CN108904582A - A kind of preparation method of licorice powder - Google Patents
A kind of preparation method of licorice powder Download PDFInfo
- Publication number
- CN108904582A CN108904582A CN201810886379.9A CN201810886379A CN108904582A CN 108904582 A CN108904582 A CN 108904582A CN 201810886379 A CN201810886379 A CN 201810886379A CN 108904582 A CN108904582 A CN 108904582A
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- CN
- China
- Prior art keywords
- preparation
- licorice powder
- licorice
- powder according
- water
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
Abstract
The invention discloses a kind of preparation methods of licorice powder, including following preparation step：Step 1, licorice raw material is pre-processed, water mentions, and obtains extracting solution；Step 2, the extracting solution is concentrated, is spray-dried, crushed, packed, sterilizing obtains licorice powder.Resulting licorice powder is brown, it is slightly sweet, with the intrinsic taste smell of Radix Glycyrrhizae, free from extraneous odour, in powdered, with preferable brew, and it is visible by naked eyes exogenous impurity, the glycyrrhizic acid content in licorice powder is met the requirements of the standard up to 8.6g/100g, net content negative bias difference, organoleptic indicator, physical and chemical index and microbiological indicator；In preparation method, use low-temperature treatment in concentration and spray drying, the loss of the effective component in licorice powder can be protected to greatest extent, will not qualitative change, the indexs such as product color taste, content substantially improve raising；Preparation method is simple, low in cost.
Description
Technical field
The present invention relates to the preparation method technical fields of solid beverage, and in particular to a kind of preparation method of licorice powder.
Background technique
Radix Glycyrrhizae is pulse family (Leguminosae) liquorice root (Glycyrrhizauralensis Fisch.), swollen fruit Radix
(GlycyrrhizainflataBat.) or the drying root and rhizome of glycyrrhiza glabra (Glycyrrhizaglabr.).Traditional Chinese medicine is recognized
For：Radix Glycyrrhizae is sweet in flavor, flat, is to invigorate the spleen and benefit qi, cough-relieving happiness disease, relieving spasm to stop pain, coordinating the drug actions of a prescription, the good medicine of removing toxic substances.It is main in Glycyrrhiza
Effective component is glycyrrhizic acid, flavonoids, Coumarins, polysaccharide, alkaloid, amino acid etc., has analgesia, cough-relieving, anti-inflammatory, anti-mistake
The pharmacological actions such as quick, removing toxic substances, AntiHIV1 RT activity, are widely used in the fields such as medicine, food, tobacco, cosmetics, chemical industry.Though Radix Glycyrrhizae is all
One object, but because of its processing procedure difference, effect is also not quite similar, and raw purging intense heat heat, ripe with exterior cold is dissipated, unpeeled RADIX GLYCYRRHIZAE is laid particular stress on
Heat, purge the sthenic heart-fire in clear.
In existing licorice powder preparation process, polyhybird has other plurality of raw materials, is unfavorable for licorice powder nutritive value itself
Give full play to, and preparation process is complex, easily causes the destruction of nutriment in licorice powder, the higher cost of production.
Summary of the invention
Aiming at the problems existing in the prior art, the purpose of the present invention is to provide a kind of preparation method of licorice powder, institutes
Licorice powder be brown, it is slightly sweet, with the intrinsic taste smell of Radix Glycyrrhizae, free from extraneous odour, in powdered, have and preferably reconstitute
Property, and it is visible by naked eyes exogenous impurity, the glycyrrhizic acid content in licorice powder is up to 8.6g/100g, net content negative bias difference, sense
Official's index, physical and chemical index and microbiological indicator are met the requirements of the standard；In preparation method, low temperature is used in concentration and spray drying
Processing, the loss of the effective component in licorice powder can be protected to greatest extent, will not qualitative change, product color taste, content etc. refer to
Mark substantially improves raising；Preparation method is simple, low in cost.
In order to achieve the above object, the present invention is achieved by the following scheme.
(1) a kind of preparation method of licorice powder, including following preparation step：
Step 1, licorice raw material is pre-processed, water mentions, and obtains extracting solution；
Step 2, the extracting solution is concentrated, is spray-dried, crushed, packed, sterilizing obtains licorice powder.
Preferably, in step 1, the moisture content of the licorice raw material is no more than 12%.
Preferably, in step 1, the pretreatment includes impurity elimination, crushing.
It is further preferred that in step 1, it is described to crush to be crushed to 20-30 mesh.
Preferably, in step 1, the water is mentioned to be carried out by following operating procedure：It is added into pretreated licorice raw material
The distilled water of 10-12 times of Radix Glycyrrhizae quality, water mention, and filtering obtains extracting solution.
Preferably, in step 1, the temperature that the water mentions is 90-110 DEG C, and the time that water mentions is 3.6-5.4 hours, and water mentions
Number be 3 times.
