CN108815025A - The preparation method of U.S. rattan fruit moisturizing emulsion - Google Patents
The preparation method of U.S. rattan fruit moisturizing emulsion Download PDFInfo
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- CN108815025A CN108815025A CN201810949476.8A CN201810949476A CN108815025A CN 108815025 A CN108815025 A CN 108815025A CN 201810949476 A CN201810949476 A CN 201810949476A CN 108815025 A CN108815025 A CN 108815025A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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Abstract
The invention discloses a kind of preparation methods of U.S. rattan fruit moisturizing emulsion, by squeezing U.S. rattan fruit to obtain oil and fat of sacha inchi, resulting pomace will be squeezed again to crush to obtain U.S. rattan fruit powder end, then oil and fat of sacha inchi, isobutyl palmitate and stearic acid are mixed to get the first mixture, U.S. rattan fruit powder end, convergence extracting solution and glycerol are mixed to get the second mixture, then the first mixture, the second mixture, compound emulsifying agent and thickened gel agent are carried out emulsifying homogeneous in high shear homogeneous emulsifying machine and obtain the U.S. rattan fruit moisturizing emulsion.
Description
Technical field
The invention belongs to skin care item preparation technical fields, and in particular to a kind of preparation method of U.S. rattan fruit moisturizing emulsion.
Background technique
Attention with people to skin care, various skin-protection products emerge one after another, and in order to protect skin, not only want moisturizing
Moisturizing will also carry out radiation protection, antiultraviolet etc. nursery work.For oily skin, smegma is more vigorous, is easy
So that facial oiliness, pore are coarse, blackhead is more and influence beauty, and it is easy to appear acne, easily stays color spot, scar.
Oil and fat of sacha inchi is a kind of natural green novel edible vegetable oil rouge, and oil and fat of sacha inchi is rich in the human body with skin affinity
Essential fatty acid is easy to be absorbed by the skin, and effectively keeps skin elasticity and moistens;Contained abundant vitamin E is anti-in oil and fat of sacha inchi
Oxidation material can eliminate facial wrinkles, prevent skin aging;In addition ultraviolet light can be resisted by smearing skin with oil and fat of sacha inchi, be prevented
Cutaneum carcinoma;Also contain unsaturated fatty acid content in oil and fat of sacha inchi, can also be played using the product skin care rich in oil and fat of sacha inchi
The effect of radiation protection.But the U.S. rattan fruit of also few exploitations is used for skin care item at present.
Summary of the invention
Present invention aim to address at least the above defects, and provide the advantages of illustrating later.
In order to realize object of the present invention and other advantages, a kind of preparation side of U.S. rattan fruit moisturizing emulsion is now provided
Method obtains oil and fat of sacha inchi by squeezing U.S. rattan fruit, then will squeeze resulting pomace and crush to obtain U.S. rattan fruit powder end, then will be beautiful
Rattan fruit oil, isobutyl palmitate and stearic acid are mixed to get the first mixture, U.S. rattan fruit powder end, convergence extracting solution and glycerol mixing
The second mixture is obtained, then by the first mixture, the second mixture, compound emulsifying agent and thickened gel agent in high shear homogeneous
Emulsifying homogeneous is carried out in mulser and obtains the U.S. rattan fruit moisturizing emulsion.
In other words, the invention discloses a kind of preparation methods of U.S. rattan fruit moisturizing emulsion, including:
U.S. rattan fruit kernel is obtained Step 1: U.S. rattan fruit is enucleated, then U.S. rattan fruit kernel is crushed, then in 45~55 DEG C of temperature
Squeezing is carried out 50~60 minutes under degree, 40~60MPa pressure, obtains oil and fat of sacha inchi and pomace.
Step 2: pomace by drying or is dried, using crushing, U.S. rattan fruit powder end is obtained.
Step 3: choosing one or both of persimmon extracting liquid or bitter buckwheat tea extract as convergence extracting solution.
Step 4: 150~350 parts of oil and fat of sacha inchi, 20~30 parts of isobutyl palmitate and 20~30 parts of stearic acid are taken respectively,
Stirring obtains the first mixture to dissolving in 60~70 DEG C.
