CN108740341A - It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology - Google Patents

It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology Download PDF

Info

Publication number
CN108740341A
CN108740341A CN201810347556.6A CN201810347556A CN108740341A CN 108740341 A CN108740341 A CN 108740341A CN 201810347556 A CN201810347556 A CN 201810347556A CN 108740341 A CN108740341 A CN 108740341A
Authority
CN
China
Prior art keywords
beet pulp
mesh sieve
copper
crushed
additive
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810347556.6A
Other languages
Chinese (zh)
Inventor
杨琳芬
符金华
徐国茂
李勇
夏骏
李瑾瑾
李俊
李旭荣
刘景湖
胡祥
叶春华
吴科盛
陈桂平
金海红
邓宇
霍光华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGXI HUANONG HENGQING AGRICULTURE ANIMAL AND HUSBANDRY CO Ltd
JIANGXI KENUO BIOTECHNOLOGY Co Ltd
Jiangxi Veterinary Drug Feed Supervision Institute
Original Assignee
JIANGXI HUANONG HENGQING AGRICULTURE ANIMAL AND HUSBANDRY CO Ltd
JIANGXI KENUO BIOTECHNOLOGY Co Ltd
Jiangxi Veterinary Drug Feed Supervision Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIANGXI HUANONG HENGQING AGRICULTURE ANIMAL AND HUSBANDRY CO Ltd, JIANGXI KENUO BIOTECHNOLOGY Co Ltd, Jiangxi Veterinary Drug Feed Supervision Institute filed Critical JIANGXI HUANONG HENGQING AGRICULTURE ANIMAL AND HUSBANDRY CO Ltd
Priority to CN201810347556.6A priority Critical patent/CN108740341A/en
Publication of CN108740341A publication Critical patent/CN108740341A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/24Compounds of alkaline earth metals, e.g. magnesium
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/37Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/163Sugars; Polysaccharides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/28Silicates, e.g. perlites, zeolites or bentonites
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/30Oligoelements
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Animal Husbandry (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Molecular Biology (AREA)
  • Mycology (AREA)
  • Physiology (AREA)
  • Fodder In General (AREA)

Abstract

Feed Copper, the additive of zinc usage amount and its production technology are reduced the present invention provides a kind of, belongs to feed additive field.The additive is by clay-activity copper and carrier in mass ratio 1:5-8 is formed;The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp 6-9 in mass ratio:1-2:10-15:8-12.The Additive Production is simple for process, operating condition is mild, high recycling rate, additive application in feed can reduce the copper additive amount of 20%-50% in feed and 50% Zinc supplementation, and keep production performance constant, the heavy metal pollution during livestock and poultry cultivation is reduced, there is good application prospect.

