) etc., wherein DHI,
Fishy smell substance is all had in DHICA and phenylpropyl alcohol thiazine, these types of fishy smell substance contains indoles and heterocycle ammonia nitrogenous compound.Yin
Contain heterocycle ammonia nitrogenous compound in diindyl, the present invention carries out processing modification to Heterocyclic nitrogen ingredient for this feature, utilizes secondary amine
The response characteristic of base and aldehyde radical connects the glucose of a upper molecule on the nitrogen-atoms of heterocycle ammonia.Studies have shown that secondary amine and aldehyde
Base can react under the catalytic action of formic acid at 60-70 DEG C, and this reaction condition will not destroy on squid ink black pigment
Active group (- SH ,-NH2).After nitrogen-atoms on squid ink black pigment is connect with glucose, what is be rich on grape sugar chain is hydrophilic
The hydroxyl of property is contacted with hydrone outwardly, and hydrophobic alkyl is then coated on the ring around nitrogen-atoms.Glucose molecule is logical
Cross the fishy smell that the mode of the nitrogen-atoms cladding on heterocycle is removed to squid ink black pigment.By the squid ink black pigment after reaction with dense
Degree is precipitated for 90-98wt% ethanol solution, and is the squid ink that 90-98wt% ethanol solution repeated flushing obtains with concentration
Melanin removes the formic acid that adheres on squid ink black pigment, is then dried to obtain deodorization treated squid ink black pigment.
Preferably, the enzyme is papain, alkali protease to a kind of one kind as oxidation resistant health product capsule of energy
Or neutral proteinase, enzyme dosage are the 0.5-5.0% of squid prepared Chinese ink weight.
The present invention first digests squid ink with papain, alkali protease or neutral proteinase, total use of enzyme
Amount is the 0.5-5.0% of squid ink weight, and the dosage of enzyme excessively will cause the waste of enzyme, while increase production cost, and enzyme
Dosage is very few, and the fat and protein removal that will lead in squid ink are not thorough, and will increase enzymolysis time, increase production when
Between cost, production efficiency is low.
A kind of one kind as oxidation resistant health product capsule of energy is preferred, the preparation method of the health product capsule, including
Following steps:
(1) powder is pelletized: will cure purple sweet potato powder, treated squid ink black pigment, pearl powder, propolis, soyabean protein powder, dimension life
Plain C, citric acid are uniformly mixed after crushing according to the parts by weight of formula, cross 50-100 mesh.
(2) capsule fill: step (1) is obtained it is particles filled into capsule, loading amount 0.4-0.6g/.
Capsule of the invention is uniformly mixed after first crushing each component according to the parts by weight of formula, is subsequently filled into glue
Finished product is made in capsule.
The step of a kind of one kind as oxidation resistant health product capsule of energy is preferred, the preparation method of the health product capsule
(1) or the mixing in (2), filling temp are lower than 36 DEG C.
Since matter is soft at 36 DEG C, toughness for propolis, it is not easy uniformly to mix with other compositions such as purple sweet potato powder, pearl powders, therefore
Mix, be seated in lower than 36 DEG C under conditions of operate.
It is compared with the prior art, the beneficial effects of the present invention are: containing purple sweet potato powder, pearl in health product capsule of the invention
A variety of natural materials such as powder, propolis, squid ink extract, soybean protein, albumen containing various plants, animal protein in capsule, tool
There is stronger anti-oxidation efficacy, nutritive value is high, and bad smell will not be returned out after.Preparation step is simple, and cost of material is low,
It is good in economic efficiency.
Specific embodiment
The present invention will be further described with reference to the examples below.Related device, connection structure in the present invention
And method, if being device well known in the art, connection structure and method without refering in particular to.
Embodiment 1
A kind of preparation method of the oxidation resistant health product capsule of energy, steps are as follows:
(1) powder pelletize: will cure 25 parts of purple sweet potato powder, treated 30 parts of squid ink black pigment, 25 parts of pearl powder, propolis 10
Part, it 5 parts of soyabean protein powder, 3 parts of vitamin C, is uniformly mixed after 1.5 parts of citric acid crushing according to the parts by weight of formula, crosses 100
Mesh.
(2) capsule is filled: the particle that step (1) obtains is filled into capsule with ZTT-40 type fully-automatic capsule filling machine
In, loading amount 0.5g/.
