CN108976999A - A kind of high intensity coating and preparation method thereof - Google Patents
A kind of high intensity coating and preparation method thereof Download PDFInfo
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- CN108976999A CN108976999A CN201810946267.8A CN201810946267A CN108976999A CN 108976999 A CN108976999 A CN 108976999A CN 201810946267 A CN201810946267 A CN 201810946267A CN 108976999 A CN108976999 A CN 108976999A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
- Surface Treatment Of Glass Fibres Or Filaments (AREA)
Abstract
The invention discloses a kind of high-intensitive coating, including below according to the raw material of parts by weight: 30-50 parts of epoxy resin, 10-20 parts of acrylic emulsion, 10-20 parts of nylon 46,2-5 parts of three isooctyl acrylate of phosphorous acid, 1-2 parts of glass bead, 3-6 parts of glass fibre, 3-6 parts of diadust, 5-10 parts of silane coupling agent, 20-40 parts of polyethylene glycol, 3-6 parts of methyl tributanoximo silane, 2-6 parts of 2-hydroxy-4-n-octoxybenzophenone, 1-2 parts of coalescing agent, 2-3 parts of adhesion agent, 30-50 parts of deionized water.The invention also discloses the preparation methods of the high-intensitive coating.Coating prepared by the present invention is under the common mating reaction of various raw materials, intensity and hardness with higher, and coating is not easy to be ground flower or stress is crushed, and aesthetics is preferable.
Description
Technical field
The present invention relates to technical field of chemical paint, specifically a kind of high intensity coating and preparation method thereof.
Background technique
Coating, in the entitled paint of Chinese tradition, so-called coating be coated in the body surface being protected or decorated, and
The continuous film of firm attachment can be formed with coated article, usually based on resin or oil or lotion, add or do not add face
Material, filler add corresponding additive, the thick liquid being formulated with organic solvent or water.
Coating belongs to one kind of industrial chemicals, and application is very extensive;The existing generally existing intensity of coating is not high, hardness compared with
The coating of low problem, coating and object surface is easy to be ground flower or stress is crushed, it is difficult to protect to the material under coating
Shield, while coating generally grinds colored or breakage, also will affect the aesthetics of object, it is cumbersome that later period coating repairs liquor ratio.
Summary of the invention
The purpose of the present invention is to provide a kind of high-intensitive coating, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of high intensity coating, including below according to the raw material of parts by weight: 30-50 parts of epoxy resin, acrylic emulsion 10-
20 parts, 10-20 parts of nylon 46,2-5 parts of three isooctyl acrylate of phosphorous acid, 1-2 parts of glass bead, 3-6 parts of glass fibre,
3-6 parts of diadust, 5-10 parts of silane coupling agent, 20-40 parts of polyethylene glycol, 3-6 parts of methyl tributanoximo silane, 2- hydroxyl
2-6 parts of base -4- oxy-octyl benzophenone, 1-2 parts of coalescing agent, 2-3 parts of adhesion agent, 30-50 parts of deionized water.
As a further solution of the present invention: including below according to the raw material of parts by weight: 35-45 parts of epoxy resin, propylene
12-18 parts of yogurt liquid, 12-18 parts of nylon 46,3-4 parts of three isooctyl acrylate of phosphorous acid, 1.2-1.8 parts of glass bead,
4-5 parts of glass fibre, 4-5 parts of diadust, 6-8 parts of silane coupling agent, 25-35 parts of polyethylene glycol, methyl tributanoximo
4-5 parts of silane, 1.2-1.8 parts of coalescing agent, 2.2-2.8 parts of adhesion agent, is gone at 3-5 parts of 2-hydroxy-4-n-octoxybenzophenone
35-45 parts of ionized water.
As further scheme of the invention: including below according to the raw material of parts by weight: 40 parts of epoxy resin, acrylic acid
15 parts of lotion, 15 parts of nylon 46,3.5 parts of three isooctyl acrylate of phosphorous acid, 1.5 parts of glass bead, glass fibre 4.5
Part, 4.5 parts of diadust, 7 parts of silane coupling agent, 30 parts of polyethylene glycol, 4.5 parts of methyl tributanoximo silane, 2- hydroxyl-
4 parts of 4- oxy-octyl benzophenone, 1.5 parts of coalescing agent, 2.5 parts of adhesion agent, 40 parts of deionized water.
