CN101928660B

CN101928660B - Method for producing cortex acanthopanacis spirits by Chinese medicinal material fluid extract method

Info

Publication number: CN101928660B
Application number: CN 201010252012
Authority: CN
Inventors: 钱建华; 方小明; 龚景华
Original assignee: ZHEJIANG ZHIZHONGHE INDUSTRIAL Co Ltd
Current assignee: ZHEJIANG ZHIZHONGHE INDUSTRIAL CO., LTD.
Priority date: 2010-08-12
Filing date: 2010-08-12
Publication date: 2013-08-28
Anticipated expiration: 2030-08-12
Also published as: CN101928660A

Abstract

The invention relates to a method for producing cortex acanthopanacis spirits, in particular to a method for producing the cortex acanthopanacis spirits, which improves a preparation method of decoction. The invention relates to a method for producing the cortex acanthopanacis spirits by a Chinese medicinal material fluid extract method, in the step of preparing the decoction of the method, liquid medicine extracted from Chinese medicinal materials is concentrated to prepare fluid extract; and in the step of preparing semi-finished spirits, the fluid extract is added into the semi-finished spirits, wherein the Chinese medicinal materials for concentrating the extracted liquid medicine to prepare the fluid extract are at least one of fragrant solomonseal rhizome, gardenia, red yeast rice, mint, cassia twig, finger citron, costustoot, villous amomum fruit, star anise, mountain spicy tree fruit, clove, rhizoma kaempferiae and tangerine peel. In the method, the extracted liquid medicine is concentrated to prepare the medicinal material fluid extract, and the medicinal material fluid extract is prepared to produce the cortex acanthopanacis spirits. Compared with the cortex acanthopanacis spirits produced from direct liquid medicine, the cortex acanthopanacis spirits produced by the method has good mouthfeel and sensory index and stable quality and maintains medicinal fragrance, and health-care components contained in the cortex acanthopanacis spirits produced by the method are the same as those of the cortex acanthopanacis spirits produced from the liquid medicine.

Description

The method of Chinese medicinal materials fluid extract method production slender acanthopanax bark spirit

Technical field

The present invention relates to a kind of production method of slender acanthopanax bark spirit, relate in particular to a kind of production method of improving concoction preparation method's slender acanthopanax bark spirit.

Background technology

Slender acanthopanax bark spirit is the traditional product in Zhejiang, is a traditional famous brand of wine that long history is arranged.Slender acanthopanax bark spirit adopts China's traditional medicine and modern nutriology knowledge, select 20 kinds of traditional Chinese medicines materials such as Wu Chia Pee, Radix Angelicae Sinensis, fructus amomi, cape jasmine, radix polygonati officinalis for use, behind the special vintage soaking in Chinese liquor, add glutinous rice-honey wine, white sugar, honey, adopt unique " fermentation of nine wines, four degree leachings " making method and Thousand-Island Lake crystal's system to form.In slender acanthopanax bark spirit's production process, need to make soup, the effective constituent in namely extracting.The technology of making soup at present can be divided into pickling process, circumfluence method and percolation.

(1) pickling process: be divided into cold pickling process, hot pickling process and pump circulation dipping

1. cold pickling process is at room temperature to flood Chinese medicinal materials, claims the normal temperature dipping method again.Be operating as get it filled material meal or fragment, be equipped with in the lid container, add quantitative basic wine, generally flood more than 14 days, in the steeping process, often stir or jolting.

2. hot pickling process, traditional method places container with lid with after the medicinal material chopping or pulverizing, and adds the wine of prescription specified amount, with after boiling certain hour, puts iced storage then.In the big production of industry, the Chinese medicinal materials after the coarse crushing is bound up with gauze, be suspended from the liquor, put into the container of sealing again, put in the water-bath and flooded 3-7 days with 40-50 ℃, also can flood twice and merge immersion liquid, place a few days after-filtration collection medicinal liquor.

3. pump circulation is flooded: will extract with the disposable preparation of wine liquid full dose intact, utilize pump to circulate and contact extraction with medicinal material extracting circulation fluid at normal temperatures, on extractor, the outlet of circulation fluid pipe should have spray equipment, evenly places in the hope of liquid stream and produces spice kind slag or channeling.

(2) percolation

Percolation is that the medicinal material coarse grain is put in the percolator, and basic wine adds from the top of percolator continuously, and percolate constantly flows out from the bottom, thereby lixiviate goes out the method for contained soluble components in the medicinal material.

(3) circumfluence method: be divided into backflow hot dipping method and backflow cold-maceration

1. backflow hot dipping method: the medicinal material processing process of preparing Chinese medicine is placed in the leacher, connect condenser on the leacher, volume (basic wine) is added in the leacher, heated solvent, solvent evaporation makes molten gas cooling become liquid by condenser, this liquid is back in the leacher again, so repeatedly, till leaching fully.