Preferably, in step 2, the vacuum degree of the concentration is 0.01-0.05MPa, and the temperature of concentration is 65-75 DEG C, dense
The time of contracting is 45-55 minutes.
Preferably, in step 2, the temperature of the spray drying is 65-75 DEG C, and the time of spray drying is 50-70 minutes,
The pressure of spray drying is 200-400Pa.
Preferably, described to crush to be crushed to 80-100 mesh in step 2.
Preferably, in step 2, the temperature of the sterilizing is 100-110 DEG C, and the time of sterilizing is 1.5-2.5 hours.
Compared with prior art, beneficial effects of the present invention are：The resulting licorice powder of the present invention is brown, slightly sweet, tool
Taste smell, the free from extraneous odour for having Radix Glycyrrhizae intrinsic have preferable brew, and be visible by naked eyes exogenous impurity, Radix Glycyrrhizae in powdered
Glycyrrhizic acid content in powder is up to 8.6g/100g, net content negative bias difference, organoleptic indicator, physical and chemical index and microbiological indicator
It meets the requirements of the standard.In preparation method, 65-75 DEG C of low-temperature treatment is used in concentration and spray drying, it can be to greatest extent
Protect the loss of the effective component in licorice powder, will not qualitative change, the indexs such as product color taste, content substantially improve raising.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
It will be appreciated that the following example is merely to illustrate the present invention, and it is not construed as limiting the scope of the invention.
Embodiment 1
A kind of preparation method of licorice powder, including following preparation step：
Step 1, it carries out an acceptance inspection after qualification to licorice raw material, using impurity elimination, is crushed to 20 mesh, throws the modes such as tank and located in advance
The distilled water of 10 times of quality of Radix Glycyrrhizae is added into pretreated licorice raw material, is heated to 100 DEG C of water and mentions three times for reason, and every time 1.5
Hour, filtering merges extracting solution three times.
Step 2, extracting solution be concentrated 50 minutes under the conditions of temperature is 70 DEG C, vacuum degree is 0.03MPa, be condensed into
Medicinal extract, then temperature is 70 DEG C, pressure is to be spray-dried 60 minutes under 30mm (300Pa) water column conditions, spray drying to water
Point content is crushed to 80 mesh less than 10%, packs, sterilize under the conditions of 105 DEG C 2 hours to get.
Embodiment 2
A kind of preparation method of licorice powder, including following preparation step：
Step 1, it carries out an acceptance inspection after qualification to licorice raw material, using impurity elimination, is crushed to 25 mesh, throws the modes such as tank and located in advance
The distilled water of 11 times of quality of Radix Glycyrrhizae is added into pretreated licorice raw material, is heated to 90 DEG C of water and mentions three times for reason, and every time 1.8
Hour, filtering merges extracting solution three times.
Step 2, extracting solution be concentrated 55 minutes under the conditions of temperature is 65 DEG C, vacuum degree is 0.01MPa, be condensed into
Medicinal extract, then temperature is 65 DEG C, pressure is to be spray-dried 70 minutes under 40mm (400Pa) water column conditions, spray drying to water
Point content is crushed to 100 mesh less than 10%, packs, sterilize under the conditions of 100 DEG C 2.5 hours to get.
Embodiment 3
A kind of preparation method of licorice powder, including following preparation step：
Step 1, it carries out an acceptance inspection after qualification to licorice raw material, using impurity elimination, is crushed to 30 mesh, throws the modes such as tank and located in advance
The distilled water of 12 times of quality of Radix Glycyrrhizae is added into pretreated licorice raw material, is heated to 110 DEG C of water and mentions three times for reason, and every time 1.2
Hour, filtering merges extracting solution three times.
Step 2, extracting solution be concentrated 45 minutes under the conditions of temperature is 75 DEG C, vacuum degree is 0.05MPa, be condensed into
Medicinal extract, then temperature is 75 DEG C, pressure is to be spray-dried 50 minutes under 20mm (200Pa) water column conditions, spray drying to water
Point content is crushed to 90 mesh less than 10%, packs, sterilize under the conditions of 110 DEG C 1.5 hours to get.
In above embodiments, the ACCEPTABLE QUALITY LEVEL of licorice raw material is as shown in table 1：
The ACCEPTABLE QUALITY LEVEL of 1 licorice raw material of table
Using Q/SXHD 0002S-2016《Licorice powder》With《Solid beverage generates licensing and examines detailed rules and regulations (2006) version》's
Examination criteria to the net content negative bias difference of the resulting licorice powder of embodiment 1, organoleptic indicator, physical and chemical index and microbiological indicator into
Row detection, specific testing result is as shown in table 2-5.
