CN101919493B - Method for preparing natural feed additive from moso bamboo processing waste - Google Patents
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- CN101919493B CN101919493B CN2010102652711A CN201010265271A CN101919493B CN 101919493 B CN101919493 B CN 101919493B CN 2010102652711 A CN2010102652711 A CN 2010102652711A CN 201010265271 A CN201010265271 A CN 201010265271A CN 101919493 B CN101919493 B CN 101919493B
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
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- 239000004182 Tylosin Substances 0.000 description 2
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- WBPYTXDJUQJLPQ-VMXQISHHSA-N tylosin Chemical compound O([C@@H]1[C@@H](C)O[C@H]([C@@H]([C@H]1N(C)C)O)O[C@@H]1[C@@H](C)[C@H](O)CC(=O)O[C@@H]([C@H](/C=C(\C)/C=C/C(=O)[C@H](C)C[C@@H]1CC=O)CO[C@H]1[C@@H]([C@H](OC)[C@H](O)[C@@H](C)O1)OC)CC)[C@H]1C[C@@](C)(O)[C@@H](O)[C@H](C)O1 WBPYTXDJUQJLPQ-VMXQISHHSA-N 0.000 description 2
- 235000019375 tylosin Nutrition 0.000 description 2
- 235000019373 virginiamycin Nutrition 0.000 description 2
- 229960003842 virginiamycin Drugs 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 244000063299 Bacillus subtilis Species 0.000 description 1
- 235000014469 Bacillus subtilis Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- OJMMVQQUTAEWLP-UHFFFAOYSA-N Lincomycin Natural products CN1CC(CCC)CC1C(=O)NC(C(C)O)C1C(O)C(O)C(O)C(SC)O1 OJMMVQQUTAEWLP-UHFFFAOYSA-N 0.000 description 1
- 229930182555 Penicillin Natural products 0.000 description 1
- JGSARLDLIJGVTE-MBNYWOFBSA-N Penicillin G Chemical compound N([C@H]1[C@H]2SC([C@@H](N2C1=O)C(O)=O)(C)C)C(=O)CC1=CC=CC=C1 JGSARLDLIJGVTE-MBNYWOFBSA-N 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 239000004098 Tetracycline Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
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- 238000005516 engineering process Methods 0.000 description 1
- 229960003276 erythromycin Drugs 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
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- 229940088597 hormone Drugs 0.000 description 1
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- 230000008676 import Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- OJMMVQQUTAEWLP-KIDUDLJLSA-N lincomycin Chemical compound CN1C[C@H](CCC)C[C@H]1C(=O)N[C@H]([C@@H](C)O)[C@@H]1[C@H](O)[C@H](O)[C@@H](O)[C@@H](SC)O1 OJMMVQQUTAEWLP-KIDUDLJLSA-N 0.000 description 1
- 229960005287 lincomycin Drugs 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 229940049954 penicillin Drugs 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
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- 229960002180 tetracycline Drugs 0.000 description 1
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- 239000000273 veterinary drug Substances 0.000 description 1
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- 229910052725 zinc Inorganic materials 0.000 description 1
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Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Landscapes
- Fodder In General (AREA)
Abstract
The invention discloses a method for preparing natural feed additive from moso bamboo processing waste, which orderly comprises the following steps: pulverizing moso bamboo processing waste to obtain bamboo powder; proportionally mixing the bamboo powder with 95% ethanol, putting the mixture into an extractor, soaking and filtering to obtain filtrate and filter residues; concentrating the filtrate at 55-60 DEG C to thick paste state to obtain paste extract; pulverizing rice hulls to obtain rice hull powder; and proportionally and evenly mixing the paste extract, which is dissolved and diluted by 95% ethanol and water, with the rice hull powder, transferring the mixture into a drying box, and drying at 50-55 DEG C to obtain the powdery natural feed additive. The invention reduces the usage of antibiotics and heavy metals in the feed additive, reduces the residue of harmful substances in animal food, such as antibiotics and the like, reduces the environmental pollution, utilizes the moso bamboo processing waste as resources, and has obvious economic, social and environmental benefits.
