CN108914611A - 一种抗菌型玻璃纤维布的制备方法 - Google Patents

一种抗菌型玻璃纤维布的制备方法 Download PDF

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CN108914611A
CN108914611A CN201811050693.XA CN201811050693A CN108914611A CN 108914611 A CN108914611 A CN 108914611A CN 201811050693 A CN201811050693 A CN 201811050693A CN 108914611 A CN108914611 A CN 108914611A
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fiber
fabric
slurry
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徐大治
王新武
张勇
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ANHUI DANFENG ELECTRONIC MATERIAL Co Ltd
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ANHUI DANFENG ELECTRONIC MATERIAL Co Ltd
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Abstract

本发明涉及一种抗菌型玻璃纤维布的制备方法，具体步骤如下：将玻璃纤维单丝平织得到基础玻纤布；将基础玻纤布置于浆料中浸渍一段时间；挤压出基础玻纤布上的多余浆料，排除气泡得到预成型玻纤布；以玻璃纤维单丝经平行集束得到原丝，将原丝切割成50～60mm长，并将其随机均匀铺设于预成型玻纤布上，接着涂覆粘结剂，加热固化得到基材；在基材的两侧均匀涂覆浆料，然后紫外固化得产物。该玻璃纤维布综合性能好，通过在环尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油等原料制成的浆料中浸泡，使得制成的玻璃纤维布具有优异的抗菌的功效，有效避免了细菌的滋生。