200~500 parts of U.S. rattan fruit powder end, convergence 400~800 parts of extracting solution and 50~100 parts of glycerol are taken respectively, in 60~
Heating water bath in 70 DEG C, and be stirred until homogeneous, the second mixture.
Step 5: first mixture and the second mixture and compound emulsifying agent, thickened gel agent of quality volume such as taking
It is respectively put into high shear homogeneous emulsifying machine and carries out emulsification thickening to get U.S. rattan fruit moisturizing emulsion is arrived.
The compound emulsifying agent includes:Sorbester p17, methyl glucoside sesquialter stearate, two kinds or two in xanthan gum
Kind or more raw material.
The thickened gel agent includes:Carbomer, gelling agent and triethanolamine, the thickened gel agent is by the following method
It is made:
Step a, 3~5 parts of carbomer are weighed, after mixing with 500~1000 parts of distilled water, standing makes its expansion, obtains
To carbomer inflation fluid.
Step b, 3~6 parts of gelling agent are weighed, after being mixed with 300~800 parts of distilled water, the heating water bath in 60~70 DEG C,
And after being stirred until homogeneous, standing makes its expansion, obtains gelling agent inflation fluid.
Step c, by 1~5 part of triethanolamine and resulting carbomer inflation fluid, gelling agent inflation fluid be mixed to get
To the thickened gel agent.
In the emulsification thickening, the mass ratio of first mixture and the second mixture is 1:1~1.5.
Preferably, the step 5 is specially:100 parts of the first mixture, 100 parts of the second mixture, compound is taken respectively
It 35 parts and 6 parts of thickened gel agent of emulsifier, is respectively put into high shear homogeneous emulsifying machine and carries out emulsification thickening to get U.S. rattan fruit is arrived
Moisturizing emulsion.
Preferably, the persimmon extracting liquid is made by the following method:
Step a, it takes persimmon leaf to crush, crushes and screen to obtain the persimmon leaf powder of 40~50 mesh after clean dry.
Step b, weigh 10g persimmon leaf powder, the ethanol solution that volume fraction is 60~70% be added, 50~60 DEG C, it is solid
Determine supersonic frequency to be 35kHZ, carry out ultrasonic wave extraction 30 minutes under conditions of power is 200W, obtains persimmon extracting liquid.
Preferably, the bitter buckwheat tea extract extracts by the following method:
Step a, bitter buckwheat tealeaves is taken, crushes and screen to obtain the bitter buckwheat tea powder of 50~60 mesh after clean dry.
Step b, 1 part of bitter buckwheat tea powder is weighed, the ethanol solution that 30 parts of volume parts are 50% is added, in fixed supersonic frequency
Ultrasonic wave extraction 30 minutes under conditions of rate is 35kHZ, power is 200W filters simultaneously constant volume, obtains bitter buckwheat tea extract.
Preferably, the high shear homogeneous emulsifying machine includes:
Fuselage, the internal cavity having for emulsifying thickening, top is provided with opening, chamber described in the open communication
Partition is arranged in body, the inside cavity, and the cavity is separated into independent left chamber body and right chamber body, the partition by the partition
Including upper spacer and lower clapboard, the upper spacer is fixed with fuselage inner wall, the upper spacer be hollow structure, the lower clapboard with
The mode being scalable in the hollow structure of the upper spacer is arranged, wherein the mode of lower clapboard setting is:Positioned at described
A pair of of electric track is set on the fuselage inner wall of the underface of upper spacer, and the electric sliding rail stretches body cavity straight down
Bottom, to slide up and down along the lower clapboard in conjunction with the electric track, the lower clapboard is upward for the two sides of the lower clapboard
Left chamber body is connected to right chamber body when sliding, is separated left chamber body and right chamber body when slide downward.
Cover, lid are bonded to the opening and close the cavity.
Microwave applicator is arranged in the bottom interior wall of the fuselage, and the microwave applicator is connected by microwave tube
Microwave generator, the microwave generator are connected to power supply by electric switch.