Wherein, the crushing temperature of propolis is 5 DEG C, and smashed propolis is sieved with 100 mesh sieve.Step in the preparation process of capsule
Suddenly the filling in the mixing sieving of (1) and step (2) carries out at 25 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 5% of squid ink weight, is filtered to remove impurity.In filtrate
95% edible ethanol of middle addition makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 55 DEG C and is dried with vacuum drier, after dry
The fine grained of 100 mesh is crushed to stainless steel pulverizer.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1.15:1, formic acid is added after being heated with stirring to 65 DEG C of dissolutions, the additional amount of formic acid is
The 2.5% of squid ink black pigment quality stirs 3h.Feed liquid after reaction is down to room temperature, addition concentration is 98% ethanol solution
Squid ink black pigment is precipitated, is filtered, cleans precipitating repeatedly with the ethanol solution that concentration is 98%, drying is simultaneously crushed to 100 mesh
Fine grained.
Embodiment 2:
A kind of preparation method of the oxidation resistant health product capsule of energy, steps are as follows:
(1) powder pelletize: will cure 20 parts of purple sweet potato powder, treated 30 parts of squid ink black pigment, 25 parts of pearl powder, propolis 10
Part, it 10 parts of soyabean protein powder, 5 parts of vitamin C, is uniformly mixed after 1 part of citric acid crushing according to the parts by weight of formula, crosses 80 mesh
Sieve.
(2) capsule is filled: the particle that step (1) obtains is filled into capsule with ZTT-40 type fully-automatic capsule filling machine
In, loading amount 0.6g/.
Wherein, the crushing temperature of propolis is 10 DEG C, and smashed propolis is crossed 80 meshes.Step in the preparation process of capsule
Suddenly the filling in the mixing sieving of (1) and step (2) carries out at 18 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 3% of squid ink weight, is filtered to remove impurity.In filtrate
98% edible ethanol of middle addition makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 55 DEG C and is dried with vacuum drier, after dry
The fine grained of 80 mesh is crushed to stainless steel pulverizer.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose is added, is added
The mass ratio of glucose, squid ink black pigment and glucose is 1:1, and formic acid is added after being heated with stirring to 65 DEG C of dissolutions, formic acid
Additional amount is the 2% of squid ink black pigment quality, stirs 3h.Feed liquid after reaction is down to room temperature, addition concentration is 95% second
Alcoholic solution precipitates squid ink black pigment, filtering, cleans precipitating repeatedly with the ethanol solution that concentration is 95%, drying is simultaneously crushed to
The fine grained of 80 mesh.
Embodiment 3:
A kind of preparation method of the oxidation resistant health product capsule of energy, steps are as follows:
(1) powder pelletize: will cure 25 parts of purple sweet potato powder, treated 25 parts of squid ink black pigment, 20 parts of pearl powder, propolis 15
Part, it 10 parts of soyabean protein powder, 5 parts of vitamin C, is uniformly mixed after 1 part of citric acid crushing according to the parts by weight of formula, crosses 80 mesh
Sieve.
(2) capsule is filled: the particle that step (1) obtains is filled into capsule with ZTT-40 type fully-automatic capsule filling machine
In, loading amount 0.5g/.
Wherein, the crushing temperature of propolis is 10 DEG C, and smashed propolis is crossed 80 meshes.Step in the preparation process of capsule
Suddenly the filling in the mixing sieving of (1) and step (2) carries out at 5 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 2.5% of squid ink weight, is filtered to remove impurity.It is filtering
98% edible ethanol is added in liquid makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 60 DEG C of, dryings dry with vacuum drier
The fine grained of 80 mesh is crushed to stainless steel pulverizer afterwards.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose, squid is added
The mass ratio of pitch-dark pigment and glucose is 1.3:1, formic acid is added after being heated with stirring to 60 DEG C of dissolutions, the additional amount of formic acid is squid
The 2% of the pitch-dark chromatoplasm amount of fish stirs 4h.Feed liquid after reaction is down to room temperature, it is that 95% ethanol solution makes squid that concentration, which is added,
The pitch-dark pigementation of fish, filtering clean precipitating with the ethanol solution that concentration is 95% repeatedly, and drying is simultaneously crushed to 80 purposes thin
Grain.
Embodiment 4:
A kind of preparation method of the oxidation resistant health product capsule of energy, steps are as follows:
(1) powder pelletize: will cure 25 parts of purple sweet potato powder, treated 30 parts of squid ink black pigment, 25 parts of pearl powder, propolis 13
Part, it 5 parts of soyabean protein powder, 3 parts of vitamin C, is uniformly mixed after 1.8 parts of citric acid crushing according to the parts by weight of formula, crosses 75
Mesh.
(2) capsule is filled: the particle that step (1) obtains is filled into capsule with ZTT-40 type fully-automatic capsule filling machine
In, loading amount 0.4g/.
