CN108853551A - A kind of preparation method of the natural botanical extraction liquid cleanser removed odors - Google Patents

A kind of preparation method of the natural botanical extraction liquid cleanser removed odors Download PDF

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Publication number
CN108853551A
CN108853551A CN201810772954.2A CN201810772954A CN108853551A CN 108853551 A CN108853551 A CN 108853551A CN 201810772954 A CN201810772954 A CN 201810772954A CN 108853551 A CN108853551 A CN 108853551A
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natural
extract
preparation
extraction
cleanser
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CN201810772954.2A
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周峰
陶云
周成昌
周贻云
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Anhui Yangzi Biotech Co Ltd
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Anhui Yangzi Biotech Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/14Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Botany (AREA)
  • Zoology (AREA)
  • Detergent Compositions (AREA)

Abstract

The present invention settles sth. according to policy or law the preparation method of natural botanical extraction liquid cleanser removed odors a kind of, includes the following steps:The selection of S1, raw material;S2, natural plant extraction object is prepared;S3, preparation natural Chinese medicinal herb extracting solution;S4, mixed plant extract and the Chinese herbal medicine extract;The natural plants cleanser that S5, preparation remove odors.When the present invention prepares natural plant extraction object, utilize the lower characteristic of subcritical fluids boiling point, air is taken out to extractor by mentioning, improve extractor vacuum degree, make extractant rapid evaporation, improve recovery rate of extraction solvent, reduce energy consumption, produce three-waste free pollution, environmental protection, health and safety, and improve extraction yield, shorten extraction time, the form combined using natural botanical extraction liquid with natural Chinese medicinal herb extracting solution, prepare deodorization eliminating greasiness, dispelling abnormal flavor, aromatic flavour, it is safe and non-toxic, and have good duration remove odors can Direct spraying natural plants cleanser.

