CN108827951B - 一种尿碘定量检测试剂盒 - Google Patents
一种尿碘定量检测试剂盒 Download PDFInfo
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- CN108827951B CN108827951B CN201810683378.4A CN201810683378A CN108827951B CN 108827951 B CN108827951 B CN 108827951B CN 201810683378 A CN201810683378 A CN 201810683378A CN 108827951 B CN108827951 B CN 108827951B
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- reagent
- iodine
- urine iodine
- urine
- detection
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- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 title claims abstract description 106
- 239000011630 iodine Substances 0.000 title claims abstract description 106
- 229910052740 iodine Inorganic materials 0.000 title claims abstract description 106
- 210000002700 urine Anatomy 0.000 title claims abstract description 85
- 238000001514 detection method Methods 0.000 title claims abstract description 37
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 66
- 239000003054 catalyst Substances 0.000 claims abstract description 14
- 239000003755 preservative agent Substances 0.000 claims abstract description 10
- 230000002335 preservative effect Effects 0.000 claims abstract description 7
- PXIPVTKHYLBLMZ-UHFFFAOYSA-N Sodium azide Chemical group [Na+].[N-]=[N+]=[N-] PXIPVTKHYLBLMZ-UHFFFAOYSA-N 0.000 claims description 12
- -1 acyl chloride peroxide Chemical class 0.000 claims description 8
- JLKDVMWYMMLWTI-UHFFFAOYSA-M potassium iodate Chemical compound [K+].[O-]I(=O)=O JLKDVMWYMMLWTI-UHFFFAOYSA-M 0.000 claims description 6
- 239000001230 potassium iodate Substances 0.000 claims description 6
- 229940093930 potassium iodate Drugs 0.000 claims description 6
- 235000006666 potassium iodate Nutrition 0.000 claims description 6
- 238000012360 testing method Methods 0.000 claims description 5
- 239000005708 Sodium hypochlorite Substances 0.000 claims description 3
- KBTJYNAFUYTSNN-UHFFFAOYSA-N [Na].OO Chemical compound [Na].OO KBTJYNAFUYTSNN-UHFFFAOYSA-N 0.000 claims description 3
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical group [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 3
- RTKIYNMVFMVABJ-UHFFFAOYSA-L thimerosal Chemical compound [Na+].CC[Hg]SC1=CC=CC=C1C([O-])=O RTKIYNMVFMVABJ-UHFFFAOYSA-L 0.000 claims description 3
- 229940033663 thimerosal Drugs 0.000 claims description 3
- 230000002485 urinary effect Effects 0.000 abstract description 6
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 abstract description 5
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 abstract description 4
- 229910001870 ammonium persulfate Inorganic materials 0.000 abstract description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- HJTAZXHBEBIQQX-UHFFFAOYSA-N 1,5-bis(chloromethyl)naphthalene Chemical compound C1=CC=C2C(CCl)=CC=CC2=C1CCl HJTAZXHBEBIQQX-UHFFFAOYSA-N 0.000 abstract 1
- GOLCXWYRSKYTSP-UHFFFAOYSA-N arsenic trioxide Inorganic materials O1[As]2O[As]1O2 GOLCXWYRSKYTSP-UHFFFAOYSA-N 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 description 5
- 229910052684 Cerium Inorganic materials 0.000 description 4
- 210000001685 thyroid gland Anatomy 0.000 description 4
- TUFLVBXBZSNFCZ-UHFFFAOYSA-N arsenic cerium Chemical compound [As].[Ce] TUFLVBXBZSNFCZ-UHFFFAOYSA-N 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 230000035935 pregnancy Effects 0.000 description 3
- 239000013589 supplement Substances 0.000 description 3
- VAZSKTXWXKYQJF-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)OOS([O-])=O VAZSKTXWXKYQJF-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 238000002798 spectrophotometry method Methods 0.000 description 2
- 238000010561 standard procedure Methods 0.000 description 2
- 230000009469 supplementation Effects 0.000 description 2
- 238000012795 verification Methods 0.000 description 2
- 206010067997 Iodine deficiency Diseases 0.000 description 1
- 108010028554 LDL Cholesterol Proteins 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000010219 correlation analysis Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 210000003754 fetus Anatomy 0.000 description 1
- 235000006479 iodine deficiency Nutrition 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 210000001161 mammalian embryo Anatomy 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 208000021510 thyroid gland disease Diseases 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