2. backflow cold-maceration: the copper wire basket that pharmaceutical decocting piece is placed leacher.Add basic wine by liquid storage cylinder through valve, when treating that leach liquor is full of siphon pipe, then flow in the evaporating pan through valve automatically, be heated evaporation in evaporating pan, steam enters condenser along conduit, flows in the liquid storage cylinder again after condensation, flow into leacher, lixiviate repeatedly by valve again.

The producer of present most of production slender acanthopanax bark spirit is most to adopt and all uses pickling process and percolation to extract Chinese medicinal materials to make soup.The advantage of pickling process is the flavour ingredient in the Chinese medicinal materials fully to be extracted, but complicated component fails effective constituent is effectively separated with other invalid components, and the speed of extracting is slow, production cycle is long, extracts active ingredients is incomplete, production efficiency is low, and flavour of a drug were denseer when preparation was produced in the slender acanthopanax bark spirit.The advantage that percolation extracts Chinese medicinal materials be can accelerate the Chinese medicinal materials extraction rate, extracts active ingredients is more complete, it is higher to give birth to tea efficient, but the soup of making preparation when producing in the slender acanthopanax bark spirit flavour of a drug denseer.

The condition of production by present slender acanthopanax bark spirit, in big production, adopt aforesaid method to extract Chinese medicinal materials and have a huge defective, be the liquor strength instability of medicinal material extract gained, thus slender acanthopanax bark spirit's unstable product quality of preparation, and mouthfeel, medicine perfume (or spice), Oranoleptic indicator are all unstable.

Summary of the invention

In order to have solved the problem of liquor strength instability, slender acanthopanax bark spirit unstable product quality, the method that the purpose of this invention is to provide a kind of Chinese medicinal materials fluid extract method production slender acanthopanax bark spirit, this method is that soup that the concentrated traditional Chinese medicine material extracts is made fluid extract and is formulated in the slender acanthopanax bark spirit, thereby improves slender acanthopanax bark spirit's product quality, the slender acanthopanax bark spirit's quality stability between guaranteeing batch.

In order to realize above-mentioned purpose, the present invention adopts following technical scheme:

The method of Chinese medicinal materials fluid extract method production slender acanthopanax bark spirit, this method comprises concoction preparation, the preparation of work in-process wine and can step, wherein: the soup that in the described concoction preparation process Chinese medicinal materials is extracted concentrates makes fluid extract, fluid extract added preparation work in-process wine then in work in-process wine preparation steps, the soup of extraction concentrates the Chinese medicinal materials of making fluid extract and is at least a kind of in radix polygonati officinalis, cape jasmine, Red kojic rice, peppermint, cassia twig, Buddha's hand, the banksia rose, fructus amomi, star anise, Mountain Spicy Tree Fruit, cloves, kaempferia galamga and the dried orange peel.

As preferably, described the soup that extracts is concentrated the Chinese medicinal materials of making fluid extract is radix polygonati officinalis, cape jasmine, Red kojic rice, peppermint, cassia twig, Buddha's hand, the banksia rose, fructus amomi, star anise, Mountain Spicy Tree Fruit, cloves, kaempferia galamga and dried orange peel.

As preferably, the concentration of described fluid extract is Chinese medicinal materials effective constituent weight and the ratio of basic wine weight 1: 1～1: 1.5.

As preferably, described in work in-process wine preparation steps the fluid extract of every flavor Chinese medicinal materials to add weight be 0.1%～0.5% of slender acanthopanax bark spirit's total amount.

As preferably, also comprise in the above-mentioned concoction preparation process and adopt traditional immersion process for preparing Chinese medicine extract, to adopt the Chinese medicine extract of traditional immersion process for preparing to add preparation work in-process wine then in work in-process wine preparation steps, the Chinese medicinal materials that adopts traditional immersion process for preparing Chinese medicine extract is Wu Chia Pee, wolfberry fruit, Herba Epimedii, Radix Angelicae Sinensis and Radix Codonopsis.

Chinese medicinal materials weight and basic wine weight ratio were at 1: 3～1: 6 during as the Chinese medicinal materials dipping of preferred again, above-mentioned employing tradition immersion process for preparing Chinese medicine extract.

As preferred again, it is 0.5%～2% of slender acanthopanax bark spirit's total amount that the above-mentioned Chinese medicine extract that adopts traditional immersion process for preparing in work in-process wine preparation steps adds weight.

The present invention is owing to adopted above-mentioned technical scheme, soup after extracting is concentrated, make the medicinal material fluid extract, then with medicinal material fluid extract preparation production slender acanthopanax bark spirit, the slender acanthopanax bark spirit that produces is better than the slender acanthopanax bark spirit's mouthfeel that adopts direct soup to produce, the fragrant feature of medicine keeps, the Oranoleptic indicator is better, and the health-care components that contains is the same with the slender acanthopanax bark spirit of soup production, more stable quality.In addition, the present invention extracts by the traditional cold pickling process for the Chinese medicinal materials that other are not suitable for making fluid extract, can not destroy the effective ingredient of other Chinese medicinal materialss.

