CN108822904A - A kind of Microbial fuel synergy cleaning solution compound additive formula and preparation method - Google Patents
A kind of Microbial fuel synergy cleaning solution compound additive formula and preparation method Download PDFInfo
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- CN108822904A CN108822904A CN201810575456.9A CN201810575456A CN108822904A CN 108822904 A CN108822904 A CN 108822904A CN 201810575456 A CN201810575456 A CN 201810575456A CN 108822904 A CN108822904 A CN 108822904A
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- microbial fuel
- compound additive
- cleaning solution
- additive
- dimethyl carbonate
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L10/00—Use of additives to fuels or fires for particular purposes
- C10L10/04—Use of additives to fuels or fires for particular purposes for minimising corrosion or incrustation
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L10/00—Use of additives to fuels or fires for particular purposes
- C10L10/08—Use of additives to fuels or fires for particular purposes for improving lubricity; for reducing wear
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
- C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
- C10L1/1824—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms mono-hydroxy
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
- C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
- C10L1/1826—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms poly-hydroxy
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/188—Carboxylic acids; metal salts thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/22—Organic compounds containing nitrogen
- C10L1/222—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
- C10L1/223—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond having at least one amino group bound to an aromatic carbon atom
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Liquid Carbonaceous Fuels (AREA)
Abstract
The invention discloses a kind of Microbial fuel synergy cleaning solution compound additive formulas, mix by following weight proportion：Dimethyl carbonate 40~80, ethyl alcohol 10~40, butanol 10~40, glycerol 5~30, Methanol/Vegetable Oil acid soap 2~20, stearate 0.5~5, BTA 0.1~3, TTA 0.1~3, T501 0.1~3, T502A 0.1~3, M 0.1~3, octylated diphenylamine 0.5~5.The a variety of materials are heated and be sufficiently stirred, the compounded compound additive of pale yellow transparent is obtained after filtering.The compound additive that the present invention makes, appearance is faint yellow, limpid bright, and smell is small, modest viscosity, has certain lubricity, comprehensive anticorrosive corrosion inhibiter is good, and stationary phase is long, good security.
Description
Technical field
The invention discloses a kind of Microbial fuel synergy cleaning solution compound additive formula and preparation methods.Micro- life
Object fuel synergistic cleaning solution Microbial fuel and polyoxy combustion adjuvant, detersive, multifunctional and composite type additive press certain weight
Amount ratio, a kind of vehicle environmental protection articles made of formulated, dedicated for the purification of gasoline locomotive emission.It is multi-functional compound
Type additive integrates the functions such as lubrication, inhibition, microemulsified, is the important component of synergy cleaning solution.
Background technique
Existing treating vehicle exhaust can be summarized as emission controls by improving combustion and external purification two major classes.But automobile exhaust pollution is controlled
Reason is a great system engineering, it is necessary to along with combustion on the emission controls by improving combustion and external purification of existing treating vehicle exhaust
Material purifies this link.So-called fuel detergenting, it not instead of simply modify to fuel oil and using clean fuel, use
New theory and technology, is transformed fuel oil, under the premise of not needing to change new vehicle, in existing vehicle operation
Significantly reduce the discharge amount of pollutant in tail gas.
As the addition composition of fuel oil, there are a whole set of product technology standard and analysis method, and these are to fire
Based on the technical indicator of oil product.For guarantee fuel oil within the engine can normal combustion, while parts can not be generated
Corrosion, this principle be us carry out Microbial fuel synergy cleaning solution compound additive must comply with and
Pay attention to.
(1) flash-point:The height of close flash point to this product or calls in the safety of scavenging solution and quality and can all have an impact.
(2) mechanical admixture:Guarantee this product is being formulated into scavenging solution, does not have an impact the index of product quality.
The lower mechanical admixture the better.
(3) pH value:Because that can not be detected to the element of some raw materials, then by means of the important parameter of some starting monomers
The variation of pH value carrys out the inherent quality of indirect reactor product.