- G01N21/78—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
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- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Pathology (AREA)
- General Health & Medical Sciences (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Immunology (AREA)
- General Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
Description
样本号 | 测定结果 |
1 | 165 |
2 | 167 |
3 | 159 |
4 | 153 |
5 | 152 |
6 | 154 |
7 | 152 |
8 | 154 |
9 | 159 |
10 | 161 |
11 | 153 |
12 | 154 |
13 | 155 |
14 | 153 |
15 | 157 |
16 | 158 |
17 | 155 |
18 | 154 |
19 | 153 |
20 | 151 |
均值 | 155.95 |
CV | 2.7% |
Claims (4)
Priority Applications (1)
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CN201810683378.4A CN108827951B (zh) | 2018-06-28 | 2018-06-28 | 一种尿碘定量检测试剂盒 |
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CN201810683378.4A CN108827951B (zh) | 2018-06-28 | 2018-06-28 | 一种尿碘定量检测试剂盒 |
Publications (2)
Publication Number | Publication Date |
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CN108827951A CN108827951A (zh) | 2018-11-16 |
CN108827951B true CN108827951B (zh) | 2020-08-25 |
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CN201810683378.4A Active CN108827951B (zh) | 2018-06-28 | 2018-06-28 | 一种尿碘定量检测试剂盒 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6192600A (ja) * | 1984-10-11 | 1986-05-10 | Shinotesuto Kenkyusho:Kk | α−グルコシダ−ゼ活性測定方法 |
CN102495203A (zh) * | 2011-11-10 | 2012-06-13 | 武汉众生生化技术有限公司 | 用于生化分析仪定量检测尿碘的试剂及尿碘检测方法 |
CN102507542A (zh) * | 2011-10-09 | 2012-06-20 | 温州医学院 | 一种快速定量测定尿碘的方法 |
CN105004719A (zh) * | 2015-07-21 | 2015-10-28 | 杨先锋 | 一种尿碘测定试剂盒及其应用 |
CN107677805A (zh) * | 2017-09-30 | 2018-02-09 | 安徽伊普诺康生物技术股份有限公司 | 一种测定尿碘的试剂盒及其制备使用方法 |
-
2018
- 2018-06-28 CN CN201810683378.4A patent/CN108827951B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6192600A (ja) * | 1984-10-11 | 1986-05-10 | Shinotesuto Kenkyusho:Kk | α−グルコシダ−ゼ活性測定方法 |
CN102507542A (zh) * | 2011-10-09 | 2012-06-20 | 温州医学院 | 一种快速定量测定尿碘的方法 |
CN102495203A (zh) * | 2011-11-10 | 2012-06-13 | 武汉众生生化技术有限公司 | 用于生化分析仪定量检测尿碘的试剂及尿碘检测方法 |
CN105004719A (zh) * | 2015-07-21 | 2015-10-28 | 杨先锋 | 一种尿碘测定试剂盒及其应用 |
CN107677805A (zh) * | 2017-09-30 | 2018-02-09 | 安徽伊普诺康生物技术股份有限公司 | 一种测定尿碘的试剂盒及其制备使用方法 |
Non-Patent Citations (4)
Title |
---|
Review of analytical methods for the quantification of iodine in complex matrices;C. Phillip Shelor 等;《Analytica Chimica Acta》;20110623;第702卷;第16-36页 * |
Urinary iodine concentration and thyroid volume of pregnant women attending antenatal care in two selected hospitals in Ashanti Region, Ghana: a comparative cross-sectional study;Daniel Gyamfi 等;《BMC Pregnancy and Childbirth》;20180515;第18卷(第166期);第1-9页 * |
农业地质样品中碘的分析方法;吴俊 等;《安徽农业科学》;20171231;第45卷(第20期);第20-26页 * |
快速定量检测试剂盒测定尿碘的方法验证;万琛 等;《中国卫生检验杂志》;20090930;第19卷(第9期);第2002-2003页 * |
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CN108827951A (zh) | 2018-11-16 |
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GR01 | Patent grant | ||
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: Urine iodine quantitative detection kit Effective date of registration: 20220324 Granted publication date: 20200825 Pledgee: Bank of China Limited Tianjin Hedong sub branch Pledgor: TIANJIN ZHONGCHENG JIAYI BIOTECHNOLOGY Co.,Ltd. Registration number: Y2022980003197 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230327 Granted publication date: 20200825 Pledgee: Bank of China Limited Tianjin Hedong sub branch Pledgor: TIANJIN ZHONGCHENG JIAYI BIOTECHNOLOGY Co.,Ltd. Registration number: Y2022980003197 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Urine Iodine Quantitative Detection Kit Effective date of registration: 20230330 Granted publication date: 20200825 Pledgee: Bank of China Limited Tianjin Hedong sub branch Pledgor: TIANJIN ZHONGCHENG JIAYI BIOTECHNOLOGY Co.,Ltd. Registration number: Y2023980037001 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20200825 Pledgee: Bank of China Limited Tianjin Hedong sub branch Pledgor: TIANJIN ZHONGCHENG JIAYI BIOTECHNOLOGY Co.,Ltd. Registration number: Y2023980037001 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |