CN108925950A - A kind of Semen sesami nigrum ball and preparation method thereof containing collagen - Google Patents
A kind of Semen sesami nigrum ball and preparation method thereof containing collagen Download PDFInfo
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- CN108925950A CN108925950A CN201810797780.5A CN201810797780A CN108925950A CN 108925950 A CN108925950 A CN 108925950A CN 201810797780 A CN201810797780 A CN 201810797780A CN 108925950 A CN108925950 A CN 108925950A
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- 102000008186 Collagen Human genes 0.000 title claims abstract description 59
- 108010035532 Collagen Proteins 0.000 title claims abstract description 59
- 229920001436 collagen Polymers 0.000 title claims abstract description 59
- 210000000582 semen Anatomy 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims description 19
- 235000004936 Bromus mango Nutrition 0.000 claims abstract description 35
- 241001093152 Mangifera Species 0.000 claims abstract description 35
- 235000014826 Mangifera indica Nutrition 0.000 claims abstract description 35
- 235000009184 Spondias indica Nutrition 0.000 claims abstract description 35
- 239000000284 extract Substances 0.000 claims abstract description 33
- 235000012907 honey Nutrition 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims description 17
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 14
- 239000012153 distilled water Substances 0.000 claims description 14
- 239000004519 grease Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 14
- 230000001376 precipitating effect Effects 0.000 claims description 14
- 238000001556 precipitation Methods 0.000 claims description 14
- 239000013049 sediment Substances 0.000 claims description 14
- 239000006228 supernatant Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 150000003839 salts Chemical class 0.000 claims description 12
- 102000004190 Enzymes Human genes 0.000 claims description 8
- 108090000790 Enzymes Proteins 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 8
- 108091005804 Peptidases Proteins 0.000 claims description 7
- 239000004365 Protease Substances 0.000 claims description 7
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 238000005119 centrifugation Methods 0.000 claims description 7
- 239000000470 constituent Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 238000002224 dissection Methods 0.000 claims description 7
- 239000012467 final product Substances 0.000 claims description 7
- 230000007062 hydrolysis Effects 0.000 claims description 7
- 238000006460 hydrolysis reaction Methods 0.000 claims description 7
- 238000007654 immersion Methods 0.000 claims description 7
- 239000012528 membrane Substances 0.000 claims description 7
- 150000007524 organic acids Chemical class 0.000 claims description 7
- 239000011780 sodium chloride Substances 0.000 claims description 7
- 238000010612 desalination reaction Methods 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 238000000108 ultra-filtration Methods 0.000 claims description 2
- 239000002002 slurry Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- 208000001132 Osteoporosis Diseases 0.000 abstract description 4
- 239000003205 fragrance Substances 0.000 abstract description 2
- 230000036039 immunity Effects 0.000 abstract description 2
- 235000015097 nutrients Nutrition 0.000 abstract description 2
- 230000009758 senescence Effects 0.000 abstract description 2
- 230000001934 delay Effects 0.000 abstract 1
- 238000005360 mashing Methods 0.000 description 6
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229930003427 Vitamin E Natural products 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 235000007215 black sesame Nutrition 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 2
- 235000019165 vitamin E Nutrition 0.000 description 2
- 229940046009 vitamin E Drugs 0.000 description 2
- 239000011709 vitamin E Substances 0.000 description 2
- 229930003451 Vitamin B1 Natural products 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 208000007502 anemia Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 210000004958 brain cell Anatomy 0.000 description 1
- 210000000845 cartilage Anatomy 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000007102 metabolic function Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 42-56 parts of Semen sesami nigrum, 24-36 parts of collagen, 4-9 parts of honey, 4-9 parts of mango extract, 3-7 parts of fructus lycii.The present invention is organically combined Semen sesami nigrum and collagen, the two nutrients is absorbed simultaneously, it can be with useful effect in osteoporosis, it enhances human immunity, it delays senescence, while crispy, also possesses the fragrance of mango, using taking for patient, has vast market prospect.
Description
Technical field
The present invention relates to field of food, specifically a kind of Semen sesami nigrum ball and preparation method thereof containing collagen.
Background technique
Semen sesami nigrum and collagen are all the nutriment that people often take, and wherein the effect of Semen sesami nigrum mainly has: black sesame
A variety of essential amino acids that fiber crops contain can accelerate the metabolism function of human body in the case where the effect of vitamin E and vitamin B1 participates in
Energy；The iron and vitamin E that Semen sesami nigrum contains are to prevent anaemia, activating brain cell, the important component for eliminating blood vessel cholesterol；Black sesame
The fat that fiber crops contain is mostly unsaturated fatty acid, plays the role of promoting longevity.The effect of collagen mainly has: collagen
It is the nutriment that human body anti-aging must supply, accounts for 30% or more of Whole Body gross protein, the body of an adult
It is interior that there are about 3 kilograms of collagens.It universally present in the skin of human body, bone, muscle, cartilage, joint, hair tissue,
Play triple anti-aging effects of support, reparation, protection.
