CN109071727A - 碱溶胀性乳液聚合物 - Google Patents

Info

Publication number

CN109071727A

CN109071727A CN201680082340.0A CN201680082340A CN109071727A CN 109071727 A CN109071727 A CN 109071727A CN 201680082340 A CN201680082340 A CN 201680082340A CN 109071727 A CN109071727 A CN 109071727A

Authority

CN

China

Prior art keywords

weight

acid

hand

alkyl

monomer

Prior art date

2015-12-23

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Pending

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• 239000004908 Emulsion polymer Substances 0.000 title claims abstract description 17
• 239000003513 alkali Substances 0.000 title abstract description 27
• 239000000203 mixture Substances 0.000 claims abstract description 328
• 229920000642 polymer Polymers 0.000 claims abstract description 213
• 239000004094 surface-active agent Substances 0.000 claims abstract description 85
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 83
• 239000013590 bulk material Substances 0.000 claims abstract description 13
• 239000002198 insoluble material Substances 0.000 claims abstract description 11
• -1 alkali metal salt Chemical class 0.000 claims description 294
• 239000000178 monomer Substances 0.000 claims description 148
• 239000003795 chemical substances by application Substances 0.000 claims description 100
• 239000002585 base Substances 0.000 claims description 79
• 239000002253 acid Substances 0.000 claims description 60
• 239000003921 oil Substances 0.000 claims description 59
• 125000000217 alkyl group Chemical group 0.000 claims description 49
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 49
• 229910052708 sodium Inorganic materials 0.000 claims description 45
• CERQOIWHTDAKMF-UHFFFAOYSA-N alpha-methacrylic acid Natural products CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 44
• 239000000463 material Substances 0.000 claims description 44
• 239000011734 sodium Substances 0.000 claims description 44
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 41
• 150000003839 salts Chemical class 0.000 claims description 41
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 40
• 229910052799 carbon Inorganic materials 0.000 claims description 32
• 239000007788 liquid Substances 0.000 claims description 32
• 239000000194 fatty acid Substances 0.000 claims description 31
• 229920002554 vinyl polymer Polymers 0.000 claims description 31
• 150000001875 compounds Chemical class 0.000 claims description 30
• 235000014113 dietary fatty acids Nutrition 0.000 claims description 30
• 229930195729 fatty acid Natural products 0.000 claims description 30
• QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 29
• 239000011324 bead Substances 0.000 claims description 28
• 239000002537 cosmetic Substances 0.000 claims description 28
• 238000004132 cross linking Methods 0.000 claims description 27
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 26
• 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 26
• 239000003945 anionic surfactant Substances 0.000 claims description 25
• 150000002148 esters Chemical class 0.000 claims description 25
• 229910052700 potassium Inorganic materials 0.000 claims description 24
• 150000001721 carbon Chemical group 0.000 claims description 23
• 230000002378 acidificating effect Effects 0.000 claims description 22
• 150000004665 fatty acids Chemical class 0.000 claims description 22
• NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 21
• KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 21
• 229960003237 betaine Drugs 0.000 claims description 21
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 20
• GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 20
• QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 19
• 239000002245 particle Substances 0.000 claims description 18
• 239000002280 amphoteric surfactant Substances 0.000 claims description 17
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 17
• 239000003205 fragrance Substances 0.000 claims description 17
• NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 16
• XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 16
• 125000002252 acyl group Chemical group 0.000 claims description 16
• 125000003342 alkenyl group Chemical group 0.000 claims description 16
• 150000001450 anions Chemical class 0.000 claims description 16
• 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 16
• 239000007787 solid Substances 0.000 claims description 15
• SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 14
• WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 claims description 14
• 229910052783 alkali metal Inorganic materials 0.000 claims description 14
• 150000001768 cations Chemical class 0.000 claims description 14
• 239000011248 coating agent Substances 0.000 claims description 14
• 238000000576 coating method Methods 0.000 claims description 14
• 125000003118 aryl group Chemical group 0.000 claims description 13
• 229910052739 hydrogen Inorganic materials 0.000 claims description 12
• 239000000049 pigment Substances 0.000 claims description 12
• HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 10
• 208000001840 Dandruff Diseases 0.000 claims description 10
• 239000000686 essence Substances 0.000 claims description 10
