CN102784094A - Mosquito dispelling toner for infants, and its preparation method - Google Patents
Mosquito dispelling toner for infants, and its preparation method Download PDFInfo
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- CN102784094A CN102784094A CN2012102511712A CN201210251171A CN102784094A CN 102784094 A CN102784094 A CN 102784094A CN 2012102511712 A CN2012102511712 A CN 2012102511712A CN 201210251171 A CN201210251171 A CN 201210251171A CN 102784094 A CN102784094 A CN 102784094A
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- charophyta
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- aqueous solution
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Abstract
The invention relates to a mosquito dispelling and skin toning product for infants, and provides a mosquito dispelling toner for the infants. The mosquito dispelling toner is characterized in that the mosquito dispelling toner comprises 15-20wt% of a stonewort extract, 1-5wt% of glycerin, 1-5wt% of an emollient, 2-7wt% of sodium hyaluronate, a proper amount of a perfume, and the balance purified water, wherein the stonewort extract is a water-soluble part obtained after removing chlorophyll and polysaccharides from a stonewort ethanol extract. The mosquito dispelling toner provided in the invention has the advantages of no harmful components, simple production technology and low cost.
Description
Technical field
The present invention relates to anophelifuge skin care item for baby, be specifically related to a kind of infant that adopts the hydrotrope in the extract that hangs down charophyta such as algae such as grade to process and use the anophelifuge cosmetic water with anophelifuge effect as main effective ingredient.
Background technology
Chemical compound and derivant thereof that its contained main matter of baby oil mosquito repellent product of selling on the market at present is a cinerins; But there is report to show at present; The pyrethrin compounds can cause toxic action to Fish; Its mosquito repellent product has certain biological safety, so possibly produce some negative effects to infant.
Charophyta is the low water plant of waiting, and distributes extensively, is prone to cultivate, and growth cycle is short, and output is big, and the water-soluble part of its extract also can play repellent effect preferably to culex pipiens pallens and Aedes albopictus except that containing nutrient substance.Almost be blank to the charophyta development and use at present, the infant that especially adopts charophyta to process as main component still belongs to initiative with the anophelifuge skin-protection product.
Summary of the invention
For solving the problem that exists in the prior art; Make full use of natural fragrance taste of charophyta and good repelling effect, the present invention attempts that charophyta is applied to infant and uses the anophelifuge cosmetic water, and the inventor is through repetition test; Successful selection proper supplementary material; Successfully add the charophyta composition to infant and use the anophelifuge cosmetic water as primary raw material, and constantly test, optimum proportioning raw materials scheme and rational processing technology have been proposed.
The present invention provides a kind of infant to use the anophelifuge cosmetic water, it is characterized in that, raw materials in percentage by weight component and content thereof comprise: charophyta extract 15%-20%; Glycerol 1%-5%; Butanediol 1%-5%, hyaluronate sodium 2%-7%, spice is an amount of; All the other are purified water, and the ethanol extraction that wherein said charophyta extract is a charophyta is removed the water-soluble part behind chlorophyll, the polysaccharide.
The present invention also provides a kind of method for preparing infant with the anophelifuge cosmetic water, comprises the steps: that (a) selects fresh charophyta, cleans and removes impurity, and drying in the shade under the room temperature grinds and cross 100 mesh sieves; (b) the charophyta powder that earlier ethanol and step (a) is made according to 10: 1 ratio mixing after, at 30-45 ℃ of concussion lixiviate 7-9h down, isolated by filtration gets the charophyta extracting solution, preferred 36 ℃ shake lixiviate 8h down; (c) step (b) is made the charophyta extracting solution and remove chlorophyll through the 18 alkyl silica gel post; (d) step (c) is made thing and make the charophyta extract 30-45 ℃ of following concentrating under reduced pressure drying, preferred 36 ℃; (e) charophyta extract that step (d) is made and water according to 1: 10 ratio mixing after, lixiviate 7-9h once more under 30-45 ℃, lixiviate 8h once more under preferred 36 ℃, isolated by filtration gets the aqueous solution of charophyta extract; (f) aqueous solution that step (e) is made is through ultrafiltration and distilling under reduced pressure, and 1/2 of the original amount of simmer down to promptly gets the concentrated aqueous solution of charophyta extract; (g) by prescription butanediol, glycerol are mixed, heating for dissolving is oil phase; Get the water-soluble heating of hyaluronate sodium, be water; Oil phase and water are heated to 70-90 ℃, and preferred 80 ℃ pump into the breast pot, stir, and start breast pot homogenizing simultaneously, cool off 30-45 ℃ through recirculated water then, preferred 36 ℃, obtain mixed liquor; (h) concentrated aqueous solution, Fructus Citri Limoniae essence that step (f) are made the charophyta extract add in the mixed liquor of step (g); Stir 10-20min with 300-500r/min speed; Preferred 400r/min speed stirs 15min, is cooled to room temperature then and shifts out, and promptly makes infant with charophyta anophelifuge cosmetic water.