Description
Technical field:
The present invention relates generally to a kind of method for preparing natural feed addictive, relates in particular to a kind of method of utilizing the mao bamboon processing waste to prepare natural feed addictive.
Background technology:
The Along with people's growth in the living standard, the consumption figure of animal foodstuffs such as meat, egg, milk and fish rises, has greatly stimulated the development of aquaculture day by day.Because antibiotic, hormone and heavy metal element copper, zinc, arsenic etc. have disease-resistant and growth promoting function to animal; Therefore; For premunition and the productivity that improves cultivated animals; General antibiotic and the heavy metal that adds high dose in violation of rules and regulations has antibiotic and heavy-metal residual thereby cause in the animal food in feed addictive, and health is worked the mischief.In recent years, because the food security incident that the feed safety problem causes constantly occurs, the livestock products of China's outlet suffer that owing to the residue of veterinary drug amount exceeds standard importer returns goods and the incident of interruption import happens occasionally.Simultaneously, also contain the antibiotic and the heavy metal of high concentration in the excreta of animal, environment is caused direct or indirect pollution.Therefore, must pay attention to the safety problem of feed safety problem, especially feed addictive.EU Committee's legislation forbids feed, adding bacillus skin, spiramvcin, virginiamycin, 4 kinds of antibiotic of tylosin from July 1st, 1999; U.S. FDA has been cancelled penicillin, tetracycline, erythromycin, lincomycin, tylosin and virginiamycin etc. from agricultural use.Therefore, antibiotic was about in the past as epoch of feed addictive, in the feed few with or without antibiotic, developing new antibiotic substitute is the inexorable trend that modern feed already develops.
China is topmost in the world product bamboo state, no matter is that bamboo kind resource, bamboo grove area or bamboo grove are accumulated output and all occupy first place in the world.Mao bamboon is the valuable renewable resource of China, have the good reputation of " second forest ".Although China mao bamboon aptitude source is abundant, because the restriction of mao bamboon material self character and the restriction of scientific and technological level, its resource utilization is extremely low, the average utilization less than 40% of mao bamboon material.The mao bamboon processing waste has become the major obstacle that the mao bamboon industry develops in a healthy way.Contain a large amount of utilizable components in the mao bamboon material, and have the natural antibacterial activity, therefore, have value of exploiting and utilizing.
Summary of the invention:
The objective of the invention is to many drawbacks to existing feed addictive; A kind of method of utilizing the mao bamboon processing waste to prepare natural feed addictive is provided; Make the mao bamboon processing waste can access resource and efficiently utilize, reduce the waste of resource, substitute or reduce the use of antibiotics feed addictive; Reduce residues of antibiotics in the animal product, help food security and environmental protection.
The present invention realizes through following technical scheme:
A kind of method of utilizing the mao bamboon processing waste to prepare natural feed addictive is characterized in that: carry out according to the following steps successively:
(1), get fresh mao bamboon processing waste and, obtain the bamboo powder its pulverizing, subsequent use;
(2), get bamboo powder and 95% ethanol, its mixing is put in the extractor of band agitating function airtight container according to the ratio of mass volume ratio 0.5-1.5: 8-10; Make its lixiviate 5-7 days at normal temperatures; The middle stirring 1-2 time carried out filtration treatment to it, filtrating that obtains being separated from each other and filter residue; The filter residue that obtains is repeated to extract 1-2 time more as stated above, and merging filtrate makes the filtrating after the merging under 55-60 ℃, be concentrated into the thick paste shape, obtains paste extract, and is subsequent use;
(3), get rice husk and with its pulverizing, powdered rice hulls, subsequent use;
(4), get paste extract, 95% second alcohol and water, mix according to 1: 1: 1 weight proportion, obtain diluted paste extract; Again with diluted paste extract and powdered rice hulls mixed according to weight proportion 0.5-1.5: 1.5-2.5; After being placed in the fodder mixing machine fully mixing and stirring; Be transferred in the drying box, temperature is controlled at 50-55 ℃ of drying down, gets the natural feed addictive of powdery.
