CN108823675A - A kind of antibacterial ventilative wig fiber - Google Patents
A kind of antibacterial ventilative wig fiber Download PDFInfo
- Publication number
- CN108823675A CN108823675A CN201810809410.9A CN201810809410A CN108823675A CN 108823675 A CN108823675 A CN 108823675A CN 201810809410 A CN201810809410 A CN 201810809410A CN 108823675 A CN108823675 A CN 108823675A
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- CN
- China
- Prior art keywords
- wig
- polyurethane resin
- wig fiber
- antibacterial
- chitosan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
- A41G3/00—Wigs
- A41G3/0083—Filaments for making wigs
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/94—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of other polycondensation products
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Artificial Filaments (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention mainly relates to staple fibre processing technique fields, disclose a kind of antibacterial ventilative wig fiber, are prepared from the following raw materials：Modified polyurethane resin 41 ~ 43, chitosan 12 ~ 14, polyacrylonitrile-based carbon 6 ~ 8；Antibacterial ventilative wig fiber provided by the invention, preparation is simple, obtained wig is a softer and smoother touch, to really send out similar, wear wig after can avoid summer high temperature generate feeling of oppression and heat, keep consumer it is happy, the bacteriostasis rate of wig reaches 83.7%, the growth that bacterium can obviously be inhibited avoids the symptom of consumer's scalp itch, wash number of the less consumer to wig；The modified polyurethane resin of addition is modified by addition nano-titanium dioxide and linolenic acid in polyurethane resin, and environment protection health improves the intensity and flexibility of polyurethane resin, similar to the feel really sent out.
Description
Technical field
The invention mainly relates to staple fibre processing technique fields, more particularly to a kind of antibacterial ventilative wig fiber.
Background technique
Wig can play preferable decoration function, can convert different hair styles at any time, and can be avoided and often scald
Dye is damaged to caused by true hair, while can save a large amount of time and expense；Wig is all that true hair is made after treatment mostly
It is standby to form, but true hair purchase is difficult at present, and purchasing price is high, to limit the production of wig, therefore gradually uses
Staple fibre replaces really sending out, but easily sultry perspiration after the poor summer wearing of the gas permeability of most of staple fibre wig, into
And lead to the growth of bacterium, make scalp itch unbearably.
Existing 106245156 A of patent document CN discloses a kind of flame-proof antibiotic emulation wig silk, and hair is by a variety of trees
Rouge ingredient and additive are prepared, and have preferable anti-flammability and antibiotic property, but the hair that main component is resin is breathed freely
Property very poor, easily generation feeling of oppression and heat, so that consumer is generated uncomfortable feeling, limit using and selling for summer wig.
Summary of the invention
In order to make up the defect of prior art, the object of the present invention is to provide a kind of antibacterial ventilative wig fibers.
A kind of antibacterial ventilative wig fiber, is made of raw material from the following weight：Modified polyurethane resin 41 ~ 43, shell are poly-
Sugared 12 ~ 14, polyacrylonitrile-based carbon 6 ~ 8.
The modified polyurethane resin, polyurethane resin is placed in container, and the speed with 0.8 ~ 1.4 DEG C/min adds
Heat is added the nano-titanium dioxide of polyurethane resin weight 0.11 ~ 0.13%, keeps the temperature 2 ~ 3 hours, stir to complete to abundant melting
Full mixing, adds the linolenic acid of polyurethane resin weight 1.2 ~ 1.4%, insulated and stirred 30 ~ 50 minutes, natural cooling obtained modification
Polyurethane resin.
A kind of preparation method of antibacterial ventilative wig fiber, includes the following steps：
（1）Chitosan is added in the acetum that volume fraction is 1 ~ 2%, tranxamic acid is added to being uniformly mixed in stirring, mixes
It closes uniformly, is gradually heated to 80 ~ 90 DEG C, keep the temperature 2 ~ 3 hours, freeze-drying to water content is 3 ~ 7%, obtains modification of chitosan；
（2）Modified polyurethane resin, modification of chitosan and polyacrylonitrile-based carbon are mixed, sufficiently melted, is uniformly mixed, obtains
Spinning material；
（3）By spinning material through melting extrusion in spinning machine, temperature is 210 ~ 220 DEG C, is cooled to 160 ~ 170 DEG C and carries out shaping,
Washing, obtains wig fiber；
（4）It is dry：Wig fiber is placed in 30 ~ 40 DEG C of baking oven and is dried, obtains antibacterial ventilative wig fiber.
The step（1）Tranxamic acid, additive amount be chitosan weight 0.04 ~ 0.06%.
The step（3）Washing, first with concentration be 20 ~ 25mg/L vitamin c solution washed, in 4 ~ 8 DEG C soak
Bubble 20 ~ 30 minutes, then washed with clear water.