The net content negative bias difference of 2 licorice powder of table
| Inspection project | Unit | Standard index | Inspection result | It is unidirectional to determine |
| Net content minus deviation | % | ≤4.5 | -0.5 | It is qualified |
Organoleptic indicator's testing result of 3 licorice powder of table
The physical and chemical index testing result of 4 licorice powder of table
The microbial indicators detected result of 5 licorice powder of table
By table 2-5 it is found that the net content negative bias difference of the resulting licorice powder of the present invention, organoleptic indicator, physical and chemical index and micro-
Biological indicators meet Q/SXHD 0002S-2016《Licorice powder》With《Solid beverage generates licensing and examines detailed rules and regulations (2006) version》's
Examination criteria requirement.
The resulting licorice powder of the present invention is brown, slightly sweet, with the intrinsic taste smell of Radix Glycyrrhizae, free from extraneous odour, in powdered,
With preferable brew, and it is visible by naked eyes exogenous impurity.Glycyrrhizic acid content in licorice powder is up to 8.6g/100g, Radix Glycyrrhizae
Acid has inhibiting effect to sarcoma, growth of cancer cells, has good inhibiting effect to AIDS, and can increase human immunity
Function, while there is apparent antidiuretic activity.
Although the present invention is described in detail with a general description of the specific embodiments in this specification,
But on the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.
Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, belong to claimed model
It encloses.
Claims (10)
1. a kind of preparation method of licorice powder, which is characterized in that including following preparation step：
Step 1, licorice raw material is pre-processed, water mentions, and obtains extracting solution；
Step 2, the extracting solution is concentrated, is spray-dried, crushed, packed, sterilizing obtains licorice powder.
2. the preparation method of licorice powder according to claim 1, which is characterized in that in step 1, the water of the licorice raw material
Content is divided to be no more than 12%.
3. the preparation method of licorice powder according to claim 1, which is characterized in that in step 1, the pretreatment is comprising going
Miscellaneous, crushing.
4. the preparation method of licorice powder according to claim 3, which is characterized in that described to crush to be crushed in step 1
20-30 mesh.
5. the preparation method of licorice powder according to claim 1, which is characterized in that in step 1, the water is mentioned by following behaviour
Make step progress：The distilled water of 10-12 times of Radix Glycyrrhizae quality is added into pretreated licorice raw material, water mentions, and filters, must extract
Liquid.
6. the preparation method of licorice powder according to claim 5, which is characterized in that in step 1, the temperature that the water mentions is
90-110 DEG C, the time that water mentions is 3.6-5.4 hours, and the number that water mentions is 3 times.
7. the preparation method of licorice powder according to claim 1, which is characterized in that in step 2, the vacuum degree of the concentration
For 0.01-0.05MPa, the temperature of concentration is 65-75 DEG C, and the time of concentration is 45-55 minutes.
8. the preparation method of licorice powder according to claim 1, which is characterized in that in step 2, the temperature of the spray drying
Degree is 65-75 DEG C, and the time of spray drying is 50-70 minutes, and the pressure of spray drying is 200-400Pa.
9. the preparation method of licorice powder according to claim 1, which is characterized in that described to crush to be crushed in step 2
80-100 mesh.
10. the preparation method of licorice powder according to claim 1, which is characterized in that in step 2, the temperature of the sterilizing
It is 100-110 DEG C, the time of sterilizing is 1.5-2.5 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810886379.9A CN108904582A (en) | 2018-08-06 | 2018-08-06 | A kind of preparation method of licorice powder |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810886379.9A CN108904582A (en) | 2018-08-06 | 2018-08-06 | A kind of preparation method of licorice powder |
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| Publication Number | Publication Date |
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| CN108904582A true CN108904582A (en) | 2018-11-30 |
Family
ID=64393499
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| CN201810886379.9A Pending CN108904582A (en) | 2018-08-06 | 2018-08-06 | A kind of preparation method of licorice powder |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101396426A (en) * | 2007-09-28 | 2009-04-01 | 未名天人中药有限公司 | Glycyrrhiza dispensing granule and preparation method and quality control method thereof |
| CN102204951A (en) * | 2011-05-24 | 2011-10-05 | 药都制药集团股份有限公司 | Method for extracting active components from licorice |
| CN102526176A (en) * | 2012-01-21 | 2012-07-04 | 保定冀中药业有限公司 | Oral administration mineral medicine manufactured by liquorice aqueous extracts |
-
2018
- 2018-08-06 CN CN201810886379.9A patent/CN108904582A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101396426A (en) * | 2007-09-28 | 2009-04-01 | 未名天人中药有限公司 | Glycyrrhiza dispensing granule and preparation method and quality control method thereof |
| CN102204951A (en) * | 2011-05-24 | 2011-10-05 | 药都制药集团股份有限公司 | Method for extracting active components from licorice |
| CN102526176A (en) * | 2012-01-21 | 2012-07-04 | 保定冀中药业有限公司 | Oral administration mineral medicine manufactured by liquorice aqueous extracts |
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Application publication date: 20181130 |
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