A kind of method of utilizing the mao bamboon processing waste to prepare natural feed addictive is characterized in that: carry out according to the following steps successively:
(1), get fresh mao bamboon processing waste and it pulverized, crossing the aperture is the sieve of 2mm, obtains the bamboo powder, subsequent use;
(2), get bamboo powder and 95% ethanol, its mixing is put in the extractor of band agitating function airtight container according to 1: 9 ratio of mass volume ratio; Make its lixiviate at normal temperatures 6 days; After the middle stirring 1 time, it is carried out filtration treatment, filtrating that obtains being separated from each other and filter residue; The filter residue that obtains is repeated to extract 2 times more as stated above, and merging filtrate makes the filtrating after the merging under 55 ℃, be concentrated into the thick paste shape, obtains paste extract, and is subsequent use;
(3), get rice husk and with its pulverizing, cross 40 mesh sieves, powdered rice hulls, subsequent use;
(4), get paste extract, 95% second alcohol and water, mix according to 1: 1: 1 weight proportion, obtain diluted paste extract; Again with diluted paste extract and powdered rice hulls according to 1: 2 mixed of weight proportion, be placed in the electronic fodder mixing machine fully mixing and stirring after, be transferred in the drying box, temperature be controlled at 55 ℃ dry down, the natural feed addictive of powdery.
Said fresh mao bamboon processing waste is bamboo bits or leftover pieces.
The extractor of said band agitating function is airtight extractor, adopts all can of stainless steel, carbon steel material.
In the step 4 with paste extract with a small amount of 95% ethanol with water-solublely separate, dilute; Again paste extract after diluted and powdered rice hulls are fully mixed in electronic fodder mixing machine; Be transferred in the drying box, 50-55 ℃ dry down, gets the natural feed addictive of powdery; The pack sealing is kept at shady and cool dry place.
Extracorporeal bacteria inhibitor test shows that the natural feed addictive that the present invention makes all has very strong inhibitory action to staphylococcus aureus, bacillus subtilis and Escherichia coli, and antibacterial circle diameter is respectively 43.7 ± 1.5mm, 45.7 ± 0.6mm, 48.3 ± 3.2mm.
The natural feed addictive of method for preparing of the present invention can add in the feeds such as chicken, pig, milk cow.Add 0.05-0.1% in the feed per ton.
Broiler trial shows; In basal diet, add 0.05% natural feed addictive; 28 age in days body weight improve 1.5% (P>0.05) than control group; 42 age in days body weight improve 6.2% (P<0.01) than control group, and 56 age in days body weight improve 2.4% (P<0.01) than control group, and the 56 age in days death rates have reduced by 3.7% respectively than control group; In basal diet, add 0.1% additive, 42 age in days body weight improve 6.9% (P<0.01) than control group, and 56 age in days body weight improve 4.6% (P<0.01) than control group, and the 56 age in days death rates have reduced by 4.7% respectively than control group.This shows that this additive has the effect that promotes growth of meat chicken, reduces the death rate.
Advantage of the present invention is:
It is to select suitable extractant to extract the active material in the mao bamboon bamboo wood that the present invention utilizes the mao bamboon processing waste to prepare natural feed addictive; Become natural feed addictive through suitable processes again; Not only can reduce the use of antibiotic and heavy metal class additive in the feed, reduce in the animal food residues of harmful substances such as antibiotic, reduce environmental pollution; And the mao bamboon processing waste is got utilization, have remarkable economical, society and environmental benefit.
The specific embodiment:
A kind of method of utilizing the mao bamboon processing waste to prepare natural feed addictive, carry out according to the following steps successively:
(1), get fresh mao bamboon processing waste and it pulverized, crossing the aperture is the sieve of 2mm, obtains the bamboo powder, subsequent use;
(2), get bamboo powder and 95% ethanol, according to 1: 9 ratio of mass volume ratio the extractor of band agitating function, airtight container are put in its mixing; Make its lixiviate at normal temperatures 6 days; The middle stirring 1 time carried out filtration treatment to it, filtrating that obtains being separated from each other and filter residue; The filter residue that obtains is repeated to extract 2 times more as stated above, and merging filtrate makes the filtrating after the merging under 55 ℃, be concentrated into the thick paste shape, obtains paste extract, and is subsequent use;
(3), get rice husk and with its pulverizing, cross 40 mesh sieves, powdered rice hulls, subsequent use;
(4), get paste extract, 95% second alcohol and water, weight proportion dissolving, dilution according to 1: 1: 1 obtain diluted paste extract; Again with diluted paste extract and powdered rice hulls according to 1: 2 mixed of weight proportion, be placed in the electronic fodder mixing machine fully mixing and stirring after, be transferred in the drying box, temperature be controlled at 55 ℃ dry down, the natural feed addictive of powdery.
