CN108704068A - A kind of concocting method of dendrobium candidum - Google Patents
A kind of concocting method of dendrobium candidum Download PDFInfo
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- CN108704068A CN108704068A CN201810557458.5A CN201810557458A CN108704068A CN 108704068 A CN108704068 A CN 108704068A CN 201810557458 A CN201810557458 A CN 201810557458A CN 108704068 A CN108704068 A CN 108704068A
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- dendrobium candidum
- stem
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- concocting method
- mannose
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a kind of concocting method of dendrobium candidum, this method applies to the technique of frying that Chinese medicine processes in the processing of dendrobium candidum, can improve the dissolution rate of active ingredient mannose, improve its drug effect.Therefore, the content of mannose significantly improves in present invention gained dendrobium candidum processed product, direct-edible or extraction mannose etc..And honey has been incorporated in dendrobium candidum, the effect that the two combines the enriching yin of dendrobium candidum when eating doubles, and effects of beautification and nourishing face is more significant, is more suitable for suitable for women for drinking.Therefore, concocting method of the invention is highly practical, of low cost, with strong points, can promote in production.
Description
Technical field
The present invention relates to a kind of concocting methods of dendrobium candidum, belong to Chinese medicine processing technique field.
Background technology
Dendrobium candidum is the drying stem of orchid family herbaceos perennial dendrobium candidum (Dendrobium officinal), 11
The moon to March in next year harvests, and removes impurity, cuts off part fibrous root, becomes heating side and is twisted into spiral shape or spring-like, drying；Or it is cut into
Section, dry or low temperature drying, is 2015 editions《Chinese Pharmacopoeia》The kind recorded.Because of its unique medical value and health-care efficacy,
It is always used as tribute, is to have the reputation of " gold in medicine ", be " enriching yin help treasure " first of " Chinese nine big celestial grass " by honor.Begin to carry
In《Sheng Nong's herbal classic》, history tree is on the books, has the uniquenesses such as reinforcing stomach reg fluid, nourishing Yin and clearing heat, strengthen immunity, antitumor
Effect, both pharmaceutically acceptable treatment consumption of YIN caused by febrile disease, deficiency of stomach-Yin, kinds cancer, cardiovascular system, respiratory system, ophthalmology, diabetes,
The diseases such as prostate；Health products are also used as applied to radioresistance, anti-aging, beauty treatment in holding, nourishing the liver to improve visual acuity, are had evolved into
For 50,000,000,000 yuan or more of industry, entire China's stem of noble dendrobium market year total demand is at ten thousand tons or more, long-term fast sale Hong Kong, Macao and Taiwan, the southeast
The ground such as sub- and Europe, the United States, the huge market demand, and artificial growth is relied primarily on to supply.Stem of noble dendrobium maple bucket is also by numerous people at home and abroad
Scholar favors, and is always important foreign exchange earning commodity.
Ancient books records the stem of noble dendrobium in addition to using fresh herb, and concocting method has water system, fire system and preparing with water and fire together：《General Records of Holy Universal Relief》Volume
In 186 Rhizoma Atractylodis Macrocephalae stem of noble dendrobium soup " stem of noble dendrobium (remove root, file, is parched with wine) ",《Complete Effective Prescriptions for Women》In volume 3 " discussing the 4th in married woman aphasia from apoplexy side "
Ledebouriellae Decoction " stem of noble dendrobium (two halves are parched with wine) ",《Thunder God processes addendum brief guide》It is painted with《Thunder God processes opinion》" steeping in wine ", " shortcake steams " method big gun
The schematic diagram of a scenario of the stem of noble dendrobium processed, it is seen that the concocting method of the stem of noble dendrobium is a lot of.After modern study has proven to medicinal material by processing, change
Study point can also change therewith, also be changed by the quality of the stem of noble dendrobium after distinct methods Processing methods.Although ancient books is for iron sheet
The concocting method that the stem of noble dendrobium is recorded is more, but the influence report processed to its quality is relatively fewer, and the country is also there is not yet increase it
The concocting method of one of main component mannose.
Invention content
The purpose of the present invention is to provide a kind of concocting method of dendrobium candidum, this method fries work by what Chinese medicine processed
Skill applies in the processing of dendrobium candidum, can improve the dissolution rate of active ingredient mannose, improves its drug effect.
Technical scheme of the present invention：A kind of concocting method of dendrobium candidum, includes the following steps：
(1) the fresh stem of dendrobium candidum is chosen, fibrous root, leaf and impurity are removed, retains stem；
(2) fresh stem is cut into the section of 3~5cm, is then placed in 20% hydromel and impregnates 12~18 hours, is taken out
After drain；
(3) machine for stir-frying Chinese medicine is preheated, and temperature adjustment, to 100~120 DEG C, the dendrobium candidum section after then draining is put into machine for stir-frying Chinese medicine
Middle stir-frying, constantly agitation during stir-frying, and control temperature；
(4) dendrobium candidum is stir-fried to dendrobium candidum when softening, is taken the dish out of the pot, dehydration in 30 DEG C of dry bellows is placed in, until arriving
Water content is down to 10% hereinafter, can be prepared by dendrobium candidum processed product.
