CN108785127A - A kind of soap base shower cream and preparation method thereof - Google Patents

A kind of soap base shower cream and preparation method thereof Download PDF

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Publication number
CN108785127A
CN108785127A CN201810668207.4A CN201810668207A CN108785127A CN 108785127 A CN108785127 A CN 108785127A CN 201810668207 A CN201810668207 A CN 201810668207A CN 108785127 A CN108785127 A CN 108785127A
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China
Prior art keywords
potassium
soap base
shower cream
subsequently placed
polymer
Prior art date
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CN201810668207.4A
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Chinese (zh)
Inventor
陈业忠
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Guangdong Yuxin New Material Co Ltd
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Guangdong Yuxin New Material Co Ltd
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Priority to CN201810668207.4A priority Critical patent/CN108785127A/en
Publication of CN108785127A publication Critical patent/CN108785127A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20Halogens; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of soap base shower creams, are made of the raw material of following weight percent meter:Acrylic acid esters co-polymer 1 ~ 5.5%;Potassium hydroxide 0.1 ~ 0.6%;Klorvess Liquid 0 ~ 6%;Aliphatic acid potassium 3 ~ 20%;Preservative 0 ~ 1%;Essence 0 ~ 2%;Surplus is water.A kind of production method of soap base shower cream, includes the following steps:Step 1 at normal temperatures into the water and stirs evenly acrylic acid esters co-polymer;Step 2 is subsequently placed into potassium hydroxide and is neutralized into alkalinity;Step 3 is subsequently placed into Klorvess Liquid and stirs evenly;Step 4 is subsequently placed into aliphatic acid potassium and stirs to being completely dissolved;Step 5, is finally putting into preservative and essence stirs evenly.Lotion will not be formed when low temperature and lamination occur, viscosity is high, and using effect is good, and uses fatty acid potassium soap base cold with production to facilitate, and saves production time and the energy, reduces production cost.

