CN109042755A - A kind of culicifuge and preparation method thereof from plant extracts - Google Patents
A kind of culicifuge and preparation method thereof from plant extracts Download PDFInfo
- Publication number
- CN109042755A CN109042755A CN201810890646.XA CN201810890646A CN109042755A CN 109042755 A CN109042755 A CN 109042755A CN 201810890646 A CN201810890646 A CN 201810890646A CN 109042755 A CN109042755 A CN 109042755A
- Authority
- CN
- China
- Prior art keywords
- culicifuge
- oil
- plant extracts
- hemp nettle
- weasel hemp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Plant Pathology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides a kind of culicifuge from plant extracts, the culicifuge includes the weasel hemp nettle extract that weight percent is 0.5%-5%, simultaneously, the culicifuge safety and environmental protection, mild irritation are small and smell is pure and fresh, it is capable of the mosquito of high-efficient and lasting, and can be compounded with existing mosquito repellent product as synergist to obtain better repelling effect.
Description
Technical field
The invention belongs to mosquito repellent product technical field more particularly to a kind of culicifuges and its preparation from plant extracts
Method, the in particular to culicifuge of the extract containing weasel hemp nettle.
Background technique
At present in the world there are about more than 3500 kinds of mosquitoes and its subspecies, the most common mosquito has Aedes, Culex and anopheles
Belong to, mosquito sucks the blood of people and various animals, harasses the mankind and propagates malaria, filariasis, Japanese Type-B encephalitis, west with this
A variety of diseases such as Nile virus disease, dengue fever, wherein it has been reported that carapuru virus type up to more than 40 kinds.
For a long time, people control mosquito using various methods, and main means are using chemical insecticide and chemical repellent
Agent, such as Metadelphene (DEET), mosquitofugal oil (DMP), citronellal, organic phosphorus, carbamates, expelling parasite amine, these medicaments
Effect is good, efficiency time is long, but mosquito is easy to produce resistance, and is used for a long time and will cause serious environmental pollution and to human body
Generate toxic side effect.
It has a long history with natural plants mosquito repellent, mainly there is plant of directly smearing and burn to carry out two kinds of sides of fumigation
Formula.Ancient Egyptian, which smears, has the tobacco tar of overpowering odor to prevent bite by mosquitos；Ancient times, Russia herdsman smeared eucalyptus leaf juice
On the skin and burning moss and pine tree leaf carry out expelling mosquito；Ancient Times in China resident is to burn plant as main expelling mosquito side
Method, common plant have dry palpus of wormwood herb, sesame slices, Jing Ye and various pericarps, corn etc..However, using plant sootiness
Method, this method are limited by raw material, and easily cause fire, and the smog generated there are hidden danger, especially sootiness is tight
Ghost image rings room air.
In recent years, plant source culicifuge with its safety, wide spectrum, it is degradable and the advantages that be not easy to produce resistance by people
Attention, be mainly derived from the extract or volatile oil at the different tissues position of each plant, such as: wild chrysanthemum, geranium oil, gold and silver
Caul-fat, Artemisia oil, catnip oil, the grey oil in mountain, retinal, wintergreen, lemongrass oil, eucalyptus citriodora oil, citronella oil, lavender oil, fourth
Sesame oil etc., but these are very short with plant volatile oil mosquito-repellent action time as main component, generally at 1~2 hour,
Repelling effect is bad.
Although having put into the various resources such as a large amount of human and material resources in the research and development of plant source culicifuge, economically may be used
The research of culicifuge capable, based on plant extracts, especially research and development safety and environmental protection, mild, irritation is small, smell is pure and fresh and
The plant source culicifuge of high-efficient and lasting is still long-term unsatisfied demand.
Summary of the invention
The purpose of the invention is to overcome the deficiencies of the prior art and provide a kind of culicifuge from plant extracts and
Preparation method, the culicifuge safety and environmental protection, mild irritation are small and smell is pure and fresh, are capable of the mosquito of high-efficient and lasting, and
It can be compounded with existing mosquito repellent product as synergist to obtain better repelling effect.
To achieve the goals above, reach above-mentioned technical effect, the invention provides the following technical scheme: a kind of be originated from plant
The culicifuge of extract, the weasel hemp nettle extract for being 0.5%-5% including weight percent.
