CN108997040A - A kind of preparation method of mango special fertilizer material - Google Patents
A kind of preparation method of mango special fertilizer material Download PDFInfo
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- CN108997040A CN108997040A CN201810838576.3A CN201810838576A CN108997040A CN 108997040 A CN108997040 A CN 108997040A CN 201810838576 A CN201810838576 A CN 201810838576A CN 108997040 A CN108997040 A CN 108997040A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D3/00—Calcareous fertilisers
- C05D3/02—Calcareous fertilisers from limestone, calcium carbonate, calcium hydrate, slaked lime, calcium oxide, waste calcium products
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/50—Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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Abstract
The invention belongs to technical field of fertilizers, and in particular to a kind of preparation method of mango special fertilizer material specifically includes the pretreatment of (1) first timber；(2) following raw material is weighed according to parts by weight: 30-50 parts of pretreated first timber, 10-20 parts of fresh cane skin, 10-20 parts of rabbit excrement, 5-10 parts of phosphorus tailing, 10-25 parts of vinasse, 8-15 parts of sludge, 10-15 parts of soybean residue, 3-5 parts of EM bacterium, 3-5 parts of cellulase in step (1)；(3) raw material in step (2) is subjected to processing post-fermentation and mango special fertilizer material is prepared.Mango special fertilizer material of the invention has that nutrition is complete can satisfy Growth of Mango demand, and environmentally protective, can improve the nutrient content of soil, improve the hardened phenomenon of soil；The applicant can also effectively raise the yield and quality of mango by the test in orchard, and then can increase economic benefit.
Description
[technical field]
The invention belongs to technical field of fertilizers, and in particular to a kind of preparation method of mango special fertilizer material.
[background technique]
Mango is the fruit being favored by people, big in the cultivated area of the Bose City of our province.In recent years, green ecological
Nuisanceless mango has become the Objective Necessity requirement of mango fruit industry development.And it largely applies chemical fertilizer and the soil organism is supplemented
Deficiency, soil hardening, soil fertility decline, and chemical fertilizer in the market does not have specific aim, designs for the growth characteristics of mango, so that
Nutrients ratio is uncoordinated, leads to soil nutrient proportional imbalance, and mango nutritional deficiency physiological disturbance happens occasionally；So that mango
Yield and quality is severely impacted.Therefore, it is extremely urgent to design a kind of mango special fertilizer material.
Current old wood furniture is mostly to be transformed into new wood furniture after being recovered or be processed into compression plate, is processed into compression
One processing mode of plate, wood surface mopping mask is toxic before existing, and will affect the quality of compression plate, toxic detecting
, also there is the method for first removing lacquer painting in the problem of off analysis, or directly cuts away lacquer painting, cuts the processing of panel still
There is an environmentally friendly solution to appear.
[summary of the invention]
The object of the present invention is to provide a kind of preparation method of mango special fertilizer material, which has the complete energy of nutrition
Enough meet Growth of Mango demand, and environmentally protective, the nutrient content of soil can be improved, improves the hardened phenomenon of soil；This
Applicant can also effectively raise the yield and quality of mango by the test in orchard, and then can increase economic benefit.
To achieve the goals above, The technical solution adopted by the invention is as follows:
A kind of preparation method of mango special fertilizer material, the specific steps are as follows:
The pretreatment of (1) first timber: waste and old furniture is recycled, and is carried out the utilization of timber secondary recovery, is first sorted out appearance
Face is the furniture of yellow and white, is cut furniture outer using cutting machine, 1-1.5cm behind the surface layer of cutting obtains surface layer
Plank clast is broken to after 1cm and obtains plank clast by plank, and it is 20-30% that mass concentration, which is added, according to 1 kilogram of plank clast
2 kilograms of acetic acid of ratio impregnated in processing pond 3-5 hours, be then sprinkled into pulverized limestone, it is broken that the additional amount of pulverized limestone accounts for plank
Bits and acetic acid gross mass 0.05, the adding manner of pulverized limestone is to be slowly added into processing pond while stirring, add pulverized limestone after