Compare the present invention with method for preparing with prior art and product and have following characteristics: (1) as the anophelifuge main component, uses saferly the charophyta extract, is that infant provides the anophelifuge effect in skin protection; (2) the reasonable raw material proportioning has reduced the production cost when guaranteeing skin protection and anophelifuge effect; (3) step of preparation process is reasonable, is easy to produce.
The specific embodiment
Infant is with the preparation of anophelifuge cosmetic water:
Composition of raw materials: the raw materials in percentage by weight component comprises: charophyta extract 15%-20%, and glycerol 1%-5%, butanediol 1%-5%, hyaluronate sodium and spice are an amount of, and all the other are purified water.
Embodiment one
(a) select fresh charophyta, clean and remove impurity, drying in the shade under the room temperature grinds and crosses 100 mesh sieves;
(b) the charophyta powder that earlier ethanol and step (a) is made according to 10: 1 ratio mixing after, at 30 ℃ of concussion lixiviate 7h down, isolated by filtration gets the charophyta extracting solution;
(c) step (b) is made the charophyta extracting solution and remove chlorophyll through the 18 alkyl silica gel post;
(d) step (c) is made thing and make the charophyta extract 30 ℃ of following concentrating under reduced pressure dryings;
(e) charophyta extract that step (d) is made and water according to 1: 10 ratio mixing after, lixiviate 7h once more under 30 ℃, isolated by filtration gets the aqueous solution of charophyta extract;
(f) aqueous solution that step (e) is made is through ultrafiltration and distilling under reduced pressure, and 1/2 of the original amount of simmer down to promptly gets the concentrated aqueous solution of charophyta extract;
(g) by prescription butanediol, glycerol are mixed, heating for dissolving is oil phase; Get the water-soluble heating of hyaluronate sodium, be water; Oil phase and water are heated to 70 ℃ pump into the breast pot, stir, start breast pot homogenizing simultaneously, cool off to 30 ℃ through recirculated water then, obtain mixed liquor;
(h) concentrated aqueous solution, Fructus Citri Limoniae essence that step (f) are made the charophyta extract add in the mixed liquor of step (g), stir 10min with 300r/min speed, are cooled to room temperature then and shift out, and promptly make infant with charophyta anophelifuge cosmetic water.
In the present embodiment, the raw materials in percentage by weight component comprises: charophyta extract 15%, and glycerol 1%, butanediol 1%, hyaluronate sodium 2%, Fructus Citri Limoniae essence 0.5%, all the other are purified water.
Use the cosmetic water of example preparation thus, by the detection method detection of GB GB-T17322.01-1998, the skin of exposure does not have mosquito bite in 2.0h, can reach repelling effect preferably; In the stability test, place the 24h taking-up in-5 ℃ ± 2 ℃ refrigerators and return to the room temperature observation, do not have deposition and do not have metachromatism; Opaque products is haze-free; 40 ℃ ± 1 ℃ couveuse is placed the 24h taking-up and is returned to the room temperature observation, does not have deposition and does not have metachromatism, and opaque products is haze-free.
Embodiment two
(a) select fresh charophyta, clean and remove impurity, drying in the shade under the room temperature grinds and crosses 100 mesh sieves;
(b) the charophyta powder that earlier ethanol and step (a) is made according to 10: 1 ratio mixing after, at 36 ℃ of concussion lixiviate 8h down, isolated by filtration gets the charophyta extracting solution;
(c) step (b) is made the charophyta extracting solution and remove chlorophyll through the 18 alkyl silica gel post;
(d) step (c) is made thing and make the charophyta extract 36 ℃ of following concentrating under reduced pressure dryings;
(e) charophyta extract that step (d) is made and water according to 1: 10 ratio mixing after, lixiviate 8h once more under 36 ℃, isolated by filtration gets the aqueous solution of charophyta extract;
(f) aqueous solution that step (e) is made is through ultrafiltration and distilling under reduced pressure, and 1/2 of the original amount of simmer down to promptly gets the concentrated aqueous solution of charophyta extract;
(g) by prescription butanediol, glycerol are mixed, heating for dissolving is oil phase; Get the water-soluble heating of hyaluronate sodium, be water; Oil phase and water are heated to 80 ℃ pump into the breast pot, stir, start breast pot homogenizing simultaneously, cool off to 36 ℃ through recirculated water then, obtain mixed liquor;
(h) concentrated aqueous solution, Fructus Citri Limoniae essence that step (f) are made the charophyta extract add in the mixed liquor of step (g), stir 15min with 400r/min speed, are cooled to room temperature then and shift out, and promptly make infant with charophyta anophelifuge cosmetic water.