The preparation method of the weasel hemp nettle extract, comprising:
(1) weasel hemp nettle herb is taken, the ethyl alcohol of 85-95% is added in crushed after being dried, after heating boiling 1-2h, collects filtrate；
The weight ratio of the ethyl alcohol of the weasel hemp nettle herb and 85-95% is 1:10-15；
(2) filter residue in step (1) is taken, the ethyl alcohol of 65-75% is added, after heating boiling 1-2h, collects filtrate；The weasel
The weight ratio of the ethyl alcohol of hemp nettle herb and 65-75% is 1:10-15；
(3) filter residue in step (2) is taken, the acetone of 50-70% is added, after heating boiling 1-2h, collects filtrate；The weasel
The weight ratio of the acetone of hemp nettle herb and 50-70% is 1:7-10；
(4) merge the filtrate that step (1)-(3) are prepared, after adjusting pH value to 7-8, concentration is prepared after dry
Weasel hemp nettle extract.
Further, step (1)-(3) preferably carry out 2-3 times respectively；
Further, the content of the weasel hemp nettle extract is preferably 1%-4%, more preferably 2-3%.
Further, the culicifuge from plant extracts includes one or more plants essential oils, selected from citronella oil, is smoked
One of clothing grass oil, caryophyllus oil, camphorated oil, tea oil, rosemary oil, eucalyptus oil, catnip oil, perilla herb oil are a variety of；It is described
The weight percent of essential oil is 1%-3%.
Further, the culicifuge from plant extracts includes one or more auxiliary materials, selected from sustained release agent, dilution
Agent, surfactant, moisturizer, preservative, thickener, emulsifier, skin sense agent etc., can be made emulsion, creme or spray.
Further, the sustained release agent include one of carbon nanotube, polyvinylpyrrolidone, carbomer, xanthan gum or
It is a variety of；
The diluent is ethyl alcohol or water；
The surfactant is anionic surfactant or nonionic surfactant, is selected from dodecyl sulphate
Sodium, neopelex, AEO carboxylic acid sodium, sorbitan ester, coconut oil single ethanol amide, coconut
Oily diglycollic amide, Tween-20, Tween-80, fatty alcohol polyoxyethylene ether it is one or more；
The moisturizer is the one or more of glycerol, polyethylene glycol or hyaluronic acid；
The preservative is the one or more of ethylparaben, isothiazolinone or imidazolidinyl urea；
The thickener be carboxymethyl cellulose, chitin, hydroxyethyl cellulose or hydroxypropyl methyl fiber one kind or
It is a variety of；
The emulsifier is stearic acid or tristerin；
The skin sense agent is microcrystalline cellulose.
Further, the present invention provides a kind of culicifuge from plant extracts, including following components in percentage by weight:
Weasel hemp nettle extract 0.5-5%, plants essential oil 1-3%, sustained release agent 5-10%, surfactant 5-10%, moisturizer 15-
20%, thickener 5-10%, preservative 0.5-2%, emulsifier 8-15%, skin sense agent 5-10%, diluent 30-50%.
Further, the present invention provides the preparation method of above-mentioned culicifuge, comprising the following steps:
(1) weasel hemp nettle extract, sustained release agent, emulsifier, moisturizer and diluent are mixed, is heated to 40-60 DEG C, high speed
Mixture is prepared after stirring 30-60min；
(2) plants essential oil and surfactant are mixed, mixture is prepared after high-speed stirred 30-60min；
(3) it by the mixture of step (1) and step (2) being prepared, is mixed with thickener, preservative and skin sense agent,
White body is prepared after high-speed stirred 50-100min, that is, is originated from the culicifuge of plant extracts.
Beneficial effects of the present invention are as follows:
(1) the weasel hemp nettle extraction process provided according to the present invention, the weasel hemp nettle extract being prepared have efficient drive
Mosquito effect, may in weasel hemp nettle terpene, glucosides or Flavonoid substances it is related；The drive being prepared by weasel hemp nettle extract
Mosquito agent safety and environmental protection, irritation is low, and smell is pure and fresh, is capable of the mosquito of high-efficient and lasting；
(2) the weasel hemp nettle extract is compounded with plants essential oil, and the two can play synergistic effect, is greatly improved
Repelling effect；Meanwhile adding sustained release agent in culicifuge and being able to extend mosquito repellent time, increase repelling effect as far as possible；
(3) present invention can greatly promote mosquito repellent by the compatibility of screening and its ratio to specific auxiliary material raw material
Effect guarantees that culicifuge has safety and environmental protection, and irritation is low, and the advantage that smell is pure and fresh.