Claims (2)
1. method of utilizing the mao bamboon processing waste to prepare natural feed addictive is characterized in that: carry out according to the following steps successively:
(1), get fresh mao bamboon processing waste and, obtain the bamboo powder its pulverizing, subsequent use;
(2), get bamboo powder and 95% ethanol, join in the extractor of band agitating function according to the ratio of mass volume ratio 0.5-1.5: 8-10, normal temperature lixiviate 5-7 days, the middle stirring 1-2 time carried out filtration treatment to it, filtrating that obtains being separated from each other and filter residue; The filter residue that obtains is repeated to extract merging filtrate 1-2 time more as stated above; Filtrating after merging is concentrated into the thick paste shape under 55-60 ℃, obtains paste extract, subsequent use;
(3), get rice husk and with its pulverizing, cross 40 mesh sieves, powdered rice hulls, subsequent use;
(4), get paste extract, 95% second alcohol and water, according to 1: 1: 1 weight proportion,, obtain diluted extract with paste extract dissolving, dilution; Again diluted extract and the powdered rice hulls ratio according to weight proportion 0.5-1.5: 1.5-2.5 is joined in the fodder mixing machine; Fully after the mixing and stirring; Be transferred in the drying box, temperature is controlled at 50-55 ℃ of drying down, gets the natural feed addictive of powdery.
2. method of utilizing the mao bamboon processing waste to prepare natural feed addictive is characterized in that: carry out according to the following steps successively:
(1), get fresh mao bamboon processing waste and it pulverized, crossing the aperture is the sieve of 2mm, obtains the bamboo powder, subsequent use;
(2), get bamboo powder and 95% ethanol, according to 1: 9 ratio of mass volume ratio its mixing is put in the extractor of band agitating function, make its lixiviate at normal temperatures 6 days, the middle stirring 1 time carried out filtration treatment to it, filtrating that obtains being separated from each other and filter residue; The filter residue that obtains is repeated to extract 2 times more as stated above, and merging filtrate makes the filtrating after the merging under 55 ℃, be concentrated into the thick paste shape, obtains paste extract, and is subsequent use;
(3), get rice husk and with its pulverizing, cross 40 mesh sieves, powdered rice hulls, subsequent use;
(4), get paste extract, 95% second alcohol and water, according to 1: 1: 1 weight proportion,, obtain diluted paste extract with paste extract dissolving, dilution; Again with diluted paste extract and powdered rice hulls according to 1: 2 mixed of weight ratio, be placed in the electronic fodder mixing machine fully mixing and stirring after, be transferred in the drying box, temperature be controlled at 55 ℃ dry down, the natural feed addictive of powdery.
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CN103070289B (en) * | 2013-01-14 | 2014-08-13 | 浙江大学 | Natural product feed additive from bamboo |
CN105325702B (en) * | 2015-11-30 | 2019-12-10 | 河南科技大学 | natural antibiotic feed additive containing gentian H and preparation method and application thereof |
CN106173276A (en) * | 2016-07-18 | 2016-12-07 | 柳州市柳南区安顺养殖协会 | A kind of preparation method of cow feed additive |
CN107319156A (en) * | 2017-07-11 | 2017-11-07 | 安佑生物科技集团股份有限公司 | A kind of preparation method and application method of piglet functional dietary fiber additive |
CN113287759A (en) * | 2021-03-29 | 2021-08-24 | 黄达模 | Processing technology of moso bamboo |
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