Temperature sensor is arranged in the bottom interior wall of the fuselage.
Whether pressure switch, be arranged on the cover to cover for incuding cover and be bonded to the opening.
Gate stirrer comprising the first gate stirrer and the second gate stirrer, first gate stirrer and
Second gate stirrer is symmetrically arranged in the cover, when the cover lid is bonded to the fuselage, first frame
Formula blender and the second gate stirrer are respectively protruding into the left chamber body and right chamber body.
Vacuum pump, setting are connected in the cavity by vacuum tube for that will take out in external fuselage, the vacuum pump
The gas of the empty cavity is provided with check-valves on the vacuum tube.
Controller, respectively with electric sliding rail, electric switch, temperature sensor, gate stirrer and vacuum pump and pressure
Switch electrical connection.
Wherein, the controller controls the electric sliding rail time opening so that the lower clapboard up slides.
The controller controls the electric switch according to the signal of temperature sensor to open or stop microwave generator
It runs and then controls microwave applicator and cavity is heated.
The controller controls the open and close of the gate stirrer according to the signal of the pressure switch.
The controller controls the operation of the vacuum pump according to the signal of the pressure switch.
Preferably, the action direction of first gate stirrer and the second gate stirrer is identical.
Preferably, the controller is configured as:The signal for receiving the pressure switch controls the gate stirrer
It is run after 5 seconds, controls the vacuum pump and run after 5 seconds.
Preferably, the controller is configured as:A heating temperature is preset, when the temperature of temperature sensor is lower than institute
When stating heating temperature, controls the electric switch and open;When the temperature of temperature sensor is higher than 1~5 DEG C of the heating temperature, control
The electric switch is made to close.
The present invention is include at least the following beneficial effects:
First, oil and fat of sacha inchi is easy to be absorbed by the skin rich in the essential fatty acid with skin affinity, effectively keeps
Skin elasticity and moist;Contained abundant vitamin E antioxidant, can eliminate facial wrinkles, prevent skin aging;In addition with beauty
Rattan fruit oil, which smears skin, can resist ultraviolet light, prevent cutaneum carcinoma;U.S. rattan fruit contains unsaturated fatty acid, can play radiation protection
Effect;Oil and fat of sacha inchi is obtained by way of cold press, the effective component that can reduce in oil and fat of sacha inchi is destroyed, along with palm fibre
The high osmosis of the different monooctyl ester of palmitic acid acid promotes nutritional ingredient in skin cream to be absorbed.
Secondly, U.S. rattan fruit moisturizing emulsion disclosed in this invention inhibits excessively dividing for sebaceous glands by convergence aqueous extract
It secretes, then to skin moisturizing, to adjust water, the oil balance of skin, hydrone filling pore simultaneously restrains pore, and it is thick to avoid pore
The big dirt for being easy to absorb in air and influence are beautiful.
Further advantage, target and feature of the invention will be partially reflected by the following instructions, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of high shear homogeneous emulsifying machine of the invention;
Fig. 2 is the structural schematic diagram of high shear homogeneous emulsifying machine of the invention.
Specific embodiment
As shown in FIG. 1 to FIG. 2, the high shear homogeneous emulsifying machine includes:Fuselage 1, it is internal to have for emulsifying thickening
Cavity, top is provided with opening, cavity described in the open communication, and the inside cavity is arranged partition, and the partition is by institute
It states cavity and is separated into independent left chamber body and right chamber body, the partition includes upper spacer 2 and lower clapboard 3, the upper spacer 2 and machine
1 inner wall of body is fixed, and the upper spacer 2 is hollow structure, and the lower clapboard 3 is to be scalable to the hollow structure of the upper spacer 2
Interior mode is arranged, wherein the mode that the lower clapboard 3 is arranged is:On the fuselage inner wall of the underface of the upper spacer 2
A pair of of electric track 4 is set, the electric sliding rail 4 stretch the bottom of body cavity straight down, the two sides of the lower clapboard 3 and
The electric track 4 along the electric track 4 in conjunction with to slide up and down, by left chamber body and the right side when 3 upward sliding of lower clapboard
Cavity connection, separates left chamber body and right chamber body when slide downward.