Specific embodiment
Embodiment 1
The preparation of weasel hemp nettle extract, comprising the following steps:
(1) weasel hemp nettle herb is taken, 90% ethyl alcohol is added in crushed after being dried, after heating boiling 2h, collects filtrate；It is described
Weasel hemp nettle herb and 90% ethyl alcohol weight ratio be 1:10；
(2) filter residue in step (1) is taken, 75%% ethyl alcohol is added, after heating boiling 2h, collects filtrate；The weasel valve
Flower herb with 75% ethyl alcohol weight ratio be 1:15；
(3) filter residue in step (2) is taken, 70% acetone is added, after heating boiling 1h, collects filtrate；The weasel hemp nettle
Herb and 70% acetone weight ratio be 1:8；
(4) merge the filtrate that is prepared of step (1)-(3), adjust pH value to after 7, weasel is prepared after dry in concentration
Hemp nettle extract.
2g weasel hemp nettle extract is added in 98g water, 40 DEG C is heated to, prepares 2% weasel hemp nettle extract solution.
The test of mosquito attack: mosquito cage 1 is taken, includes 350 (sex ration about 1:1) aedes albopictus, tester is by hand
The skin of exposure 40mm × 40mm is carried on the back, rest part tightly covers.Hand is protruded into mosquito cage after stopping 2min, close observation mosquito
Flight progress, discovery are shaken arm when having mosquito land and stop and are expelled, this situation, which has been denoted as 1 mosquito, to be stopped falling and bite.
If stopping falling the mosquito for biting skin more than 30, this tester can be sentenced and mosquito is that attack is qualified, can be carried out following
Repellent activity test.
Repellent activity measurement: skin method test culicifuge is applied to the repellent effect of aedes albopictus using part；Test is being equipped with
It is carried out in the mosquito cage of 350 aedes albopictus (sex ration is about 1:1), the personnel of 7 mosquito attack test passes is selected, one
The back of hand draws the range of a 40mm × 40mm, and the back of another hand is blank control, and dosage used is 1.5mg/
cm2It puts his hand into mosquito cage after natural air drying and is tested after 2min, it is primary every 0.5h test, it is continued for observing the
Until one mosquito stops falling or attempting to bite, it is considered as complete shielding failure.Experiment is repeated 3 times, and experimental result, which takes, every time tests
Average value.As a result: 2% solution of weasel hemp nettle extract prepared by embodiment 1 is under the experiment condition to the complete of aedes albopictus
The full guard time is 2.9h.
Embodiment 2
A kind of culicifuge from plant extracts, including following components in percentage by weight: weasel hemp nettle extract 3%,
Plants essential oil 3%, sustained release agent 8%, surfactant 10%, moisturizer 15%, thickener 8%, preservative 1%, emulsifier
10%, skin sense agent 10%, diluent 32%.
Preparation method is as follows:
(1) weasel hemp nettle extract, sustained release agent, emulsifier, moisturizer and diluent are mixed, is heated to 40 DEG C, high-speed stirring
Mixture is prepared after mixing 60min；
(2) plants essential oil and surfactant are mixed, mixture is prepared after high-speed stirred 60min；
(3) it by the mixture of step (1) and step (2) being prepared, is mixed with thickener, preservative and skin sense agent,
White body is prepared after high-speed stirred 50min, that is, is originated from the culicifuge of plant extracts.
Wherein, plants essential oil is rosemary oil, and sustained release agent is carbomer, and surfactant is the dodecane of mass ratio 1:1
Base benzene sulfonic acid sodium salt and fatty alcohol polyoxyethylene ether；Moisturizer is glycerol, and thickener is carboxymethyl cellulose, and preservative is nipalgin
Ethyl ester；Emulsifier is stearic acid, and skin sense agent is microcrystalline cellulose, and diluent is water.
Embodiment 3-10
In addition to plants essential oil is different from embodiment 2, remaining component, proportion and preparation method and embodiment 2 are completely the same.
Comparative example 1-9
Weasel hemp nettle extract in the culicifuge of embodiment 2-10 replaces with to the plants essential oil of same weight, remaining component,
Proportion and preparation method and embodiment 2 are completely the same.
Embodiment 2-10 and comparative example 1-9 is subjected to repellent activity experiment, is as a result recorded in table 1.