In the above method, the fresh stem of dendrobium candidum is the fresh stem of triennial dendrobium candidum that film quality leaf sheath is born on stem.
By adopting the above-described technical solution, the advantage of the invention is that：It is sweet in gained dendrobium candidum processed product of the invention
The content of dew sugar significantly improves, direct-edible or extraction mannose etc..And honey has been incorporated in dendrobium candidum, the two combination
The effect of the enriching yin of dendrobium candidum doubles when edible, and effects of beautification and nourishing face is more significant, is more suitable for suitable for women for drinking.Therefore, of the invention
Concocting method it is highly practical, of low cost, with strong points, can promote in production.
Specific implementation mode
To make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiment to the present invention make into
The detailed description of one step.
The embodiment of the present invention：A kind of concocting method of dendrobium candidum of the present invention, includes the following steps：
(1) the fresh stem of dendrobium candidum for choosing the triennial for bearing film quality leaf sheath on stem removes fibrous root, leaf and impurity, retains
Stem；
(2) fresh stem is cut into the section of 5cm, is then placed in 20% hydromel and impregnates 12 hours, drained after taking-up；
(3) machine for stir-frying Chinese medicine is preheated, and temperature adjustment, to 100 DEG C, the dendrobium candidum section after then draining, which is put into machine for stir-frying Chinese medicine, to be turned over
It fries, constantly agitation during stir-frying, and controls temperature；
(4) dendrobium candidum is stir-fried to dendrobium candidum when softening, is taken the dish out of the pot, dehydration in 30 DEG C of dry bellows is placed in, until arriving
Water content is down to 10% hereinafter, can be prepared by dendrobium candidum processed product.
In order to further illustrate the present invention the advantages of and advantageous effect now provide following experiment and are verified：
1 material
1.1 instrument
1100 type high performance liquid chromatograph of Agilent, L-550 types Hunan instrument centrifuge；Digital display thermostat water bath HH-6 (China of state
Electrical Appliances Co., Ltd)；Cs101[1°]Type electric drying oven with forced convection (Chongqing testing equipment factory)；Electronic balance (Beijing Sai Duolisi
Instrument system Co., Ltd)
1.2 reagent
The mixed mark solution of mannose, lot number：131109, it buys in Chengdu Zhi Biaohuachun Bioisystech Co., Ltd.In experiment
Acetonitrile used, ammonium acetate, methanol are chromatographically pure, ethyl alcohol be analyze it is pure.
2 methods and result
2.1 chromatographic condition：20 DEG C of column temperature, sample size 10 μ L, flow velocity 1mL/min, acetonitrile-ammonium acetate (0.02moL/L) 17:
83 chromatographic columns:ACE Excel 5 c18(250×4.6mm)A198169
2..2 correction factor
Reference《Chinese Pharmacopoeia》2015 editions first page 283, Tie Pishihu [Han Liangceding ]The measurement of correction factor under：
Take aminoglucose hydrochloride appropriate, it is accurately weighed, add water that solution of every 1ml containing 12mg is made, as inner mark solution.Separately take sweet dew
Sugared reference substance about 10mg, it is accurately weighed, it sets in 100ml measuring bottles, inner mark solution 1ml is added in precision, and appropriate amount of water is added to make dissolving and dilute
It releases to scale, shakes up, draw 400 μ l, each 400 μ of sodium hydroxide solution of the PMP methanol solutions and 0.3mol/L that add 0.5mol/L
L, mixing, 70 DEG C of water-baths 100 minutes.Again plus the hydrochloric acid solution of 0.3mol/L, mixing washs 3 times, every time with chloroform
2ml discards chloroform liquid and takes 10 μ l of supernatant after water layer centrifugation, injects liquid chromatograph, measure, calculate to obtain correction factor
It is 0.8022.
2.3 measuring method
Reference《Chinese Pharmacopoeia》2015 editions first page 283, Tie Pishihu [Han Liangceding ]The measurement side of mannose under
Method：Dendrobium candidum powder (crossing No. three sieves) about 0.12g is taken, it is accurately weighed, it sets in Soxhlet extractor, adds 80% appropriate amount of ethanol, add
Circumfluence distillation 4 hours discards ethanol, and the dregs of a decoction volatilize ethyl alcohol, and filtration paper cylinder, which is dismantled, to be placed in beaker, adds water 100ml, then accurate
Inner mark solution 2ml is added, decoct 1 hour and constantly stirs, lets cool, water is added to mend to about 100ml, mixing, centrifugation, Aspirate supernatant
1ml is set in ampoule bottle or ml headspace bottle, adds the hydrochloric acid solution 0.5ml of 3.0mol/L, sealing, mixing, and 110 DEG C hydrolyze 1 hour, put
It is cold, pH value is adjusted to neutrality with the sodium hydroxide solution of 3.0mol/L, is drawn 400 μ l, according to correction factor assay method, " is added certainly
The PMP methanol solutions of 0.5mol/L " rise, and operate in accordance with the law, take 10 μ l of supernatant, inject liquid chromatograph, measure to get.