(4) moisture:Raw material selected by additive is all organic matter, should be free from moisture.Moisture is smaller, illustrates institute
The raw material quality of selection is better.Moisture is high, may is that production control process is problematic, influences the appearance and storage life of product.
(5) lubricity:Contain a large amount of solvent in compound additive and cleaning solution, it is necessary to there is compound additive certain
Lubricity, to prevent the abrasion of conveyer tool.
(6) comprehensive corrosion inhibition:The important indicator of additive, must item ensure, to guarantee the product quality of scavenging solution.
Microbial fuel refers in particular to the organic sewage for high concentration, by obtained after special biochemical treatment it is a kind of environmental protection,
Clean green energy resource.With the surge and sustained economic development of big city population, trade effluent and sanitary sewage is caused to discharge
Amount increasingly increases, these organic sewages have the feature of high toxicity, high pollution, high organic matter.And it is complex in composition, amount it is huge.
The Microbial fuel obtained after special biochemical treatment can be used as a kind of good alcohol fuel, because of the organic sewage of high concentration
Measure huge, obtained this good Microbial fuel fuel is also a kind of very important alternative energy source.Develop this substitution
The energy is the Major Strategic behave for ensureing national energy security, mitigating petroleum import pressure, alleviating resource and environmental constraints.
The development of this environment-protecting clean Microbial fuel synergy cleaning solution and additive, first is that in order to solve the problems, such as resource scarcity；Two
It is the pollution in order to mitigate automotive emission to atmosphere；Third is that being to be obtained after utilizing biochemical treatment organic sewage on a large scale
High-quality alcohol fuel seek optimal outlet.
Summary of the invention
The object of the present invention is to propose a kind of Microbial fuel synergy cleaning solution additive formulations and preparation method.Micro- life
Object fuel synergistic cleaning solution is pressed centainly to be a kind of with Microbial fuel and polyoxy combustion adjuvant, detersive, Mobyneb additive
Weight ratio, a kind of vehicle environmental protection fuel articles made of formulated, dedicated for the purification of gasoline locomotive emission.
Technical solution of the present invention：For the compound additive of Microbial fuel synergy cleaning solution, formula is：Carbonic acid two
Methyl esters 40~80, ethyl alcohol 10~40, butanol 10~40, glycerol 5~30, Methanol/Vegetable Oil acid soap 2~20, stearate 0.5~
5, BTA0.1~3, TTA0.1~3, T5010.1~3, T502A0.1~3, M0.1~3, octylated diphenylamine 0.5~5.By institute
It is heated and be sufficiently stirred to state a variety of materials, obtains the compounded compound additive of pale yellow transparent after filtering.
Multi-functional (compound) 5~10 parts of additive additive amount of the compounded additions for Microbial fuel synergy cleaning solution,
It selects a variety of oxidizing combustibles and is aided with multi-functional composite additive and be formulated for primary raw material；The raw material weight proportioning of soup processed：It is micro-
Bio-fuel 50~85, dimethoxymethane 10~30, dimethyl carbonate 10~30.Normal use accounts for fuel oil (gasoline or bavin
Oil, especially gasoline) weight ratio 20%, can be dissolved each other with national standard oil with arbitrary proportion, it is not stratified, non-discolouring.
The compound additive that the present invention makes, appearance is faint yellow, limpid bright, and smell is small, modest viscosity, there is certain lubrication
Property, comprehensive anticorrosive corrosion inhibiter is good, and stationary phase is long, good security.
For Microbial fuel synergy, cleaning solution additive applicant is mainly studied in following several respects：
(1) several inherent quality standards of Microbial fuel synergy cleaning solution additive, mainly by several primary raw materials
It deploys.Such as comprehensive corrosion inhibition, pH value, flash-point (silent).
(2) to the research of additive.Certain performances of solution additive are cleaned in Microbial fuel synergy, are that can pass through addition
Several functions additive and improved.What is more concentrated is stability, comprehensive corrosion inhibition of additive etc..
(3) several external quality standards of Microbial fuel synergy cleaning solution additive, are that can lead to if mechanical admixture
Technology controlling and process is crossed to realize.
