CN108828029A - Moisture percentage measuring apparatus based on plug-in capacitance sensor - Google Patents

Moisture percentage measuring apparatus based on plug-in capacitance sensor Download PDF

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Publication number
CN108828029A
CN108828029A CN201810923285.4A CN201810923285A CN108828029A CN 108828029 A CN108828029 A CN 108828029A CN 201810923285 A CN201810923285 A CN 201810923285A CN 108828029 A CN108828029 A CN 108828029A
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amplifier
capacitance sensor
electrode
capacitance
water
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CN108828029B (en
Inventor
王超
曹晴晴
孙宏军
张帅
李潇亮
王伟
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Tianjin University
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Tianjin University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/02Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
    • G01N27/22Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance
    • G01N27/223Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance for determining moisture content, e.g. humidity
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/02Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
    • G01N27/22Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance
    • G01N27/228Circuits therefor

Abstract

The present invention relates to a kind of moisture percentage measuring apparatus based on plug-in capacitance sensor, including capacitance sensor, signal processing unit, effective value measurement unit and computing unit.Capacitance sensor includes two guard electrodes as excitation electrode and excitation measuring electrode and the side of being fixed thereon and lower section of measuring electrode simultaneously;Signal processing unit includes front-end amplifier, coaxial cable, AC signal generator and difference amplifier; the negative input end of front-end amplifier is connected by coaxial signal lines with the excitation measuring electrode in capacitance sensor; the positive input terminal of front-end amplifier is connected with AC signal generator, while two be connected in capacitance sensor guard electrode, the shielded layer of coaxial cable and the negative input end of difference amplifier;The negative input end and output end of front-end amplifier are connected to after one measuring resistance and capacitor are in parallel;The output end of front-end amplifier is connected to the positive input terminal of difference amplifier.