Table 1:
It can be defined according to the experimental data in table 1, it, can be very big after weasel hemp nettle extract is compounded with plants essential oil mixing
Raising culicifuge repelling effect, the two can generate good synergy, and possible principle is attributed to weasel hemp nettle extraction
Active constituent in object enables to plants essential oil to be preferably dispersed in culicifuge, plays extension mosquito repellent time, increases mosquito repellent
The effect of effect.Wherein, the compounding effect of weasel hemp nettle extract and eucalyptus oil is best, followed by camphorated oil.
Embodiment 11-15
Selection weasel hemp nettle extract and eucalyptus oil are compounded, auxiliary material selection and preparation method and embodiment 2 complete one
It causes, difference is only in that the compound proportion of adjustment weasel hemp nettle extract and eucalyptus oil, and it is living that embodiment 11-15 is carried out repellent
Property experiment, be as a result recorded in table 2.
Table 2
| Serial number | Weasel hemp nettle extract | Eucalyptus oil | Repellent effect (h) |
| Embodiment 11 | 0.5% | 3% | 6.8 |
| Embodiment 12 | 1.5% | 3% | 7.0 |
| Embodiment 13 | 2% | 3% | 7.8 |
| Embodiment 14 | 4% | 3% | 7.2 |
| Embodiment 15 | 5% | 2% | 7.0 |
It can be defined according to the experimental data in table 2, weasel hemp nettle extract is with eucalyptus oil when being compounded, and the two is in weight
Amount than 1:1 when effect it is best, the content of weasel hemp nettle extract it is too low or it is excessively high cause repellent effect present downward trend.
Embodiment 16
A kind of culicifuge from plant extracts, including following components in percentage by weight: weasel hemp nettle extract 3%,
Plants essential oil 3%, sustained release agent 7%, surfactant 9%, moisturizer 18%, thickener 6%, preservative 0.5%, emulsifier
15%, skin sense agent 8%, diluent 40.5%.
Preparation method is as follows:
(1) weasel hemp nettle extract, sustained release agent, emulsifier, moisturizer and diluent are mixed, is heated to 50 DEG C, high-speed stirring
Mixture is prepared after mixing 50min；
(2) plants essential oil and surfactant are mixed, mixture is prepared after high-speed stirred 50min；
(3) it by the mixture of step (1) and step (2) being prepared, is mixed with thickener, preservative and skin sense agent,
White body is prepared after high-speed stirred 80min, that is, is originated from the culicifuge of plant extracts.
Wherein, plants essential oil is eucalyptus oil, and sustained release agent is carbon nanotube, and surfactant is the dodecane of mass ratio 1:1
Base benzene sulfonic acid sodium salt and fatty alcohol polyoxyethylene ether；Moisturizer is polyethylene glycol, and thickener is carboxymethyl cellulose, and preservative is Buddhist nun
Moor golden ethyl ester；Emulsifier is stearic acid, and skin sense agent is microcrystalline cellulose, and diluent is ethyl alcohol.After tested, repellent effect is
8.9h。
Embodiment 17
A kind of culicifuge from plant extracts, including following components in percentage by weight: weasel hemp nettle extract 2%,
Plants essential oil 1.5%, sustained release agent 9%, surfactant 8%, moisturizer 20%, thickener 6%, preservative 0.5%, emulsifier
12%, skin sense agent 10%, diluent 32%.
Preparation method is as follows:
(1) weasel hemp nettle extract, sustained release agent, emulsifier, moisturizer and diluent are mixed, is heated to 50 DEG C, high-speed stirring
Mixture is prepared after mixing 50min；
(2) plants essential oil and surfactant are mixed, mixture is prepared after high-speed stirred 50min；
(3) it by the mixture of step (1) and step (2) being prepared, is mixed with thickener, preservative and skin sense agent,
White body is prepared after high-speed stirred 70min, that is, is originated from the culicifuge of plant extracts.
Wherein, plants essential oil is eucalyptus oil, and sustained release agent is carbon nanotube, and surfactant is the fatty alcohol of mass ratio 1:1
Polyoxyethylene ether carboxylic acid sodium and sorbitan ester；Moisturizer is hyaluronic acid, and thickener is carboxymethyl cellulose, and preservative is
Ethylparaben；Emulsifier is stearic acid, and skin sense agent is microcrystalline cellulose, and diluent is ethyl alcohol.After tested, repellent effect is
7.4h。
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all this
Made any modifications, equivalent replacements, and improvements etc., should be included in the claims in the present invention within the spirit and principle of invention
Protection scope within.
Claims (10)
1. a kind of culicifuge from plant extracts, it is characterised in that: the weasel hemp nettle for being 0.5%-5% including weight percent
Extract.