Description

一种抗菌型玻璃纤维布的制备方法
技术领域
本发明涉及一种玻璃纤维布，具体涉及一种抗菌型玻璃纤维布的制备方法。
背景技术
玻璃纤维是一种性能优异的无机非金属材料，其成分为二氧化硅、氧化铝、氧化钙、氧化硼、氧化镁和氧化钠等，它是以玻璃球或废旧玻璃为原料经高温熔制、拉丝、络纱、织布等工艺，最后形成各类产品。玻璃纤维单丝的直径从几个微米到二十几个微米，相当于一根头发丝的1/20～1/5，每束纤维原丝都有数百根甚至上千根单丝组成。
玻璃纤维是非常好的金属替代材料，在建筑、船舶、化工管道、汽车、航空、风力发电等领域有着广阔的应用前景，并且其应用领域仍在不断拓展，全球市场空间巨大。如何提供一种抗菌型玻璃纤维布的制备方法是十分重要的。
发明内容
本发明的目的在于：提供一种抗菌型玻璃纤维布的制备方法。
为了实现上述目的，本发明提供如下技术方案：
一种抗菌型玻璃纤维布的制备方法，具体步骤如下：
S1：将环氧树脂乳液、纳米碳酸钙、邻苯二甲酸二丁酯、聚乙烯醇、海藻酸钠、羧甲基纤维素、膨胀珍珠岩、尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油加入适量水后搅拌均匀后得浆料备用；
S2：玻璃纤维单丝平织，得到基础玻纤布；
S3：将基础玻纤布置于浆料中浸渍一段时间；
S4：挤压出基础玻纤布上的多余浆料，排除气泡，得到预成型玻纤布；
S5：以玻璃纤维单丝经平行集束得到原丝，将原丝切割成50～60mm长，并将其随机均匀铺设于预成型玻纤布上，接着涂覆粘结剂，加热固化，得到基材；
S6：在基材的两侧均匀涂覆步骤S1中的浆料，然后将其进行紫外固化，即得产物。
优选地，步骤S6中紫外固化的处理时间为1.5～3h。
优选地，步骤S6中紫外固化的处理时间为2h。
优选地，步骤S3中基础玻纤布置于浆料中浸渍时间为1.5～3h。
优选地，步骤S3中基础玻纤布置于浆料中浸渍时间为2h。
优选地，步骤S1中各原料的具体重量份数如下：
环氧树脂乳液4～7份、纳米碳酸钙0.1～0.2份、邻苯二甲酸二丁酯0.3～0.5份、聚乙烯醇2～3份、海藻酸钠0.6～0.8份、羧甲基纤维素0.01～0.02份、膨胀珍珠岩4～6份、尼泊金丙酯钠0.1～0.3份、载银沸石0.1～0.3份、薰衣草精油0.1～0.3份、天竺葵精油0.1～0.3份。
优选地，步骤S1中各原料的具体重量份数如下：
环氧树脂乳液5份、纳米碳酸钙0.15份、邻苯二甲酸二丁酯0.4份、聚乙烯醇2.5份、海藻酸钠0.7份、羧甲基纤维素0.015份、膨胀珍珠岩5份、尼泊金丙酯钠0.2份、载银沸石0.2份、薰衣草精油02份、天竺葵精油0.2份。
本发明的有益效果在于：本发明的玻璃纤维布综合性能好，通过在环尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油等原料制成的浆料中浸泡，使得制成的玻璃纤维布具有优异的抗菌的功效，有效避免了细菌的滋生。
具体实施例
实施例1
一种抗菌型玻璃纤维布的制备方法，具体步骤如下：
S1：将环氧树脂乳液、纳米碳酸钙、邻苯二甲酸二丁酯、聚乙烯醇、海藻酸钠、羧甲基纤维素、膨胀珍珠岩、尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油加入适量水后搅拌均匀后得浆料备用；
S2：玻璃纤维单丝平织，得到基础玻纤布；
S3：将基础玻纤布置于浆料中浸渍1.5h；
S4：挤压出基础玻纤布上的多余浆料，排除气泡，得到预成型玻纤布；
S5：以玻璃纤维单丝经平行集束得到原丝，将原丝切割成50～60mm长，并将其随机均匀铺设于预成型玻纤布上，接着涂覆粘结剂，加热固化，得到基材；
S6：在基材的两侧均匀涂覆步骤S1中的浆料，然后将其进行紫外固化处理1.5h，即得产物。
步骤S1中各原料的具体重量份数如下：
环氧树脂乳液4份、纳米碳酸钙0.1份、邻苯二甲酸二丁酯0.3份、聚乙烯醇2份、海藻酸钠0.6份、羧甲基纤维素0.01份、膨胀珍珠岩4份、尼泊金丙酯钠0.1份、载银沸石0.1份、薰衣草精油0.1份、天竺葵精油0.1份。
实施例2
一种抗菌型玻璃纤维布的制备方法，具体步骤如下：
S1：将环氧树脂乳液、纳米碳酸钙、邻苯二甲酸二丁酯、聚乙烯醇、海藻酸钠、羧甲基纤维素、膨胀珍珠岩、尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油加入适量水后搅拌均匀后得浆料备用；
S2：玻璃纤维单丝平织，得到基础玻纤布；
S3：将基础玻纤布置于浆料中浸渍2h；
S4：挤压出基础玻纤布上的多余浆料，排除气泡，得到预成型玻纤布；
S5：以玻璃纤维单丝经平行集束得到原丝，将原丝切割成50～60mm长，并将其随机均匀铺设于预成型玻纤布上，接着涂覆粘结剂，加热固化，得到基材；
S6：在基材的两侧均匀涂覆步骤S1中的浆料，然后将其进行紫外固化处理2h，即得产物。
步骤S1中各原料的具体重量份数如下：
环氧树脂乳液5份、纳米碳酸钙0.15份、邻苯二甲酸二丁酯0.4份、聚乙烯醇2.5份、海藻酸钠0.7份、羧甲基纤维素0.015份、膨胀珍珠岩5份、尼泊金丙酯钠0.2份、载银沸石0.2份、薰衣草精油02份、天竺葵精油0.2份。
实施例3
一种抗菌型玻璃纤维布的制备方法，具体步骤如下：
S1：将环氧树脂乳液、纳米碳酸钙、邻苯二甲酸二丁酯、聚乙烯醇、海藻酸钠、羧甲基纤维素、膨胀珍珠岩、尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油加入适量水后搅拌均匀后得浆料备用；
S2：玻璃纤维单丝平织，得到基础玻纤布；
S3：将基础玻纤布置于浆料中浸渍3h；
S4：挤压出基础玻纤布上的多余浆料，排除气泡，得到预成型玻纤布；
S5：以玻璃纤维单丝经平行集束得到原丝，将原丝切割成50～60mm长，并将其随机均匀铺设于预成型玻纤布上，接着涂覆粘结剂，加热固化，得到基材；
S6：在基材的两侧均匀涂覆步骤S1中的浆料，然后将其进行紫外固化处理3h，即得产物。
步骤S1中各原料的具体重量份数如下：
环氧树脂乳液7份、纳米碳酸钙0.2份、邻苯二甲酸二丁酯0.5份、聚乙烯醇3份、海藻酸钠0.8份、羧甲基纤维素0.02份、膨胀珍珠岩6份、尼泊金丙酯钠0.3份、载银沸石0.3份、薰衣草精油0.3份、天竺葵精油0.3份。
实施例4
对实施例1-3所得玻璃纤维布进行抗菌测试，结果如下表所示：
金黄色葡萄球菌 大肠杆菌
实施例1 99.6％ 99.4％
实施例2 99.8％ 99.7％
实施例3 99.4％ 99.6％

