CN103417407A - Shower gel formulation and preparation technology thereof - Google Patents

Shower gel formulation and preparation technology thereof Download PDF

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Publication number
CN103417407A
CN103417407A CN2013103674548A CN201310367454A CN103417407A CN 103417407 A CN103417407 A CN 103417407A CN 2013103674548 A CN2013103674548 A CN 2013103674548A CN 201310367454 A CN201310367454 A CN 201310367454A CN 103417407 A CN103417407 A CN 103417407A
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mutually
expects
comprised
stirring
weight percent
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李禄玲
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ZHONGSHAN JIALI FINE CHEMICAL Co Ltd
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ZHONGSHAN JIALI FINE CHEMICAL Co Ltd
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Priority to CN2013103674548A priority Critical patent/CN103417407A/en
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Abstract

The invention discloses a shower gel formulation and a preparation technology thereof. Shower gel comprises, by weight, 10-18% of A-phase materials, 8-12% of B-phase materials, 15-22% of C-phase materials, 26-33% of D-phase materials, 18-25% of E-phase materials, 0.1-1% of F-phase materials, 2-7% of G-phase materials and 1-3% of H-phase materials. The preparation technology of the shower gel includes the steps: firstly, blending the A-phase materials, the B-phase materials, the C-phase materials and the D-phase materials with different containers respectively; secondly, adding the D-phase materials and a stirred B-phase material solution into a stirred C-phase material solution for stirring; thirdly, adding the F-phase materials into a stirred E-phase material solution for stirring; fourthly, putting a stirred solution in the third step, a stirred A-phase material solution, the G-phase materials and the H-phase materials into a solution in the second step for stirring. The shower gel prepared through the formulation and the preparation technology has the advantages of lasting smooth feeling, skin moisturizing and low irritation.

Description

A kind of formula of bath cream and preparation technology thereof
[technical field]
The present invention relates to a kind of skin cleaner technical field, relate to specifically a kind of formula of bath cream and preparation technology thereof.
[background technology]
Bath gel, be a kind of liquid ceanser used while having a bath, and according to the batching difference, can be divided into alkaline bath gel and acid bath gel.Popular bath gel kind is more in the market, the following several respects shortcoming of these bath gel ubiquities: the first, and bath gel is larger to the zest of skin; The second, after flushing, skin or some drying, skin is moist, soft; The 3rd, be not easy to clean, the skin residue is more.
Therefore be necessary formula and the preparation technology of existing bath gel are improved further.
[summary of the invention]
The technical problem that the present invention solves be to provide a kind of can durable antibiotic, purify air, adsorb the harmful substance such as flue dust, regulate humidity, the anti-algae of mildew-resistant and keep the paint film apparent functional and ornamental perfect unity such as water-fast, alkaline-resisting, build comfortable human settlement's formula of bath cream.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is: a kind of formula of bath cream, and described bath gel is comprised of the component of following weight percent: A expects that 10~18%, B expects that 8~12%, C expects that 15~22%, D expects 26~33% mutually mutually mutually mutually; E expects that 18~25%, F expects that 0.1~1%, G expects that 2~7%, H expects 1~3% mutually mutually mutually mutually;
Described A expects to be comprised of the component of following weight percent mutually: deionized water 55~70%, potassium hydroxide 30~40%;
Described B expects to be comprised of the component of following weight percent mutually: deionized water 60~75%, and EDTA-disodium 0.5~2%, polyquaternary ammonium salt-7 account for 25~38%;
Described C expects to be comprised of the component of following weight percent mutually: deionized water 98~99.5%, hydroxypropyl emthylcellulose 0.3~2%;
Described D expects to be comprised of the component of following weight percent mutually: glycerol 1~5%, sodium laureth sulfate 10~20%, lauryl alcohol both sexes sodium acetate 5~10%, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 15~20% %, propylene glycol 38~45%, SF-1 ACR emulsion 1~5%, cocamido propyl betaine 15~20%;
Described E expects to be comprised of the component of following weight percent mutually: lauric acid 30~40%, and myristic acid 24~30%, Palmic acid 1601 accounts for 25~30%, stearic acid 1~8%, butylated hydroxytoluene 0.1~1%, methyl hydroxybenzoate 0.5~2%, propyl hydroxybenzoate 0.1~1%, coconut monoethanol amide 3~9%;
Described F expects to be comprised of the component of following weight percent mutually: maleic acid polymerized castor oil esteramides 23~30%, olive oil 15~22%, almond oil 15~22%, tocopherol acetas 30~40%;
Described G expects to be 3800 pearlescent flake glycol distearates mutually;
Described H expects to be comprised of the component of following weight percent mutually: essence 90~96%, yellow 5[CI19140] account for 0.001~0.006%, yellow 6[CI15985] account for 0.001~0.007%, Methylisothiazolinone 3~10%.