It is continuous to be stirred continuously 10-15 minutes, plank clast is then salvaged, the outer surface of plank clast is rinsed well using clear water, is connect
Plank clast is kept moisture content is 10%-20%, discarded molasses are added, the additional amount for discarding molasses is plank clast gross weight
After mixing, fermentation Mixed Microbes are added in the 1/2 of amount, and the amount of the fermentation Mixed Microbes of addition is plank clast total weight
0.01%, heap is built after being followed by stirring for uniformly and is fermented 20-30 days, then filters out fermentation Mixed Microbes, the first timber can be obtained；
The fermentation Mixed Microbes include in parts by weight 1-3 parts of germ oligotrophy unit cell, 1-3 parts of bacillus,
1-3 parts of Penicillium notatum；
(2) following raw material is weighed according to parts by weight: 30-50 parts of pretreated first timber in step (1), fresh sweet
10-20 parts of sugarcane skin, 10-20 parts of rabbit excrement, 5-10 parts of phosphorus tailing, 10-25 parts of vinasse, 8-15 parts of sludge, 10-15 parts of soybean residue, EM
3-5 parts of bacterium, 3-5 parts of cellulase；
(3) raw material in step (2) is subjected to processing post-fermentation and mango special fertilizer material is prepared, concrete operations are as follows:
A, after being crushed fresh cane skin, cellulase is added and mixes, accumulates 2-3 hours；
B, warm water is added in EM bacterium, the ratio of EM bacterium and warm water is 1g:100ml, is subsequently added into mango polysaccharide, mango polysaccharide
Weight ratio with EM bacterium is 1:2；
C, rabbit excrement is put into process tank the progress anaerobic expanded explosion of high pressure, the time of pressure 60-80MPa, explosion is
20-30S after explosion, continues to be placed in process tank Anaerobic Treatment 20-30 minutes；
D, carry out the phosphorus tailing to be crushed 10 meshes and obtain phosphorus tailing powder, then carry out being preheated to 40-45 DEG C, then plus
Enter organic acid grind 1-3 minutes, the weight ratio of organic acid and phosphorus tailing powder is 1:2-3；The organic acid be lactic acid,
Malic acid, tartaric acid are obtained by mixing according to weight ratio for 1:2-3:3-5；
E, step a, b, c, d treated raw material are taken out, pre fermentation material are obtained after mixing with vinasse, sludge, soybean residue,
Then the entrance of screw conveyor is put into, screw conveyor launches pre fermentation material from screw conveyor outlet, into fermentation vat,
The lid of fermentation vat is covered, venthole is reserved on lid, guarantees have oxygen to be passed through in fermentation vat, after fermentation 20-30 days
Obtain mango special fertilizer material.
It further illustrates, in step (1), discards molasses before being added as raw material, first pass through and be preheated to 40 DEG C.
It further illustrates, in step (1), the viable count of the germ oligotrophy unit cell is hundred million CFU/ of 1.01-1.35
ML, bacillus viable count be hundred million CFU/mL of 1.24-1.52, the viable count of Penicillium notatum is hundred million CFU/mL of 0.68-0.85.
It further illustrates, C1 enzyme, Cx enzyme and β glucosidase accounting are 15:4:1 in the cellulase, and enzyme activity is
9000-10000 unit/mL.
It further illustrates, the temperature of the warm water is 38-42 DEG C.
It further illustrates, the vinasse are that He Prefecture China Resources group prepares the vinasse generated after Snowflake Beer, neutrality in vinasse
Wash fiber 36.08%, acid detergent fiber 22.33%, lignin 2.96%, soluble protein 5.12%, crude fibre
11.39%.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:
Old timber is recycled the lacquer painting disposed and is recycled by the application, as fermentation fertilizer raw material it
One, a kind of environment-friendly treatment method can be effectively provided, timber can effectively reduce lead content after treatment, ferment
One of the available fertilizer element in dedicated fertilizer is acted on after afterwards carbons a large amount of in timber capable of being discharged.The raw material of the application is rich
Containing big, middle and trace element, after the technological means processing of the application, carbon-nitrogen ratio content is reasonable, and fertilizer efficiency is high.
[specific embodiment]
In the following description, numerous specific details are set forth in order to facilitate a full understanding of the present invention.But the present invention can be with
Much it is different from other way described herein to implement, those skilled in the art can be without prejudice to intension of the present invention the case where
Under do similar improvement, therefore the present invention is not limited to the specific embodiments disclosed below.
The vinasse of buying are that He Prefecture China Resources group prepares the vinasse generated after Snowflake Beer, neutral detergent fiber in vinasse
36.08%, acid detergent fiber 22.33%, lignin 2.96%, soluble protein 5.12%, crude fibre 11.39%.