Description

Moisture percentage measuring apparatus based on plug-in capacitance sensor
Technical field
The present invention relates to field of oilfield exploitation, in particular to a kind of moisture content based on plug-in capacitance sensor Measuring device.
Background technique
Demand of the development of today's society to the energy constantly increases, and petroleum is as " first energy ", in national economy, country There is highly important status in strategy.But petroleum is a kind of non-renewable energy, so subtracting as far as possible in recovery process Few exploitation losses make full use of resource to have very great meaning.In petroleum works, in order to improve crude oil production effect Rate, often using high pressure water injection, the technology of polymer injection in the secondary recovery of oil well.But this process makes the original produced Contain water in oil, generally existing oil-water two-phase flow in the transmit process after leading to oil mining and exploitation.Crude oil production takes off The processes such as water, collection are defeated, measure, smelt will receive directly affecting for crude oil water content.In conveyance conduit, crude oil water content Precise measurement, for determining the yield and quality for developing service life, oil field of water outlet or oil entry, estimated output and prediction oil well Control, oil well state-detection, raising secondary oil recovery quality etc. play an important role.Therefore, moisture content is one very heavy The detection parameters wanted, real-time online detection moisture content have a very important significance, while being also the accurate on-line metering in oil field Difficulties.
At oil exploitation initial stage, the oil-water two-phase flow of low-water-content is full of in most of oil well.In this case, water phase For discrete phase, oil is mutually continuous phase, and capacitance method measurement of water ratio technology is primary selection.Traditional capacitance sensor is flat by a pair Plate electrode composition, one of as excitation electrode, another is measuring electrode.Although this electrode exciting field is evenly distributed, But there are power line edge effects and electrode positive area, electrode spacing to be difficult to the problems such as determining, is suitable for square pipe;Together Axis cylindrical capacitive transducer is largely clean cut system installation, and installation is complicated, difficult in maintenance;(skill is imaged in such as ECT to section multi-electrode Art) distribution situation of two phase flow in pipeline accurate can be measured, but its structure is complex, installation is inconvenient and at high cost.Cause This needs the sensor and survey that proposition exciting field is uniform and structure is simple, is easily installed for the oil-water two-phase flow of low-water-content Measure device.
Summary of the invention
For the low aqueous oil-water two-phase flow measurement of water ratio problem of oil well, the present invention proposes a kind of plug-in capacitance sensing Device device, it is intended to go out structure simply with the oily measuring and design mutually for the low aqueous water two phase flow moisture content of continuous phase and motivating The uniform forms of sensor in field provides new measuring device.When the conducting medium in pipeline is discrete phase, dielectric is continuous Blending agent in pipeline is equivalent to a capacitor by Xiang Shi, and when the phase content of blending agent changes, capacitor becomes therewith Change, finally moisture content can be obtained by functional relation between the two.Technical solution is as follows:
A kind of moisture percentage measuring apparatus based on plug-in capacitance sensor, for using oil as the low aqueous water of continuous phase Measurement of water ratio in Two-phase Flow Pipeline Transport, including capacitance sensor, signal processing unit, effective value measurement unit and calculating are single Member, which is characterized in that
Capacitance sensor is fixed at the union elbow of vertical duct and horizontal pipeline, along vertical pipeline direction on to Lower insertion, capacitance sensor include simultaneously as excitation electrode and measuring electrode excitation measuring electrode and the side of being fixed thereon with Two guard electrodes of lower section;
Signal processing unit includes front-end amplifier, coaxial cable, AC signal generator and difference amplifier, and front end is put The negative input end of big device is connected by coaxial signal lines with the excitation measuring electrode in capacitance sensor, front-end amplifier Positive input terminal be connected with AC signal generator, while two be connected in capacitance sensor guard electrode, coaxial cable Shielded layer and difference amplifier negative input end;One measuring resistance RfWith capacitor CfFront-end amplifier is connected to after parallel connection Negative input end and output end;The output end of front-end amplifier is connected to the positive input terminal of difference amplifier.
Effective value measurement unit converts voltage effective value for the exchange output sine voltage signal of difference amplifier, obtains Obtain the output voltage directly proportional to the capacitance of the oil-water two-phase flow in tested pipeline.
Computing unit, according to the acquisition output voltage directly proportional to the capacitance of the oil-water two-phase flow in tested pipeline, Using the functional relationship model of oil-water two-phase flow capacitance and moisture content, moisture content is calculated.
In being based on plug in construction, the same electrode of excitation measuring electrode share sensor of the invention, metal tube Road is used as with reference to ground, installation more more convenient than pipeline section type structure;The present invention measures the biography of signal using coaxial signal lines Defeated, the shielded layer of the coaxial cable connects AC signal generator, shadow of the distribution capacity to measuring signal in elimination measuring circuit It rings;In the present invention, signal processing unit and plug in sensor cooperate, 1) reduce the influence of cable distribution parameter;2) Ensure that excitation measuring electrode at electric field it is uniform;3) output voltage directly proportional to measured capacitance values is obtained.
Detailed description of the invention
Fig. 1 is measuring principle figure;
Fig. 2 is measurement equivalent circuit;
Fig. 3 is sensor structure figure;
Label in above-mentioned figure is:
1, measuring electrode, 2, guard electrode, 3, coaxial cable, 4, shielded layer, 5, AC signal generator, 6, front end are motivated Amplifier, 7, difference amplifier, 8, metallic conduit, 9, display instrument shell, 10, flange
Specific embodiment
The present invention will be described in detail with reference to the accompanying drawings and examples.
The invention mainly comprises setting for sensor design, signal processing unit, effective value measurement unit and computing unit Meter, specific design are as follows:
1. sensor design
As shown in Figure 1, plug-in capacitance sensor is by intermediate excitation measuring electrode and two upper and lower guard electrode groups At.Wherein, the same electrode for motivating and measuring share sensor, using even metallic conduit as with reference to ground.When installation, sensing Device is inserted into from up to down along vertical pipeline direction, and electrode is made to be located at vertical pipeline axle center.The excitation measuring electrode of sensor and Guard electrode distinguishes lead to signal processing unit, and lead uses shielded cable, drawn by center sensor.