Embodiment

The method of Chinese medicinal materials fluid extract method production slender acanthopanax bark spirit, this method comprise concoction preparation, liquid glucose preparation, the preparation of work in-process wine and can step.

Slender acanthopanax bark spirit tests at finished product, and the fluid extract that the soup that the concentrated traditional Chinese medicine material is extracted is made and be mixed to join in the slender acanthopanax bark spirit by the soup that traditional pickling process is made is tested.The soup that Chinese medicinal materials extracts concentrates makes having of fluid extract: radix polygonati officinalis, cape jasmine, Red kojic rice, peppermint, cassia twig, Buddha's hand, the banksia rose, fructus amomi, star anise, Mountain Spicy Tree Fruit, cloves, kaempferia galamga, dried orange peel, the concentration of fluid extract are Chinese medicinal materials weight and the ratio of basic wine weight 1: 1.2.Adopt the medicinal material of traditional pickling process to have: Wu Chia Pee, wolfberry fruit, Herba Epimedii, Radix Angelicae Sinensis, Radix Codonopsis, Chinese medicinal materials weight and basic wine weight ratio were at 1: 5 during the Chinese medicinal materials dipping.

The processing condition that fluid extract is made: get herbal medicine according to the percolation under fluid extract and the extractum item, make solvent with 50%-70% ethanol, flood after 24 hours, with the speed of per minute 1-3ml diacolation slowly, collect percolate, container is preserved in addition, be concentrated into the thick paste shape below 60 ℃, use the 50%-70% alcohol dilution, leave standstill a few days, filter namely.

Usage quantity: operate by slender acanthopanax bark spirit's proportioning, tested number is that radix polygonati officinalis, cape jasmine, Red kojic rice, peppermint, cassia twig, Buddha's hand, the banksia rose, fructus amomi, star anise, Mountain Spicy Tree Fruit, cloves, kaempferia galamga, each fluid extract of dried orange peel add preparation by 0.3% of slender acanthopanax bark spirit's total amount, and wolfberry fruit, Herba Epimedii, Radix Angelicae Sinensis, each Chinese medicinal materials dipping extracting solution of Radix Codonopsis add preparation by 1% of slender acanthopanax bark spirit's total amount.

The relative merits contrast of Chinese medicinal materials soup and the concentrated fluid extract of making

Claims

1. the method for Chinese medicinal materials fluid extract method production slender acanthopanax bark spirit, this method comprises the concoction preparation, the preparation of work in-process wine and can step, described Chinese medicinal materials comprises Wu Chia Pee, wolfberry fruit, Herba Epimedii, Radix Angelicae Sinensis, Radix Codonopsis, radix polygonati officinalis, cape jasmine, Red kojic rice, peppermint, cassia twig, Buddha's hand, the banksia rose, fructus amomi, star anise, Mountain Spicy Tree Fruit, cloves, kaempferia galamga and dried orange peel, it is characterized in that: the soup that in the concoction preparation process Chinese medicinal materials is extracted concentrates makes fluid extract, in work in-process wine preparation steps fluid extract is added preparation work in-process wine then, the fluid extract of every flavor Chinese medicinal materials adding weight is 0.1%～0.5% of slender acanthopanax bark spirit's total amount in work in-process wine preparation steps; It is radix polygonati officinalis, cape jasmine, Red kojic rice, peppermint, cassia twig, Buddha's hand, the banksia rose, fructus amomi, star anise, Mountain Spicy Tree Fruit, cloves, kaempferia galamga and dried orange peel that the soup that extracts concentrates the Chinese medicinal materials of making fluid extract; The concentration of described fluid extract is Chinese medicinal materials effective constituent weight and the ratio 1:1～1:1.5 of basic wine weight; Also comprise in the concoction preparation process and adopt traditional immersion process for preparing Chinese medicine extract, to adopt the Chinese medicine extract of traditional immersion process for preparing to add preparation work in-process wine then in work in-process wine preparation steps, adopting the Chinese medicine extract adding weight of traditional immersion process for preparing in work in-process wine preparation steps is 0.5%～2% of slender acanthopanax bark spirit's total amount; The Chinese medicinal materials that adopts traditional immersion process for preparing Chinese medicine extract is Wu Chia Pee, wolfberry fruit, Herba Epimedii, Radix Angelicae Sinensis and Radix Codonopsis; Adopt Chinese medicinal materials when dipping Chinese medicinal materials weight of traditional immersion process for preparing Chinese medicine extract and basic wine weight ratio at 1:3～1:6.