Collagen is that treatment osteoporosis has a good effect, but individually to take mouthfeel poor for collagen, if
Semen sesami nigrum and collagen can be organically combined, can undoubtedly be brought great convenience to sufferers of osteoporosis face.
Summary of the invention
The purpose of the present invention is to provide a kind of Semen sesami nigrum ball and preparation method thereof containing collagen, it is above-mentioned to solve
The problem of being proposed in background technique.
To achieve the above object, the invention provides the following technical scheme:
A kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 42-56 parts of Semen sesami nigrum, collagen egg
24-36 parts white, 4-9 parts of honey, 4-9 parts of mango extract, 3-7 parts of fructus lycii.
As a further solution of the present invention: including below according to the raw material of parts by weight: 47-51 parts of Semen sesami nigrum, collagen egg
28-32 parts white, 5-8 parts of honey, 5-8 parts of mango extract, 4-6 parts of fructus lycii.
As further scheme of the invention: including below according to the raw material of parts by weight: 49 parts of Semen sesami nigrum, collagen
30 parts, 6 parts of honey, 6 parts of mango extract, 5 parts of fructus lycii.
As further scheme of the invention: the extracting method of the collagen are as follows: by pigskin unhairing, be cut into small
Block is smashed to pieces, removes liposoluble constituent with SCF-CO 2 method, the pigskin after obtaining grease removal；Add into the pigskin after grease removal
Enter NaCl solution, extraction twice, merges extracting solution twice, and centrifugation takes albumen precipitation；Albumen precipitation is rushed with distilled water
It washes, is centrifuged, the precipitating after removing salt；Organic acid soln and protease are added in precipitating after desalination, extracts, then from
The heart takes supernatant, and supernatant is concentrated into the half of original volume to obtain the final product.
As the present invention further scheme: the mango extract the preparation method comprises the following steps: by mango wash clean, going
Skin, dissection, with acid solution immersion treatment, reusable heat hydro-thermal is scalded several minutes, cooling, mashing, carries out carrying out enzyme again after enzyme hydrolysis going out
It is living, isolate clear liquid；Clear liquid carries out ultrafiltration with filter membrane, collect filter liquor to get.
The preparation method of the Semen sesami nigrum ball containing collagen, comprising the following steps:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 4-9 times of quality times of the two is added, in normal temperature environment
Lower stirring 3-5min, obtains the first mixed liquor；
2) collagen is added in mixed liquor, 60-78 DEG C at a temperature of react 25-36min, then temperature is promoted to
82-110 DEG C of the reaction was continued 12-18min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 3-5min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
As further scheme of the invention: being stirred with needing intermittence in the reaction process of the step 2.
Compared with prior art, the beneficial effects of the present invention are:
The present invention is organically combined Semen sesami nigrum and collagen, and the two nutrients is absorbed simultaneously, can be with
Useful effect is enhanced human immunity in osteoporosis, is delayed senescence, while crispy, is also possessed the fragrance of mango, benefit
With taking for patient, has vast market prospect.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 42 parts of Semen sesami nigrum, collagen 24
Part, 4 parts of honey, 4 parts of mango extract, 3 parts of fructus lycii.
The wherein extracting method of collagen are as follows: by pigskin unhairing, be cut into small pieces, smash to pieces, with SCF-CO 2 method
Remove liposoluble constituent, the pigskin after obtaining grease removal；NaCl solution is added into the pigskin after grease removal, extraction twice, merges two
Secondary extracting solution, centrifugation, takes albumen precipitation；Albumen precipitation is rinsed with distilled water, is centrifuged, the precipitating after removing salt；It is removing
Organic acid soln and protease are added in precipitating after salt, extracts, is then centrifuged for, take supernatant, supernatant is concentrated into
The half of original volume to obtain the final product.
Mango extract the preparation method comprises the following steps: by mango wash clean, peeling, dissection, with acid solution immersion treatment, reusable heat
Hydro-thermal is scalded several minutes, and cooling, mashing carries out enzyme-deactivating after carrying out enzyme hydrolysis again, isolates clear liquid；Clear liquid is surpassed with filter membrane
Filter, collect filter liquor to get.
The preparation method of Semen sesami nigrum ball described in the present embodiment containing collagen, comprising the following steps:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 4 times of the two quality times is added, under normal temperature environment
3min is stirred, the first mixed liquor is obtained；
2) collagen is added in mixed liquor, 60 DEG C at a temperature of react 25min, then by temperature be promoted to 82 DEG C after
Continuous reaction 12min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 3min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
Wherein it is stirred with needing intermittence in the reaction process of step 2.