Description

It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology
Technical field
The present invention relates to feed additive field more particularly to a kind of additions reducing Feed Copper, zinc usage amount Agent and its production technology.
Background technology
Feed addictive refers to a small amount of or micro substance added during Feed Manufacturing processing, use, feed addition Dosage is seldom in feed but effect is notable for agent.Feed addictive is the raw material that modern feed industry necessarily uses, to strengthening base Plinth feed nutritive value improves breeding performonce fo animals, ensures animal health, saves feed cost, improves the side such as livestock products quality Face has obvious effects on.Zinc oxide as a kind of common feed addictive, play the role of it is very positive, such as research shows that 2500-4000mg/kg zinc is added in early-weaned piglets daily ration, can significantly reduce the diarrhea rate of piglet.But with oxidation Zinc also brings the problem of series in the application of feed, for example high zinc can inhibit piglet to the absorption of iron, reduces the immune of piglet Ability leads to slightly long random, the skin tarnish of piglet hair.Most important is exactly the common zinc oxide that conventional method is process, It is often accompanied by heavy metals exceeding standard, the problems such as absorptivity is low, a large amount of unabsorbed zinc oxide are excreted with excrement, to soil, water Body etc. causes seriously to pollute.
Research shows that adding the copper sulphate of 250mg/kg in feed, there is 95% or more copper ion to be absorbed and utilized, it is a large amount of in this way Copper by metabolic cycles, a part is deposited in body tissue, and significant fraction is excreted(90%), this is not only resulted in Animal body slow poisoning, tissue residue increase the waste with resource, it is often more important that animal tissue remains and a large amount of excretion meetings Very important influence and harm are come to the mankind and entire ecological chain health care belt.
Clay-activity copper with poultry, aquatic products and other animals, can improve as feed addictive first Application Intestinal flora;By controlling pathogenic flora and the growth of beneficial bacterium being promoted to prevent flora imbalance;Promote digestion and absorbs;Reduce poultry Heavy metal pollution in fowl breeding process, is good for the environment in this way, has very big utilization background.
Invention content
The object of the present invention is to provide it is a kind of reduce Feed Copper, zinc usage amount additive, the use of the additive The copper additive amount of 20%-50% in feed and 50% Zinc supplementation can be reduced, and keeps production performance constant, is supported to reducing livestock and poultry Heavy metal pollution during growing has very big help.
It is a further object of the present invention to provide the production technologies of the additive.
It is a kind of reduce Feed Copper, zinc usage amount additive, by clay-activity copper and carrier in mass ratio 1:5-8 groups At;
The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp 6-9 in mass ratio:1-2:10-15:8-12;
The calcium carbonate crushed 1300 mesh sieve;
The glucose crushed 1200 mesh sieve;
The wheat-middlings crushed 1300 mesh sieve.
It is heretofore described it is a kind of reduce Feed Copper, zinc usage amount additive, production technology is:
(One)The preparation of clay-activity copper:
(1)Montmorillonite crude product is crushed, 180 mesh sieve is crossed, by solid-to-liquid ratio 1:Deionized water is added in 6-8, and 2h is stirred under the conditions of 80 DEG C, It is then allowed to stand 2h;Impurities at bottom is removed, is then filtered, drying and crushing crosses 400 mesh sieve, obtains pretreatment montmorillonite;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment montmorillonite:Deionized water is added in 4-5, stirs evenly, obtains suspension ore pulp, then adds Enter CuSO4·5H2O and sodium carbonate, addition are to pre-process the 13-18% and 4-7% of montmorillonite quality;It is stirred under the conditions of 55 DEG C 16h;Filtering, filter residue are washed with deionized 5 times;
(3)Filter residue is dried in vacuo, 60 DEG C of drying temperature, crushed 1500 mesh sieve to get clay-activity copper;
(Two)The preparation of refined beet pulp:
(1)By beet pulp dries pulverizing, 80 mesh sieve is crossed, by solid-to-liquid ratio 1:10% sodium hydroxide solution, 50 DEG C of immersions are added in 3-5 Then 2h is filtered, filter residue is washed with distilled water 5 times, pretreatment beet pulp is obtained;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment beet pulp:A concentration of 75% ethanol solution is added in 10-14, flows back under the conditions of 45 DEG C 2h is extracted, then ethanol solution is volatilized using Rotary Evaporators, obtains alcohol processing beet pulp, alcohol processing beet pulp is used into steam 2h is handled, is then dried in vacuo, crushed 1200 mesh sieve to get refined beet pulp;
(Three)Clay-activity copper is uniformly mixed with calcium carbonate, glucose, wheat-middlings and refined beet pulp, you can.
The present invention it is a kind of reduce Feed Copper, zinc usage amount additive, wherein content of copper ion >=1250ppm;Production Product grain size:1-11 μm, homogeneity is good;Surface area >=800 ㎡/g.