(4) to the research in terms of Microbial fuel synergy cleaning solution additive application.
Main technical schemes of the invention：Selecting dimethyl carbonate and being equipped with ethyl alcohol, butanol, glycerine is that primary solvent is former
Material, and be aided with multi-functional composite additive and deploy.In formula, it is rich that dimethyl carbonate, which is used as primary solvent ingredient again,
Oxygen additive；It is lubricant again that glycerine, which is used as solvent composition,；T501 be antioxidant but also as rubber parts it is anti-melt it is swollen
Property etc..Its ratio be：Solvent 50~80, lubricant class 5~30, multifunction additive 2~10.
Optimization formula 1 of the invention, raw material are formulated by the mixing of following weight proportion:Dimethyl carbonate 50, second
Alcohol 30, butanol 10, glycerol 5, Methanol/Vegetable Oil acid soap 4, stearate 0.4, BTA0.1, T5010.1, M0.1, octylatcd hexichol
Amine 0.3.
Optimization formula 2 of the invention, raw material are formulated by the mixing of following weight proportion:Dimethyl carbonate 40, second
Alcohol 25, butanol 25, glycerol 6, Methanol/Vegetable Oil acid soap 3, stearate 0.3, BTA0.1, TTA0.1, T502A0.1, octylatcd two
Aniline 0.4.
Optimization formula 3 of the invention, raw material are formulated by the mixing of following weight proportion:Dimethyl carbonate 60, second
Alcohol 15, butanol 15, glycerol 5, Methanol/Vegetable Oil acid soap 4, stearate 0.3, BTA0.15, T5010.1.5, M0.1, octylatcd two
Aniline 0.3.
In multifunction additive of the invention, other auxiliary agents, including catalyst, corrosion inhibiter can be added, agent etc. is melted in increasing.
Beneficial effect：It is Microbial fuel synergy cleaning solution Microbial fuel and polyoxy combustion adjuvant of the present invention, peace and quiet
Agent, multifunctional and composite type additive by a certain percentage of the weight, a kind of vehicle environmental protection articles made of formulated, dedicated for vapour
The purification of oil machine vehicle emission.Multifunctional and composite type additive integrates the functions such as lubrication, inhibition, microemulsified, is synergy
The important component of cleaning solution.The present invention is a kind of to integrate Conventional solvents, fuel-rich fuel and several functions additive
Environment-friendly microbial fuel synergistic clean solution additive.Its main feature：Appearance is faint yellow, limpid bright, and smell is small, viscosity
It is moderate, there is certain lubricity, comprehensive anticorrosive corrosion inhibiter is good, and stationary phase is long, good security.
Specific embodiment
It is further described below with reference to embodiment invention.
Embodiment selects dimethyl carbonate, and is equipped with ethyl alcohol, butanol, glycerine and is main solvent materials, and is aided with more function
Energy additive is deployed.In formula, it is oxygen-enriched additive that dimethyl carbonate, which is used as primary solvent ingredient again,；Glycerine is
It is lubricant again as solvent composition；T501 is that antioxidant but also as the anti-of rubber parts melts swollen property etc..Various solvents are led to
Weight proportion is crossed, multifunction additive after metering is added under stirring, is obtained after filtering after stirring 120min faint yellow
Solution additive is cleaned in transparent compounded Microbial fuel synergy.Also other auxiliary agents, including catalysis can be added in above-mentioned ingredient
Agent etc. is melted in agent, corrosion inhibiter, increasing.
Embodiment 1, raw material are mixed by following weight (part) proportion and are formulated:Dimethyl carbonate 50, ethyl alcohol 30, fourth
Alcohol 10, glycerol 5, Methanol/Vegetable Oil acid soap 4, stearate 0.4, BTA0.1, T5010.1, M0.1, octylated diphenylamine 0.3.
Embodiment 2, raw material are formulated by the mixing of following weight proportion:Dimethyl carbonate 40, ethyl alcohol 25, butanol
25, glycerol 6, Methanol/Vegetable Oil acid soap 3, stearate 0.3, BTA0.1, TTA0.1, T502A0.1, octylated diphenylamine 0.4.