In the present embodiment, the raw materials in percentage by weight component comprises: charophyta extract 17%, and glycerol 3%, butanediol 3%, hyaluronate sodium 5%, Fructus Citri Limoniae essence 1%, all the other are purified water.
Use the cosmetic water of example preparation thus, by the detection method detection of GB GB-T17322.01-1998, the skin of exposure does not have mosquito bite in 3.3h, can reach repelling effect preferably; In the stability test, place the 24h taking-up in-5 ℃ ± 2 ℃ refrigerators and return to the room temperature observation, do not have deposition and do not have metachromatism; Opaque products is haze-free; 40 ℃ ± 1 ℃ couveuse is placed the 24h taking-up and is returned to the room temperature observation, does not have deposition and does not have metachromatism, and opaque products is haze-free.。
Embodiment three
(a) select fresh charophyta, clean and remove impurity, drying in the shade under the room temperature grinds and crosses 100 mesh sieves;
(b) the charophyta powder that earlier ethanol and step (a) is made according to 10: 1 ratio mixing after, at 45 ℃ of concussion lixiviate 9h down, isolated by filtration gets the charophyta extracting solution;
(c) step (b) is made the charophyta extracting solution and remove chlorophyll through the 18 alkyl silica gel post;
(d) step (c) is made thing and make the charophyta extract 45 ℃ of following concentrating under reduced pressure dryings;
(e) charophyta extract that step (d) is made and water according to 1: 10 ratio mixing after, lixiviate 9h once more under 45 ℃, isolated by filtration gets the aqueous solution of charophyta extract;
(f) aqueous solution that step (e) is made is through ultrafiltration and distilling under reduced pressure, and 1/2 of the original amount of simmer down to promptly gets the concentrated aqueous solution of charophyta extract;
(g) by prescription butanediol, glycerol are mixed, heating for dissolving is oil phase; Get the water-soluble heating of hyaluronate sodium, be water; Oil phase and water are heated to 90 ℃ pump into the breast pot, stir, start breast pot homogenizing simultaneously, cool off to 45 ℃ through recirculated water then, obtain mixed liquor;
(h) concentrated aqueous solution, Fructus Citri Limoniae essence that step (f) are made the charophyta extract add in the mixed liquor of step (g), stir 20min with 500r/min speed, are cooled to room temperature then and shift out, and promptly make infant with charophyta anophelifuge cosmetic water.。
In the present embodiment, the raw materials in percentage by weight component comprises: charophyta extract 20%, and glycerol 5%, butanediol 5%, hyaluronate sodium 7%, Fructus Citri Limoniae essence 2%, all the other are purified water.
Use the cosmetic water of example preparation thus, by the detection method detection of GB GB-T17322.01-1998, the skin of exposure does not have mosquito bite in 3.1h, can reach repelling effect preferably; In the stability test, place the 24h taking-up in-5 ℃ ± 2 ℃ refrigerators and return to the room temperature observation, do not have deposition and do not have metachromatism; Opaque products is haze-free; 40 ℃ ± 1 ℃ couveuse is placed the 24h taking-up and is returned to the room temperature observation, does not have deposition and does not have metachromatism, and opaque products is haze-free.
In design of the present invention and the process of the test, the effort below the inventor has mainly made:
1, creatively proposed fragrant odour, charophyta with advantages such as repelling effects are incorporated in the infant cosmetic water as important source material, overcome traditional cosmetic water and had possibility causes dysgenic chemical constituent to infant shortcoming.
2,,, successfully the charophyta extract is joined in baby's cosmetic water, and propose optimum proportioning raw materials and preparation technology parameter through adding appropriate amount of auxiliary materials through repetition test.Through evidence the repelling effect and the stability of product.
The above is merely preferred embodiment of the present invention, and is in order to restriction the present invention, not all within spirit of the present invention and principle, any modification of being made, is equal to replacement, improvement etc., all should be included within the scope that the present invention protects.
Claims (5)
1. an infant is used the anophelifuge cosmetic water, it is characterized in that, raw materials in percentage by weight component and content thereof comprise:
Charophyta extract 15%-20%,
Glycerol 1%-5%,
Emollient 1%-5%,
Hyaluronate sodium 2%-7%,
Spice is an amount of,
All the other are purified water,
The ethanol extraction that wherein said charophyta extract is a charophyta is removed the water-soluble part behind chlorophyll, the polysaccharide.
2. infant as claimed in claim 1 is used the anophelifuge cosmetic water, it is characterized in that, said emollient is a butanediol, and said spice is Fructus Citri Limoniae essence.
