CN108125868B - Refreshing shower gel and preparation method thereof - Google Patents
Refreshing shower gel and preparation method thereof Download PDFInfo
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- CN108125868B CN108125868B CN201810096154.3A CN201810096154A CN108125868B CN 108125868 B CN108125868 B CN 108125868B CN 201810096154 A CN201810096154 A CN 201810096154A CN 108125868 B CN108125868 B CN 108125868B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses refreshing shower gel which is prepared from the following raw materials in percentage by mass: 5-10% of lauric acid, 2-5% of myristic acid, 1-3% of stearic acid, 1-3% of potassium hydroxide, 0.5-2% of sodium cocoyl glycinate, 3-8% of glycerol, 0.2-0.5% of xanthan gum, 0.2-0.5% of hydroxypropyl methylcellulose, 0.5-0.5% of carbopol 9340.2, 0.2-0.5% of MELALEUCA leucadron CAJAPUT (MELALEUCA leucadondron CAJAPUT) oil and 0.2-0.5% of juga burley (sclerocarpa BIRREA) seed oil. The thickening agent adopted by the refreshing shower gel is a compound composition which mainly contains organic natural polymer xanthan gum, organic semi-synthetic water-soluble polymer hydroxypropyl methyl cellulose, carbopol 934 and natural plant extract oil. The thickener composition in the shower gel fully utilizes the synergistic effect of various components, and greatly improves the thickening effect of a soap base system.
Description
Technical Field
The invention relates to the technical field of daily chemical industry, and particularly relates to refreshing shower gel and a preparation method thereof.
Background
In recent years, with the improvement of daily life of people, the shower gel gradually replaces the perfumed soap, and as the shower gel is more convenient and safer to use, a user can select shower gel products more when bathing and showering. Previously, shower gel products generally seen in the market only have washing and sterilizing effects, but at the present stage, the requirement of people on the use comfort of the shower gel is higher and higher, and the higher and higher requirement is provided for formula engineers: rich foam, good cleaning ability, high mildness and refreshing skin feel after bathing. At present, in the aspect of bath cream formulation technology, the main formulation systems of the bath cream mainly comprise two types, and the two types of bath creams have the defects, wherein the main surfactant, namely, anionic surfactant represented by sulfate, such as lauryl alcohol ether sulfate, lauryl alcohol sulfate and the like, and the surface active type bath cream compounded with other acceptable components have the defects that the skin feeling after bathing is not fresh enough, and the feeling of washing is not clean for the old; the second is saponification type bath lotion which is prepared by soap base formed by saponifying fatty acid and potassium hydroxide or sodium hydroxide and other acceptable components; the disadvantages are that the formulation is difficult to thicken and the skin feels tight after bathing.
At present, the prior art has disclosed some technical schemes of soap-based system body wash with better thickening effect, for example, chinese patent application with publication number CN105213220A discloses a refreshing body wash, which contains 5-10% by weight of distearyl polyether-75 IPDI as thickener and emollient, solves the disadvantage of difficult thickening of the saponification type body wash, and has abundant foam and refreshing skin feel after washing. However, the thickening agent is purchased from ALZO International Inc. in the United states, and is named Dermothix 75, so that the price is high, the production cost of the shower gel product is high, and the requirements of most of low-consumption-level people cannot be met. Therefore, the development of a soap-based system shower gel which can replace Dermothix 75, is low in price and has a better thickening effect is an urgent need of the technicians in the field.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the soap-based system refreshing shower gel which can replace Dermothix 75, is low in price and has a better thickening effect. The invention is realized by the following technical scheme:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 5-10%
Myristic acid 2-5%
Stearic acid 1-3%
1 to 3 percent of potassium hydroxide
Coconut oil acyl sodium glycinate 0.5-2%
3-8% of glycerin
Xanthan gum 0.2-0.5%
Hydroxypropyl methylcellulose 0.2-0.5%
Carbolpol 934 0.2-0.5%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.2-0.5%
Semen Juglandis Billericae (SCLOCARYA BIRREA) oil 0.2-0.5%
Deionized water was added to 100%.
Preferably, the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 5%
Myristic acid 5%
Stearic acid 1%
3 percent of potassium hydroxide
Cocoyl sodium glycinate 0.5%
8 percent of glycerin
Xanthan gum 0.2%
Hydroxypropyl methylcellulose 0.5%
Carbolpol 934 0.2%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.5%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.2%
Deionized water was added to 100%.
Preferably, the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 10%
Myristic acid 2%
Stearic acid 3%
1 percent of potassium hydroxide
2 percent of cocoyl sodium glycinate
3 percent of glycerin
Xanthan gum 0.5%
Hydroxypropyl methylcellulose 0.2%
Carbolpol 934 0.5%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.2%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.5%
Deionized water was added to 100%.
Preferably, the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.3%
Hydroxypropyl methylcellulose 0.3%
Carbolpol 934 0.3%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.3%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.3%
Deionized water was added to 100%.
The preparation method of the refreshing shower gel comprises the following steps: adding deionized water into a reaction kettle, heating to 80-85 deg.C, adding glycerol and potassium hydroxide, stirring and dispersing at 40-60R/min, adding lauric acid, myristic acid, stearic acid, xanthan gum, hydroxypropyl methylcellulose, carbopol 934, Melaleuca leucadendra (Melaleuca leucadendra) oil and Perilla seed oil, maintaining the rotation speed to completely disperse the substances, stirring for 20-30 min, and cooling; when the temperature is reduced to 40-50 ℃, adding the cocoyl sodium glycinate, and continuously stirring for 10-30 minutes to obtain a uniform mixture, namely a finished product. During actual production, a proper amount of essence and preservative can be added according to the requirement.
The Melaleuca leucadendra CAJAPUT oil and the Perilla frutescens (sclerocaraya birera) seed oil in the invention are conventional cosmetic raw materials and can be obtained commercially.
Compared with the prior art, the invention has the beneficial effects that: the refreshing shower gel is a soap-based formula system, adopts a thickener which is a compound composition and mainly contains organic natural polymer xanthan gum, organic semi-synthetic water-soluble polymer hydroxypropyl methyl cellulose, carbopol 934 and specific natural plant extract oil. The thickener composition in the shower gel disclosed by the invention fully utilizes the synergistic effect of various components, greatly improves the thickening effect of a soap base system, can completely replace distearyl polyether-75 IPDI in the prior art, is more excellent in thickening effect, does not influence the refreshing effect of a shower gel product, and provides a new technical scheme for the technical field of daily chemical industry.
Detailed Description
The present invention will be further specifically described with reference to the following examples.
Example 1:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 5%
Myristic acid 5%
Stearic acid 1%
3 percent of potassium hydroxide
Cocoyl sodium glycinate 0.5%
8 percent of glycerin
Xanthan gum 0.2%
Hydroxypropyl methylcellulose 0.5%
Carbolpol 934 0.2%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.5%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.2%
Deionized water was added to 100%.
The preparation method of the shower gel comprises the following steps: adding deionized water into a reaction kettle, heating to 80 deg.C, adding glycerol and potassium hydroxide, stirring and dispersing at 50R/min, adding lauric acid, myristic acid, stearic acid, xanthan gum, hydroxypropyl methylcellulose, carbopol 934, Melaleuca leucadendra CAJAPUT (Melaleuca leucadendra) oil and Burkholderia walnut (Schlerocarya birecana) seed oil, maintaining the rotation speed to completely disperse the above substances, stirring for 20 min, and cooling; when the temperature is reduced to 45 ℃, adding the cocoyl sodium glycinate, and continuously stirring for 20 minutes to obtain a uniform mixture, namely a finished product.
Example 2:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 10%
Myristic acid 2%
Stearic acid 3%
1 percent of potassium hydroxide
2 percent of cocoyl sodium glycinate
3 percent of glycerin
Xanthan gum 0.5%
Hydroxypropyl methylcellulose 0.2%
Carbolpol 934 0.5%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.2%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.5%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Example 3:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.3%
Hydroxypropyl methylcellulose 0.3%
Carbolpol 934 0.3%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.3%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.3%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Comparative example 1:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Hydroxypropyl methylcellulose 0.4%
Carbolpol 934 0.35%
Melaleuca alternifolia (Melaleuca LEUCADENDRON CAJAPUT) oil 0.35%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.4%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Comparative example 1 increased the amount of hydroxypropyl methylcellulose, carbopol 934, MELALEUCA LEUCADENDRON CAJAPUT oil, and sclareca burreya BIRREA seed oil, compared to example 3 without the addition of xanthan gum.