Description

A kind of preparation method of the natural botanical extraction liquid cleanser removed odors
Technical field
The invention belongs to natural botanical extraction liquid cleanser technical fields, and in particular to a kind of natural plants removed odors The preparation method of extracting solution cleanser.
Background technique
With the improvement of living standards, requirement of the people to air quality is also higher and higher, environmental odors to human health, Mood, working efficiency etc. can affect.Air purifying preparation use is also more and more extensive, they are offseted except environment is different Taste is improved the quality of living, and has certain meaning.Air purifying preparation is varied, has essence covering type, physics to inhale by composition point Attached type, chemical reaction type, packing type have aerial fog type, aerosol type, a natural volatilizing, natural plant essential oils be it is a kind of it is volatile, With intense flavors, can with steam distillation come out oily liquids general name, due to natural perfume material plants essential oil and its spread out The olfactory and organoleptic feature that biology has are that synthetic perfume is difficult to substitute, in addition Gu of the people to synthesis spices and essence safety Consider and to the preference of natural perfume material so that natural plant essence oil is able to maintain that its firm market position.However the prior art The cleanser for preparing and can remove odors is not designed using natural botanical extraction liquid.
For this purpose, it is proposed that a kind of natural botanical extraction liquid combine with natural Chinese medicinal herb extracting solution can Direct spraying The preparation method of the natural botanical extraction liquid cleanser removed odors solves the above problems.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of natural botanical extraction liquid cleanser removed odors, with solution Certainly the problems mentioned above in the background art.
To achieve the above object, the present invention provides the following technical solutions:A kind of natural botanical extraction liquid removed odors is net The preparation method of agent, includes the following steps:
The selection of S1, raw material:Selecting fir, tea tree, folium eucalypti, peppermint, wintergreen, cortex moutan, Radix Glycyrrhizae and tea fruit is natural plants Raw material, choosing tsaoko, dried orange peel and semen myristicae is natural Chinese medicinal herb raw material;
S2, natural plant extraction object is prepared:Respectively by step S1 fir, tea tree, folium eucalypti, peppermint, wintergreen, cortex moutan, The natural plant raw materials such as Radix Glycyrrhizae and tea fruit are sent into the extractor of construction of pressure vessel with conveyer, and it is molten to squeeze into liquefied extraction Agent carries out multiple counter-current extraction, carries out hot water heating by extractor collet, makes the control of extraction process temperature at 40 DEG C, and pressure is Extract liquor is transferred in evaporator by 0.5MPa after extracting 40min;Then liquefied extractant is injected into extractor again, carried out Reextraction, entire extraction process totally four times;The extract liquor extracted every time is squeezed into evaporator and is evaporated, when in evaporator After extractant is gasified totally, remaining is exactly the target product extracted, as natural plant extraction object, and it is spare to take out cooling;
S3, preparation natural Chinese medicinal herb extracting solution:Respectively by the natural Chinese medicinal herb raw material of tsaoko, dried orange peel and semen myristicae in step S1 Corresponding natural Chinese medicinal herb powder is made after being pulverized and sieved with plant pulverizer, weighs corresponding a certain amount of medium-height grass respectively Medicine, after 70% ethyl alcohol is added, bored profit 2-3h is placed in percolation vat after being percolated and ethanol extract is made, and the dregs of a decoction after diafiltration are added Low temperature deionized water leaching, is made pure water leachate, pure water leachate and ethanol extract is mixed with naturally after filtering The Chinese herbal medicine extract is spare;
S4, mixed plant extract and the Chinese herbal medicine extract:The preparation of step S2, S3 natural plant extraction object and it is natural in In herbal medicine extracting solution, taking accounting is respectively 15-20% tsaoko extracting solution, 15-20% dried orange peel extracting solution, the extraction of 15-20% semen myristicae Liquid, 4-8% fir extract, 4-8% tea tree extract, 4-8% folium eucalypti extract, 4-8% peppermint extract, 4-8% deer hoof Careless extract, 4-8% cortex moutan extract, 4-8% Radix Glycyrrhizae extract and 4-8% tea fruit extract carry out compounding mixing;
The natural plants cleanser that S5, preparation remove odors:Solution mixed in step S4 is dissolved in 5--10% surface-active In agent, the essence of 0.1-0.2 is added, thus removed odors can Direct spraying natural plants cleanser.
Preferably, it is normal butane that liquefied extractant is squeezed into the step S2, and is expected molten than being 1.5:1.
Preferably, in the step S2 under the heating of evaporator, the extractant in extract liquor constantly gasifies, gasification Extractant becomes liquid by condensation cooling after compressor compresses, flows back into solvent tank recycling.
Preferably, the mass ratio of Chinese herbal medicine selected in the step S3 and the ethyl alcohol of addition is 1:1.
Preferably, the step S3 Chinese medicine slag and the mass ratio of the deionized water of addition are 1:1.