2. a kind of culicifuge from plant extracts according to claim 1, it is characterised in that: the weasel hemp nettle is extracted
The preparation method of object, comprising:
(1) weasel hemp nettle herb is taken, the ethyl alcohol of 85-95% is added in crushed after being dried, after heating boiling 1-2h, collects filtrate；It is described
The weight ratio of the ethyl alcohol of weasel hemp nettle herb and 85-95% is 1:10-15；
(2) filter residue in step (1) is taken, the ethyl alcohol of 65-75% is added, after heating boiling 1-2h, collects filtrate；The weasel hemp nettle
The weight ratio of the ethyl alcohol of herb and 65-75% is 1:10-15；
(3) filter residue in step (2) is taken, the acetone of 50-70% is added, after heating boiling 1-2h, collects filtrate；The weasel hemp nettle
The weight ratio of the acetone of herb and 50-70% is 1:7-10；
(4) merge the filtrate that step (1)-(3) are prepared, after adjusting pH value to 7-8, weasel valve is prepared after dry in concentration
Flower extract.
3. a kind of culicifuge from plant extracts described in any one of -2 according to claim 1, it is characterised in that: described
Step (1)-(3) carry out 2-3 times respectively.
4. a kind of culicifuge from plant extracts described in any one of -2 according to claim 1, it is characterised in that: described
Culicifuge contains one or more plants essential oils, and the weight percent of the plants essential oil is 1%-3%.
5. a kind of culicifuge from plant extracts according to claim 4, it is characterised in that: the plants essential oil choosing
From one of citronella oil, lavender oil, caryophyllus oil, camphorated oil, tea oil, rosemary oil, eucalyptus oil, catnip oil, perilla herb oil
Or it is a variety of.
6. a kind of culicifuge from plant extracts described in any one of -2 according to claim 1, it is characterised in that: described
Culicifuge include one or more auxiliary materials, the auxiliary material be selected from sustained release agent, diluent, surfactant, moisturizer, preservative,
One of thickener, emulsifier, skin sense agent are a variety of.
7. a kind of culicifuge from plant extracts, it is characterised in that: including following components in percentage by weight: weasel hemp nettle mentions
Take object 0.5-5%, plants essential oil 1-3%, sustained release agent 5-10%, surfactant 5-10%, moisturizer 15-20%, thickener
5-10%, preservative 0.5-2%, emulsifier 8-15%, skin sense agent 5-10%, diluent 30-50%.
8. a kind of preparation method of culicifuge from plant extracts according to claim 7, it is characterised in that: including
Following steps:
(1) weasel hemp nettle extract, sustained release agent, emulsifier, moisturizer and diluent are mixed, is heated to 40-60 °C, high-speed stirred
Mixture is prepared after 30-60min；
(2) plants essential oil and surfactant are mixed, mixture is prepared after high-speed stirred 30-60min；
(3) it by the mixture of step (1) and step (2) being prepared, is mixed with thickener, preservative and skin sense agent, high speed
White body is prepared after stirring 50-100min to get the culicifuge from plant extracts is arrived.
9. a Plant Extracts are preparing the application in culicifuge, it is characterised in that: the plant extracts mentions for weasel hemp nettle
Take object.