As further scheme of the invention: the acrylic emulsion is pressed by pure-acrylic emulsion, silicone acrylic emulsion, acrylate and vinyl acetate emulsion
Weight ratio 1:3:2 composition.
As further scheme of the invention: the glass fibre is alkali-free glass fibre, and the length is 0.8-
1.5mm, diameter are 2-5 μm.
As further scheme of the invention: after coating coating is dry, irradiating 3-5min by ultraviolet light, ultraviolet light is strong
Degree is 300-500 μ W/cm^2.
The preparation method of the high intensity coating, steps are as follows:
1) 300-400 mesh is crossed after crushing epoxy resin, and acrylic emulsion, nylon 46, phosphorous acid is added
Three isooctyl acrylates add polyethylene glycol, deionized water, carry out microwave treatment, the processing time of microwave treatment after mixing
For 30-50min, power 300-400W, microwave treatment mixed liquor is obtained;
2) to step 1) obtain microwave treatment mixed liquor in be added glass bead, glass fibre, diadust with
The revolving speed of 500-800r/min stirs 20-30min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, 2- hydroxyl -4- is being added just in the mixture obtained to step 2)
Octyloxybenzophenone, coalescing agent, adhesion agent, it is auxiliary in whipping process with the revolving speed stirring 10-20min of 300-500r/min
Dispersed with ultrasonic wave, ultrasonic power 30-50KHz, is discharged.
Application of the above-mentioned coating in chemical field.
Compared with prior art, the beneficial effects of the present invention are:
Coating prepared by the present invention is under the common mating reaction of various raw materials, intensity and hardness with higher, coating
It is not easy to be ground flower or stress is crushed, aesthetics is preferable, long service life, can effectively be protected to the material under coating
Shield, improves the service life of object.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
It is a kind of high intensity coating, including below according to the raw material of parts by weight: 30 parts of epoxy resin, 10 parts of acrylic emulsion,
10 parts of nylon 46,2 parts of three isooctyl acrylate of phosphorous acid, 1 part of glass bead, 3 parts of glass fibre, 3 parts of diadust,
5 parts of silane coupling agent, 20 parts of polyethylene glycol, 3 parts of methyl tributanoximo silane, 2-hydroxy-4-n-octoxybenzophenone 2
Part, 1 part of coalescing agent, 2 parts of adhesion agent, 30 parts of deionized water.
Wherein, the acrylic emulsion is made of pure-acrylic emulsion, silicone acrylic emulsion, acrylate and vinyl acetate emulsion by weight 1:3:2.
Wherein, the glass fibre is alkali-free glass fibre, and the length is 0.8mm, diameter is 2 μm.
After coating coating is dry, 3min is irradiated by ultraviolet light, uitraviolet intensity is 300 μ W/cm^2.
In the present embodiment, the preparation method of the high intensity coating, steps are as follows:
1) 300 meshes are crossed after crushing epoxy resin, and it is different that acrylic emulsion, nylon 46, phosphorous acid three is added
Octyl ester adds polyethylene glycol, deionized water, carries out microwave treatment after mixing, and the processing time of microwave treatment is
30min, power 300W obtain microwave treatment mixed liquor;
2) to step 1) obtain microwave treatment mixed liquor in be added glass bead, glass fibre, diadust with
The revolving speed of 500r/min stirs 20min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, 2- hydroxyl -4- is being added just in the mixture obtained to step 2)
Octyloxybenzophenone, coalescing agent, adhesion agent stir 10min with the revolving speed of 300r/min, are aided with ultrasonic wave in whipping process
Dispersion, ultrasonic power 30KHz, discharging.
Embodiment 2
It is a kind of high intensity coating, including below according to the raw material of parts by weight: 35 parts of epoxy resin, 12 parts of acrylic emulsion,
12 parts of nylon 46,3 parts of three isooctyl acrylate of phosphorous acid, 1.2 parts of glass bead, 4 parts of glass fibre, diadust 4
Part, 8 parts of silane coupling agent, 35 parts of polyethylene glycol, 5 parts of methyl tributanoximo silane, 2-hydroxy-4-n-octoxybenzophenone
5 parts, 1.8 parts of coalescing agent, 2.8 parts of adhesion agent, 45 parts of deionized water.