2. signal processing unit, which is played, converts measurable electricity for the capacitance signal of oil-water two-phase flow in capacitance sensor The effect of signal is the core of measuring system.The composition of signal processing unit includes front-end amplifier, coaxial cable, friendship Flow signal generator and difference amplifier.Signal processing unit converts the collected signal of sensor by front-end amplifier For voltage signal vo1(t), sinusoidal voltage v is obtained using difference amplifiero2(t), it is then output to effective value measurement unit, The latter extracts wherein output voltage of the voltage effective value comprising capacitance information as entire unit.Concrete condition is as follows:
(1) sensor and signal processing unit are connected by coaxial cable first, that is, by coaxial signal lines One end connection sensor excitation measuring electrode, the other end connects the negative input end of front-end amplifier, makes measuring signal through same Shaft cable signal wire is transmitted on front-end amplifier;
(2) AC signal generator is used to provide driving voltage v for sensori(t)=VimSin (ω t), in order to reduce The influence of the electrode edge effect at measuring electrode is motivated, the output of AC signal generator is applied to sensor by the present invention The positive input terminal of guard electrode and front-end amplifier, according to " empty short " principle, the excitation of connection front-end amplifier negative input end is surveyed Amount electrode is identical as the potential of guard electrode, since the distortion of electrode edge electric field occurs near guard electrode, to avoid The influence of electrode edge effect to excitation measuring electrode measurement capacitor;
(3) under the connection type in (2), the output of AC signal generator is applied to connection excitation measurement by the present invention The shielded layer of electrode coaxial cable and the positive input terminal of front-end amplifier, according to " empty short " principle, the signal wire of coaxial cable with Shielding line equipotentiality, to reduce influence of the cable distributed capacitance to measurement;
(4) measuring resistance RfWith capacitor CfIt is connected to the negative input end and output end of front-end amplifier after parallel connection, flows through Motivate the electric current of measuring electrode and metallic conduit and the capacitance C of oil-water two-phase flowxIt is proportional.The present invention is by water-oil phase Stream is equivalent to capacitor Cx, it is equivalent after measuring circuit as shown in Fig. 2, its correspond to capacitive reactance beWherein, ω is excitation Voltage angular frequency.It is through frontend amplifying circuit output voltage
(5) in voltage signal vo1(t) in, to obtain the voltage signal directly proportional to measured capacitance, which introduces difference The output end of the output end of front-end amplifier and AC signal generator is connected to the just defeated of difference amplifier by amplifier Enter end and negative input end.Above-mentioned voltage vo1(t) signal is converted to sine voltage signal through difference amplifierAs j ω CfRfWhen > > 1, above formula can be approximately
3. the exchange of difference amplifier is exported sinusoidal voltage v through effective value measurement unito2(t) it is effective to be converted into voltage Value Vo.The virtual value is directly proportional to the capacitance of the oil-water two-phase flow in tested pipeline.
4. computing unit
After obtaining the output voltage directly proportional to measured capacitance values, by formulaWater-oil phase can be obtained The capacitance C of streamx, finally, moisture content can be calculated using the functional relationship model of oil-water two-phase flow capacitance and moisture content.
For the functional relationship model of above-mentioned oil-water two-phase flow capacitance and moisture content, common model mainly includes simply going here and there Parallel model, Maxwell-Garnett model, Bruggeman model, Hanai model, exponential model and logarithmic model etc.. Further, it is also possible to obtain specific capacitance and moisture content by experimental calibration, physical relationship between the two is established, and then obtain Functional relationship model out.
The design of plug-in capacitance sensor provided in this embodiment is as shown in figure 3, this sensor application is smaller in internal diameter And the pipeline with bent tube section.Plug-in capacitance sensor is installed from up to down along vertical pipeline direction, makes electrode position In vertical pipeline axle center.The same electrode of excitation and measurement share sensor, using even metallic conduit as with reference to ground.Sensing Device is made of intermediate excitation measuring electrode and two upper and lower guard electrodes.Measuring electrode and guard electrode is motivated to distinguish lead To signal processing unit, lead uses shielded cable, is drawn by center sensor.Sensor passes through the method that is installed on above electrode Orchid is attached with pipeline.
In the present embodiment, in order to guarantee that the relative position between electrode and guard electrode is motivated to fix, when processing, be should ensure that There are the insulation gaps of 1-2mm between excitation electrode and guard electrode.In order to make the field distribution near measuring electrode more Uniformly, it requires duct section locating for excitation measuring electrode without bending tube section in the present embodiment, that is, it is vertical that pipeline section herein is completely secured. By in this present embodiment, tube wall is conductive material, and carry out ground connection operation, it is therefore desirable to prevent short between guard electrode and tube wall Road, therefore it is required that the top edge of upside guard electrode is lower than insertion portion and bend pipe interface point 10-15mm.
After starting excitation, the signal of sensor measurement is transmitted to signal processing unit by coaxial signal lines.Through The processing of front-end amplifier, difference amplifier is crossed, voltage signal is obtainedThis signal is input to effectively Be worth measuring unit, handled through internal circuit, it is final obtain it is directly proportional to the capacitance of the oil-water two-phase flow in tested pipeline defeated Voltage effective value out
Obtain the capacitance C of oil-water two-phase flowxAfterwards, the present embodiment derives electricity using Maxwell-Garnett formula Specific respective function relationship between capacitance and moisture content, can finally obtain corresponding water cut value.Derivation process is as follows:
(1) from the foregoing it will be appreciated that driving voltage is vi(t), mixed phase capacitor is Cx, the measurement voltage after processing of circuit has Valid value is
(2) Maxwell-Garnett formula is used
It is derived from:
Wherein, CWFor water phase capacitor, CoilFor oily phase capacitor, CxFor the moisture content of oil-water two-phase flow;
(3) it can be derived by the proportional relation in (1) between measurement voltage and capacitor:
(4) thus formula can calculate the moisture content α of oil-water two-phase flowW
The principle of the invention and structure are simple, are easily installed, have a wide range of application, suitable for containing for low aqueous oil-water two-phase flow The measurement of water rate.