3. infant as claimed in claim 2 is used the anophelifuge cosmetic water, it is characterized in that, raw materials in percentage by weight component and content thereof are: charophyta extract 18%, and glycerol 3%, butanediol 3%, hyaluronate sodium 5% and Fructus Citri Limoniae essence 1%, all the other are purified water.
4. one kind prepares like claim 1, the 2 or 3 described infant method with the anophelifuge cosmetic water, comprises the steps:
(a) select fresh charophyta, clean and remove impurity, drying in the shade under the room temperature grinds and crosses 100 mesh sieves;
(b) the charophyta powder that earlier ethanol and step (a) is made according to 10: 1 ratio mixing after, at 30-45 ℃ of concussion lixiviate 7-9h down, isolated by filtration gets the charophyta extracting solution;
(c) step (b) is made the charophyta extracting solution and remove chlorophyll through the 18 alkyl silica gel post;
(d) step (c) is made thing and make the charophyta extract 30-45 ℃ of following concentrating under reduced pressure drying;
(e) charophyta extract that step (d) is made and water according to 1: 10 ratio mixing after, lixiviate 7-9h once more under 30-45 ℃, isolated by filtration gets the aqueous solution of charophyta extract;
(f) aqueous solution that step (e) is made is through ultrafiltration and distilling under reduced pressure, and 1/2 of the original amount of simmer down to promptly gets the concentrated aqueous solution of charophyta extract;
(g) by prescription butanediol, glycerol are mixed, heating for dissolving is oil phase; Get the water-soluble heating of hyaluronate sodium, be water; Oil phase and water are heated to 70-90 ℃ pump into the breast pot, stir, start breast pot homogenizing simultaneously, cool off 30-45 ℃ through recirculated water then, obtain mixed liquor;
(h) concentrated aqueous solution, Fructus Citri Limoniae essence that step (f) are made the charophyta extract add in the mixed liquor of step (g), stir 10-20min with 300-500r/min speed, are cooled to room temperature then and shift out, and promptly make infant with charophyta anophelifuge cosmetic water.
5. one kind prepares like claim 1, the 2 or 3 described infant method with the anophelifuge cosmetic water, comprises the steps:
(a) select fresh charophyta, clean and remove impurity, drying in the shade under the room temperature grinds and crosses 100 mesh sieves;
(b) the charophyta powder that earlier ethanol and step (a) is made according to 10: 1 ratio mixing after, at 36 ℃ of concussion lixiviate 8h down, isolated by filtration gets the charophyta extracting solution;
(c) step (b) is made the charophyta extracting solution and remove chlorophyll through the 18 alkyl silica gel post;
(d) step (c) is made thing and make the charophyta extract 36 ℃ of following concentrating under reduced pressure dryings;
(e) charophyta extract that step (d) is made and water according to 1: 10 ratio mixing after, lixiviate 8h once more under 36 ℃, isolated by filtration gets the aqueous solution of charophyta extract;
(f) aqueous solution that step (e) is made is through ultrafiltration and distilling under reduced pressure, and 1/2 of the original amount of simmer down to promptly gets the concentrated aqueous solution of charophyta extract;
(g) by prescription butanediol, glycerol are mixed, heating for dissolving is oil phase; Get the water-soluble heating of hyaluronate sodium, be water; Oil phase and water are heated to 80 ℃ pump into the breast pot, stir, start breast pot homogenizing simultaneously, cool off to 36 ℃ through recirculated water then, obtain mixed liquor;
(h) concentrated aqueous solution, Fructus Citri Limoniae essence that step (f) are made the charophyta extract add in the mixed liquor of step (g), stir 15min with 400r/min speed, are cooled to room temperature then and shift out, and promptly make infant with charophyta anophelifuge cosmetic water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012102511712A CN102784094A (en) | 2012-07-19 | 2012-07-19 | Mosquito dispelling toner for infants, and its preparation method |
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| CN2012102511712A CN102784094A (en) | 2012-07-19 | 2012-07-19 | Mosquito dispelling toner for infants, and its preparation method |
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| CN102784094A true CN102784094A (en) | 2012-11-21 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106137855A (en) * | 2016-08-17 | 2016-11-23 | 朱维 | A kind of natural infant mosquito-driving liquid containing Thallus Porphyrae extract |
| CN109042755A (en) * | 2018-08-07 | 2018-12-21 | 刘经校 | A kind of culicifuge and preparation method thereof from plant extracts |
-
2012
- 2012-07-19 CN CN2012102511712A patent/CN102784094A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106137855A (en) * | 2016-08-17 | 2016-11-23 | 朱维 | A kind of natural infant mosquito-driving liquid containing Thallus Porphyrae extract |
| CN109042755A (en) * | 2018-08-07 | 2018-12-21 | 刘经校 | A kind of culicifuge and preparation method thereof from plant extracts |
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Application publication date: 20121121 |