Further, the purity of described potassium hydroxide is 90%.
Further, the active ingredient of described sodium laureth sulfate is 70%.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is: comprise the steps:
A, the deionized water during A is expected are mutually put in plastic containers, and then gradation slowly adds potassium hydroxide, carry out stirring and dissolving even under the room temperature state;
B, the various raw materials during B is expected mutually drop into successively rustless steel and move in pot and stir 10 minutes, and each raw material is fully dissolved;
C, the deionized water during C is expected are mutually put into the emulsifying pot, then add hydroxypropyl emthylcellulose to be stirred, and mixing speed is 500~550 rev/mins, until solution is transparent and just stop stirring without precipitation;
D, open internal recycle drop into successively glycerol that D expects mutually and sodium laureth sulfate in the solution of step c after, rotating speed is 2200-2500 rev/min, and the persistent period is 10~12 minutes;
E, drop into successively material prepared by lauryl alcohol both sexes sodium acetate, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium, propylene glycol, SF-1 ACR emulsion, cocamido propyl betaine and step b that D expects mutually in the solution of steps d, and be heated with stirring to 75~78 degree, keep constant temperature to be stirred to raw material and all dissolve;
F, the lauric acid that E is expected mutually, myristic acid, Palmic acid 1601, stearic acid, butylated hydroxytoluene, methyl hydroxybenzoate, propyl hydroxybenzoate and coconut monoethanol amide add in oil cauldron successively, are heated to 75~78 degree, keep constant temperature to be stirred to raw material and fully dissolve;
G, drop into successively maleic acid polymerized castor oil esteramides, olive oil, almond oil and the tocopherol acetas that F expects mutually carry out mix and blend 3 minutes in the solution of step f;
H, while stirring the material of oil cauldron is pumped in the emulsifying pot, first stirs 5~8 minutes with the rotating speed that stirs 650-700 rev/min; Then slowly add the material prepared in step a, and keep temperature 80~85 degree, adopt the mixing speed of 500-550 rev/min to carry out saponification stirring 30 minutes;
I, in the solution of step h, add 3800 pearlescent flake glycol distearates to be stirred to raw material all to dissolve;
J, on the basis of step I, drive water quench emulsifying pot, simultaneously mixing speed is down to 450~500 rev/mins; Make in the emulsifying pot to be cooled to 40 degree, then open internal recycle, rotating speed is 1600~1800 rev/mins, and the persistent period is 5~8 minutes;
K, the essence that adds successively the H phase in the solution of step j, yellow 5[CI19140], yellow 6[CI15985], Methylisothiazolinone, continue to stir cooling, cool to 35 degree and stop stirring when following; Finally make the pH value of solution reach 8.8~9.4, and viscosity reach 2300~2800mpa.s and get final product.
Further, described stirring is stirred when each step feeds intake.
Further, described stirring is stirred after each step feeds intake again.
Further, the preparation time of described a step is than the preparation time of g step Zao 6~12 hours.
The present invention's beneficial effect compared with prior art is:
1, the present invention adds polyquaternary ammonium salt-7, can greatly improve the sliding sense of smearing bath gel;
2, the present invention adds propylene glycol, VE, olive oil and almond oil, has both made skin wash very totally, can not make skin that dry sensation is arranged, and skin care effect is preferably arranged again, can make skin become more soft, lubricated:
3, the present invention adds lauroyl both sexes sodium acetate and methyl cocos nucifera oil sodium acyl taurine, greatly reduces the zest of bath gel to skin, can effectively protect skin.
[specific embodiment]
Below in conjunction with specific embodiment, describe the present invention, following embodiment and explanation only are used for explaining the present invention, but not as a limitation of the invention.
Embodiment 1:
Be equipped with 100kg bath gel of the present invention, formulated by the component of following weight:
Described bath gel is comprised of the component of following weight percent: A expects 15.46kg mutually, and B expects 9.69kg mutually, and C expects 18.2kg mutually, and D expects 29.5kg mutually; E expects 21.2kg mutually, and F expects 0.55kg mutually, and G expects 4kg mutually, and H expects 1.4kg mutually; Described A expects to be comprised of the component of following weight percent mutually: deionized water 10kg, potassium hydroxide 5.46kg; Described B expects to be comprised of the component of following weight percent mutually: deionized water 6.59kg, and EDTA-disodium 0.1kg, polyquaternary ammonium salt-7 account for 3kg; Described C expects to be comprised of the component of following weight percent mutually: deionized water 18kg, hydroxypropyl emthylcellulose 0.2kg; Described D expects to be comprised of the component of following weight percent mutually: glycerol 1kg, sodium laureth sulfate 4kg, lauryl alcohol both sexes sodium acetate 2kg, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 5kg, propylene glycol 12kg, SF-1 ACR emulsion 0.5kg, cocamido propyl betaine 5kg; Described E expects to be comprised of the component of following weight percent mutually: lauric acid 7kg, and myristic acid 5.8kg, Palmic acid 1601 accounts for 6kg, stearic acid 1kg, butylated hydroxytoluene 0.1kg, methyl hydroxybenzoate 0.2kg, propyl hydroxybenzoate 0.1kg, coconut monoethanol amide 1kg; Described F expects to be comprised of the component of following weight percent mutually: maleic acid polymerized castor oil esteramides 0.15kg, olive oil 0.1kg, almond oil 0.1kg, tocopherol acetas 0.2kg; Described G expects to be comprised of the 3800 pearlescent flake glycol distearates of 4kg mutually; Described H expects to be comprised of the component of following weight percent mutually: essence 1.3kg, yellow 5[CI19140] account for 0.00006kg, yellow 6[CI15985] account for 0.00006kg, Methylisothiazolinone 0.1kg.The purity of described potassium hydroxide is 90%; The active ingredient of described sodium laureth sulfate is 70%.
Be equipped with 100kg bath gel of the present invention, realize by following preparation technology: comprise the steps:
A, the deionized water 10kg during A is expected mutually put in plastic containers, and then gradation slowly adds potassium hydroxide 5.46kg, carry out stirring and dissolving even under the room temperature state; B, the deionized water 6.59kg during B is expected mutually, EDTA-disodium 0.1kg, polyquaternary ammonium salt-7 account for 3kg and drop into successively rustless steel and move in pot and stir 10 minutes, and each raw material is fully dissolved; C, the deionized water 18kg during C is expected mutually put into the emulsifying pot, then add hydroxypropyl emthylcellulose 0.2kg to be stirred, and mixing speed is 500~550 rev/mins, until solution is transparent and just stop stirring without precipitation; D, open internal recycle drop into successively glycerol 1kg that D expects mutually and sodium laureth sulfate 4kg in the solution of step c after, rotating speed is 2200-2500 rev/min, and the persistent period is 10~12 minutes; E, drop into successively material prepared by lauryl alcohol both sexes sodium acetate 2kg, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 5kg, propylene glycol 12kg, SF-1 ACR emulsion 0.5kg, cocamido propyl betaine 5kg and step b that D expects mutually in the solution of steps d, and be heated with stirring to 75~78 degree, keep constant temperature to be stirred to raw material and all dissolve; F, the lauric acid 7kg that E is expected mutually, the Palmic acid 1601 of myristic acid 5.8kg, 6kg, stearic acid 1kg, butylated hydroxytoluene 0.1kg, methyl hydroxybenzoate 0.2kg, propyl hydroxybenzoate 0.1kg, coconut monoethanol amide 1kg add in oil cauldron successively, be heated to 75~78 degree, keep constant temperature to be stirred to raw material and fully dissolve; G, drop into successively maleic acid polymerized castor oil esteramides 0.15kg, olive oil 0.1kg, almond oil 0.1kg, the tocopherol acetas 0.2kg that F expects mutually carry out mix and blend 3 minutes in the solution of step f; H, while stirring the material of oil cauldron is pumped in the emulsifying pot, first stirs 5~8 minutes with the rotating speed that stirs 650-700 rev/min; Then slowly add the material prepared in step a, and keep temperature 80~85 degree, adopt the mixing speed of 500-550 rev/min to carry out saponification stirring 30 minutes; I, in the solution of step h, add 3800 pearlescent flake glycol distearate 4kg to be stirred to raw material all to dissolve; J, on the basis of step I, drive water quench emulsifying pot, simultaneously mixing speed is down to 450~500 rev/mins; Make in the emulsifying pot to be cooled to 40 degree, then open internal recycle, rotating speed is 1600~1800 rev/mins, and the persistent period is 5~8 minutes; K, add successively the yellow 5[CI19140 of essence 1.3kg, the 0.00006kg of H phase in the solution of step j], the yellow 6[CI15985 of 0.00006kg], Methylisothiazolinone 0.1kg continues to stir cooling, cool to 35 degree and stop stirring when following; Finally make the pH value of solution reach 8.8~9.4, and viscosity reach 2300~2800mpa.s and get final product.
Described stirring is stirred when each step feeds intake.
Described stirring is stirred after each step feeds intake again.
The preparation time of described a step Zao 6~12 hours than the preparation time of g step.
Embodiment 2:
Be equipped with 100kg bath gel of the present invention, formulated by the component of following weight:
Described bath gel is comprised of the component of following weight percent: A expects 14.8kg mutually, and B expects 10.6kg mutually, and C expects 19.2kg mutually, and D expects 29.95kg mutually; E expects 20kg mutually, and F expects 0..55kg mutually, and G expects 3.5kg mutually, and H expects 1.4kg mutually; Described A expects to be comprised of the component of following weight percent mutually: deionized water 9kg, potassium hydroxide 5.8kg; Described B expects to be comprised of the component of following weight percent mutually: deionized water 7kg, and EDTA-disodium 0.1kg, polyquaternary ammonium salt-7 account for 3.5kg; Described C expects to be comprised of the component of following weight percent mutually: deionized water 19kg, hydroxypropyl emthylcellulose 0.2kg; Described D expects to be comprised of the component of following weight percent mutually: glycerol 0.5kg, sodium laureth sulfate 5kg, lauryl alcohol both sexes sodium acetate 1kg, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 6kg, propylene glycol 13kg, SF-1 ACR emulsion 0.45kg, cocamido propyl betaine 4kg; Described E expects to be comprised of the component of following weight percent mutually: lauric acid 7kg, and myristic acid 6kg, Palmic acid 1601 accounts for 5kg, stearic acid 0.8kg, butylated hydroxytoluene 0.1kg, methyl hydroxybenzoate 0.2kg, propyl hydroxybenzoate 0.1kg, coconut monoethanol amide 0.8kg; Described F expects to be comprised of the component of following weight percent mutually: maleic acid polymerized castor oil esteramides 0.15kg, olive oil 0.1kg, almond oil 0.1kg, tocopherol acetas 0.2kg; Described G expects to be comprised of the 3800 pearlescent flake glycol distearates of 3.5kg mutually; Described H expects to be comprised of the component of following weight percent mutually: the yellow 5[CI19140 of essence 1.3kg, 0.00006kg], the yellow 6[CI15985 of 0.00006kg], Methylisothiazolinone 0.1kg.The purity of described potassium hydroxide is 90%; The active ingredient of described sodium laureth sulfate is 70%.
Be equipped with 100kg bath gel of the present invention, realize by following preparation technology: comprise the steps:
A, the deionized water 9kg during A is expected mutually put in plastic containers, and then gradation slowly adds potassium hydroxide 5.8kg, carry out stirring and dissolving even under the room temperature state; The polyquaternary ammonium salt-7 of b, the deionized water 7kg during B is expected mutually, EDTA-disodium 0.1kg, 3.5kg drops into successively rustless steel and moves in pot and stir 10 minutes, and each raw material is fully dissolved; C, the deionized water 19kg during C is expected mutually put into the emulsifying pot, then add hydroxypropyl emthylcellulose 0.2kg to be stirred, and mixing speed is 500~550 rev/mins, until solution is transparent and just stop stirring without precipitation; D, open internal recycle drop into successively glycerol 0.5kg that D expects mutually and sodium laureth sulfate 5kg in the solution of step c after, rotating speed is 2200-2500 rev/min, and the persistent period is 10~12 minutes; E, drop into successively material prepared by lauryl alcohol both sexes sodium acetate 1kg, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 6kg, propylene glycol 13kg, SF-1 ACR emulsion 0.45kg, cocamido propyl betaine 4kg and step b that D expects mutually in the solution of steps d, and be heated with stirring to 75~78 degree, keep constant temperature to be stirred to raw material and all dissolve; F, the lauric acid 7kg that E is expected mutually, the Palmic acid 1601 of myristic acid 6kg, 5kg, stearic acid 0.8kg, butylated hydroxytoluene 0.1kg, methyl hydroxybenzoate 0.2kg, propyl hydroxybenzoate 0.1kg, coconut monoethanol amide 0.8kg add in oil cauldron successively, be heated to 75~78 degree, keep constant temperature to be stirred to raw material and fully dissolve; G, drop into successively the maleic acid polymerized castor oil esteramides 0.15kg that F expects mutually in the solution of step f, olive oil 0.1kg, almond oil 0.1kg, tocopherol acetas 0.2kg carry out mix and blend 3 minutes; H, while stirring the material of oil cauldron is pumped in the emulsifying pot, first stirs 5~8 minutes with the rotating speed that stirs 650-700 rev/min; Then slowly add the material prepared in step a, and keep temperature 80~85 degree, adopt the mixing speed of 500-550 rev/min to carry out saponification stirring 30 minutes; I, in the solution of step h, add 3800 pearlescent flake glycol distearate 3.5kg to be stirred to raw material all to dissolve; J, on the basis of step I, drive water quench emulsifying pot, simultaneously mixing speed is down to 450~500 rev/mins; Make in the emulsifying pot to be cooled to 40 degree, then open internal recycle, rotating speed is 1600~1800 rev/mins, and the persistent period is 5~8 minutes; K, add successively the yellow 5[CI19140 of essence 1.3kg, the 0.00006kg of H phase in the solution of step j], the yellow 6[CI15985 of 0.00006kg], Methylisothiazolinone 0.1kg continues to stir cooling, cool to 35 degree and stop stirring when following; Finally make the pH value of solution reach 8.8~9.4, and viscosity reach 2300~2800mpa.s and get final product.
Described stirring is stirred when each step feeds intake.
Described stirring is stirred after each step feeds intake again.
The preparation time of described a step Zao 6~12 hours than the preparation time of g step.
Embodiment 3:
Be equipped with 100kg bath gel of the present invention, formulated by the component of following weight:
Described bath gel is comprised of the component of following weight percent: A expects 16kg mutually, and B expects 8.4kg mutually, and C expects 17.3kg mutually, and D expects 29kg mutually; E expects 23.4kg mutually, and F expects 05kg mutually, and G expects 4kg mutually, and H expects 1.4kg mutually; Described A expects to be comprised of the component of following weight percent mutually: deionized water 11kg, potassium hydroxide 5kg; Described B expects to be comprised of the component of following weight percent mutually: deionized water 5.5kg, EDTA-disodium 0.1kg, the polyquaternary ammonium salt of 2.8kg-7; Described C expects to be comprised of the component of following weight percent mutually: deionized water 17kg, hydroxypropyl emthylcellulose 0.3kg; Described D expects to be comprised of the component of following weight percent mutually: glycerol 1.2kg, sodium laureth sulfate 3.8kg, lauryl alcohol both sexes sodium acetate 2.5kg, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 4kg, propylene glycol 10kg, SF-1 ACR emulsion 0.5kg, cocamido propyl betaine 7kg; Described E expects to be comprised of the component of following weight percent mutually: lauric acid 9kg, myristic acid 5kg, the Palmic acid 1601 of 6.5kg, stearic acid 1.3kg, butylated hydroxytoluene 0.1kg, methyl hydroxybenzoate 0.2kg, propyl hydroxybenzoate 0.1kg, coconut monoethanol amide 1.2kg; Described F expects to be comprised of the component of following weight percent mutually: maleic acid polymerized castor oil esteramides 0.1kg, olive oil 0.1kg, almond oil 0.1kg, tocopherol acetas 0.2kg; Described G expects to be comprised of the 3800 pearlescent flake glycol distearates of 4kg mutually; Described H expects to be comprised of the component of following weight percent mutually: essence 1.3kg, yellow 5[CI19140] account for 0.00006kg, yellow 6[CI15985] account for 0.00006kg, Methylisothiazolinone 0.1kg.The purity of described potassium hydroxide is 90%; The active ingredient of described sodium laureth sulfate is 70%.
Be equipped with 100kg bath gel of the present invention, realize by following preparation technology: comprise the steps:
A, the deionized water 11kg during A is expected mutually put in plastic containers, and then gradation slowly adds potassium hydroxide 5kg, carry out stirring and dissolving even under the room temperature state; B, the deionized water 5.5kg during B is expected mutually, EDTA-disodium 0.1kg, the polyquaternary ammonium salt of 2.8kg-7 are dropped into successively rustless steel and are moved in pot and stir 10 minutes, and each raw material is fully dissolved; C, the deionized water 17kg during C is expected mutually put into the emulsifying pot, then add hydroxypropyl emthylcellulose 0.3kg to be stirred, and mixing speed is 500~550 rev/mins, until solution is transparent and just stop stirring without precipitation; D, open internal recycle drop into successively glycerol 1.2kg that D expects mutually and sodium laureth sulfate 3.8kg in the solution of step c after, rotating speed is 2200-2500 rev/min, and the persistent period is 10~12 minutes; E, drop into successively the lauryl alcohol both sexes sodium acetate 2.5kg that D expects mutually in the solution of steps d, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 4kg, propylene glycol 10kg, SF-1 ACR emulsion 0.5kg, material prepared by cocamido propyl betaine 7kg and step b, and be heated with stirring to 75~78 degree, keep constant temperature to be stirred to raw material and all dissolve; The Palmic acid 1601 of f, the lauric acid 9kg that E is expected mutually, myristic acid 5kg, 6.5kg, stearic acid 1.3kg, butylated hydroxytoluene 0.1kg, methyl hydroxybenzoate 0.2kg, propyl hydroxybenzoate 0.1kg, coconut monoethanol amide 1.2kg; Add successively in oil cauldron, be heated to 75~78 degree, keep constant temperature to be stirred to raw material and fully dissolve; G, drop into successively maleic acid polymerized castor oil esteramides 0.1kg, olive oil 0.1kg, almond oil 0.1kg, the tocopherol acetas 0.2kg that F expects mutually carry out mix and blend 3 minutes in the solution of step f; H, while stirring the material of oil cauldron is pumped in the emulsifying pot, first stirs 5~8 minutes with the rotating speed that stirs 650-700 rev/min; Then slowly add the material prepared in step a, and keep temperature 80~85 degree, adopt the mixing speed of 500-550 rev/min to carry out saponification stirring 30 minutes; I, in the solution of step h, add the 3800 pearlescent flake glycol distearates of 4kg to be stirred to raw material all to dissolve; J, on the basis of step I, drive water quench emulsifying pot, simultaneously mixing speed is down to 450~500 rev/mins; Make in the emulsifying pot to be cooled to 40 degree, then open internal recycle, rotating speed is 1600~1800 rev/mins, and the persistent period is 5~8 minutes; K, the essence 1.3kg that adds successively the H phase in the solution of step j, yellow 5[CI19140] account for 0.00006kg, yellow 6[CI15985] account for 0.00006kg, Methylisothiazolinone 0.1kg and continue to stir cooling, cool to 35 degree and stop stirring when following; Finally make the pH value of solution reach 8.8~9.4, and viscosity reach 2300~2800mpa.s and get final product.
Described stirring is stirred when each step feeds intake.
Described stirring is stirred after each step feeds intake again.
The preparation time of described a step Zao 6~12 hours than the preparation time of g step.
The above is only in order to convenient explanation the present invention, and in the spiritual category that does not break away from the present invention's creation, that is familiar with that those skilled in the art of this technology does various simple in a disguised form should belong to protection scope of the present invention with modification.

Claims (7)

1. a formula of bath cream, it is characterized in that: described bath gel is comprised of the component of following weight percent: A expects that 10~18%, B expects that 8~12%, C expects that 15~22%, D expects 26~33% mutually mutually mutually mutually; E expects that 18~25%, F expects that 0.1~1%, G expects that 2~7%, H expects 1~3% mutually mutually mutually mutually;
Described A expects to be comprised of the component of following weight percent mutually: deionized water 55~70%, potassium hydroxide 30~40%;
Described B expects to be comprised of the component of following weight percent mutually: deionized water 60~75%, and EDTA-disodium 0.5~2%, polyquaternary ammonium salt-7 account for 25~38%;
Described C expects to be comprised of the component of following weight percent mutually: deionized water 98~99.5%, hydroxypropyl emthylcellulose 0.3~2%;
Described D expects to be comprised of the component of following weight percent mutually: glycerol 1~5%, sodium laureth sulfate 10~20%, lauryl alcohol both sexes sodium acetate 5~10%, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium 15~20%, propylene glycol 38~45%, SF-1 ACR emulsion 1~5%, cocamido propyl betaine 15~20%;
Described E expects to be comprised of the component of following weight percent mutually: lauric acid 30~40%, and myristic acid 24~30%, Palmic acid 1601 accounts for 25~30%, stearic acid 1~8%, butylated hydroxytoluene 0.1~1%, methyl hydroxybenzoate 0.5~2%, propyl hydroxybenzoate 0.1~1%, coconut monoethanol amide 3~9%;
Described F expects to be comprised of the component of following weight percent mutually: maleic acid polymerized castor oil esteramides 23~30%, olive oil 15~22%, almond oil 15~22%, tocopherol acetas 30~40%;
Described G expects to be 3800 pearlescent flake glycol distearates mutually;
Described H expects to be comprised of the component of following weight percent mutually: essence 90~96%, yellow 5[CI19140] account for 0.001~0.006%, yellow 6[CI15985] account for 0.001~0.007%, Methylisothiazolinone 3~10%.
2. a kind of formula of bath cream according to claim 1, it is characterized in that: the purity of described potassium hydroxide is 90%.
3. a kind of formula of bath cream according to claim 1, it is characterized in that: the active ingredient of described sodium laureth sulfate is 70%.
4. a bath gel preparation technology, is characterized in that, comprises the steps:
A, the deionized water during A is expected are mutually put in plastic containers, and then gradation slowly adds potassium hydroxide, carry out stirring and dissolving even under the room temperature state;
B, the various raw materials during B is expected mutually drop into successively rustless steel and move in pot and stir 10 minutes, and each raw material is fully dissolved;
C, the deionized water during C is expected are mutually put into the emulsifying pot, then add hydroxypropyl emthylcellulose to be stirred, and mixing speed is 500~550 rev/mins, until solution is transparent and just stop stirring without precipitation;
D, open internal recycle drop into successively glycerol that D expects mutually and sodium laureth sulfate in the solution of step c after, rotating speed is 2200-2500 rev/min, and the persistent period is 10~12 minutes;
E, drop into successively material prepared by lauryl alcohol both sexes sodium acetate, N-methyltaurine cocos nucifera oil acyl methyl taurine ester sodium, propylene glycol, SF-1 ACR emulsion, cocamido propyl betaine and step b that D expects mutually in the solution of steps d, and be heated with stirring to 75~78 degree, keep constant temperature to be stirred to raw material and all dissolve;
F, the lauric acid that E is expected mutually, myristic acid, Palmic acid 1601, stearic acid, butylated hydroxytoluene, methyl hydroxybenzoate, propyl hydroxybenzoate and coconut monoethanol amide add in oil cauldron successively, are heated to 75~78 degree, keep constant temperature to be stirred to raw material and fully dissolve;
G, drop into successively maleic acid polymerized castor oil esteramides, olive oil, almond oil and the tocopherol acetas that F expects mutually carry out mix and blend 3 minutes in the solution of step f;
H, while stirring the material of oil cauldron is pumped in the emulsifying pot, first stirs 5~8 minutes with the rotating speed that stirs 650-700 rev/min; Then slowly add the material prepared in step a, and keep temperature 80~85 degree, adopt the mixing speed of 500-550 rev/min to carry out saponification stirring 30 minutes;
I, in the solution of step h, add 3800 pearlescent flake glycol distearates to be stirred to raw material all to dissolve;
J, on the basis of step I, drive water quench emulsifying pot, simultaneously mixing speed is down to 450~500 rev/mins; Make in the emulsifying pot to be cooled to 40 degree, then open internal recycle, rotating speed is 1600~1800 rev/mins, and the persistent period is 5~8 minutes;
K, the essence that adds successively the H phase in the solution of step j, yellow 5[CI19140], yellow 6[CI15985], Methylisothiazolinone, continue to stir cooling, cool to 35 degree and stop stirring when following; Finally make the pH value of solution reach 8.8~9.4, and viscosity reach 2300~2800mpa.s and get final product.
5. a kind of bath gel preparation technology according to claim 4, is characterized in that, described stirring is stirred when each step feeds intake.
6. a kind of bath gel preparation technology according to claim 4, is characterized in that, described stirring is stirred after each step feeds intake again.
7. a kind of bath gel preparation technology according to claim 4, is characterized in that the preparation time of described a step Zao 6~12 hours than the preparation time of g step.
CN2013103674548A 2013-08-19 2013-08-19 Shower gel formulation and preparation technology thereof Pending CN103417407A (en)

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CN109833219A (en) * 2019-04-02 2019-06-04 广东六芙生物科技有限公司 A kind of easy cleaning is water-saving to moisten compound shower cream and its manufacture craft
CN111297721A (en) * 2019-11-16 2020-06-19 广东科誉新材料有限公司 Application of hydroxyethyl diphosphate in soap-based shower gel

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Application publication date: 20131204