Embodiment 2
A kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 47 parts of Semen sesami nigrum, collagen 28
Part, 5 parts of honey, 5 parts of mango extract, 4 parts of fructus lycii.
The wherein extracting method of collagen are as follows: by pigskin unhairing, be cut into small pieces, smash to pieces, with SCF-CO 2 method
Remove liposoluble constituent, the pigskin after obtaining grease removal；NaCl solution is added into the pigskin after grease removal, extraction twice, merges two
Secondary extracting solution, centrifugation, takes albumen precipitation；Albumen precipitation is rinsed with distilled water, is centrifuged, the precipitating after removing salt；It is removing
Organic acid soln and protease are added in precipitating after salt, extracts, is then centrifuged for, take supernatant, supernatant is concentrated into
The half of original volume to obtain the final product.
Mango extract the preparation method comprises the following steps: by mango wash clean, peeling, dissection, with acid solution immersion treatment, reusable heat
Hydro-thermal is scalded several minutes, and cooling, mashing carries out enzyme-deactivating after carrying out enzyme hydrolysis again, isolates clear liquid；Clear liquid is surpassed with filter membrane
Filter, collect filter liquor to get.
The preparation method of Semen sesami nigrum ball described in the present embodiment containing collagen, comprising the following steps:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 6 times of the two quality times is added, under normal temperature environment
4min is stirred, the first mixed liquor is obtained；
2) collagen is added in mixed liquor, 72 DEG C at a temperature of react 30min, then by temperature be promoted to 90 DEG C after
Continuous reaction 15min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 5min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
Wherein it is stirred with needing intermittence in the reaction process of step 2.
Embodiment 3
A kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 49 parts of Semen sesami nigrum, collagen 30
Part, 6 parts of honey, 6 parts of mango extract, 5 parts of fructus lycii.
The wherein extracting method of collagen are as follows: by pigskin unhairing, be cut into small pieces, smash to pieces, with SCF-CO 2 method
Remove liposoluble constituent, the pigskin after obtaining grease removal；NaCl solution is added into the pigskin after grease removal, extraction twice, merges two
Secondary extracting solution, centrifugation, takes albumen precipitation；Albumen precipitation is rinsed with distilled water, is centrifuged, the precipitating after removing salt；It is removing
Organic acid soln and protease are added in precipitating after salt, extracts, is then centrifuged for, take supernatant, supernatant is concentrated into
The half of original volume to obtain the final product.
Mango extract the preparation method comprises the following steps: by mango wash clean, peeling, dissection, with acid solution immersion treatment, reusable heat
Hydro-thermal is scalded several minutes, and cooling, mashing carries out enzyme-deactivating after carrying out enzyme hydrolysis again, isolates clear liquid；Clear liquid is surpassed with filter membrane
Filter, collect filter liquor to get.
The preparation method of Semen sesami nigrum ball described in the present embodiment containing collagen, comprising the following steps:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 7 times of the two quality times is added, under normal temperature environment
5min is stirred, the first mixed liquor is obtained；
2) collagen is added in mixed liquor, 70 DEG C at a temperature of react 35min, then by temperature be promoted to 90 DEG C after
Continuous reaction 15min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 4min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
Wherein it is stirred with needing intermittence in the reaction process of step 2.
Embodiment 4
A kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 51 parts of Semen sesami nigrum, collagen 32
Part, 8 parts of honey, 8 parts of mango extract, 6 parts of fructus lycii.
The wherein extracting method of collagen are as follows: by pigskin unhairing, be cut into small pieces, smash to pieces, with SCF-CO 2 method
Remove liposoluble constituent, the pigskin after obtaining grease removal；NaCl solution is added into the pigskin after grease removal, extraction twice, merges two
Secondary extracting solution, centrifugation, takes albumen precipitation；Albumen precipitation is rinsed with distilled water, is centrifuged, the precipitating after removing salt；It is removing
Organic acid soln and protease are added in precipitating after salt, extracts, is then centrifuged for, take supernatant, supernatant is concentrated into
The half of original volume to obtain the final product.
Mango extract the preparation method comprises the following steps: by mango wash clean, peeling, dissection, with acid solution immersion treatment, reusable heat
Hydro-thermal is scalded several minutes, and cooling, mashing carries out enzyme-deactivating after carrying out enzyme hydrolysis again, isolates clear liquid；Clear liquid is surpassed with filter membrane
Filter, collect filter liquor to get.
The preparation method of Semen sesami nigrum ball described in the present embodiment containing collagen, comprising the following steps:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 8 times of the two quality times is added, under normal temperature environment
5min is stirred, the first mixed liquor is obtained；
2) collagen is added in mixed liquor, 75 DEG C at a temperature of react 35min, temperature is then promoted to 110 DEG C
The reaction was continued 17min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 5min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
Wherein it is stirred with needing intermittence in the reaction process of step 2.