Wherein, the acrylic emulsion is made of pure-acrylic emulsion, silicone acrylic emulsion, acrylate and vinyl acetate emulsion by weight 1:3:2.
Wherein, the glass fibre is alkali-free glass fibre, and the length is 1.2mm, diameter is 3 μm.
After coating coating is dry, 4min is irradiated by ultraviolet light, uitraviolet intensity is 400 μ W/cm^2.
In the present embodiment, the preparation method of the high intensity coating, steps are as follows:
1) 325 meshes are crossed after crushing epoxy resin, and it is different that acrylic emulsion, nylon 46, phosphorous acid three is added
Octyl ester adds polyethylene glycol, deionized water, carries out microwave treatment after mixing, and the processing time of microwave treatment is
40min, power 350W obtain microwave treatment mixed liquor;
2) to step 1) obtain microwave treatment mixed liquor in be added glass bead, glass fibre, diadust with
The revolving speed of 650r/min stirs 25min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, 2- hydroxyl -4- is being added just in the mixture obtained to step 2)
Octyloxybenzophenone, coalescing agent, adhesion agent stir 15min with the revolving speed of 400r/min, are aided with ultrasonic wave in whipping process
Dispersion, ultrasonic power 40KHz, discharging.
Embodiment 3
It is a kind of high intensity coating, including below according to the raw material of parts by weight: 40 parts of epoxy resin, 15 parts of acrylic emulsion,
15 parts of nylon 46,3.5 parts of three isooctyl acrylate of phosphorous acid, 1.5 parts of glass bead, 4.5 parts of glass fibre, diamond are micro-
4.5 parts of powder, 7 parts of silane coupling agent, 30 parts of polyethylene glycol, 4.5 parts of methyl tributanoximo silane, 2- hydroxyl -4- n-octyloxy
4 parts of benzophenone, 1.5 parts of coalescing agent, 2.5 parts of adhesion agent, 40 parts of deionized water.
Wherein, the acrylic emulsion is made of pure-acrylic emulsion, silicone acrylic emulsion, acrylate and vinyl acetate emulsion by weight 1:3:2.
Wherein, the glass fibre is alkali-free glass fibre, and the length is 1.2mm, diameter is 3 μm.
After coating coating is dry, 4min is irradiated by ultraviolet light, uitraviolet intensity is 400 μ W/cm^2.
In the present embodiment, the preparation method of the high intensity coating, steps are as follows:
1) 325 meshes are crossed after crushing epoxy resin, and it is different that acrylic emulsion, nylon 46, phosphorous acid three is added
Octyl ester adds polyethylene glycol, deionized water, carries out microwave treatment after mixing, and the processing time of microwave treatment is
40min, power 350W obtain microwave treatment mixed liquor;
2) to step 1) obtain microwave treatment mixed liquor in be added glass bead, glass fibre, diadust with
The revolving speed of 650r/min stirs 25min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, 2- hydroxyl -4- is being added just in the mixture obtained to step 2)
Octyloxybenzophenone, coalescing agent, adhesion agent stir 15min with the revolving speed of 400r/min, are aided with ultrasonic wave in whipping process
Dispersion, ultrasonic power 40KHz, discharging.
Embodiment 4
It is a kind of high intensity coating, including below according to the raw material of parts by weight: 45 parts of epoxy resin, 18 parts of acrylic emulsion,
18 parts of nylon 46,4 parts of three isooctyl acrylate of phosphorous acid, 1.8 parts of glass bead, 5 parts of glass fibre, diadust 5
Part, 6 parts of silane coupling agent, 25 parts of polyethylene glycol, 4 parts of methyl tributanoximo silane, 2-hydroxy-4-n-octoxybenzophenone
3 parts, 1.2 parts of coalescing agent, 2.2 parts of adhesion agent, 35 parts of deionized water.
Wherein, the acrylic emulsion is made of pure-acrylic emulsion, silicone acrylic emulsion, acrylate and vinyl acetate emulsion by weight 1:3:2.
Wherein, the glass fibre is alkali-free glass fibre, and the length is 1.2mm, diameter is 3 μm.
After coating coating is dry, 4min is irradiated by ultraviolet light, uitraviolet intensity is 400 μ W/cm^2.