Embodiment 1:
A kind of preparation method of mango special fertilizer material, the specific steps are as follows:
The pretreatment of (1) first timber: waste and old furniture is recycled, and is carried out the utilization of timber secondary recovery, is first sorted out appearance
Face is the furniture of yellow and white, is cut furniture outer using cutting machine, and 1cm behind the surface layer of cutting obtains surface layer plank,
Plank clast is broken to after 1cm and obtains plank clast, the acetic acid 2 that mass concentration is 20% is added according to 1 kilogram of plank clast
Kilogram ratio impregnated in processing pond 3 hours, be then sprinkled into pulverized limestone, the additional amount of pulverized limestone accounts for plank clast and acetic acid is total
The 0.05 of quality, the adding manner of pulverized limestone are to be slowly added into processing pond while stirring, add pulverized limestone and keep stirring
10 minutes, plank clast is then salvaged, the outer surface of plank clast is rinsed well using clear water, then protects plank clast
Holding moisture content is 10%, and addition is preheated to 40 DEG C of discarded molasses, and the additional amount for discarding molasses is the 1/ of plank clast total weight
2, after mixing, fermentation Mixed Microbes are added, the amount of the fermentation Mixed Microbes of addition is the 0.01% of plank clast total weight, then
Heap is built after mixing evenly to ferment 30 days, then filters out fermentation Mixed Microbes, the first timber can be obtained；
The fermentation Mixed Microbes include the thermophilic malt oligotrophy unit cell that viable count is 1.01 hundred million CFU/mL in parts by weight
1 part of bacterium, 1 part of the bacillus that viable count is 1.24 hundred million CFU/mL, 1 part of Penicillium notatum that viable count is 0.68 hundred million CFU/mL；
(2) following raw material is weighed according to parts by weight: 30 parts of pretreated first timber, fresh cane in step (1)
10 parts of skin, 10 parts of rabbit excrement, 5 parts of phosphorus tailing, 10 parts of vinasse, 8 parts of sludge, 10 parts of soybean residue, 3 parts of EM bacterium, 3 parts of cellulase；
(3) raw material in step (2) is subjected to processing post-fermentation and mango special fertilizer material is prepared, concrete operations are as follows:
A, by fresh cane skin it is broken after, additions enzyme activity is 9000 units/mL, and C1 enzyme, Cx enzyme and β glucosidase accounting
It mixes, accumulates 2 hours for the cellulase of 15:4:1；
B, EM bacterium is added 38 DEG C of warm water, the ratio of EM bacterium and warm water is 1g:100ml, is subsequently added into mango polysaccharide, awns
Fruit polysaccharide and the weight ratio of EM bacterium are 1:2；
C, rabbit excrement being put into the progress anaerobic expanded explosion of high pressure in process tank, pressure 60MPa, the time of explosion is 20S,
After explosion, continue to be placed on Anaerobic Treatment 20 minutes in process tank；
D, it carries out the phosphorus tailing to be crushed 10 meshes and obtains phosphorus tailing powder, then carry out being preheated to 40 DEG C, then be added
Organic acid grind 1 minute, and the weight ratio of organic acid and phosphorus tailing powder is 1:2；The organic acid is lactic acid, apple
Acid, tartaric acid are obtained by mixing according to weight ratio for 1:2:3；
E, step a, b, c, d treated raw material are taken out, pre fermentation material are obtained after mixing with vinasse, sludge, soybean residue,
Then the entrance of screw conveyor is put into, screw conveyor launches pre fermentation material from screw conveyor outlet, into fermentation vat,
The lid of fermentation vat is covered, venthole is reserved on lid, guarantees have oxygen to be passed through in fermentation vat, after fermentation 20 days, can obtain
To mango special fertilizer material.
Embodiment 2:
A kind of preparation method of mango special fertilizer material, the specific steps are as follows:
The pretreatment of (1) first timber: waste and old furniture is recycled, and is carried out the utilization of timber secondary recovery, is first sorted out appearance
Face is the furniture of yellow and white, is cut furniture outer using cutting machine, 1.5cm behind the surface layer of cutting, and surface layer wood is obtained
Plank clast is broken to after 1cm and obtains plank clast by plate, and the vinegar that mass concentration is 30% is added according to 1 kilogram of plank clast
The ratio of 2 kilograms of acid is impregnated 5 hours in processing pond, is then sprinkled into pulverized limestone, the additional amount of pulverized limestone accounts for plank clast and vinegar
The 0.05 of sour gross mass, the adding manner of pulverized limestone are to be slowly added into processing pond while stirring, add pulverized limestone and keep
Stirring 15 minutes, is then salvaged plank clast, is rinsed well the outer surface of plank clast using clear water, then that plank is broken
It is 20% that bits, which keep moisture content, and addition is preheated to 40 DEG C of discarded molasses, and the additional amount for discarding molasses is plank clast total weight