Embodiment 5
A kind of Semen sesami nigrum ball containing collagen, including below according to the raw material of parts by weight: 56 parts of Semen sesami nigrum, collagen 36
Part, 9 parts of honey, 9 parts of mango extract, 7 parts of fructus lycii.
The wherein extracting method of collagen are as follows: by pigskin unhairing, be cut into small pieces, smash to pieces, with SCF-CO 2 method
Remove liposoluble constituent, the pigskin after obtaining grease removal；NaCl solution is added into the pigskin after grease removal, extraction twice, merges two
Secondary extracting solution, centrifugation, takes albumen precipitation；Albumen precipitation is rinsed with distilled water, is centrifuged, the precipitating after removing salt；It is removing
Organic acid soln and protease are added in precipitating after salt, extracts, is then centrifuged for, take supernatant, supernatant is concentrated into
The half of original volume to obtain the final product.
Mango extract the preparation method comprises the following steps: by mango wash clean, peeling, dissection, with acid solution immersion treatment, reusable heat
Hydro-thermal is scalded several minutes, and cooling, mashing carries out enzyme-deactivating after carrying out enzyme hydrolysis again, isolates clear liquid；Clear liquid is surpassed with filter membrane
Filter, collect filter liquor to get.
The preparation method of Semen sesami nigrum ball described in the present embodiment containing collagen, comprising the following steps:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 9 times of the two quality times is added, under normal temperature environment
5min is stirred, the first mixed liquor is obtained；
2) collagen is added in mixed liquor, 78 DEG C at a temperature of react 36min, temperature is then promoted to 110 DEG C
The reaction was continued 18min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 5min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
Wherein it is stirred with needing intermittence in the reaction process of step 2.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of Semen sesami nigrum ball containing collagen, which is characterized in that including below according to the raw material of parts by weight: Semen sesami nigrum
42-56 parts, 24-36 parts of collagen, 4-9 parts of honey, 4-9 parts of mango extract, 3-7 parts of fructus lycii.
2. the Semen sesami nigrum ball according to claim 1 containing collagen, which is characterized in that including below according to parts by weight
Raw material: 47-51 parts of Semen sesami nigrum, 28-32 parts of collagen, 5-8 parts of honey, 5-8 parts of mango extract, 4-6 parts of fructus lycii.
3. the Semen sesami nigrum ball according to claim 2 containing collagen, which is characterized in that including below according to parts by weight
Raw material: 49 parts of Semen sesami nigrum, 30 parts of collagen, 6 parts of honey, 6 parts of mango extract, 5 parts of fructus lycii.
4. the Semen sesami nigrum ball according to claim 3 containing collagen, which is characterized in that the extraction of the collagen
Method are as follows: by pigskin unhairing, be cut into small pieces, smash to pieces, liposoluble constituent is removed with SCF-CO 2 method, after obtaining grease removal
Pigskin；NaCl solution is added into the pigskin after grease removal, extraction twice, merges extracting solution twice, and centrifugation takes albumen precipitation；
Albumen precipitation is rinsed with distilled water, is centrifuged, the precipitating after removing salt；Organic acid soln is added in precipitating after desalination
And protease, it extracts, is then centrifuged for, take supernatant, supernatant is concentrated into the half of original volume to obtain the final product.
5. the Semen sesami nigrum ball according to claim 3 containing collagen, which is characterized in that the system of the mango extract
Preparation Method are as follows: by mango wash clean, peeling, dissection, with acid solution immersion treatment, reusable heat hydro-thermal is scalded several minutes, cooling, beat
Slurry carries out enzyme-deactivating after carrying out enzyme hydrolysis again, isolates clear liquid；Clear liquid carries out ultrafiltration with filter membrane, collect filter liquor to get.
6. a kind of preparation method of the Semen sesami nigrum ball a method as claimed in any one of claims 1 to 5 containing collagen, which is characterized in that
The following steps are included:
1) Semen sesami nigrum and fructus lycii are weighed, crushes, sieves with 100 mesh sieve, the distilled water of 4-9 times of quality times of the two is added, in normal temperature environment
Lower stirring 3-5min, obtains the first mixed liquor；
2) collagen is added in mixed liquor, 60-78 DEG C at a temperature of react 25-36min, then temperature is promoted to
82-110 DEG C of the reaction was continued 12-18min, obtains the second mixed liquor；
3) it by mango extract, is added in the second mixed liquor, is stirred, be then ultrasonically treated under normal temperature environment,
Time 3-5min is handled, third mixed liquor is obtained；
4) third mixed liquor is centrifuged, takes lower sediment, be put into mold and make after lower sediment is mixed with honey
Glomeration to get.
7. the preparation method of the Semen sesami nigrum ball according to claim 6 containing collagen, which is characterized in that the step
2) it is stirred with needing intermittence in reaction process.
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