Cover 5, lid are bonded to the opening and close the cavity.
Microwave applicator 6 is arranged in the bottom interior wall of the fuselage 1, and the microwave applicator 6 is connected by microwave tube
Microwave generator 7 is connect, the microwave generator 7 is connected to power supply by electric switch.
Temperature sensor 8 is arranged in the bottom interior wall of the fuselage 1.
Whether pressure switch 9, be arranged on the cover 5 to cover for incuding cover 5 and be bonded to the opening.
Gate stirrer 10 comprising the first gate stirrer and the second gate stirrer, first gate stirrer
It is symmetrically arranged in the cover 5 with the second gate stirrer, when the cover 5 lid is bonded to the fuselage 1, described the
One gate stirrer and the second gate stirrer are respectively protruding into the left chamber body and right chamber body.
Vacuum pump 11, setting are connected in the cavity by vacuum tube 12 and are used in external fuselage, the vacuum pump 11
In being provided with check-valves 13 on the gas that will evacuate the cavity, the vacuum tube 12.
Controller 14, respectively with electric sliding rail 4, electric switch, temperature sensor 8, gate stirrer 10 and vacuum pump 11
And pressure switch 9 is electrically connected.
Wherein, the controller 14 controls 4 time opening of electric sliding rail so that the lower clapboard 3 up slides.
The controller 14 controls the electric switch according to the signal of temperature sensor 8 to open or stop microwave generator
7 operation controls microwave applicator 6 in turn and heats to cavity.
The controller 14 controls the open and close of the gate stirrer 10 according to the signal of the pressure switch 9.
The controller 14 controls the operation of the vacuum pump 11 according to the signal of the pressure switch 9.
Further, the action direction of first gate stirrer and the second gate stirrer is identical.
Further, the controller 14 is configured as:Receive the signal of the pressure switch 9.
It controls the gate stirrer 10 to run after 5 seconds, controls the vacuum pump 11 and run after 5 seconds.
Further, the controller 14 is configured as:A heating temperature is preset, when the temperature of temperature sensor 8 is low
When the heating temperature, controls the electric switch and open;When the temperature of temperature sensor 8 is higher than 1~5 DEG C of the heating temperature
When, it controls the electric switch and closes.
Embodiment 1
A kind of preparation method of U.S. rattan fruit moisturizing emulsion, specifically includes following steps:
Obtain U.S. rattan fruit kernel Step 1: U.S. rattan fruit is enucleated, then U.S. rattan fruit kernel crushed, then 50 DEG C of temperature,
Squeezing 60 minutes is carried out under 50MPa pressure, obtains oil and fat of sacha inchi and pomace.
Step 2: pomace by drying or is dried, using 100 mesh are crushed to, U.S. rattan fruit powder end is obtained.
Step 3: preparing persimmon extracting liquid, following steps are specifically included:
Step a, it takes persimmon leaf to crush, crushes and screen to obtain the persimmon leaf powder of 50 mesh after clean dry.
Step b, 30g persimmon leaf powder is weighed, the ethanol solution that 600 milliliters of volume fractions are 65% is added, in 55 DEG C, fixation
It is carried out ultrasonic wave extraction 30 minutes under conditions of supersonic frequency is 35kHZ, power is 200W, obtains persimmon extracting liquid.
Step 4: preparing thickened gel agent with distilled water, carbomer and gelling agent, following steps are specifically included:
Step a, carbomer 3g is weighed, after mixing with 500 milliliters of distilled water, standing makes its expansion, obtains carbomer
Inflation fluid.
Step b, gelling agent 3g is weighed, after being mixed with 500 milliliters of part distilled water, the heating water bath in 65 DEG C, and stir extremely
After uniformly, standing makes its expansion, obtains gelling agent inflation fluid.
Step c, triethanolamine 3g and resulting carbomer inflation fluid, gelling agent inflation fluid are mixed to get institute is arrived
State thickened gel agent.