1/2, after mixing, fermentation Mixed Microbes are added, the amounts of the fermentation Mixed Microbes of addition is the 0.01% of plank clast total weight,
Heap is built after being followed by stirring for uniformly to ferment 20 days, then filters out fermentation Mixed Microbes, the first timber can be obtained；
The fermentation Mixed Microbes include the thermophilic malt oligotrophy unit cell that viable count is 1.35 hundred million CFU/mL in parts by weight
3 parts of bacterium, 3 parts of the bacillus that viable count is 1.52 hundred million CFU/mL, 3 parts of Penicillium notatum that viable count is 0.85 hundred million CFU/mL；
(2) following raw material is weighed according to parts by weight: 50 parts of pretreated first timber, fresh cane in step (1)
20 parts of skin, 20 parts of rabbit excrement, 10 parts of phosphorus tailing, 25 parts of vinasse, 15 parts of sludge, 15 parts of soybean residue, 5 parts of EM bacterium, 5 parts of cellulase；
(3) raw material in step (2) is subjected to processing post-fermentation and mango special fertilizer material is prepared, concrete operations are as follows:
A, after being crushed fresh cane skin, addition enzyme activity is 10000 units/mL, and C1 enzyme, Cx enzyme and β glucosidase account for
Than the cellulase mixing for 15:4:1, accumulate 3 hours；
B, EM bacterium is added 42 DEG C of warm water, the ratio of EM bacterium and warm water is 1g:100ml, is subsequently added into mango polysaccharide, awns
Fruit polysaccharide and the weight ratio of EM bacterium are 1:2；
C, rabbit excrement being put into the progress anaerobic expanded explosion of high pressure in process tank, pressure 80MPa, the time of explosion is 30S,
After explosion, continue to be placed on Anaerobic Treatment 30 minutes in process tank；
D, it carries out the phosphorus tailing to be crushed 10 meshes and obtains phosphorus tailing powder, then carry out being preheated to 45 DEG C, then be added
Organic acid grind 3 minutes, and the weight ratio of organic acid and phosphorus tailing powder is 1:3；The organic acid is lactic acid, apple
Acid, tartaric acid are obtained by mixing according to weight ratio for 1:3:5；
E, step a, b, c, d treated raw material are taken out, pre fermentation material are obtained after mixing with vinasse, sludge, soybean residue,
Then the entrance of screw conveyor is put into, screw conveyor launches pre fermentation material from screw conveyor outlet, into fermentation vat,
The lid of fermentation vat is covered, venthole is reserved on lid, guarantees have oxygen to be passed through in fermentation vat, after fermentation 30 days, can obtain
To mango special fertilizer material.
Embodiment 3:
A kind of preparation method of mango special fertilizer material, the specific steps are as follows:
The pretreatment of (1) first timber: waste and old furniture is recycled, and is carried out the utilization of timber secondary recovery, is first sorted out appearance
Face is the furniture of yellow and white, is cut furniture outer using cutting machine, 1.2cm behind the surface layer of cutting, and surface layer wood is obtained
Plank clast is broken to after 1cm and obtains plank clast by plate, and the vinegar that mass concentration is 25% is added according to 1 kilogram of plank clast
2 kilograms of ratio of acid is impregnated 3.5 hours in processing pond, is then sprinkled into pulverized limestone, the additional amount of pulverized limestone account for plank clast with
The 0.05 of acetic acid gross mass, the adding manner of pulverized limestone are to be slowly added into processing pond while stirring, add pulverized limestone and continue not
Disconnected stirring 13 minutes, is then salvaged plank clast, is rinsed well the outer surface of plank clast using clear water, then by plank
It is 15% that clast, which keeps moisture content, and addition is preheated to 40 DEG C of discarded molasses, and the additional amount for discarding molasses is plank clast gross weight
After mixing, fermentation Mixed Microbes are added in the 1/2 of amount, and the amount of the fermentation Mixed Microbes of addition is plank clast total weight
0.01%, heap is built after being followed by stirring for uniformly and is fermented 23 days, then filters out fermentation Mixed Microbes, the first timber can be obtained；
The fermentation Mixed Microbes include the thermophilic malt oligotrophy unit cell that viable count is 1.14 hundred million CFU/mL in parts by weight
2 parts of bacterium, 2 parts of the bacillus that viable count is 1.34 hundred million CFU/mL, 2 parts of Penicillium notatum that viable count is 0.72 hundred million CFU/mL；
(2) following raw material is weighed according to parts by weight: 40 parts of pretreated first timber, fresh cane in step (1)
16 parts of skin, 17 parts of rabbit excrement, 7 parts of phosphorus tailing, 18 parts of vinasse, 10 parts of sludge, 12 parts of soybean residue, 4 parts of EM bacterium, 4 parts of cellulase；
(3) raw material in step (2) is subjected to processing post-fermentation and mango special fertilizer material is prepared, concrete operations are as follows:
A, by fresh cane skin it is broken after, additions enzyme activity is 9500 units/mL, and C1 enzyme, Cx enzyme and β glucosidase accounting
It mixes, accumulates 2.5 hours for the cellulase of 15:4:1；
B, EM bacterium is added 40 DEG C of warm water, the ratio of EM bacterium and warm water is 1g:100ml, is subsequently added into mango polysaccharide, awns
Fruit polysaccharide and the weight ratio of EM bacterium are 1:2；
C, rabbit excrement being put into the progress anaerobic expanded explosion of high pressure in process tank, pressure 70MPa, the time of explosion is 25S,
After explosion, continue to be placed on Anaerobic Treatment 25 minutes in process tank；
D, it carries out the phosphorus tailing to be crushed 10 meshes and obtains phosphorus tailing powder, then carry out being preheated to 42 DEG C, then be added
Organic acid grind 2 minutes, and the weight ratio of organic acid and phosphorus tailing powder is 1:2；The organic acid is lactic acid, apple
Acid, tartaric acid are obtained by mixing according to weight ratio for 1:3:4；
E, step a, b, c, d treated raw material are taken out, pre fermentation material are obtained after mixing with vinasse, sludge, soybean residue,
Then the entrance of screw conveyor is put into, screw conveyor launches pre fermentation material from screw conveyor outlet, into fermentation vat,
The lid of fermentation vat is covered, venthole is reserved on lid, guarantees have oxygen to be passed through in fermentation vat, after fermentation 28 days, can obtain
To mango special fertilizer material.
Comparative example 1:
Essentially identical with 3 step of embodiment, difference is, the first timber pre-processes in step (1), only to picking out
Outer surface is the furniture of yellow and white, is cut furniture outer using cutting machine, 1.2cm behind the surface layer of cutting obtains table
Layer plank, plank clast is broken to after 1cm and obtains plank clast.
Comparative example 2:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), and acetic acid is replaced using water
It changes.
Comparative example 3:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), does not carry out alkaline place
Reason.
Comparative example 4:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), and discarded molasses do not carry out
The pre-heat treatment.
Comparative example 5:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), is mixed without fermentation
Discarded molasses are not added in bacterium processing yet.
Comparative example 6:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), in Mixed Microbes of fermenting only
Contain 2 parts of germ oligotrophy unit cell that viable count is 1.14 hundred million CFU/mL.
Comparative example 7:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), in Mixed Microbes of fermenting only
Contain 2 parts of bacillus that viable count is 1.34 hundred million CFU/mL.
Comparative example 8:
Essentially identical with 3 step of embodiment, difference is that the first timber pre-processes in step (1), in Mixed Microbes of fermenting only
Contain 2 parts of Penicillium notatum that viable count is 0.72 hundred million CFU/mL.
Test 1:
The detection of lead element ingredient, the knot of detection are carried out to the first timber that embodiment 1-3 and comparative example 1-8 are prepared
Fruit is as follows:
Table 1
| Lead content μ g/g before handling | Lead content μ g/g after processing | |
| Embodiment 1 | 518±12 | 88±12 |
| Embodiment 2 | 500±15 | 75±10 |
| Embodiment 3 | 514±12 | 44±11 |
| Comparative example 1 | 514±12 | 507±8 |
| Comparative example 2 | 514±12 | 192±10 |
| Comparative example 3 | 514±12 | 188±7 |
| Comparative example 4 | 514±12 | 207±11 |
| Comparative example 5 | 514±12 | 298±12 |
| Comparative example 6 | 514±12 | 328±10 |
| Comparative example 7 | 514±12 | 346±9 |
| Comparative example 8 | 514±12 | 337±11 |
It is seen by upper table 1, the removal rate using the lead element of only a few scheme treated the first timber of the application reaches
80% or more；It is phase using acidification, basic treatment and microbiological treatment collective effect in terms of embodiment 3 and comparative example 1-4
It mutually acts synergistically, if only single use removal rate is without so significant, 1 removal rate of comparative example is almost unchanged, comparative example 2 is gone
Reach 59.7% except rate reaches 62.6%, comparative example, 3 removal rate and reaches 63.4%, comparative example, 4 removal rate, is used in comparative example 4
Microbiological treatment but blackstrap are not handled reasonably, so that removal rate effect is also not so obvious, from right
Ratio 5 is seen, microbiological treatment is not added with, and removal rate reaches 42%, this illustrates three factors to the shadow of removal lead element effect
Sound is ordered as microbiological treatment > basic treatment > acidification；In terms of from the removal rate of comparative example 5-8 and the present embodiment, using three
Kind strain collective effect carries out microbiological treatment, and effect can be more preferable, and 6 removal rate of comparative example reaches 36.2%, comparative example, 7 removal rate
Reach 32.6%, comparative example, 8 removal rate and reach 34.4%, illustrates in microbiological treatment to the influential effect of lead element more
Significantly.