It is of the present invention it is a kind of reduce Feed Copper, zinc usage amount additive amount of the additive in feed:200g/ T。
Advantageous effect
(1)The present invention is used processed through industrial machinery obtained from montmorillonite crude product for raw material, wide raw material source, price are low It is honest and clean;
(2)Compared with prior art, the present invention its simple production process, equipment are easy to get, production cost is low, high recycling rate, It is environmental;
(3)Intestinal flora can be improved;By controlling pathogenic flora and the growth of beneficial bacterium being promoted to prevent flora imbalance;Promote Digestion and absorption;Improve livestock and poultry production performance;The copper additive amount of 20%-50% in feed and 50% Zinc supplementation can be reduced, and is protected It is constant to hold production performance;Reduce the heavy metal pollution during livestock and poultry cultivation.It is good for the environment in this way, there is very big exploitation Utility value.
Specific implementation mode
Embodiment 1
It is a kind of reduce Feed Copper, zinc usage amount additive, by clay-activity copper and carrier in mass ratio 1:5 compositions;
The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp in mass ratio 6:1:10:8;
The calcium carbonate crushed 1300 mesh sieve;
The glucose crushed 1200 mesh sieve;
The wheat-middlings crushed 1300 mesh sieve.
It is heretofore described it is a kind of reduce Feed Copper, zinc usage amount additive, production technology is:
(One)The preparation of clay-activity copper:
(1)Montmorillonite crude product is crushed, 180 mesh sieve is crossed, by solid-to-liquid ratio 1:6 are added deionized water, stir 2h under the conditions of 80 DEG C, so After stand 2h;Impurities at bottom is removed, is then filtered, drying and crushing crosses 400 mesh sieve, obtains pretreatment montmorillonite;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment montmorillonite:4 are added deionized water, stir evenly, obtain suspension ore pulp, be then added CuSO4·5H2O and sodium carbonate, addition are pre-process montmorillonite quality 13% and 4%;16h is stirred under the conditions of 55 DEG C;It crosses Filter, filter residue are washed with deionized 5 times;
(3)Filter residue is dried in vacuo, 60 DEG C of drying temperature, crushed 1500 mesh sieve to get clay-activity copper;
(Two)The preparation of refined beet pulp:
(1)By beet pulp dries pulverizing, 80 mesh sieve is crossed, by solid-to-liquid ratio 1:3 are added 10% sodium hydroxide solution, and 50 DEG C are impregnated 2h, Then it filters, filter residue is washed with distilled water 5 times, pretreatment beet pulp is obtained;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment beet pulp:10 are added a concentration of 75% ethanol solution, refluxing extraction under the conditions of 45 DEG C Then 2h is volatilized ethanol solution using Rotary Evaporators, alcohol processing beet pulp is obtained, and alcohol processing beet pulp is used steam treatment Then 2h is dried in vacuo, crushed 1200 mesh sieve to get refined beet pulp;
(Three)Clay-activity copper is uniformly mixed with calcium carbonate, glucose, wheat-middlings and refined beet pulp, you can.
The present invention it is a kind of reduce Feed Copper, zinc usage amount additive, wherein content of copper ion >=1250ppm;Production Product grain size:1-11 μm, homogeneity is good;Surface area >=800 ㎡/g.
It is of the present invention it is a kind of reduce Feed Copper, zinc usage amount additive amount of the additive in feed:200g/T.
Embodiment 2
It is a kind of reduce Feed Copper, zinc usage amount additive, by clay-activity copper and carrier in mass ratio 1:7 compositions;
The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp in mass ratio 8:2:13:10;
The calcium carbonate crushed 1300 mesh sieve;
The glucose crushed 1200 mesh sieve;
The wheat-middlings crushed 1300 mesh sieve.
It is heretofore described it is a kind of reduce Feed Copper, zinc usage amount additive, production technology is:
(One)The preparation of clay-activity copper:
(1)Montmorillonite crude product is crushed, 180 mesh sieve is crossed, by solid-to-liquid ratio 1:7 are added deionized water, stir 2h under the conditions of 80 DEG C, so After stand 2h;Impurities at bottom is removed, is then filtered, drying and crushing crosses 400 mesh sieve, obtains pretreatment montmorillonite;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment montmorillonite:5 are added deionized water, stir evenly, obtain suspension ore pulp, then add Enter CuSO4·5H2O and sodium carbonate, addition are pre-process montmorillonite quality 16% and 6%;16h is stirred under the conditions of 55 DEG C;It crosses Filter, filter residue are washed with deionized 5 times;
(3)Filter residue is dried in vacuo, 60 DEG C of drying temperature, crushed 1500 mesh sieve to get clay-activity copper;
(Two)The preparation of refined beet pulp:
(1)By beet pulp dries pulverizing, 80 mesh sieve is crossed, by solid-to-liquid ratio 1:4 are added 10% sodium hydroxide solution, and 50 DEG C are impregnated 2h, Then it filters, filter residue is washed with distilled water 5 times, pretreatment beet pulp is obtained;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment beet pulp:12 are added a concentration of 75% ethanol solution, refluxing extraction under the conditions of 45 DEG C Then 2h is volatilized ethanol solution using Rotary Evaporators, alcohol processing beet pulp is obtained, and alcohol processing beet pulp is used steam treatment Then 2h is dried in vacuo, crushed 1200 mesh sieve to get refined beet pulp;