2.7 experimental design
60-80 DEG C, 80-100 DEG C, 100-120 DEG C, 120-140 DEG C of different frying temperature have been investigated in experiment, as a result when
After temperature is higher than 120 DEG C, dendrobium candidum section will soon fry into surface coking, and the time is too short, be unfavorable for operating, therefore select frying
Temperature is 100-120 DEG C and is preferred.
Drying temperature screening test：Using drying temperature as investigation object, using mannose as evaluation index, using single factor test reality
Proved recipe method, with spss17.0 analysis methods, experimental result see the table below：
It is significantly improved by the content of dendrobium candidum processed product mannose made from the above method.Golden appearance has light
It is damp degree, clean.
In conclusion the content of mannose significantly improves in present invention gained dendrobium candidum processed product, it is direct-edible or
Extract mannose etc..And honey has been incorporated in dendrobium candidum, the effect that the two combines the enriching yin of dendrobium candidum when eating doubles,
Effects of beautification and nourishing face is more significant, is more suitable for suitable for women for drinking.Therefore, concocting method of the invention it is highly practical, it is of low cost, be directed to
Property is strong, can promote in production.
Claims (2)
1. a kind of concocting method of dendrobium candidum, it is characterised in that include the following steps：
(1) the fresh stem of dendrobium candidum is chosen, fibrous root, leaf and impurity are removed, retains stem；
(2) fresh stem is cut into the section of 3~5cm, is then placed in 20% hydromel and impregnates 12~18 hours, dripped after taking-up
It is dry；
(3) machine for stir-frying Chinese medicine is preheated, and temperature adjustment, to 100~120 DEG C, the dendrobium candidum section after then draining, which is put into machine for stir-frying Chinese medicine, to be turned over
It fries, constantly agitation during stir-frying, and controls temperature；
(4) dendrobium candidum is stir-fried to dendrobium candidum when softening, is taken the dish out of the pot, be placed in dehydration in 30 DEG C of dry bellows, it is aqueous to arriving
Amount is down to 10% hereinafter, can be prepared by dendrobium candidum processed product.
2. the concocting method of dendrobium candidum according to claim 1, it is characterised in that：The fresh stem of dendrobium candidum is on stem
Bear the fresh stem of triennial dendrobium candidum of film quality leaf sheath.
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| CN201810557458.5A CN108704068A (en) | 2018-06-01 | 2018-06-01 | A kind of concocting method of dendrobium candidum |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111494284A (en) * | 2020-06-01 | 2020-08-07 | 中国科学院昆明植物研究所 | Dendrobium officinale extract processed by special method and application thereof in skin care products |
Citations (4)
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|---|---|---|---|---|
| CN104083639A (en) * | 2014-07-30 | 2014-10-08 | 乐清王十堂生物科技有限公司 | Preparation method of dendrobium officinale |
| CN104605127A (en) * | 2015-01-28 | 2015-05-13 | 袁晓健 | Preparation method of honey-flavor dried persimmons |
| CN105116088A (en) * | 2015-08-19 | 2015-12-02 | 汤臣倍健股份有限公司 | Detection method for mannose content in dendrobium officinale |
| CN105412617A (en) * | 2015-09-10 | 2016-03-23 | 海南石斛健康产业股份有限公司 | Dendrobium processing method |
-
2018
- 2018-06-01 CN CN201810557458.5A patent/CN108704068A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104083639A (en) * | 2014-07-30 | 2014-10-08 | 乐清王十堂生物科技有限公司 | Preparation method of dendrobium officinale |
| CN104605127A (en) * | 2015-01-28 | 2015-05-13 | 袁晓健 | Preparation method of honey-flavor dried persimmons |
| CN105116088A (en) * | 2015-08-19 | 2015-12-02 | 汤臣倍健股份有限公司 | Detection method for mannose content in dendrobium officinale |
| CN105412617A (en) * | 2015-09-10 | 2016-03-23 | 海南石斛健康产业股份有限公司 | Dendrobium processing method |
Non-Patent Citations (1)
| Title |
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| 上海市卫生局: "《上海市中药饮片炮制规范1980》", 31 May 1983, 上海科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111494284A (en) * | 2020-06-01 | 2020-08-07 | 中国科学院昆明植物研究所 | Dendrobium officinale extract processed by special method and application thereof in skin care products |
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Application publication date: 20181026 |