Plank clast first carries out to after acidification then biological treatment can be effective carrying out basic treatment in the application
Remove the content of noxious material lead element；Acidification can soften lead composition, will be disengaged from plank clast, then use pulverized limestone, meet
Start to generate heat to acetic acid and be neutralized with acetic acid, and the lead element released is wrapped up, lead element under conditions of heat
More towards being adsorbed on lime, it then will salvage on the plank clast to get up and also speckle with some lime, repeatedly rinsed using clear water
Fall, then mix molasses and plank clast, molasses have preferably viscosity through excess temperatureization, can gather around when stirring with plank clast
Plank clast has when having certain thickness that molasses is enabled slowly to be absorbed into the heat calcination due to passing through pulverized limestone
Porous surface, the fermentation Mixed Microbes added so more uniform can be distributed growth on plank clast, and can be most
Growing in plank chip surface for short distance, can further remove absorption lead element, effectively reduce on plank clast
Toxic lead element content, until fermentation Mixed Microbes enrichment intracellular after, filter out fermentation Mixed Microbes after lead content can be obtained
First timber up to standard, enables the first timber to discharge nutritious substance in subsequent fermentation, has reached that nocuousness is useless
The purpose that gurry environmental protection utilizes, and the reason of recycling that have opened one new.
Test 2:
Control group 1: identical as the raw material of embodiment 2, difference is that fresh cane skin, rabbit excrement, phosphorus tailing do not carry out reality
The additional pre-treatment of example 2 is applied, and is put into screw conveyor using after directly being mixed with other raw materials.
Control group 2: identical as the raw material of embodiment 2, difference is that fresh cane skin does not carry out the additional pre- of embodiment 2
Processing, and put into screw conveyor using after directly being mixed with other raw materials.
Control group 3: identical as the raw material of embodiment 2, difference is the additional pre-treatment that rabbit excrement does not carry out embodiment 2,
And it is put into screw conveyor using after directly being mixed with other raw materials.
Control group 4: identical as the raw material of embodiment 2, difference is the additional pre- place that phosphorus tailing does not carry out embodiment 2
Reason, and put into screw conveyor using after directly being mixed with other raw materials.
To the mango special fertilizer material that embodiment 1-3 and control group 1-4 are prepared, the detection of nutrient content is carried out -- with often
The analysis of rule method, testing result are as follows:
Table 2
| Organic matter/% | Full nitrogen/mg/kg | Available phosphorus/mg/kg | Available potassium/mg/kg | Effective magnesium/mg/kg | Conductivity/ms/cm | PH value | |
| Embodiment 1 | 1.89±0.24 | 578.15±1.24 | 60.26±0.28 | 74.02±0.14 | 31.05±0.12 | 0.15±0.01 | 5.17 |
| Embodiment 2 | 1.79±0.18 | 564.24±1.47 | 57.69±0.31 | 75.13±0.17 | 32.34±0.11 | 0.13±0.01 | 5.11 |
| Embodiment 3 | 1.82±0.20 | 589.17±1.11 | 67.13±0.26 | 76.79±0.21 | 33.76±0.10 | 0.14±0.00 | 5.23 |
| Contrast groups 1 | 1.01±0.03 | 404.23±1.01 | 30.21±0.12 | 60.13±0.15 | 28.46±0.11 | 0.11±0.00 | 4.98 |
| Contrast groups 2 | 1.29±0.32 | 463.76±2.46 | 49.23±0.16 | 60.34±0.21 | 29.13±0.20 | 0.11±0.01 | 4.89 |
| Contrast groups 3 | 1.31±0.20 | 497.21±2.67 | 50.38±0.17 | 61.47±0.18 | 29.73±0.23 | 0.10±0.01 | 4.67 |
| Contrast groups 4 | 1.75±0.18 | 501.39±3.24 | 40.11±0.15 | 60.25±0.27 | 29.74±0.24 | 0.11±0.00 | 4.87 |
It is seen by upper table, effective magnesium component content difference is little；It is seen on organic matter in the processing step of contrast groups 1-4 and lacks it
Link in as soon as, will affect the release of nutritional ingredient, influences fertility.Control group 1-4 makes a concrete analysis of compared with Example 2, has
Machine matter content control group 1-4 successively reduces by 43.6%, 28%, 26.8%, 2.2% respectively；Total nitrogen content control group 1-4 successively divides
It Jiang Di by 28.4%, 17.8%, 11.8%, 11.1%；Available phosphorus content control group 1-4 successively respectively reduce by 47.6%,
14.68%, 12.6%, 30.4%；Quick-acting potassium content control group 1-4 successively respectively reduce by 19.9%, 91.6%, 18.1%,
19.8%.