(Three)Clay-activity copper is uniformly mixed with calcium carbonate, glucose, wheat-middlings and refined beet pulp, you can.
The present invention it is a kind of reduce Feed Copper, zinc usage amount additive, wherein content of copper ion >=1250ppm;Production Product grain size:1-11 μm, homogeneity is good;Surface area >=800 ㎡/g.
It is of the present invention it is a kind of reduce Feed Copper, zinc usage amount additive amount of the additive in feed:200g/T.
Embodiment 3
It is a kind of reduce Feed Copper, zinc usage amount additive, by clay-activity copper and carrier in mass ratio 1:8 compositions;
The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp in mass ratio 9:2:15:12;
The calcium carbonate crushed 1300 mesh sieve;
The glucose crushed 1200 mesh sieve;
The wheat-middlings crushed 1300 mesh sieve.
It is heretofore described it is a kind of reduce Feed Copper, zinc usage amount additive, production technology is:
(One)The preparation of clay-activity copper:
(1)Montmorillonite crude product is crushed, 180 mesh sieve is crossed, by solid-to-liquid ratio 1:8 are added deionized water, stir 2h under the conditions of 80 DEG C, so After stand 2h;Impurities at bottom is removed, is then filtered, drying and crushing crosses 400 mesh sieve, obtains pretreatment montmorillonite;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment montmorillonite:5 are added deionized water, stir evenly, obtain suspension ore pulp, be then added CuSO4·5H2O and sodium carbonate, addition are pre-process montmorillonite quality 18% and 7%;16h is stirred under the conditions of 55 DEG C;It crosses Filter, filter residue are washed with deionized 5 times;
(3)Filter residue is dried in vacuo, 60 DEG C of drying temperature, crushed 1500 mesh sieve to get clay-activity copper;
(Two)The preparation of refined beet pulp:
(1)By beet pulp dries pulverizing, 80 mesh sieve is crossed, by solid-to-liquid ratio 1:5 are added 10% sodium hydroxide solution, and 50 DEG C are impregnated 2h, Then it filters, filter residue is washed with distilled water 5 times, pretreatment beet pulp is obtained;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment beet pulp:14 are added a concentration of 75% ethanol solution, refluxing extraction under the conditions of 45 DEG C Then 2h is volatilized ethanol solution using Rotary Evaporators, alcohol processing beet pulp is obtained, and alcohol processing beet pulp is used steam treatment Then 2h is dried in vacuo, crushed 1200 mesh sieve to get refined beet pulp;
(Three)Clay-activity copper is uniformly mixed with calcium carbonate, glucose, wheat-middlings and refined beet pulp, you can.
The present invention it is a kind of reduce Feed Copper, zinc usage amount additive, wherein content of copper ion >=1250ppm;Production Product grain size:1-11 μm, homogeneity is good;Surface area >=800 ㎡/g.
It is of the present invention it is a kind of reduce Feed Copper, zinc usage amount additive amount of the additive in feed:200g/T.
Embodiment:In order to study it is of the present invention it is a kind of reduce Feed Copper, zinc usage amount additive pannage, chicken raise Expect that service condition, existing data are as follows:
It is used in pannage:
In piglet feed, in 27 experiments, additive obtained in the embodiment of the present invention 2,78% positive-effect, wherein body are added Weightening averagely increases by 5%, and feedstuff-meat ratio averagely declines 2.9%;
Additive body weight gains obtained averagely increase in 7 experiments that wean pig early stage carries out show to add the embodiment of the present invention 2 Add 5%, feedstuff-meat ratio averagely declines 1.4%;In growth 11 experiments early period, additive obtained in the embodiment of the present invention 2 is added Body weight gains average 4.8%, feedstuff-meat ratio averagely declines 2.4%;It is used in growth and fattening period, body weight gains averagely increase by 3.3%, expect meat Than declining 3.4%.
It is used in broiler chicken material:
In broiler chicken material, in 36 experiments, additive obtained in the embodiment of the present invention 2 is added, broiler chicken body weight gains averagely increase 2.9%, feedstuff-meat ratio declines 1.8%;
Wherein poor in 25 place sanitary conditions, body weight gains averagely increase by 3.7%, and feedstuff-meat ratio declines 2.2%;
Wherein 11 place sanitary conditions are relatively good, and body weight gains averagely increase by 2.0%, and feedstuff-meat ratio declines 1.5%;
Prove that the additive of the present invention farm benefit poor to sanitary condition becomes apparent.
The basic principles and main features and advantages of the present invention of the present invention have been shown and described above.Industry technology people Member is it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this hairs Bright principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these variations It all fall within the protetion scope of the claimed invention with improvement.The claimed range of the present invention by appended claims and its Equivalent thereof.