Comparative example 2:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.35%
Carbolpol 934 0.35%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.4%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.4%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Comparative example 2 the amounts of xanthan gum, carbopol 934, MELALEUCA LEUCADENDRON CAJAPUT oil, and sclareca buryan (sclerocara BIRREA) seed oil were increased compared to example 3 without the addition of hydroxypropyl methylcellulose.
Comparative example 3:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.4%
Hydroxypropyl methylcellulose 0.4%
Melaleuca alternifolia (Melaleuca LEUCADENDRON CAJAPUT) oil 0.35%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.35%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Comparative example 3 the amounts of xanthan gum, hydroxypropyl methylcellulose, MELALEUCA leucadron CAJAPUT oil, and burkholdia nut (SCLEROCARYA BIRREA) seed oil were increased compared to example 3 without the addition of carbopol 934.
Comparative example 4:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.4%
Hydroxypropyl methylcellulose 0.4%
Carbolpol 934 0.35%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.35%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Comparative example 4 the amount of xanthan gum, hydroxypropyl methylcellulose, carbopol 934, and sclareca (sclerocarpa BIRREA) seed oil was increased compared to example 3 without the addition of MELALEUCA leucadron oil.
Comparative example 5:
the refreshing shower gel is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.4%
Hydroxypropyl methylcellulose 0.4%
Carbolpol 934 0.35%
Melaleuca alternifolia (Melaleuca LEUCADENDRON CAJAPUT) oil 0.35%
Deionized water was added to 100%.
The preparation method of the shower gel is the same as that of example 1.
Comparative example 5 the amount of xanthan gum, hydroxypropyl methylcellulose, carbopol 934, cajeput (MELALEUCA leucadron CAJAPUT) oil was increased compared to example 3 without the addition of bushy walnut (sclerocara BIRREA) seed oil.
Firstly, the viscosity test of the shower gel of the embodiments 1 to 3 and the comparative examples 1 to 5 of the invention is as follows:
the results of the tests using the Brookfield viscometer are shown in Table 1:
TABLE 1
| Viscosity (mPa. s) | |
| Example 1 | 9450 |
| Example 2 | 9630 |
| Example 3 | 11200 |
| Comparative example 1 | 6500 |
| Comparative example 2 | 5300 |
| Comparative example 3 | 4500 |
| Comparative example 4 | 6850 |
| Comparative example 5 | 7160 |
Secondly, the use effect comparison tests of the shower gel of the embodiments 1 to 3 and the comparative examples 1 to 5 of the invention are as follows:
160 volunteers, 80 male and female in summer, and 25-56 years old are selected as construction workers, and have no skin diseases and allergic history. The volunteers were randomly and equally divided into 8 groups of 20 individuals, and each group was not statistically different and was comparable. The shower gel of the examples 1-3 and the shower gel of the comparative examples 1-5 are respectively used for each test component, the shower gel is used for 1 time every night, the shower gel is continuously used for 7 days, the volunteers score according to the feeling after use, the scoring standard adopts a score of 5, 1 score (skin is tight or itchy) represents the worst, 5 scores (skin is comfortable, fresh and has no reaction) represents the best, and the higher the score is, the better the effect is. The statistical results for each group were averaged as shown in table 2:
TABLE 2
| Scoring | |
| Example 1 | 4.3 |
| Example 2 | 4.5 |
| Example 3 | 4.9 |
| Comparative example 1 | 3.2 |
| Comparative example 2 | 3.6 |
| Comparative example 3 | 3.4 |
| Comparative example 4 | 3.3 |
| Comparative example 5 | 3.1 |
The test results show that the thickening agent adopted by the shower gel of the embodiments 1 to 3 is compounded by an organic natural polymer xanthan gum, an organic semisynthetic water-soluble polymer hydroxypropyl methylcellulose, carbopol 934 and two specific natural plant extract oils, and compared with the shower gel of the comparative examples 1 to 5 which does not completely contain the components, the shower gel has a better thickening effect and is more refreshing and comfortable to use. The thickener composition in the shower gel fully utilizes the synergistic effect of various components, greatly improves the thickening effect of a soap base system, has a refreshing and comfortable use effect, and obtains the technical effect which is not expected by technical personnel in the field.