In the present embodiment, the preparation method of the high intensity coating, steps are as follows:
1) 325 meshes are crossed after crushing epoxy resin, and it is different that acrylic emulsion, nylon 46, phosphorous acid three is added
Octyl ester adds polyethylene glycol, deionized water, carries out microwave treatment after mixing, and the processing time of microwave treatment is
40min, power 350W obtain microwave treatment mixed liquor;
2) to step 1) obtain microwave treatment mixed liquor in be added glass bead, glass fibre, diadust with
The revolving speed of 650r/min stirs 25min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, 2- hydroxyl -4- is being added just in the mixture obtained to step 2)
Octyloxybenzophenone, coalescing agent, adhesion agent stir 15min with the revolving speed of 400r/min, are aided with ultrasonic wave in whipping process
Dispersion, ultrasonic power 40KHz, discharging.
Embodiment 5
It is a kind of high intensity coating, including below according to the raw material of parts by weight: 50 parts of epoxy resin, 20 parts of acrylic emulsion,
20 parts of nylon 46,5 parts of three isooctyl acrylate of phosphorous acid, 2 parts of glass bead, 6 parts of glass fibre, 6 parts of diadust,
10 parts of silane coupling agent, 40 parts of polyethylene glycol, 6 parts of methyl tributanoximo silane, 2-hydroxy-4-n-octoxybenzophenone 6
Part, 2 parts of coalescing agent, 3 parts of adhesion agent, 50 parts of deionized water.
Wherein, the acrylic emulsion is made of pure-acrylic emulsion, silicone acrylic emulsion, acrylate and vinyl acetate emulsion by weight 1:3:2.
Wherein, the glass fibre is alkali-free glass fibre, and the length is 1.5mm, diameter is 5 μm.
After coating coating is dry, 5min is irradiated by ultraviolet light, uitraviolet intensity is 500 μ W/cm^2.
In the present embodiment, the preparation method of the high intensity coating, steps are as follows:
1) 400 meshes are crossed after crushing epoxy resin, and it is different that acrylic emulsion, nylon 46, phosphorous acid three is added
Octyl ester adds polyethylene glycol, deionized water, carries out microwave treatment after mixing, and the processing time of microwave treatment is
50min, power 400W obtain microwave treatment mixed liquor;
2) to step 1) obtain microwave treatment mixed liquor in be added glass bead, glass fibre, diadust with
The revolving speed of 800r/min stirs 30min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, 2- hydroxyl -4- is being added just in the mixture obtained to step 2)
Octyloxybenzophenone, coalescing agent, adhesion agent stir 20min with the revolving speed of 500r/min, are aided with ultrasonic wave in whipping process
Dispersion, ultrasonic power 50KHz, discharging.
Comparative example 1
Compared with Example 3, glass fibre, Buddha's warrior attendant are free of, other are same as Example 3.
Comparative example 2
Compared with Example 3,2-hydroxy-4-n-octoxybenzophenone is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3, glass fibre, Buddha's warrior attendant and 2-hydroxy-4-n-octoxybenzophenone, other and implementation are free of
Example 3 is identical.
Coating prepared by embodiment 1-5 and comparative example 1-3 is tested for the property, test result is as shown in table 1.
Table 1
From can be seen that coating prepared by the present invention in result above under the common mating reaction of various raw materials, have
Higher intensity and hardness, coating is not easy to be ground flower or stress is crushed, and aesthetics is preferable, long service life, can be to coating
Under material be effectively protected, improve the service life of object.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (8)
1. a kind of high intensity coating, which is characterized in that including below according to the raw material of parts by weight: 30-50 parts of epoxy resin, propylene
10-20 parts of yogurt liquid, 10-20 parts of nylon 46,2-5 parts of three isooctyl acrylate of phosphorous acid, 1-2 parts of glass bead, glass
3-6 parts of fiber, 3-6 parts of diadust, 5-10 parts of silane coupling agent, 20-40 parts of polyethylene glycol, methyl tributanoximo silane
3-6 parts, 2-6 parts of 2-hydroxy-4-n-octoxybenzophenone, 1-2 parts of coalescing agent, 2-3 parts of adhesion agent, deionized water 30-50
Part.