Step 5: taking oil and fat of sacha inchi 200g, isobutyl palmitate 15g and stearic acid 25g respectively, stir in 65 DEG C to molten
Solution, obtains the first mixture.
Take U.S. rattan fruit powder end 300g, 500 milliliters of persimmon extracting liquid and 100 milliliters of glycerol respectively, the heating water bath in 65 DEG C,
And it is stirred until homogeneous, the second mixture.
Step 6: taking 300 milliliters of 300 milliliters of the first mixture and the second mixture and 10 milliliters of sorbester p17 and methyl
Glucoside sesquialter stearate 10g, 60 milliliters of thickened gel agent be respectively put into high shear homogeneous emulsifying machine and carry out emulsification increasing
It is thick to get to U.S. rattan fruit moisturizing emulsion.
Embodiment 2
The difference of the embodiment and embodiment is:
Step 3: preparing bitter buckwheat tea extract, following steps are specifically included:
Step a, bitter buckwheat tealeaves is taken, crushes and screen to obtain the bitter buckwheat tea powder of 60 mesh after clean dry.
Step b, 5g bitter buckwheat tea powder is weighed, the ethanol solution that 150 milliliters of volume parts are 50% is added, in fixed ultrasound
Ultrasonic wave extraction 30 minutes under conditions of frequency is 35kHZ, power is 200W filters and distilled water is added to be settled to 500 milliliters, obtains
To bitter buckwheat tea extract.
Step 5: taking oil and fat of sacha inchi 200g, isobutyl palmitate 15g and stearic acid 25g respectively, stir in 65 DEG C to molten
Solution, obtains the first mixture.
U.S. rattan fruit powder end 300g, 500 milliliters of bitter buckwheat tea extract and 100 milliliters of glycerol are taken respectively, and water-bath adds in 65 DEG C
Heat, and be stirred until homogeneous, the second mixture.
Remaining parameter is identical with embodiment 1, and technical process is also identical.
Embodiment 3
The difference of the embodiment and embodiment is:
Step 3: preparing persimmon extracting liquid, following steps are specifically included:
Step a, it takes persimmon leaf to crush, crushes and screen to obtain the persimmon leaf powder of 50 mesh after clean dry.
Step b, 30g persimmon leaf powder is weighed, the ethanol solution that 600 milliliters of volume fractions are 65% is added, in 55 DEG C, fixation
It is carried out ultrasonic wave extraction 30 minutes under conditions of supersonic frequency is 35kHZ, power is 200W, obtains persimmon extracting liquid.
Bitter buckwheat tea extract is prepared, following steps are specifically included:
Step a, bitter buckwheat tealeaves is taken, crushes and screen to obtain the bitter buckwheat tea powder of 60 mesh after clean dry.
Step b, 5g bitter buckwheat tea powder is weighed, the ethanol solution that 150 milliliters of volume parts are 50% is added, in fixed ultrasound
Ultrasonic wave extraction 30 minutes under conditions of frequency is 35kHZ, power is 200W filters and distilled water is added to be settled to 500 milliliters, obtains
To bitter buckwheat tea extract.
Step 5: taking oil and fat of sacha inchi 200g, isobutyl palmitate 15g and stearic acid 25g respectively, stir in 65 DEG C to molten
Solution, obtains the first mixture.
U.S. rattan fruit powder end 300g, 100 milli of 250 milliliters of persimmon extracting liquid, 250 milliliters of bitter buckwheat tea extract and glycerol are taken respectively
It rises, the heating water bath in 65 DEG C, and is stirred until homogeneous, the second mixture.
Remaining parameter is identical with embodiment 1, and technical process is also identical.
Embodiment 4
The difference of the embodiment and embodiment is:
Step 6: taking 450 milliliters of 300 milliliters of the first mixture and the second mixture and 10 milliliters of sorbester p17 and methyl
Glucoside sesquialter stearate 15g, 75 milliliters of thickened gel agent be respectively put into high shear homogeneous emulsifying machine and carry out emulsification increasing
It is thick to get to U.S. rattan fruit moisturizing emulsion.