Claims (5)

1. it is a kind of reduce Feed Copper, zinc usage amount additive, it is characterised in that:Quality is pressed by clay-activity copper and carrier Than 1:5-8 is formed;
The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp 6-9 in mass ratio:1-2:10-15:8-12;
The calcium carbonate crushed 1300 mesh sieve;
The glucose crushed 1200 mesh sieve;
The wheat-middlings crushed 1300 mesh sieve.
2. it is according to claim 1 it is a kind of reduce Feed Copper, zinc usage amount additive, it is characterised in that:It is a kind of Can reduce Feed Copper, zinc usage amount additive, by clay-activity copper and carrier in mass ratio 1:7 compositions;
The carrier is calcium carbonate, glucose, wheat-middlings and refined beet pulp in mass ratio 8:2:13:10;
The calcium carbonate crushed 1300 mesh sieve;
The glucose crushed 1200 mesh sieve;
The wheat-middlings crushed 1300 mesh sieve.
3. it is according to claim 1 or 2 it is a kind of reduce Feed Copper, zinc usage amount additive, it is characterised in that its Production technology is:
(One)The preparation of clay-activity copper:
(1)Montmorillonite crude product is crushed, 180 mesh sieve is crossed, by solid-to-liquid ratio 1:Deionized water is added in 6-8, and 2h is stirred under the conditions of 80 DEG C, It is then allowed to stand 2h;Impurities at bottom is removed, is then filtered, drying and crushing crosses 400 mesh sieve, obtains pretreatment montmorillonite;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment montmorillonite:Deionized water is added in 4-5, stirs evenly, obtains suspension ore pulp, then adds Enter CuSO4·5H2O and sodium carbonate, addition are to pre-process the 13-18% and 4-7% of montmorillonite quality;It is stirred under the conditions of 55 DEG C 16h;Filtering, filter residue are washed with deionized 5 times;
(3)Filter residue is dried in vacuo, 60 DEG C of drying temperature, crushed 1500 mesh sieve to get clay-activity copper;
(Two)The preparation of refined beet pulp:
(1)By beet pulp dries pulverizing, 80 mesh sieve is crossed, by solid-to-liquid ratio 1:10% sodium hydroxide solution, 50 DEG C of immersions are added in 3-5 Then 2h is filtered, filter residue is washed with distilled water 5 times, pretreatment beet pulp is obtained;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment beet pulp:A concentration of 75% ethanol solution is added in 10-14, flows back under the conditions of 45 DEG C 2h is extracted, then ethanol solution is volatilized using Rotary Evaporators, obtains alcohol processing beet pulp, alcohol processing beet pulp is used into steam 2h is handled, is then dried in vacuo, crushed 1200 mesh sieve to get refined beet pulp;
(Three)Clay-activity copper is uniformly mixed with calcium carbonate, glucose, wheat-middlings and refined beet pulp, you can.
4. it is according to claim 1 or 2 it is a kind of reduce Feed Copper, zinc usage amount additive, it is characterised in that:Its Production technology is:
(One)The preparation of clay-activity copper:
(1)Montmorillonite crude product is crushed, 180 mesh sieve is crossed, by solid-to-liquid ratio 1:7 are added deionized water, stir 2h under the conditions of 80 DEG C, so After stand 2h;Impurities at bottom is removed, is then filtered, drying and crushing crosses 400 mesh sieve, obtains pretreatment montmorillonite;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment montmorillonite:5 are added deionized water, stir evenly, obtain suspension ore pulp, then add Enter CuSO4·5H2O and sodium carbonate, addition are pre-process montmorillonite quality 16% and 6%;16h is stirred under the conditions of 55 DEG C;It crosses Filter, filter residue are washed with deionized 5 times;
(3)Filter residue is dried in vacuo, 60 DEG C of drying temperature, crushed 1500 mesh sieve to get clay-activity copper;
(Two)The preparation of refined beet pulp:
(1)By beet pulp dries pulverizing, 80 mesh sieve is crossed, by solid-to-liquid ratio 1:4 are added 10% sodium hydroxide solution, and 50 DEG C are impregnated 2h, Then it filters, filter residue is washed with distilled water 5 times, pretreatment beet pulp is obtained;
(2)Solid-to-liquid ratio 1 is pressed into pretreatment beet pulp:12 are added a concentration of 75% ethanol solution, refluxing extraction under the conditions of 45 DEG C Then 2h is volatilized ethanol solution using Rotary Evaporators, alcohol processing beet pulp is obtained, and alcohol processing beet pulp is used steam treatment Then 2h is dried in vacuo, crushed 1200 mesh sieve to get refined beet pulp;
(Three)Clay-activity copper is uniformly mixed with calcium carbonate, glucose, wheat-middlings and refined beet pulp, you can.
5. according to claim 1-4 it is any it is described it is a kind of reduce Feed Copper, zinc usage amount additive, it is characterised in that Wherein content of copper ion >=1250ppm, product cut size:1-11 μm, surface area >=800 ㎡/g.
CN201810347556.6A 2018-04-18 2018-04-18 It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology Pending CN108740341A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810347556.6A CN108740341A (en) 2018-04-18 2018-04-18 It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810347556.6A CN108740341A (en) 2018-04-18 2018-04-18 It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology

Publications (1)

Publication Number Publication Date
CN108740341A true CN108740341A (en) 2018-11-06

Family

ID=64011143

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810347556.6A Pending CN108740341A (en) 2018-04-18 2018-04-18 It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology

Country Status (1)

Country Link
CN (1) CN108740341A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1826945A (en) * 2006-04-07 2006-09-06 浙江大学 Antibacterial and health-caring feedstuff addictive and preparation method thereof
CN1861095A (en) * 2006-04-12 2006-11-15 浙江大学 Load type super-fine copper-powder copper-complementary agent, its prepn. method and use
CN106666125A (en) * 2016-12-21 2017-05-17 中粮集团有限公司 Solid feed and preparation method thereof
CN106819478A (en) * 2017-02-10 2017-06-13 深圳市金新农科技股份有限公司 A kind of premixed feed and mixed fodder that can be used to improve prevention of sow constipation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1826945A (en) * 2006-04-07 2006-09-06 浙江大学 Antibacterial and health-caring feedstuff addictive and preparation method thereof
CN1861095A (en) * 2006-04-12 2006-11-15 浙江大学 Load type super-fine copper-powder copper-complementary agent, its prepn. method and use
CN106666125A (en) * 2016-12-21 2017-05-17 中粮集团有限公司 Solid feed and preparation method thereof
CN106819478A (en) * 2017-02-10 2017-06-13 深圳市金新农科技股份有限公司 A kind of premixed feed and mixed fodder that can be used to improve prevention of sow constipation

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
李琳等: "甜菜废粕中食用纤维的制取 ", 《中国甜菜糖业》 *
马东升,邢有权,杨金平,王振荣: "从甜菜粕中提取纤维素的研究 ", 《黑龙江大学(自然科学学报)》 *

Similar Documents

Publication Publication Date Title
CN101971922B (en) Environment-friendly sea cucumber streak feed and preparation method thereof
CN102835610B (en) Feed additive for broiler chickens and preparation method thereof
CN103947907A (en) Pig immune-enhanced feed additive capable of replacing antibiotic
CN107455573A (en) A kind of natural feed addictive and preparation method and application
CN102356892A (en) Method for removing heavy metal lead and cadmium in gracilaria seaweed
KR101226722B1 (en) Calcium fertilizer for soil improvement using organic wastes
CN101919493B (en) Method for preparing natural feed additive from moso bamboo processing waste
CN108740341A (en) It is a kind of to reduce Feed Copper, the additive of zinc usage amount and its production technology
CN102919544A (en) Method for preparing protein calcium powder for feed by crawfish shells
CN102815975A (en) Novel ecological preparation for resource utilization of municipal refuse
CN107156491A (en) It is a kind of to reduce the pig feed for feeding number of times
CN106879861A (en) A kind of high-quality egg feedstuff
RU2545667C2 (en) Method of for pre-planting treatment of potato tubers
CN104273345B (en) A kind of Macrobrachium rosenbergii composite immune reinforcing agent and its application
CN112195213A (en) Method for extracting protein powder by cultivating hermetia illucens with food waste solids
CN116391795A (en) Preparation method of meat and bone powder
Zhang et al. Study on feed fermented from seaweed waste
CN105693501B (en) Activated carbon briquetting to be decolourized for potassium sorbate and preparation method thereof
CN115024400A (en) Livestock feed added with tea powder, preparation method and application thereof
CN103621790A (en) Composite earthworm enzymatic hydrolysate feed additive and preparation method thereof
CN111990537A (en) Functional nutritional enzymatic squid paste and preparation method thereof
RU2371975C1 (en) Method of obtaining biologically active feeding additive
CN105104753A (en) Feed additive for treating recessive cow mastitis of dairy cows
CN107484886A (en) It is a kind of to be used to improve plant extracts additive of meat and preparation method and application
CN109198279A (en) A kind of feed addictive enhancing Tilapia mossambica immunity

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20181106

RJ01 Rejection of invention patent application after publication