Description

A kind of soap base shower cream and preparation method thereof
Technical field
The present invention relates to a kind of shower creams, and in particular to a kind of soap base shower cream and preparation method thereof.
Background technology
Shower cream is a kind of liquid ceanser used when having a bath.The national standard of shower cream is used main according to its formula Shower cream is divided into two classes, i.e. soap base type and non-soap fundamental mode surfactant type by the kind of surfactant.Soap base type shower cream Principle based on soapmaking is modified, and foaming abundancy is readily cleaned.But there are asked below this for existing soap base type shower cream Topic:1, it is easy to form lotion when low temperature, is not easy to extract and uses;2, it is easy to be divided into multilayer when low temperature, the cleaning of shower cream is made to imitate Fruit reduces, and due cleaning effect is not achieved;3, shower cream increase consistency is difficult, and production cost is high.Therefore the present inventor is to washing one's hair Bath lotion has carried out innovative research.
Invention content
It is provided by the present invention a kind of to be not easy to form lotion, being not easy to be layered, the soap base shower cream that production cost is low and its system Make method.
The technical solution adopted by the present invention to solve the technical problems is:
A kind of soap base shower cream is made of the raw material of following weight percent meter:
Acrylic acid esters co-polymer 1 ~ 5.5%;
Potassium hydroxide 0.1 ~ 0.6%;
Klorvess Liquid 0 ~ 6%;
Aliphatic acid potassium 3 ~ 20%;
Preservative 0 ~ 1%;
Essence 0 ~ 2%;
Surplus is water.
In the present invention, the pH value of shower cream is 9.0 ~ 10.
A kind of production method of soap base shower cream, includes the following steps:
Step 1 at normal temperatures into the water and stirs evenly acrylic acid esters co-polymer;
Step 2 is subsequently placed into potassium hydroxide and is neutralized into alkalinity;
Step 3 is subsequently placed into Klorvess Liquid and stirs evenly;
Step 4 is subsequently placed into aliphatic acid potassium and stirs to being completely dissolved;
Step 5, is finally putting into preservative and essence stirs evenly.
In the free-moving system of chemical molecular, fatty acid potassium soap is easily contacted with hydrogen ion in system, under low-temperature condition Aliphatic acid is formed as fatty acid solubility reduces, after being combined with hydrogen ion and escapes system, and product is caused to be layered.Esters of acrylic acid Copolymer has extremely strong suspending power, can prevent moving freely for chemical molecular, reduce fatty acid potassium soap molecule and body The possibility that hydrogen ion contacts in system, also prevents the formation of aliphatic acid, avoids product layering.
Sodium chloride or Klorvess Liquid are electrically charged using itself institute simultaneously, can promotion system micelle forma-tion, and generate increasing Thick effect;But soap base system has certain tolerance limit to sodium chloride, when sodium chloride content is excessively high, sodium ion can be with fat Potassium ion forms displacement and forms sodium soap in sour potassium, and when low temperature will tie cream, and soap base content is higher, to the molten of sodium chloride It is lower to solve limit.But this problem is not present in potassium chloride, can largely use and increase consistency, but can not infinitely thicken, when Salt content is excessively high, and institute is electrically charged to neutralize system micellar charge in turn, and product viscosity is caused to reduce.
Therefore the beneficial effects of the invention are as follows:Lotion will not be formed when low temperature and lamination occur, viscosity is high, uses Effect is good, and uses fatty acid potassium soap base cold with production to facilitate, and saves production time and the energy, reduces production cost.
Specific implementation mode
The present invention is further described below by way of specific implementation mode, but the present invention is not limited only to following embodiment.? It in the scope of the present invention or is not departing from present disclosure, in spirit and scope, antibacterial soap base of the present invention is being washed one's hair Bath lotion and preparation method thereof is suitably modified, replaces the identical component of effect, be to those skilled in the art it is aobvious and It is clear to, they are considered as being included within the scope of the present invention.
Embodiment one, a kind of soap base shower cream and preparation method thereof that the present embodiment is provided.
Formula:The soap base shower cream is made of the raw material of following weight percent meter:
Acrylic acid esters co-polymer 2.5%, the present invention is interior upon mixing to be formed with fatty acid potassium soap, the fatty acid potassium soap and system Middle hydrogen ion contacts, and forming aliphatic acid as fatty acid solubility reduces under low-temperature condition, after being combined with hydrogen ion escapes system, Product is caused to be layered;Acrylic acid esters co-polymer has extremely strong suspending power, can prevent moving freely for chemical molecular, subtract The possibility that fatty acid potassium soap molecule is contacted with hydrogen ion in system is lacked, has also prevented the formation of aliphatic acid, avoid product Layering;
Potassium hydroxide 0.32% realizes the suspending power of acrylic acid esters co-polymer for neutralizing acrylic acid esters co-polymer;
Klorvess Liquid 1.2%, the water that potassium chloride powder is first dissolved in three times form Klorvess Liquid;Potassium chloride utilizes itself institute It is electrically charged, promotion system micelle forma-tion, and generate thickening power;However soap base system restrains oneself limit to sodium chloride with certain Degree, when sodium chloride content is excessively high, sodium ion can form displacement with potassium ion in aliphatic acid potassium and form sodium soap, and when low temperature will Tie cream;Soap base content is higher, lower to the solubility limit of sodium chloride;This problem, therefore preferably chlorination is not present in potassium chloride Potassium;But can not infinitely thicken, when salt content is excessively high, institute is electrically charged to neutralize system micellar charge in turn, cause product viscous Degree reduces;
Aliphatic acid potassium 5%, aliphatic acid potassium are also known as fatty acid potassium soap, are a kind of anion surfactants, can be used as and efficiently clean The main body active matter of the advanced shower cream of type and liquid soap under alkaline condition can be arbitrarily positive with anion, nonionic and high polymer Ionic surface active agent compounds, and bather is made to feel refreshing clean, comfortable from beginning to end;
Pearlite slurry 1% assigns product pearlescent, increases the aesthetic feeling and attraction of product;
Kathon CG solution 0.2%, as preservative, the ratio of Kathon CG and water in Kathon CG solution is 1:3;
Essence 0.2% enhances fragrance;
Surplus is water.The pH value of shower cream is adjusted to 9.0 by final products.
Preparation method:
The acrylic acid esters co-polymer of 2.5kg is put into the water of 90.58kg and is stirred evenly at normal temperatures by step 1;
Step 2, the potassium hydroxide for being subsequently placed into 0.32kg are neutralized into alkalinity;
Step 3 is subsequently placed into the Klorvess Liquid of 1.2kg and stirs evenly;
Step 4 is subsequently placed into the aliphatic acid potassium of 5kg;Then pH value determination, to ensure pH value 9.0 or more;
The essence of step 5, the Kathon CG solution and 0.2kg that are finally putting into 0.2kg stirs evenly, final pH value determination, with true PH value is protected 9.0 or more, pH value is adjusted by way of increasing alkali or acid if having deviation.
Embodiment two, a kind of soap base shower cream and preparation method thereof that the present embodiment is provided.
Formula:The soap base shower cream is made of the raw material of following weight percent meter:
Acrylic acid esters co-polymer 3.5%, the present invention is interior upon mixing to be formed with fatty acid potassium soap, the fatty acid potassium soap and system Middle hydrogen ion contacts, and forming aliphatic acid as fatty acid solubility reduces under low-temperature condition, after being combined with hydrogen ion escapes system, Product is caused to be layered;Acrylic acid esters co-polymer has extremely strong suspending power, can prevent moving freely for chemical molecular, subtract The possibility that fatty acid potassium soap molecule is contacted with hydrogen ion in system is lacked, has also prevented the formation of aliphatic acid, avoid product Layering;
Potassium hydroxide 0.45% realizes the suspending power of acrylic acid esters co-polymer for neutralizing acrylic acid esters co-polymer;
Klorvess Liquid 3.6%, the water that potassium chloride powder is first dissolved in three times form Klorvess Liquid;Potassium chloride utilizes itself institute It is electrically charged, promotion system micelle forma-tion, and generate thickening power;However soap base system restrains oneself limit to sodium chloride with certain Degree, when sodium chloride content is excessively high, sodium ion can form displacement with potassium ion in aliphatic acid potassium and form sodium soap, and when low temperature will Tie cream;Soap base content is higher, lower to the solubility limit of sodium chloride;This problem, therefore preferably chlorination is not present in potassium chloride Potassium;But can not infinitely thicken, when salt content is excessively high, institute is electrically charged to neutralize system micellar charge in turn, cause product viscous Degree reduces;
Aliphatic acid potassium 14%, aliphatic acid potassium are also known as fatty acid potassium soap, are a kind of anion surfactants, can be used as and efficiently wash The main body active matter of the net advanced shower cream of type and liquid soap, under alkaline condition, can arbitrarily with anion, nonionic and high polymer Cationic surfactant compounds, and bather is made to feel refreshing clean, comfortable from beginning to end;
Pearlite slurry 1% assigns product pearlescent, increases the aesthetic feeling and attraction of product;
Kathon CG solution 0.1%, as preservative, the ratio of Kathon CG and water in Kathon CG solution is 1:3;
Essence 0.1% enhances fragrance;
Surplus is water.The pH value of shower cream is adjusted to 9.5 by final products.
Preparation method:
The acrylic acid esters co-polymer of 3.5kg is put into the water of 78.25kg and is stirred evenly at normal temperatures by step 1;
Step 2, the potassium hydroxide for being subsequently placed into 0.45kg are neutralized into alkalinity;
Step 3 is subsequently placed into the Klorvess Liquid of 3.6kg and stirs evenly;
Step 4 is subsequently placed into the aliphatic acid potassium of 14kg;Then pH value determination, to ensure pH value 9.5 or so;
The essence of step 5, the Kathon CG solution and 0.1kg that are finally putting into 0.1kg stirs evenly, final pH value determination, with true PH value is protected 9.5 or so, pH value is adjusted by way of increasing alkali or acid if having deviation.
Embodiment three, a kind of soap base shower cream and preparation method thereof that the present embodiment is provided.
Formula:The soap base shower cream is made of the raw material of following weight percent meter:
Acrylic acid esters co-polymer 5.5%, the present invention is interior upon mixing to be formed with fatty acid potassium soap, the fatty acid potassium soap and system Middle hydrogen ion contacts, and forming aliphatic acid as fatty acid solubility reduces under low-temperature condition, after being combined with hydrogen ion escapes system, Product is caused to be layered;Acrylic acid esters co-polymer has extremely strong suspending power, can prevent moving freely for chemical molecular, subtract The possibility that fatty acid potassium soap molecule is contacted with hydrogen ion in system is lacked, has also prevented the formation of aliphatic acid, avoid product Layering;
Potassium hydroxide 0.6% realizes the suspending power of acrylic acid esters co-polymer for neutralizing acrylic acid esters co-polymer;
Klorvess Liquid 6%, the water that potassium chloride powder is first dissolved in three times form Klorvess Liquid;Potassium chloride utilizes itself institute's band Charge, promotion system micelle forma-tion, and generate thickening power;However soap base system has certain tolerance limit to sodium chloride, When sodium chloride content is excessively high, sodium ion can form displacement with potassium ion in aliphatic acid potassium and form sodium soap, and when low temperature will tie Cream;Soap base content is higher, lower to the solubility limit of sodium chloride;This problem, therefore preferably potassium chloride is not present in potassium chloride; But can not infinitely thicken, when salt content is excessively high, institute is electrically charged to neutralize system micellar charge in turn, and product viscosity is caused to drop It is low;
Aliphatic acid potassium 20%, aliphatic acid potassium are also known as fatty acid potassium soap, are a kind of anion surfactants, can be used as and efficiently wash The main body active matter of the net advanced shower cream of type and liquid soap, under alkaline condition, can arbitrarily with anion, nonionic and high polymer Cationic surfactant compounds, and bather is made to feel refreshing clean, comfortable from beginning to end;
Pearlite slurry 1% assigns product pearlescent, increases the aesthetic feeling and attraction of product;
Kathon CG solution 1%, as preservative, the ratio of Kathon CG and water in Kathon CG solution is 1:3;
Essence 1.5% enhances fragrance;
Surplus is water.The pH value of shower cream is adjusted to 9.8 by final products.
Preparation method:
The acrylic acid esters co-polymer of 5.5kg is put into the water of 65.4kg and is stirred evenly at normal temperatures by step 1;
Step 2, the potassium hydroxide for being subsequently placed into 0.6kg are neutralized into alkalinity;
Step 3 is subsequently placed into the Klorvess Liquid of 6kg and stirs evenly;
Step 4 is subsequently placed into the aliphatic acid potassium of 20kg;Then pH value determination, to ensure pH value 9.8 or so;
The essence of step 5, the Kathon CG solution and 1.5kg that are finally putting into 1kg stirs evenly, final pH value determination, to ensure PH value adjusts pH value if having deviation 9.8 or so by way of increasing alkali or acid.
The foregoing is merely the preferred embodiments of the present invention, as long as realizing the skill of the object of the invention with essentially identical means Art scheme belongs within protection scope of the present invention.