The above-mentioned embodiments are merely preferred embodiments of the present invention, and the scope of the present invention should not be limited thereby, and those skilled in the art should not make any insubstantial changes and substitutions based on the present invention.
Claims (5)
1. The refreshing shower gel is characterized by being prepared from the following raw materials in percentage by mass:
lauric acid 5-10%
Myristic acid 2-5%
Stearic acid 1-3%
1 to 3 percent of potassium hydroxide
Coconut oil acyl sodium glycinate 0.5-2%
3-8% of glycerin
Xanthan gum 0.2-0.5%
Hydroxypropyl methylcellulose 0.2-0.5%
Carbolpol 934 0.2-0.5%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.2-0.5%
Semen Juglandis Billericae (SCLOCARYA BIRREA) oil 0.2-0.5%
Deionized water was added to 100%.
2. The refreshing shower gel according to claim 1, which is prepared from the following raw materials in percentage by mass:
lauric acid 5%
Myristic acid 5%
Stearic acid 1%
3 percent of potassium hydroxide
Cocoyl sodium glycinate 0.5%
8 percent of glycerin
Xanthan gum 0.2%
Hydroxypropyl methylcellulose 0.5%
Carbolpol 934 0.2%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.5%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.2%
Deionized water was added to 100%.
3. The refreshing shower gel according to claim 1, which is prepared from the following raw materials in percentage by mass:
lauric acid 10%
Myristic acid 2%
Stearic acid 3%
1 percent of potassium hydroxide
2 percent of cocoyl sodium glycinate
3 percent of glycerin
Xanthan gum 0.5%
Hydroxypropyl methylcellulose 0.2%
Carbolpol 934 0.5%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.2%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.5%
Deionized water was added to 100%.
4. The refreshing shower gel according to claim 1, which is prepared from the following raw materials in percentage by mass:
lauric acid 7%
Myristic acid 3%
Stearic acid 2%
2 percent of potassium hydroxide
1 percent of cocoyl sodium glycinate
5 percent of glycerin
Xanthan gum 0.3%
Hydroxypropyl methylcellulose 0.3%
Carbolpol 934 0.3%
Melaleuca leucadendra (Melaleuca leucadendra CAJAPUT) oil 0.3%
Perch hard walnut (SCLOCARYA BIRREA) seed oil 0.3%
Deionized water was added to 100%.
5. The method of preparing a refreshing body wash according to any one of claims 1 to 4, characterized in that the method of preparation is as follows: adding deionized water into a reaction kettle, heating to 80-85 deg.C, adding glycerol and potassium hydroxide, stirring and dispersing at 40-60R/min, adding lauric acid, myristic acid, stearic acid, xanthan gum, hydroxypropyl methylcellulose, carbopol 934, Melaleuca leucadendra (Melaleuca leucadendra) oil and Perilla seed oil, maintaining the rotation speed to completely disperse the substances, stirring for 20-30 min, and cooling; when the temperature is reduced to 40-50 ℃, adding the cocoyl sodium glycinate, and continuously stirring for 10-30 minutes to obtain a uniform mixture, namely a finished product.
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| CN105213220A (en) * | 2015-09-22 | 2016-01-06 | 拉芳家化股份有限公司 | A kind of salubrious bath gel |
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| DE102016209964A1 (en) * | 2016-06-07 | 2017-12-07 | Henkel Ag & Co. Kgaa | Cold cream containing stable cosmetic cleansing compositions |
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2018
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|---|---|---|---|---|
| WO2009085058A1 (en) * | 2007-12-27 | 2009-07-09 | Guthy-Renker Corporation | Cosmetic cleanser |
| CN106456522A (en) * | 2014-03-24 | 2017-02-22 | 拜洛嘉有限责任公司 | Formulation for personal hygiene |
| CN105213220A (en) * | 2015-09-22 | 2016-01-06 | 拉芳家化股份有限公司 | A kind of salubrious bath gel |
| CN107638322A (en) * | 2016-07-20 | 2018-01-30 | 江苏欧佩日化股份有限公司 | A kind of shower cream |
| CN107296773A (en) * | 2017-08-08 | 2017-10-27 | 林秀凤 | A kind of salubrious shower cream |
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