Remaining parameter is identical with embodiment 1, and technical process is also identical.
Comparative example 1
The difference of the comparative example and embodiment is:
Step 5: taking apricot kernel oil 200g, isobutyl palmitate 15g and stearic acid 25g respectively, stir in 65 DEG C to molten
Solution, obtains the first mixture.
500 milliliters of persimmon extracting liquid and 65 milliliters of glycerol, the heating water bath in 65 DEG C are taken respectively, and are stirred until homogeneous, the
Two mixtures.
Remaining parameter is identical with embodiment 1, and technical process is also identical.
Following experiment is done with regard to moisturizing emulsion obtained by embodiment and comparative example respectively, group 1~4 is the knot of Examples 1 to 4
Fruit, group 5 are comparative example 1 as a result, group 6 is negative control group as a result, group 7 is positive controls as a result, obtaining data such as
Table 1:
Wherein, organoleptic properties are evaluated:Moisturizing emulsion visual observations lotion color under the conditions of 25 DEG C, non-direct sunlight is taken respectively
Pool whether uniformity, have free from admixture, sediment.
PH value test:Moisturizing emulsion 1g is taken respectively, 15 milliliters of purified waters are added and is stirred evenly, in 35~37 DEG C of conditions
Lower detection pH value.
Stability experiment:It weighs each two parts of moisturizing emulsion 10g respectively to be put in beaker, the constant temperature that portion is placed on 42 DEG C dries
Case, portion is placed on -15 DEG C of freezer compartment of refrigerator, takes out after 24 hours, after spontaneous recovery to room temperature, has seen whether point
Layer, precipitating or water outlet phenomenon.
Radiation protection experiment:The made moisturizing emulsion of 50g is weighed respectively, and moisturizing emulsion is uniformly applied to face paper
On, 10 million-electron-volts are used as the energy of incident electron, and the face paper for having smeared moisturizing emulsion is covered on radioactivity instrument
On device, the electron number projected is detected.Negative control is covered on radioactive instrument for the face paper of blank and detects;Positive control
It is uniformly applied on face paper for the succinct purely antioxidant emulsion 100g of natural hall snowy region.
Anti-oxidant experiment:An apple is taken, is averagely cut into 8, weighs moisturizing emulsion 10g is applied to apple one respectively
Side surface is placed 8 hours, primary every observation in 2 hours, and records the variation of apple surface color.Negative control is blank
Apple flakes;Positive control is the side surface that the succinct purely antioxidant emulsion 50g of nature hall snowy region is applied to apple.Wherein, color
Variation is from shallowly 5 grades are divided into deep, and most light to be denoted as 1, most dark to be denoted as 5, it is better that color more shallowly represents antioxidant effect.
Table 1:
From above data it is found that U.S. rattan fruit moisturizing emulsion color obtained by the method disclosed in the present is uniform, without miscellaneous
Matter, without precipitating, stability is good, if having preferable radiation protection ability, antioxidant effect is excellent in alkalinity.
Skin test is done with regard to moisturizing emulsion obtained by embodiment and comparative example respectively:
Each 5 people of men and women for the oily skin that age bracket is 16~25,26~35 is chosen, altogether 20 people, point completion in 6 days is surveyed
Examination, is all tested using 1 moisturizing emulsion of embodiment, is all surveyed using 2 moisturizing emulsion of embodiment within second day for first day
Examination, is sequentially tested to the 6th day with this and is tested using purified water.
Test request:Tester dries after cleaning face using same money facial cleanser 3g, then moisturizing emulsion 3g is taken to be applied to
Face does not wash one's face in 8 hours, without using other skin care item, recorded after 8 hours whether dry or it is greasy, have tight feeling.
Group 1~4 is Examples 1 to 4 as a result, group 5 is comparative example 1 as a result, group 6 is blank control group as a result, obtaining
To data such as table 2:
Table 2:
Above data is illustrated using U.S. rattan fruit moisturizing emulsion, replenishing water and preserving moisture obtained by the method disclosed in the present
Effect is good.