The application method of the antibacterial ventilative wig fiber, antibacterial ventilative wig fiber is fixed on wig base, root
According to being dyed, dyeing is placed on 50 ~ 60 DEG C of heating fixation 30 ~ 40 minutes, and cleaning in 2 ~ 3 months is primary after wearing.
It is an advantage of the invention that：Antibacterial ventilative wig fiber provided by the invention, preparation is simple, and obtained wig softness is suitable
It is sliding, and really send out similar, can avoid the feeling of oppression and heat that summer high temperature generates after wearing wig, keep consumer happy, wig
Bacteriostasis rate reaches 83.7%, can obviously inhibit the growth of bacterium, avoids the symptom of consumer's scalp itch, less consumer couple
The wash number of wig；The modified polyurethane resin of addition is carried out by nano-titanium dioxide and linolenic acid are added in polyurethane resin
Modified, environment protection health improves the intensity and flexibility of polyurethane resin, similar to the feel really sent out；Chitosan is changed
Tranxamic acid is added during property, the antibiotic property and fibre strength of chitosan can be significantly improved, increase the mechanicalness of wig
Can, avoid wig from occurring being broken and deform during being familiar with and arranging；By modified polyurethane resin, modification of chitosan and gather
Acrylonitrile group carbon is mixed, and polyacrylonitrile-based carbon can increase the intensity and microcellular structure of wig, scalp can be promoted to generate
Heat and sweat be quickly discharged, avoid generating feeling of oppression and heat, while microcellular structure can also adsorb bacterium and spot, bacterium inhibited to grow
It is raw, and clean and dry the microcellular structure of rear wig and can restore, the wash number of wig is reduced, wig comfort level is improved；It is molten
Wig is first washed through vitamin c solution after melting sizing, the stability of deformation chitosan can be enhanced, improves wig fiber
Intensity and durability, then washed with clear water, increase the flexibility of wig fiber；After wearing can according to hobby to wig into
Row dyeing, and without often being cleaned to wig, save a large amount of time and efforts of wearer.
Specific embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of antibacterial ventilative wig fiber, is made of raw material from the following weight：Modified polyurethane resin 41, gathers chitosan 12
Acrylonitrile group carbon 6.
The modified polyurethane resin, polyurethane resin is placed in container, is heated to 0.8 DEG C/min of speed
The nano-titanium dioxide of polyurethane resin weight 0.11% is added in sufficiently melting, keeps the temperature 2 hours, stirring to being thoroughly mixed, then plus
Enter the linolenic acid of polyurethane resin weight 1.2%, insulated and stirred 30 minutes, natural cooling obtained modified polyurethane resin.
A kind of preparation method of antibacterial ventilative wig fiber, includes the following steps：
（1）Chitosan is added in the acetum that volume fraction is 1%, tranxamic acid, mixing is added to being uniformly mixed in stirring
Uniformly, 80 ~ 90 DEG C are gradually heated to, keeps the temperature 2 ~ 3 hours, freeze-drying to water content is 3 ~ 7%, obtains modification of chitosan；The step
Suddenly（1）Tranxamic acid, additive amount be chitosan weight 0.04%；
（2）Modified polyurethane resin, modification of chitosan and polyacrylonitrile-based carbon are mixed, sufficiently melted, is uniformly mixed, obtains
Spinning material；
（3）By spinning material through melting extrusion in spinning machine, temperature is 210 ~ 220 DEG C, is cooled to 160 ~ 170 DEG C and carries out shaping,
Washing, obtains wig fiber；The step（3）Washing, first washed with the vitamin c solution that concentration is 20mg/L, in 4 DEG C
It impregnates 20 minutes, then is washed with clear water；
（4）It is dry：Wig fiber is placed in 30 DEG C of baking oven and is dried, obtains antibacterial ventilative wig fiber.
The application method of the antibacterial ventilative wig fiber, antibacterial ventilative wig fiber is fixed on wig base, root
According to being dyed, dyeing is placed on 50 ~ 60 DEG C of heating fixation 30 ~ 40 minutes, and cleaning in 2 ~ 3 months is primary after wearing.
Embodiment 2
A kind of antibacterial ventilative wig fiber, is made of raw material from the following weight：Modified polyurethane resin 42, gathers chitosan 13
Acrylonitrile group carbon 7.
The modified polyurethane resin, polyurethane resin is placed in container, is heated to 1.1 DEG C/min of speed
The nano-titanium dioxide of polyurethane resin weight 0.12% is added in sufficiently melting, keeps the temperature 2.5 hours, stirring to being thoroughly mixed, then
The linolenic acid of polyurethane resin weight 1.3% is added, insulated and stirred 40 minutes, natural cooling obtained modified polyurethane resin.