• XHZPRMZZQOIPDS-UHFFFAOYSA-N 2-Methyl-2-[(1-oxo-2-propenyl)amino]-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(C)(C)NC(=O)C=C XHZPRMZZQOIPDS-UHFFFAOYSA-N 0.000 claims description 9
• 229910021529 ammonia Inorganic materials 0.000 claims description 9
• 150000003863 ammonium salts Chemical class 0.000 claims description 9
• 239000003093 cationic surfactant Substances 0.000 claims description 9
• 239000003094 microcapsule Substances 0.000 claims description 9
• JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 claims description 8
• 150000001335 aliphatic alkanes Chemical class 0.000 claims description 8
• 125000002877 alkyl aryl group Chemical group 0.000 claims description 8
• 150000008051 alkyl sulfates Chemical group 0.000 claims description 8
• 239000010445 mica Substances 0.000 claims description 7
• 229910052618 mica group Inorganic materials 0.000 claims description 7
• 125000001421 myristyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 7
• QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 6
• WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 6
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
• 230000003213 activating effect Effects 0.000 claims description 6
• 150000001340 alkali metals Chemical class 0.000 claims description 6
• 150000005846 sugar alcohols Polymers 0.000 claims description 6
• 229920000536 2-Acrylamido-2-methylpropane sulfonic acid Polymers 0.000 claims description 5
• FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 5
• 229910003202 NH4 Inorganic materials 0.000 claims description 5
• 239000004927 clay Substances 0.000 claims description 5
• TVFJAZCVMOXQRK-UHFFFAOYSA-N ethenyl 7,7-dimethyloctanoate Chemical compound CC(C)(C)CCCCCC(=O)OC=C TVFJAZCVMOXQRK-UHFFFAOYSA-N 0.000 claims description 5
• 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 claims description 5
• BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 5
• 239000005977 Ethylene Substances 0.000 claims description 4
• ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 claims description 4
• WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 4
• 239000008103 glucose Substances 0.000 claims description 4
• 229930182478 glucoside Natural products 0.000 claims description 4
• 229910052736 halogen Inorganic materials 0.000 claims description 4
• 150000002367 halogens Chemical class 0.000 claims description 4
• 235000003642 hunger Nutrition 0.000 claims description 4
• PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims description 4
• 229920006395 saturated elastomer Polymers 0.000 claims description 4
• 235000021122 unsaturated fatty acids Nutrition 0.000 claims description 4
• 150000004670 unsaturated fatty acids Chemical class 0.000 claims description 4
• 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims description 3
• 206010020466 Hunger Diseases 0.000 claims description 3
• CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims description 3
• 229930006000 Sucrose Natural products 0.000 claims description 3
• 125000005210 alkyl ammonium group Chemical group 0.000 claims description 3
• 125000003368 amide group Chemical group 0.000 claims description 3
• 229940031098 ethanolamine Drugs 0.000 claims description 3
• SUMDYPCJJOFFON-UHFFFAOYSA-N isethionic acid Chemical compound OCCS(O)(=O)=O SUMDYPCJJOFFON-UHFFFAOYSA-N 0.000 claims description 3
• 229940094506 lauryl betaine Drugs 0.000 claims description 3
• SNVLJLYUUXKWOJ-UHFFFAOYSA-N methylidenecarbene Chemical compound C=[C] SNVLJLYUUXKWOJ-UHFFFAOYSA-N 0.000 claims description 3
• DVEKCXOJTLDBFE-UHFFFAOYSA-N n-dodecyl-n,n-dimethylglycinate Chemical compound CCCCCCCCCCCC[N+](C)(C)CC([O-])=O DVEKCXOJTLDBFE-UHFFFAOYSA-N 0.000 claims description 3
• 239000005720 sucrose Substances 0.000 claims description 3
• LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 2
• CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
• 150000001447 alkali salts Chemical class 0.000 claims description 2
• 229920000223 polyglycerol Polymers 0.000 claims description 2
• HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 2
• 229920001567 vinyl ester resin Polymers 0.000 claims description 2
• 239000004711 α-olefin Substances 0.000 claims description 2
• JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims 4
• CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims 4
• 229920002818 (Hydroxyethyl)methacrylate Polymers 0.000 claims 3
• WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 claims 3
• AGBXYHCHUYARJY-UHFFFAOYSA-N 2-phenylethenesulfonic acid Chemical compound OS(=O)(=O)C=CC1=CC=CC=C1 AGBXYHCHUYARJY-UHFFFAOYSA-N 0.000 claims 1
• KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims 1
• 125000003295 alanine group Chemical class N[C@@H](C)C(=O)* 0.000 claims 1
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• PCHPORCSPXIHLZ-UHFFFAOYSA-N diphenhydramine hydrochloride Chemical compound [Cl-].C=1C=CC=CC=1C(OCC[NH+](C)C)C1=CC=CC=C1 PCHPORCSPXIHLZ-UHFFFAOYSA-N 0.000 claims 1
• MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 claims 1
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• HLERILKGMXJNBU-UHFFFAOYSA-N norvaline betaine Chemical compound CCCC(C([O-])=O)[N+](C)(C)C HLERILKGMXJNBU-UHFFFAOYSA-N 0.000 claims 1
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