Concrete case analysis:
Wu, male, Oily, pore is coarse blackhead, and after this product three months, pore is shunk and blackhead disappears substantially
It loses, no sense of discomfort.
Liang, female, Oily, face easily it is greasy, acne are more, after this product three months, acne disappear substantially and
The phenomenon that facial oiliness, is rare, no sense of discomfort.
More than, illustrate that inhibition skin can be played using U.S. rattan fruit moisturizing emulsion obtained by the method disclosed in the present
The excessive secretion of adipose gland, adjust skin water, oil balance so that pore refining effect, be used in Oily.
Although the embodiments of the present invention have been disclosed as above, but its is not only in the description and the implementation listed
With.It can be applied to various suitable the field of the invention completely.It for those skilled in the art, can be easily
Realize other modification.Therefore, without departing from the general concept defined in the claims and the equivalent scope, the present invention and unlimited
In specific details.
Claims (8)
1. a kind of preparation method of U.S. rattan fruit moisturizing emulsion, which is characterized in that including:
Obtain U.S. rattan fruit kernel Step 1: U.S. rattan fruit is enucleated, then U.S. rattan fruit kernel crushed, then 45~55 DEG C of temperature,
It is carried out under 40~60MPa pressure squeezing 50~60 minutes, obtains oil and fat of sacha inchi and pomace;
Step 2: pomace by drying or is dried, using crushing, U.S. rattan fruit powder end is obtained;
Step 3: choosing one or both of persimmon extracting liquid or bitter buckwheat tea extract as convergence extracting solution;
Step 4: 150~350 parts of oil and fat of sacha inchi, 20~30 parts of isobutyl palmitate and 20~30 parts of stearic acid are taken respectively, in 60
Stirring obtains the first mixture to dissolving in~70 DEG C;
200~500 parts of U.S. rattan fruit powder end is taken respectively, restrains 400~800 parts of extracting solution and 50~100 parts of glycerol, in 60~70 DEG C
Middle heating water bath, and be stirred until homogeneous, the second mixture;
Step 5: first mixture and the second mixture and compound emulsifying agent, thickened gel agent difference of quality volume such as taking
It is put into high shear homogeneous emulsifying machine and carries out emulsification thickening to get U.S. rattan fruit moisturizing emulsion is arrived;
The compound emulsifying agent includes:Sorbester p17, methyl glucoside sesquialter stearate, two kinds or two kinds in xanthan gum with
Upper raw material;
The thickened gel agent includes:Carbomer, gelling agent and triethanolamine, the thickened gel agent are made by the following method
?:
Step a, 3~5 parts of carbomer are weighed, after mixing with 500~1000 parts of distilled water, standing makes its expansion, is blocked
Wave nurse inflation fluid;
Step b, 3~6 parts of gelling agent are weighed, after being mixed with 300~800 parts of distilled water, the heating water bath in 60~70 DEG C, and stir
Mix to uniformly after, standing make its expansion, obtain gelling agent inflation fluid;
Step c, 1~5 part of triethanolamine is mixed with resulting carbomer inflation fluid, gelling agent inflation fluid to get institute is arrived
State thickened gel agent;
In the emulsification thickening, the mass ratio of first mixture and the second mixture is 1:1~1.5.
2. the preparation method of U.S. rattan fruit moisturizing emulsion as described in claim 1, which is characterized in that the step 5 is specially:
100 parts of the first mixture, 100 parts of the second mixture, 35 parts of compound emulsifying agent and 6 parts of thickened gel agent are taken respectively, respectively
It is put into high shear homogeneous emulsifying machine and carries out emulsification thickening to get U.S. rattan fruit moisturizing emulsion is arrived.
3. the preparation method of U.S. rattan fruit moisturizing emulsion as described in claim 1, which is characterized in that the persimmon extracting liquid passes through
Following methods are made:
It takes persimmon leaf to crush, crushes and screen to obtain the persimmon leaf powder of 40~50 mesh after clean dry;
10g persimmon leaf powder is weighed, the ethanol solution that volume fraction is 60~70% is added, in 50~60 DEG C, fixed supersonic frequency
It is carried out ultrasonic wave extraction 30 minutes under conditions of being 200W for 35kHZ, power, obtains persimmon extracting liquid.