Wherein, the crushing temperature of propolis is 10 DEG C, and smashed propolis is crossed 75 meshes.Step in the preparation process of capsule
Suddenly the filling in the mixing sieving of (1) and step (2) carries out at 35 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 0.3% of squid ink weight, is filtered to remove impurity.It is filtering
98% edible ethanol is added in liquid makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 60 DEG C of, dryings dry with vacuum drier
The fine grained of 75 mesh is crushed to stainless steel pulverizer afterwards.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose is added, is added
The mass ratio of glucose, squid ink black pigment and glucose is 1.2:1, and formic acid, formic acid is added after being heated with stirring to 60 DEG C of dissolutions
Additional amount be squid ink black pigment quality 3%, stir 4h.Feed liquid after reaction is down to room temperature, it is 98% that concentration, which is added,
Ethanol solution precipitates squid ink black pigment, filtering, cleans precipitating repeatedly with the ethanol solution that concentration is 98%, drying simultaneously crushes
To the fine grained of 75 mesh.
Embodiment 5:
A kind of preparation method of the oxidation resistant health product capsule of energy, steps are as follows:
(1) powder pelletize: will cure 25 parts of purple sweet potato powder, treated 25 parts of squid ink black pigment, 20 parts of pearl powder, propolis 10
Part, it 10 parts of soyabean protein powder, 3.5 parts of vitamin C, is uniformly mixed after 1 part of citric acid crushing according to the parts by weight of formula, mistake
100 meshes.
(2) capsule is filled: the particle that step (1) obtains is filled into capsule with ZTT-40 type fully-automatic capsule filling machine
In, loading amount 0.5g/.
Wherein, the crushing temperature of propolis is 15 DEG C, and smashed propolis is sieved with 100 mesh sieve.In the preparation process of capsule
The mixing sieving and the filling in step (2) of step (1) carry out at 20 DEG C.
The wherein extracting method of squid ink black pigment are as follows: manually take squid ink, then use lipase and neutral proteinase water
The fat and protein in squid ink are solved, total dosage of two kinds of enzymes is the 3% of squid ink weight, is filtered to remove impurity.In filtrate
98% edible ethanol of middle addition makes prepared Chinese ink melanin deposition, after filtering, will be deposited in 65 DEG C and is dried with vacuum drier, after dry
The fine grained of 100 mesh is crushed to stainless steel pulverizer.
The wherein method of squid ink black pigment deodorization processing are as follows: squid melanin is added to the water, glucose is added, is added
The mass ratio of glucose, squid ink black pigment and glucose is 1.25:1, and formic acid, formic acid is added after being heated with stirring to 70 DEG C of dissolutions
Additional amount be squid ink black pigment quality 4%, stir 3h.Feed liquid after reaction is down to room temperature, it is 98% that concentration, which is added,
Ethanol solution precipitates squid ink black pigment, filtering, cleans precipitating repeatedly with the ethanol solution that concentration is 98%, drying simultaneously crushes
To the fine grained of 100 mesh.
Sensory evaluation: the present invention tests to the fishy smell of deodorization treated squid ink black pigment, carries out with control group
Comparison, control group is without the processing of smelling removal, and using " the five-grade marking system ", score value is respectively 5,4,3,2,1, and evaluating member is by 5 people
Composition, final assessment result take 5 people to provide the average value of score value, and subjective appreciation standards of grading and specific appraisal result are shown in Table 1 He
Table 2.
1 squid ink black pigment subjective appreciation standards of grading of table
The fishy smell evaluation result of deodorization is handled in 2 embodiment 1-5 of table squid ink black pigment and control group (non-deodorization)
| Fishy smell | |
| Embodiment 1 | 1 |
| Embodiment 2 | 1 |
| Embodiment 3 | 1.6 |
| Embodiment 4 | 1.2 |
| Embodiment 5 | 1.4 |
| Control group | 5 |
The above is only presently preferred embodiments of the present invention, is not intended to limit the invention in any way, all technologies according to the present invention
Essence any simple modification, change and equivalent structure transformation to the above embodiments, still fall within the technology of the present invention side
The protection scope of case.
Claims (10)
1. a kind of oxidation resistant health product capsule of energy, it is characterised in that the material composition including following parts by weight: curing purple sweet potato
15 ~ 25 parts of powder, 25~35 parts of squid ink black pigment, 20~30 parts of pearl powder, 10~15 parts of propolis, 5~10 parts of soyabean protein powder,
2.5 ~ 5 parts of vitamin Cs, 1 ~ 2.5 part of citric acid.
2. a kind of oxidation resistant health product capsule of energy according to claim 1, it is characterised in that: the propolis is natural bee
The pure propolis obtained after glue purification.
3. a kind of oxidation resistant health product capsule of energy according to claim 1 or 2, it is characterised in that: the propolis is in 5-
The little particle of 50-100 mesh is ground under conditions of 15 DEG C.