Preferably, surfactant is fatty alcohol polyoxyethylene ether in the step S5.
Technical effect and advantage of the invention:The preparation method of the natural botanical extraction liquid cleanser removed odors, system When standby natural plant extraction object, using the lower characteristic of subcritical fluids boiling point, air is taken out to extractor by mentioning, improves extraction Device vacuum degree makes extractant rapid evaporation, improves recovery rate of extraction solvent, reduces energy consumption, and production no three wastes is dirty Dye, environmental protection, health and safety, and improve extraction yield, shorten extraction time, utilize natural botanical extraction liquid and natural Chinese medicinal herb The form that extracting solution combines prepares deodorization eliminating greasiness, dispelling abnormal flavor, aromatic flavour, safe and non-toxic, and has good duration Remove odors can Direct spraying natural plants cleanser.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
A kind of preparation method of the natural botanical extraction liquid cleanser removed odors, includes the following steps:
The selection of S1, raw material:Selecting fir, tea tree, folium eucalypti, peppermint, wintergreen, cortex moutan, Radix Glycyrrhizae and tea fruit is natural plants Raw material, choosing tsaoko, dried orange peel and semen myristicae is natural Chinese medicinal herb raw material;
S2, natural plant extraction object is prepared:Respectively by step S1 fir, tea tree, folium eucalypti, peppermint, wintergreen, cortex moutan, The natural plant raw materials such as Radix Glycyrrhizae and tea fruit are sent into the extractor of construction of pressure vessel with conveyer, and it is molten to squeeze into liquefied extraction Agent carries out multiple counter-current extraction, carries out hot water heating by extractor collet, makes the control of extraction process temperature at 40 DEG C, and pressure is Extract liquor is transferred in evaporator by 0.5MPa after extracting 40min;Then liquefied extractant is injected into extractor again, carried out Reextraction, entire extraction process totally four times;The extract liquor extracted every time is squeezed into evaporator and is evaporated, when in evaporator After extractant is gasified totally, remaining is exactly the target product extracted, as natural plant extraction object, and it is spare to take out cooling;
S3, preparation natural Chinese medicinal herb extracting solution:Respectively by the natural Chinese medicinal herb raw material of tsaoko, dried orange peel and semen myristicae in step S1 Corresponding natural Chinese medicinal herb powder is made after being pulverized and sieved with plant pulverizer, weighs corresponding a certain amount of medium-height grass respectively Medicine, after 70% ethyl alcohol is added, bored profit 2-3h is placed in percolation vat after being percolated and ethanol extract is made, and the dregs of a decoction after diafiltration are added Low temperature deionized water leaching, is made pure water leachate, pure water leachate and ethanol extract is mixed with naturally after filtering The Chinese herbal medicine extract is spare;
S4, mixed plant extract and the Chinese herbal medicine extract:The preparation of step S2, S3 natural plant extraction object and it is natural in In herbal medicine extracting solution, taking accounting is respectively 15-20% tsaoko extracting solution, 15-20% dried orange peel extracting solution, the extraction of 15-20% semen myristicae Liquid, 4-8% fir extract, 4-8% tea tree extract, 4-8% folium eucalypti extract, 4-8% peppermint extract, 4-8% deer hoof Careless extract, 4-8% cortex moutan extract, 4-8% Radix Glycyrrhizae extract and 4-8% tea fruit extract carry out compounding mixing;
The natural plants cleanser that S5, preparation remove odors:Solution mixed in step S4 is dissolved in 5--10% surface-active In agent, the essence of 0.1-0.2 is added, thus removed odors can Direct spraying natural plants cleanser.
Specifically, squeezing into liquefied extractant in the step S2 is normal butane, and expect molten than being 1.5:1.
Specifically, the extractant in extract liquor constantly gasifies, gasification in the step S2 under the heating of evaporator Extractant becomes liquid by condensation cooling after compressor compresses, flows back into solvent tank recycling.
Specifically, the mass ratio of the ethyl alcohol of Chinese herbal medicine and addition selected in the step S3 is 1:1.
Specifically, the step S3 Chinese medicine slag and the mass ratio of the deionized water of addition are 1:1.
Specifically, surfactant is fatty alcohol polyoxyethylene ether in the step S5.
The preparation method of the natural botanical extraction liquid cleanser removed odors when preparing natural plant extraction object, utilizes The lower characteristic of subcritical fluids boiling point takes out air to extractor by mentioning, improves extractor vacuum degree, keep extractant quick Evaporation, improves recovery rate of extraction solvent, reduces energy consumption, produces three-waste free pollution, environmentally friendly, health and safety, and It improves extraction yield, shorten extraction time, the form combined using natural botanical extraction liquid with natural Chinese medicinal herb extracting solution, preparation Deodorization eliminating greasiness, dispelling abnormal flavor, aromatic flavour, safe and non-toxic out, and have good duration remove odors can Direct spraying Natural plants cleanser.
Finally it should be noted that:The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features, All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention Within protection scope.