4. the preparation method of U.S. rattan fruit moisturizing emulsion as described in claim 1, which is characterized in that the bitter buckwheat tea extract is logical
Cross following methods extraction:
Bitter buckwheat tealeaves is taken, crushes and screen to obtain the bitter buckwheat tea powder of 50~60 mesh after clean dry;
Weigh 1 part of bitter buckwheat tea powder, the ethanol solution that 30 parts of volume parts are 50% be added, fixed supersonic frequency be 35kHZ,
Power is to filter ultrasonic wave extraction 30 minutes under conditions of 200W and constant volume obtains bitter buckwheat tea extract.
5. the preparation method of U.S. rattan fruit moisturizing emulsion as described in claim 1, which is characterized in that the high shear emulsifying
Machine includes:
Fuselage, the internal cavity having for emulsifying thickening, top is provided with opening, cavity described in the open communication, institute
Inside cavity setting partition is stated, the cavity is separated into independent left chamber body and right chamber body by the partition, and the partition includes
Upper spacer and lower clapboard, the upper spacer are fixed with fuselage inner wall, and the upper spacer is hollow structure, and the lower clapboard is can stretch
The mode being reduced in the hollow structure of the upper spacer is arranged, wherein the mode of lower clapboard setting is:On described every
A pair of of electric track is set on the fuselage inner wall of the underface of plate, and the electric sliding rail stretches the bottom of body cavity straight down
Portion, to slide up and down along the lower clapboard in conjunction with the electric track, the lower clapboard is slid up for the two sides of the lower clapboard
Left chamber body be connected to right chamber body when dynamic, by left chamber body and the separation of right chamber body when slide downward;
Cover, lid are bonded to the opening and close the cavity;
Microwave applicator is arranged in the bottom interior wall of the fuselage, and the microwave applicator connects microwave by microwave tube
Generator, the microwave generator are connected to power supply by electric switch;
Temperature sensor is arranged in the bottom interior wall of the fuselage;
Whether pressure switch, be arranged on the cover to cover for incuding cover and be bonded to the opening;
Gate stirrer comprising the first gate stirrer and the second gate stirrer, first gate stirrer and second
Gate stirrer is symmetrically arranged in the cover, and when the cover lid is bonded to the fuselage, first frame is stirred
It mixes device and the second gate stirrer is respectively protruding into the left chamber body and right chamber body;
Vacuum pump, setting are connected in the cavity by vacuum tube for that will evacuate institute in external fuselage, the vacuum pump
The gas of cavity is stated, is provided with check-valves on the vacuum tube;
Controller, respectively with electric sliding rail, electric switch, temperature sensor, gate stirrer and vacuum pump and pressure switch
Electrical connection;
Wherein, the controller controls the electric sliding rail time opening so that the lower clapboard up slides;
The controller controls the electric switch according to the signal of temperature sensor to open or stop the operation of microwave generator
And then it controls microwave applicator and cavity is heated;
The controller controls the open and close of the gate stirrer according to the signal of the pressure switch;
The controller controls the operation of the vacuum pump according to the signal of the pressure switch.
6. the preparation method of U.S. rattan fruit moisturizing emulsion as claimed in claim 5, which is characterized in that first gate stirrer
It is identical with the action direction of the second gate stirrer.
7. the preparation method of U.S. rattan fruit moisturizing emulsion as described in claim 1, which is characterized in that the controller is configured
For:
Receive the signal of the pressure switch;
It controls the gate stirrer to run after 5 seconds, controls the vacuum pump and run after 5 seconds.
8. the preparation method of U.S. rattan fruit moisturizing emulsion as described in claim 1, which is characterized in that the controller is configured
For:
Preset a heating temperature;
When the temperature of temperature sensor is lower than the heating temperature, controls the electric switch and open;
When the temperature of temperature sensor is higher than 1~5 DEG C of the heating temperature, controls the electric switch and close.
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