A kind of preparation method of antibacterial ventilative wig fiber, includes the following steps：
（1）Chitosan is added in the acetum that volume fraction is 1.5%, tranxamic acid is added to being uniformly mixed in stirring, mixes
It closes uniformly, is gradually heated to 80 ~ 90 DEG C, keep the temperature 2 ~ 3 hours, freeze-drying to water content is 3 ~ 7%, obtains modification of chitosan；It is described
Step（1）Tranxamic acid, additive amount be chitosan weight 0.05%；
（2）Modified polyurethane resin, modification of chitosan and polyacrylonitrile-based carbon are mixed, sufficiently melted, is uniformly mixed, obtains
Spinning material；
（3）By spinning material through melting extrusion in spinning machine, temperature is 210 ~ 220 DEG C, is cooled to 160 ~ 170 DEG C and carries out shaping,
Washing, obtains wig fiber；The step（3）Washing, first washed with the vitamin c solution that concentration is 23mg/L, in 6 DEG C
It impregnates 25 minutes, then is washed with clear water；
（4）It is dry：Wig fiber is placed in 35 DEG C of baking oven and is dried, obtains antibacterial ventilative wig fiber.
The application method of the antibacterial ventilative wig fiber, antibacterial ventilative wig fiber is fixed on wig base, root
According to being dyed, dyeing is placed on 50 ~ 60 DEG C of heating fixation 30 ~ 40 minutes, and cleaning in 2 ~ 3 months is primary after wearing.
Embodiment 3
A kind of antibacterial ventilative wig fiber, is made of raw material from the following weight：Modified polyurethane resin 43, gathers chitosan 14
Acrylonitrile group carbon 8.
The modified polyurethane resin, polyurethane resin is placed in container, is heated to 1.4 DEG C/min of speed
The nano-titanium dioxide of polyurethane resin weight 0.13% is added in sufficiently melting, keeps the temperature 3 hours, stirring to being thoroughly mixed, then plus
Enter the linolenic acid of polyurethane resin weight 1.4%, insulated and stirred 50 minutes, natural cooling obtained modified polyurethane resin.
A kind of preparation method of antibacterial ventilative wig fiber, includes the following steps：
（1）Chitosan is added in the acetum that volume fraction is 2%, tranxamic acid, mixing is added to being uniformly mixed in stirring
Uniformly, 80 ~ 90 DEG C are gradually heated to, keeps the temperature 2 ~ 3 hours, freeze-drying to water content is 3 ~ 7%, obtains modification of chitosan；The step
Suddenly（1）Tranxamic acid, additive amount be chitosan weight 0.06%；
（2）Modified polyurethane resin, modification of chitosan and polyacrylonitrile-based carbon are mixed, sufficiently melted, is uniformly mixed, obtains
Spinning material；
（3）By spinning material through melting extrusion in spinning machine, temperature is 210 ~ 220 DEG C, is cooled to 160 ~ 170 DEG C and carries out shaping,
Washing, obtains wig fiber；The step（3）Washing, first washed with the vitamin c solution that concentration is 25mg/L, in 8 DEG C
It impregnates 30 minutes, then is washed with clear water；
（4）It is dry：Wig fiber is placed in 40 DEG C of baking oven and is dried, obtains antibacterial ventilative wig fiber.
The application method of the antibacterial ventilative wig fiber, antibacterial ventilative wig fiber is fixed on wig base, root
According to being dyed, dyeing is placed on 50 ~ 60 DEG C of heating fixation 30 ~ 40 minutes, and cleaning in 2 ~ 3 months is primary after wearing.
Comparative example 1
Remove modified polyurethane resin, remaining preparation and application, with embodiment 1.
Comparative example 2
Remove chitosan, remaining preparation and application, with embodiment 1.
Comparative example 3
Remove polyacrylonitrile-based carbon, remaining preparation and application, with embodiment 1.
Comparative example 4
Remove step（1）In chitin modified, remaining preparation and application, with embodiment 1.
Comparative example 5
Remove step（3）In vitamin c solution, remaining preparation and application, with embodiment 1.
Comparative example 6
106245156 A of patent document CN discloses a kind of flame-proof antibiotic emulation wig silk.
The mechanical property of embodiment and comparative example wig fiber：
Example and the wig fiber of comparative example are appropriate respectively, according to " fibre strength detection technique and instrument, Zhu Genfeng etc. "
Method, use the dry strong of YG029-I full automatic single yarn tester detection wig fiber（CN/dtex）, it is wet strong（CN/dtex）And
It is dry to stretch（%）, and Escherichia coli are inoculated on each group wig fiber, and after culture 24 hours, the bacteriostasis rate of detection wig fiber, every group
Detection 3 times is repeated, results are averaged, and the mechanical property of embodiment and comparative example wig fiber is shown in Table 1.