Claims (6)

1. a kind of preparation method of the natural botanical extraction liquid cleanser removed odors, which is characterized in that include the following steps:
The selection of S1, raw material:Selecting fir, tea tree, folium eucalypti, peppermint, wintergreen, cortex moutan, Radix Glycyrrhizae and tea fruit is natural plants Raw material, choosing tsaoko, dried orange peel and semen myristicae is natural Chinese medicinal herb raw material;
S2, natural plant extraction object is prepared:Respectively by step S1 fir, tea tree, folium eucalypti, peppermint, wintergreen, cortex moutan, The natural plant raw materials such as Radix Glycyrrhizae and tea fruit are sent into the extractor of construction of pressure vessel with conveyer, and it is molten to squeeze into liquefied extraction Agent carries out multiple counter-current extraction, carries out hot water heating by extractor collet, makes the control of extraction process temperature at 40 DEG C, and pressure is Extract liquor is transferred in evaporator by 0.5MPa after extracting 40min;Then liquefied extractant is injected into extractor again, carried out Reextraction, entire extraction process totally four times;The extract liquor extracted every time is squeezed into evaporator and is evaporated, when in evaporator After extractant is gasified totally, remaining is exactly the target product extracted, as natural plant extraction object, and it is spare to take out cooling;
S3, preparation natural Chinese medicinal herb extracting solution:Respectively by the natural Chinese medicinal herb raw material of tsaoko, dried orange peel and semen myristicae in step S1 Corresponding natural Chinese medicinal herb powder is made after being pulverized and sieved with plant pulverizer, weighs corresponding a certain amount of medium-height grass respectively Medicine, after 70% ethyl alcohol is added, bored profit 2-3h is placed in percolation vat after being percolated and ethanol extract is made, and the dregs of a decoction after diafiltration are added Low temperature deionized water leaching, is made pure water leachate, pure water leachate and ethanol extract is mixed with naturally after filtering The Chinese herbal medicine extract is spare;
S4, mixed plant extract and the Chinese herbal medicine extract:The preparation of step S2, S3 natural plant extraction object and it is natural in In herbal medicine extracting solution, taking accounting is respectively 15-20% tsaoko extracting solution, 15-20% dried orange peel extracting solution, the extraction of 15-20% semen myristicae Liquid, 4-8% fir extract, 4-8% tea tree extract, 4-8% folium eucalypti extract, 4-8% peppermint extract, 4-8% deer hoof Careless extract, 4-8% cortex moutan extract, 4-8% Radix Glycyrrhizae extract and 4-8% tea fruit extract carry out compounding mixing;
The natural plants cleanser that S5, preparation remove odors:Solution mixed in step S4 is dissolved in 5--10% surface-active In agent, the essence of 0.1-0.2 is added, thus removed odors can Direct spraying natural plants cleanser.
2. a kind of preparation method of natural botanical extraction liquid cleanser removed odors according to claim 1, feature It is:It is normal butane that liquefied extractant is squeezed into the step S2, and is expected molten than being 1.5:1.
3. a kind of preparation method of natural botanical extraction liquid cleanser removed odors according to claim 1, feature It is:In the step S2 under the heating of evaporator, the extractant in extract liquor constantly gasifies, the extractant warp of gasification Liquid is become by condensation cooling after compressor compresses, flows back into solvent tank recycling.
4. a kind of preparation method of natural botanical extraction liquid cleanser removed odors according to claim 1, feature It is:The mass ratio of selected Chinese herbal medicine and the ethyl alcohol of addition is 1 in the step S3:1.
5. a kind of preparation method of natural botanical extraction liquid cleanser removed odors according to claim 1, feature It is:The step S3 Chinese medicine slag and the mass ratio of the deionized water of addition are 1:1.
6. a kind of preparation method of natural botanical extraction liquid cleanser removed odors according to claim 1, feature It is:Surfactant is fatty alcohol polyoxyethylene ether in the step S5.
CN201810772954.2A 2018-07-14 2018-07-14 A kind of preparation method of the natural botanical extraction liquid cleanser removed odors Withdrawn CN108853551A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109865419A (en) * 2019-02-28 2019-06-11 河南传宇生物科技有限公司 A kind of plant eliminating smell agent and preparation method thereof
CN110452775A (en) * 2019-08-26 2019-11-15 匠领(厦门)科技有限公司 A kind of preparation method of plants essential oil eliminating smell agent
CN113201249A (en) * 2021-05-31 2021-08-03 湖北绿新环保包装科技有限公司 High-stability water-based ink

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109865419A (en) * 2019-02-28 2019-06-11 河南传宇生物科技有限公司 A kind of plant eliminating smell agent and preparation method thereof
CN110452775A (en) * 2019-08-26 2019-11-15 匠领(厦门)科技有限公司 A kind of preparation method of plants essential oil eliminating smell agent
CN113201249A (en) * 2021-05-31 2021-08-03 湖北绿新环保包装科技有限公司 High-stability water-based ink

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