Claims (1)

1. a kind of moisture percentage measuring apparatus based on plug-in capacitance sensor, for using oil as the low aqueous water two of continuous phase Measurement of water ratio in phase flow tube road, including capacitance sensor, signal processing unit, effective value measurement unit and computing unit. It is characterized in that,
Capacitance sensor is fixed at the union elbow of vertical duct and horizontal pipeline, is inserted from up to down along vertical pipeline direction Enter, capacitance sensor includes simultaneously as the excitation measuring electrode of excitation electrode and measuring electrode and the side of being fixed thereon and lower section Two guard electrodes;
Signal processing unit includes front-end amplifier, coaxial cable, AC signal generator and difference amplifier, front-end amplifier Negative input end be connected by coaxial signal lines with the excitation measuring electrode in capacitance sensor, front-end amplifier is just Input terminal is connected with AC signal generator, while the screen of two be connected in capacitance sensor guard electrode, coaxial cable Cover the negative input end of layer and difference amplifier;One measuring resistance RfWith capacitor CfThe negative of front-end amplifier is connected to after parallel connection Input terminal and output end;The output end of front-end amplifier is connected to the positive input terminal of difference amplifier;
The exchange of difference amplifier output sine voltage signal is converted voltage effective value by effective value measurement unit, obtain with The directly proportional output voltage of the capacitance of oil-water two-phase flow in tested pipeline;
Computing unit, according to the acquisition output voltage directly proportional to the capacitance of the oil-water two-phase flow in tested pipeline, use The functional relationship model of oil-water two-phase flow capacitance and moisture content calculates moisture content.
CN201810923285.4A 2018-08-14 2018-08-14 Moisture content measuring device based on plug-in capacitive sensor Expired - Fee Related CN108828029B (en)

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