Table 1：The mechanical property of embodiment and comparative example wig fiber
From table 1 the result shows that, the antibacterial ventilative wig fiber of embodiment is done strong, wet strong and dry mechanical property of stretching and is substantially better than
Comparative example illustrates that antibacterial ventilative wig fiber provided by the invention has good mechanical property and service performance, and intensity is suitable,
Distortion caused by avoiding intensity excessively high, it is higher with the similarity really sent out.
The dyeability of embodiment and comparative example wig fiber：
Example and the wig fiber 0.5g of comparative example are placed in 100g reactive dyeing bath foam respectively, are heated to 50 DEG C, protect
Temperature 30 minutes observes the colouring situation of each group wig fiber, as a result：
Embodiment 1, embodiment 2, embodiment 3 and 1 coloring effect of comparative example are best, upper color depth；
Comparative example 4, comparative example 5, comparative example 6, dyeing effect are taken second place, and are painted slightly shallow；
The dyeing effect of comparative example 2 and comparative example 3 is worst, paints most shallow.
Claims (6)
1. a kind of antibacterial ventilative wig fiber, which is characterized in that be made of raw material from the following weight：Modified polyurethane resin 41
~ 43, chitosan 12 ~ 14, polyacrylonitrile-based carbon 6 ~ 8.
2. antibacterial ventilative wig fiber according to claim 1, which is characterized in that the modified polyurethane resin will gather
Urethane resin is placed in container, is heated to sufficiently melting with 0.8 ~ 1.4 DEG C/min of speed, and polyurethane resin weight is added
0.11 ~ 0.13% nano-titanium dioxide, keep the temperature 2 ~ 3 hours, stir to being thoroughly mixed, add polyurethane resin weight 1.2 ~
1.4% linolenic acid, insulated and stirred 30 ~ 50 minutes, natural cooling obtained modified polyurethane resin.
3. a kind of preparation method of ventilative wig fiber antibacterial according to claim 1, which is characterized in that including following step
Suddenly：
（1）Chitosan is added in the acetum that volume fraction is 1 ~ 2%, tranxamic acid is added to being uniformly mixed in stirring, mixes
It closes uniformly, is gradually heated to 80 ~ 90 DEG C, keep the temperature 2 ~ 3 hours, freeze-drying to water content is 3 ~ 7%, obtains modification of chitosan；
（2）Modified polyurethane resin, modification of chitosan and polyacrylonitrile-based carbon are mixed, sufficiently melted, is uniformly mixed, obtains
Spinning material；
（3）By spinning material through melting extrusion in spinning machine, temperature is 210 ~ 220 DEG C, is cooled to 160 ~ 170 DEG C and carries out shaping,
Washing, obtains wig fiber；
（4）It is dry：Wig fiber is placed in 30 ~ 40 DEG C of baking oven and is dried, obtains antibacterial ventilative wig fiber.
4. the preparation method of antibacterial ventilative wig fiber according to claim 3, which is characterized in that the step（1）Only
Hemal ring acid, additive amount are the 0.04 ~ 0.06% of chitosan weight.
5. the preparation method of antibacterial ventilative wig fiber according to claim 3, which is characterized in that the step（3）Wash
It washs, is first washed, impregnated 20 ~ 30 minutes in 4 ~ 8 DEG C, then carried out with clear water with the vitamin c solution that concentration is 20 ~ 25mg/L
Washing.
6. a kind of application method of any one of claim 1 ~ 5 antibacterial ventilative wig fiber, which is characterized in that will be antibacterial
Gas wig fiber is fixed on wig base, is dyed as needed, and dyeing is placed on 30 ~ 40 points of fixation of 50 ~ 60 DEG C of heating
Clock, cleaning in 2 ~ 3 months is primary after wearing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810809410.9A CN108823675A (en) | 2018-07-23 | 2018-07-23 | A kind of antibacterial ventilative wig fiber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810809410.9A CN108823675A (en) | 2018-07-23 | 2018-07-23 | A kind of antibacterial ventilative wig fiber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108823675A true CN108823675A (en) | 2018-11-16 |
Family
ID=64141325
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810809410.9A Withdrawn CN108823675A (en) | 2018-07-23 | 2018-07-23 | A kind of antibacterial ventilative wig fiber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108823675A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109518302A (en) * | 2018-11-26 | 2019-03-26 | 合肥卓汇新材料科技有限公司 | A kind of automatically cleaning wig fiber |
-
2018
- 2018-07-23 CN CN201810809410.9A patent/CN108823675A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109518302A (en) * | 2018-11-26 | 2019-03-26 | 合肥卓汇新材料科技有限公司 | A kind of automatically cleaning wig fiber |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181116 |