4. a kind of oxidation resistant health product capsule of energy according to claim 1, it is characterised in that: the pearl powder is pearl
The pearl powder obtained after physical grinding.
5. a kind of oxidation resistant health product capsule of energy according to claim 1, it is characterised in that: the squid is Zhoushan squid
Fish.
6. a kind of oxidation resistant health product capsule of energy according to claim 1, it is characterised in that: the squid ink black pigment
Extracting method are as follows: take squid prepared Chinese ink, with the fat and protein in enzyme hydrolysis squid prepared Chinese ink, be filtered to remove impurity；In filtrate
The ethanol solution that middle addition concentration is 90-98wt% precipitates squid ink black pigment, filters, dry, is then crushed to 50-100
Mesh, that is, finished product squid ink black pigment.
7. a kind of oxidation resistant health product capsule of energy according to claim 1 or 6, it is characterised in that: the squid is pitch-dark
The method of pigment deodorization processing are as follows: squid ink black pigment is added to the water dissolution, the mass ratio of squid ink black pigment and glucose
For 1-1.3:1, it is heated to 60-70 DEG C, formic acid is added, the additional amount of formic acid is the 2-5% of squid ink black pigment quality, stirs 2-
4h；Feed liquid after reaction is down to room temperature, the ethanol solution that concentration is 90-98wt%, which is added, precipitates squid ink black pigment, mistake
Filter, the ethanol solution for being 90-98wt% with concentration cleans precipitating repeatedly, dry, pulverize that treated to 50-100 mesh i.e. deodorization
Squid ink black pigment.
8. a kind of oxidation resistant health product capsule of energy according to claim 5, it is characterised in that: the enzyme is Papain
Enzyme, alkali protease or neutral proteinase, enzyme dosage are the 0.5-5.0% of squid prepared Chinese ink weight.
9. a kind of oxidation resistant health product capsule of energy according to claim 1, which is characterized in that the health product capsule
Preparation method the following steps are included:
(1) powder is pelletized: it will cure purple sweet potato powder, deodorization treated squid ink black pigment, and pearl powder, propolis, soyabean protein powder,
Vitamin C and citric acid are uniformly mixed after crushing according to the parts by weight in formula, cross 50-100 mesh；
(2) capsule is filled: step (1) is obtained it is particles filled into capsule, loading amount 0.4-0.6g/.
10. a kind of according to claim 1 or described in 9 can oxidation resistant health product capsule, which is characterized in that the health care product glue
The step of preparation method of capsule (1) or the mixing in (2), filling temp are lower than 36 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810818756.5A CN109090525A (en) | 2018-07-24 | 2018-07-24 | It is a kind of can oxidation resistant health product capsule and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810818756.5A CN109090525A (en) | 2018-07-24 | 2018-07-24 | It is a kind of can oxidation resistant health product capsule and preparation method thereof |
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| CN109090525A true CN109090525A (en) | 2018-12-28 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1895665A (en) * | 2006-06-26 | 2007-01-17 | 宁波超星海洋生物制品有限公司 | Scorpionfish-ink polysaccharide and its preparation |
| CN103041057A (en) * | 2011-10-14 | 2013-04-17 | 涂波 | Anti-oxidization capsule |
| CN103190613A (en) * | 2013-03-18 | 2013-07-10 | 石发军 | Preparation method of purple sweet potato health product composition |
| CN104544321A (en) * | 2013-10-21 | 2015-04-29 | 大连市沙河口区中小微企业服务中心 | Soluble squid inkiness pigment |
| CN107410842A (en) * | 2017-05-02 | 2017-12-01 | 江南大学 | A kind of preparation of soluble squid ink black pigment through deodorant and its application in food |
-
2018
- 2018-07-24 CN CN201810818756.5A patent/CN109090525A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1895665A (en) * | 2006-06-26 | 2007-01-17 | 宁波超星海洋生物制品有限公司 | Scorpionfish-ink polysaccharide and its preparation |
| CN103041057A (en) * | 2011-10-14 | 2013-04-17 | 涂波 | Anti-oxidization capsule |
| CN103190613A (en) * | 2013-03-18 | 2013-07-10 | 石发军 | Preparation method of purple sweet potato health product composition |
| CN104544321A (en) * | 2013-10-21 | 2015-04-29 | 大连市沙河口区中小微企业服务中心 | Soluble squid inkiness pigment |
| CN107410842A (en) * | 2017-05-02 | 2017-12-01 | 江南大学 | A kind of preparation of soluble squid ink black pigment through deodorant and its application in food |
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Application publication date: 20181228 |