Being rich in each raw material in the application has a large amount of organic matter, inorganic matter, can not still be effectively obtained benefit
With, and there are the problem of each raw material it is single be only build heap fermentation, organic matter, the burst size of inorganic matter be not high, benefit
Not high with rate, in order to solve the problems, such as that this is big, the applicant has found after experimental study, and the broken addition of fresh cane skin is fine
After tieing up plain enzyme pre fermentation, cell wall is greatly destroyed, and can be more advantageous to beneficial microorganism during the fermentation and be decomposed it
Organic matter, thus achieve the purpose that improve burst size, and rabbit excrement have stench, contain the substances such as hydrogen sulfide, often progress
The staff of processing fermentation needs to wear several layers of mask house incoming call foul smell, this Shen when building heap processing and observation situation
Ask someone discovery by the anaerobic expanded explosion treatment of high pressure not only can deodorization, and increase the gap between rabbit excrement organic matter, send out
The activation bacterium of ferment can more rapidly sufficient decomposing organic matter element, and the harmful microorganism flora contained in rabbit excrement can be eliminated,
It prevents from being formed with activation bacterium and contradict, influence course of fermentation；Plant mango lack phosphorus can it is serious influence mango growth so that awns
Branches of fruit trees is very thin, and leaf nutrition is bad, and photosynthesis is obstructed, yield degradation, and a large amount of P elements are rich in phosphorus tailing,
But P elements cannot be directly utilized, and all be existed with certain compound, sequestering properties, after the applicant crushes phosphorus tailing
Powder periphery has electronics and energy after preheating, and can be swapped with the structure in phosphorus tailing by the hydroxyl in organic acid makes
It obtains and is converted into active portion phosphoric acid between P elements-calcium constituent in phosphorus tailing, the activity of P elements can be greatly improved, own
A large amount of organic matter, inorganic matter have been rich in raw material, nutritional need needed for capable of adequately meeting Growth of Mango, and can
The raw material of fermented pretreatment is activated by way of activation, can be improved the activity of fermentation fertilizer, and EM after the two superposition
Bacterium can give full play to the effect of decomposition by having preferably activity after activation during the fermentation；In conclusion the application
Raw material can complement each other, synergistic effect can have more preferable active fertilizer efficiency after fermentation process.
Test 3:
The fertilizer embodiment 1-3 of the application being prepared is tested on Tiandong County mango farm, test is big
Field is divided into 4 areas, and each section is every 100 meters, one mu of each area, and area 1 is applied fertilizer using 1 fertilizer of embodiment, and area 2 uses embodiment 2
Fertilizer fertilising, area 3 are applied fertilizer using 3 fertilizer of embodiment, and area 4 (control group) (fertility of common fertilizer is using common fertilizer fertilising
Organic matter 1.10%, full nitrogen 471.04mg/kg, available phosphorus 35.21mg/kg, available potassium 41.05mg/kg, effective magnesium 24.38mg/
Kg, conductivity 0.12ms/cm, pH value 5.12), each cell has been colonized 100 plants of mango platform agriculture No.1s, and mango is
Cultivating and growing 2 years, top dressing 2 times is carried out to mango now, once in October, 2017, second in March, 2018, other
Field management it is identical, exploited in June, 2018, at random to five points in all directions pick 1 fruit carry out it is soluble solid
Shape object is measured using MASTER-53T type electronics refractometer, and Vc is measured with 2,6 dichloroindophenol titrations (GB6195-86), can be dripped
Fixed acid is measured using standard acid-base titrimetric method (GB 12293-1990)；And all fruits are claimed when picking
Yield is recorded again, as a result as follows:
Table 3
As seen from the above table, had very using the fruit soluble solids content that the mango special fertilizer material of the application plants out
Big promotion, Vc content are also significantly improved, and the content of titratable acid reduces, so that the mouthfeel of mango entirety is more beautiful
Taste.It can also be significantly improved in terms of yield.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
Limitation of the scope of the invention therefore cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art,
Without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection model of the invention
It encloses.Therefore, protection scope of the present invention should be determined by the appended claims.