10. a Plant Extracts according to claim 9 are preparing the application in culicifuge, it is characterised in that: described
The preparation method of weasel hemp nettle extract, comprising:
(1) weasel hemp nettle herb is taken, the ethyl alcohol of 85-95% is added in crushed after being dried, after heating boiling 1-2h, collects filtrate；It is described
The weight ratio of the ethyl alcohol of weasel hemp nettle herb and 85-95% is 1:10-15；
(2) filter residue in step (1) is taken, the ethyl alcohol of 65-75% is added, after heating boiling 1-2h, collects filtrate；The weasel hemp nettle
The weight ratio of the ethyl alcohol of herb and 65-75% is 1:10-15；
(3) filter residue in step (2) is taken, the acetone of 50-70% is added, after heating boiling 1-2h, collects filtrate；The weasel hemp nettle
The weight ratio of the acetone of herb and 50-70% is 1:7-10；
(4) merge the filtrate that step (1)-(3) are prepared, after adjusting pH value to 7-8, weasel valve is prepared after dry in concentration
Flower extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810890646.XA CN109042755A (en) | 2018-08-07 | 2018-08-07 | A kind of culicifuge and preparation method thereof from plant extracts |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810890646.XA CN109042755A (en) | 2018-08-07 | 2018-08-07 | A kind of culicifuge and preparation method thereof from plant extracts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109042755A true CN109042755A (en) | 2018-12-21 |
Family
ID=64678093
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810890646.XA Pending CN109042755A (en) | 2018-08-07 | 2018-08-07 | A kind of culicifuge and preparation method thereof from plant extracts |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109042755A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI792314B (en) * | 2021-05-17 | 2023-02-11 | 大葉大學 | Method to identify natural essential oils with lure mosquitoes effect or repel mosquitoes effect to prevent mosquito breeding |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BG49399A1 (en) * | 1989-10-16 | 1991-11-15 | Vissh Selskostopanski Inst V K | Insect- fungicide means |
| BG50527A1 (en) * | 1990-06-14 | 1992-09-15 | Agronomicheski Uni | Insecticide device |
| CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
| CN102784094A (en) * | 2012-07-19 | 2012-11-21 | 太原师范学院 | Mosquito dispelling toner for infants, and its preparation method |
-
2018
- 2018-08-07 CN CN201810890646.XA patent/CN109042755A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BG49399A1 (en) * | 1989-10-16 | 1991-11-15 | Vissh Selskostopanski Inst V K | Insect- fungicide means |
| BG50527A1 (en) * | 1990-06-14 | 1992-09-15 | Agronomicheski Uni | Insecticide device |
| CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
| CN102784094A (en) * | 2012-07-19 | 2012-11-21 | 太原师范学院 | Mosquito dispelling toner for infants, and its preparation method |
Non-Patent Citations (2)
| Title |
|---|
| ZHONG PINGSHENG等: "Effect of the ethanol extracts from the non-host plant species on the feeding of the brown planthopper, Nilaparvata lugens", 《CHINESE BULLETIN OF ENTOMOLOGY》 * |
| 冼继东等: "植物乙醇提取物对小菜蛾实验种群作用的研究", 《走向21世纪的中国昆虫学——中国昆虫学会2000年学术年会论文集》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI792314B (en) * | 2021-05-17 | 2023-02-11 | 大葉大學 | Method to identify natural essential oils with lure mosquitoes effect or repel mosquitoes effect to prevent mosquito breeding |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105594755B (en) | A kind of plant mosquito-repellent and the preparation method with repelling effect fabric | |
| CN106511133B (en) | Essential oil nano-particles, preparation method thereof and application thereof in preparing mosquito-repellent products | |
| CN104054758A (en) | Harmless plant insecticide | |
| CN101326920A (en) | Raticide | |
| CN101390525B (en) | Plant source mosquito driving and killing agent | |
| CN1134786A (en) | Multi-purpose, no-polution composite agricultural chemicals for plants and method for mfg. same | |
| CN106332921B (en) | A kind of plant insecticide and its preparation method and application | |
| US20050112164A1 (en) | Insect repellent composition containing essential oils | |
| CN105010337B (en) | Method of preparing mosquito repellant by utilizing cassia oil extraction waste liquid | |
| CN112640922B (en) | Mosquito-repellent composition and preparation method and application thereof | |
| CN109042755A (en) | A kind of culicifuge and preparation method thereof from plant extracts | |
| CN106726871A (en) | Sweet wormwood mosquito-expelling and antipruritic floral water and preparation method thereof | |
| CN106922751A (en) | Natural plants insecticide | |
| CN1754432A (en) | Pokeberry-containing compound plant insecticide | |
| Ohia et al. | Larvicidal Activity of Aqeous Extract of Moringa oleifera Seeds on Anopheles gambiae and its Effects on Poecilia reticulata | |
| KR20200137703A (en) | A natural composition for mosquito repellent | |
| CN112219844B (en) | Botanical mosquito repellent and preparation method thereof | |
| KR20110045440A (en) | Mosquito repellent compositions | |
| CN107897217A (en) | A kind of natural volatile mosquito driving and killing agent of plant source property and preparation method thereof | |
| CN108450475A (en) | A kind of mosquito-repellent | |
| CN110024803B (en) | Spirotetramat-containing insecticidal composition and preparation thereof | |
| CN111011401A (en) | Mosquito killing medicament and preparation process thereof | |
| CN106538636A (en) | A kind of plant insecticide and preparation method thereof | |
| KR100484887B1 (en) | Natural composition of repelling mosquitoes | |
| CN1158927C (en) | Prepn. of incense used as herbal mosquito repelling agent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181221 |