Embodiment 3, raw material are formulated by the mixing of following weight proportion:Dimethyl carbonate 60, ethyl alcohol 15, butanol
15, glycerol 5, Methanol/Vegetable Oil acid soap 4, stearate 0.3, BTA0.15, T5010.1.5, M0.1, octylated diphenylamine 0.3.
Microbial fuel synergy cleaning solution additive product conventional detection data:
Claims (5)
1. a kind of compound additive for Microbial fuel synergy cleaning solution, which is characterized in that mixed by following weight proportion
It forms：Dimethyl carbonate 40 ~ 80, ethyl alcohol 10 ~ 40, butanol 10 ~ 40, glycerol 5 ~ 30, Methanol/Vegetable Oil acid soap 2 ~ 20, stearate
0.5 ~ 5, BTA0.1 ~ 3, TTA0.1 ~ 3, T5010.1 ~ 3, T502A0.1 ~ 3, M0.1 ~ 3, octylated diphenylamine 0.5 ~ 5.
2. the compound additive of Microbial fuel synergy cleaning solution according to claim 1, which is characterized in that press following weight
Proportion mixes：Dimethyl carbonate 50, ethyl alcohol 30, butanol 10, glycerol 5, Methanol/Vegetable Oil acid soap 4, stearate 0.4,
BTA0.1, T5010.1, M0.1, octylated diphenylamine 0.3.
3. the compound additive of Microbial fuel synergy cleaning solution according to claim 1, which is characterized in that press following weight
Proportion mixes：Dimethyl carbonate 40, ethyl alcohol 25, butanol 25, glycerol 6, Methanol/Vegetable Oil acid soap 3, stearate 0.3,
BTA0.1, TTA0.1, T502A0.1, octylated diphenylamine 0.4.
4. the compound additive of Microbial fuel synergy cleaning solution according to claim 1, which is characterized in that press following weight
Proportion mixes：Dimethyl carbonate 60, ethyl alcohol 15, butanol 15, glycerol 5, Methanol/Vegetable Oil acid soap 4, stearate 0.3,
BTA0.15, T5010.1.5, M0.1, octylated diphenylamine 0.3.
5. the preparation method of the compound additive of one of -4 Microbial fuel synergy cleaning solutions according to claim 1, characterized in that
In dimethyl carbonate by the multi-solvents type auxiliary agent under stirring plus after metering, various functions are added after 30min and help
Agent stops stirring after 60min, obtains the compounded composite multi-functional additive of pale yellow transparent after filtering.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810575456.9A CN108822904A (en) | 2018-06-06 | 2018-06-06 | A kind of Microbial fuel synergy cleaning solution compound additive formula and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810575456.9A CN108822904A (en) | 2018-06-06 | 2018-06-06 | A kind of Microbial fuel synergy cleaning solution compound additive formula and preparation method |
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| Publication Number | Publication Date |
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| CN108822904A true CN108822904A (en) | 2018-11-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201810575456.9A Pending CN108822904A (en) | 2018-06-06 | 2018-06-06 | A kind of Microbial fuel synergy cleaning solution compound additive formula and preparation method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111944569A (en) * | 2020-08-02 | 2020-11-17 | 南京沿江资源生态科学研究院有限公司 | Oxygen-enriched additive for diesel locomotive fuel by using recovered alcohol as raw material and preparation method thereof |
| CN113430021A (en) * | 2021-03-25 | 2021-09-24 | 浙江吉利控股集团有限公司 | Methanol fuel additive and preparation method thereof |
-
2018
- 2018-06-06 CN CN201810575456.9A patent/CN108822904A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111944569A (en) * | 2020-08-02 | 2020-11-17 | 南京沿江资源生态科学研究院有限公司 | Oxygen-enriched additive for diesel locomotive fuel by using recovered alcohol as raw material and preparation method thereof |
| CN113430021A (en) * | 2021-03-25 | 2021-09-24 | 浙江吉利控股集团有限公司 | Methanol fuel additive and preparation method thereof |
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Application publication date: 20181116 |