Claims (6)
1. a kind of preparation method of mango special fertilizer material, it is characterised in that: specific step is as follows:
The pretreatment of (1) first timber: waste and old furniture is recycled, and carries out the utilization of timber secondary recovery, being first sorted out outer surface is
The furniture of yellow and white, is cut furniture outer using cutting machine, and 1-1.5cm behind the surface layer of cutting obtains surface layer plank,
Plank clast is broken to after 1cm and obtains plank clast, the vinegar that mass concentration is 20-30% is added according to 1 kilogram of plank clast
2 kilograms of ratio of acid is impregnated 3-5 hours in processing pond, is then sprinkled into pulverized limestone, the additional amount of pulverized limestone account for plank clast with
The 0.05 of acetic acid gross mass, the adding manner of pulverized limestone are to be slowly added into processing pond while stirring, add pulverized limestone and continue not
Disconnected stirring 10-15 minutes, is then salvaged plank clast, is rinsed well the outer surface of plank clast using clear water, then will
It is 10%-20% that plank clast, which keeps moisture content, and discarded molasses are added, and the additional amount for discarding molasses is plank clast total weight
1/2, after mixing, fermentation Mixed Microbes are added, the amount of the fermentation Mixed Microbes of addition is the 0.01% of plank clast total weight, is connect
Build after mixing evenly heap ferment 20-30 days, then filter out fermentation Mixed Microbes, the first timber can be obtained；
The fermentation Mixed Microbes include 1-3 parts of germ oligotrophy unit cell, 1-3 parts of bacillus, mould in parts by weight
1-3 parts of bacterium；
(2) following raw material is weighed according to parts by weight: 30-50 parts of pretreated first timber, fresh cane skin in step (1)
10-20 parts, 10-20 parts of rabbit excrement, 5-10 parts of phosphorus tailing, 10-25 parts of vinasse, 8-15 parts of sludge, 10-15 parts of soybean residue, EM bacterium 3-5
Part, 3-5 parts of cellulase；
(3) raw material in step (2) is subjected to processing post-fermentation and mango special fertilizer material is prepared, concrete operations are as follows:
A, after being crushed fresh cane skin, cellulase is added and mixes, accumulates 2-3 hours；
B, warm water is added in EM bacterium, the ratio of EM bacterium and warm water is 1g:100ml, is subsequently added into mango polysaccharide, mango polysaccharide and EM
The weight ratio of bacterium is 1:2；
C, rabbit excrement is put into the progress anaerobic expanded explosion of high pressure in process tank, pressure 60-80MPa, the time of explosion is 20-
30S after explosion, continues to be placed in process tank Anaerobic Treatment 20-30 minutes；
D, it carries out the phosphorus tailing to be crushed 10 meshes and obtains phosphorus tailing powder, then carry out being preheated to 40-45 DEG C, being then added has
Machine acid grind 1-3 minutes, and the weight ratio of organic acid and phosphorus tailing powder is 1:2-3；The organic acid is lactic acid, apple
Acid, tartaric acid are obtained by mixing according to weight ratio for 1:2-3:3-5；
E, step a, b, c, d treated raw material are taken out, pre fermentation material is obtained after mixing with vinasse, sludge, soybean residue, then
The entrance of screw conveyor is put into, pre fermentation material is launched from screw conveyor outlet, into fermentation vat, covered by screw conveyor
The lid of fermentation vat is reserved with venthole on lid, guarantees have oxygen to be passed through in fermentation vat, after fermentation 20-30 days, can be obtained
Mango special fertilizer material.
2. a kind of preparation method of mango special fertilizer material as described in claim 1, it is characterised in that: in step (1), discard
Molasses first pass through before being added as raw material and are preheated to 40 DEG C.
3. a kind of preparation method of mango special fertilizer material as described in claim 1, it is characterised in that: described in step (1)
The viable count of germ oligotrophy unit cell is hundred million CFU/mL of 1.01-1.35, the viable count of bacillus is hundred million CFU/ of 1.24-1.52
ML, Penicillium notatum viable count be hundred million CFU/mL of 0.68-0.85.
4. a kind of preparation method of mango special fertilizer material as described in claim 1, it is characterised in that: C1 in the cellulase
Enzyme, Cx enzyme and β glucosidase accounting are 15:4:1, and enzyme activity is 9000-10000 unit/mL.
5. a kind of preparation method of mango special fertilizer material as described in claim 1, it is characterised in that: the temperature of the warm water is
38-42℃。
6. a kind of preparation method of mango special fertilizer material as described in claim 1, it is characterised in that: the vinasse are He Prefecture China
Profit group prepares the vinasse generated after Snowflake Beer, neutral detergent fiber 36.08% in vinasse, acid detergent fiber 22.33%,
Lignin 2.96%, soluble protein 5.12%, crude fibre 11.39%.
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