2. high intensity coating according to claim 1, which is characterized in that including below according to the raw material of parts by weight: epoxy
35-45 parts of resin, 12-18 parts of acrylic emulsion, 12-18 parts of nylon 46,3-4 parts of three isooctyl acrylate of phosphorous acid, glass
Change microballon 1.2-1.8 parts, 4-5 parts of glass fibre, 4-5 parts of diadust, 6-8 parts of silane coupling agent, polyethylene glycol 25-35
Part, 4-5 parts of methyl tributanoximo silane, 3-5 parts of 2-hydroxy-4-n-octoxybenzophenone, 1.2-1.8 parts of coalescing agent,
2.2-2.8 parts of adhesion agent, 35-45 parts of deionized water.
3. high intensity coating according to claim 2, which is characterized in that including below according to the raw material of parts by weight: epoxy
40 parts of resin, 15 parts of acrylic emulsion, 15 parts of nylon 46,3.5 parts of three isooctyl acrylate of phosphorous acid, glass bead 1.5
Part, 4.5 parts of glass fibre, 4.5 parts of diadust, 7 parts of silane coupling agent, 30 parts of polyethylene glycol, methyl tributanoximo silicon
4.5 parts of alkane, 4 parts of 2-hydroxy-4-n-octoxybenzophenone, 1.5 parts of coalescing agent, 2.5 parts of adhesion agent, 40 parts of deionized water.
4. high intensity coating according to claim 1, which is characterized in that the acrylic emulsion is by pure-acrylic emulsion, silicon third
Lotion, acrylate and vinyl acetate emulsion are formed by weight 1:3:2.
5. high intensity coating according to claim 4, which is characterized in that the glass fibre is alkali-free glass fibre,
The length is 0.8-1.5mm, diameter is 2-5 μm.
6. a kind of high-intensitive coating a method as claimed in any one of claims 1 to 5, which is characterized in that after coating coating is dry, pass through purple
3-5min is irradiated in outside line, and uitraviolet intensity is 300-500 μ W/cm^2.
7. a kind of preparation method of high-intensitive coating a method as claimed in any one of claims 1 to 5, which is characterized in that including following step
It is rapid:
1) 300-400 mesh is crossed after crushing epoxy resin, and it is different that acrylic emulsion, nylon 46, phosphorous acid three is added
Octyl ester adds polyethylene glycol, deionized water, carries out microwave treatment after mixing, and the processing time of microwave treatment is 30-
50min, power 300-400W obtain microwave treatment mixed liquor;
2) glass bead, glass fibre, diadust are added in the microwave treatment mixed liquor obtained to step 1) with 500-
The revolving speed of 800r/min stirs 20-30min, obtains mixture;
3) silane coupling agent, methyl tributanoximo silane, the just pungent oxygen of 2- hydroxyl -4- is added in the mixture obtained to step 2
Base benzophenone, coalescing agent, adhesion agent stir 10-20min with the revolving speed of 300-500r/min, are aided in whipping process super
Sound wave dispersion, ultrasonic power 30-50KHz, discharging.
8. a kind of application of coating a method as claimed in any one of claims 1 to 5 in chemical field.
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CN201810946267.8A CN108976999A (en) | 2018-08-20 | 2018-08-20 | A kind of high intensity coating and preparation method thereof |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002105392A (en) * | 2001-07-12 | 2002-04-10 | Kansai Paint Co Ltd | Ultraviolet curing type coating composition for can |
CN101050065A (en) * | 2007-05-15 | 2007-10-10 | 朱建强 | Composition of insulating mold coating in use for glass, and preparation method |
CN107760137A (en) * | 2017-11-21 | 2018-03-06 | 江苏艾科赛特新材料有限公司 | It is a kind of to improve long-term water-fast and weather resistance roofing waterproof paint |
-
2018
- 2018-08-20 CN CN201810946267.8A patent/CN108976999A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002105392A (en) * | 2001-07-12 | 2002-04-10 | Kansai Paint Co Ltd | Ultraviolet curing type coating composition for can |
CN101050065A (en) * | 2007-05-15 | 2007-10-10 | 朱建强 | Composition of insulating mold coating in use for glass, and preparation method |
CN107760137A (en) * | 2017-11-21 | 2018-03-06 | 江苏艾科赛特新材料有限公司 | It is a kind of to improve long-term water-fast and weather resistance roofing waterproof paint |
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