Claims (3)

1. a kind of soap base shower cream, it is characterised in that:It is made of the raw material of following weight percent meter:
Acrylic acid esters co-polymer 1 ~ 5.5%;
Potassium hydroxide 0.1 ~ 0.6%;
Klorvess Liquid 0 ~ 6%;
Aliphatic acid potassium 3 ~ 20%;
Preservative 0 ~ 1%;
Essence 0 ~ 2%;
Surplus is water.
2. a kind of soap base shower cream according to claim 1, it is characterised in that:The pH value of shower cream is 9.0 ~ 10.
3. a kind of production method of soap base shower cream as described in claim 1-2 any one, it is characterised in that including following Step:
Step 1 at normal temperatures into the water and stirs evenly acrylic acid esters co-polymer;
Step 2 is subsequently placed into potassium hydroxide and is neutralized into alkalinity;
Step 3 is subsequently placed into Klorvess Liquid and stirs evenly;
Step 4 is subsequently placed into aliphatic acid potassium and stirs to being completely dissolved;
Step 5, is finally putting into preservative and essence stirs evenly.
CN201810668207.4A 2018-06-26 2018-06-26 A kind of soap base shower cream and preparation method thereof Pending CN108785127A (en)

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Application Number Priority Date Filing Date Title
CN201810668207.4A CN108785127A (en) 2018-06-26 2018-06-26 A kind of soap base shower cream and preparation method thereof

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CN108785127A true CN108785127A (en) 2018-11-13

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110897931A (en) * 2019-11-16 2020-03-24 广东科誉新材料有限公司 Transparent shower gel adopting cold blending process and preparation method thereof
CN111019776A (en) * 2019-11-16 2020-04-17 广东科誉新材料有限公司 Liquid soap base added with acrylate copolymer and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1633985A (en) * 2004-11-01 2005-07-06 江苏隆力奇生物科技股份有限公司 Easily-rinsed shower cream for moistening the skin
CN103417407A (en) * 2013-08-19 2013-12-04 中山市佳丽精细化工有限公司 Shower gel formulation and preparation technology thereof
CN105878056A (en) * 2014-12-05 2016-08-24 江南大学 Mild and moist soap-based shower gel
CN106333873A (en) * 2016-08-29 2017-01-18 澳宝化妆品(惠州)有限公司 Soap-based body wash

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1633985A (en) * 2004-11-01 2005-07-06 江苏隆力奇生物科技股份有限公司 Easily-rinsed shower cream for moistening the skin
CN103417407A (en) * 2013-08-19 2013-12-04 中山市佳丽精细化工有限公司 Shower gel formulation and preparation technology thereof
CN105878056A (en) * 2014-12-05 2016-08-24 江南大学 Mild and moist soap-based shower gel
CN106333873A (en) * 2016-08-29 2017-01-18 澳宝化妆品(惠州)有限公司 Soap-based body wash

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
孙宝国: "《日用化工辞典》", 30 June 2002, 化学工业出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110897931A (en) * 2019-11-16 2020-03-24 广东科誉新材料有限公司 Transparent shower gel adopting cold blending process and preparation method thereof
CN111019776A (en) * 2019-11-16 2020-04-17 广东科誉新材料有限公司 Liquid soap base added with acrylate copolymer and preparation method thereof

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Application publication date: 20181113

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