Claims (7)

1.一种抗菌型玻璃纤维布的制备方法，其特征在于：具体步骤如下：
S1：将环氧树脂乳液、纳米碳酸钙、邻苯二甲酸二丁酯、聚乙烯醇、海藻酸钠、羧甲基纤维素、膨胀珍珠岩、尼泊金丙酯钠、载银沸石、薰衣草精油、天竺葵精油加入适量水后搅拌均匀后得浆料备用；
S2：将玻璃纤维单丝平织，得到基础玻纤布；
S3：将基础玻纤布置于浆料中浸渍一段时间；
S4：挤压出基础玻纤布上的多余浆料，排除气泡，得到预成型玻纤布；
S5：以玻璃纤维单丝经平行集束得到原丝，将原丝切割成50～60mm长，并将其随机均匀铺设于预成型玻纤布上，接着涂覆粘结剂，加热固化，得到基材；
S6：在基材的两侧均匀涂覆步骤S1中的浆料，然后将其进行紫外固化，即得产物。
2.根据权利要求1所述的一种抗菌型玻璃纤维布的制备方法，其特征在于：步骤S6中紫外固化的处理时间为1.5～3h。
3.根据权利要求1所述的一种抗菌型玻璃纤维布的制备方法，其特征在于：步骤S6中紫外固化的处理时间为2h。
4.根据权利要求1所述的一种抗菌型玻璃纤维布的制备方法，其特征在于：步骤S3中基础玻纤布置于浆料中浸渍时间为1.5～3h。
5.根据权利要求1所述的一种抗菌型玻璃纤维布的制备方法，其特征在于：步骤S3中基础玻纤布置于浆料中浸渍时间为2h。
6.根据权利要求1所述的一种抗菌型玻璃纤维布的制备方法，其特征在于：步骤S1中各原料的具体重量份数如下：
环氧树脂乳液4～7份、纳米碳酸钙0.1～0.2份、邻苯二甲酸二丁酯0.3～0.5份、聚乙烯醇2～3份、海藻酸钠0.6～0.8份、羧甲基纤维素0.01～0.02份、膨胀珍珠岩4～6份、尼泊金丙酯钠0.1～0.3份、载银沸石0.1～0.3份、薰衣草精油0.1～0.3份、天竺葵精油0.1～0.3份。
7.根据权利要求1所述的一种抗菌型玻璃纤维布的制备方法，其特征在于：步骤S1中各原料的具体重量份数如下：
环氧树脂乳液5份、纳米碳酸钙0.15份、邻苯二甲酸二丁酯0.4份、聚乙烯醇2.5份、海藻酸钠0.7份、羧甲基纤维素0.015份、膨胀珍珠岩5份、尼泊金丙酯钠0.2份、载银沸石0.2份、薰衣草精油02份、天竺葵精油0.2份。
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CN111926571A (zh) * 2020-08-19 2020-11-13 安徽唯宏新材料科技有限公司 一种高耐磨玻璃纤维布及其制备方法
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