CN106754155A - Pueraria root health care liquor and preparation method thereof - Google Patents
Pueraria root health care liquor and preparation method thereof Download PDFInfo
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- CN106754155A CN106754155A CN201710085031.5A CN201710085031A CN106754155A CN 106754155 A CN106754155 A CN 106754155A CN 201710085031 A CN201710085031 A CN 201710085031A CN 106754155 A CN106754155 A CN 106754155A
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- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
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- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
- A61K36/074—Ganoderma
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/60—Moraceae (Mulberry family), e.g. breadfruit or fig
- A61K36/605—Morus (mulberry)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A61K36/88—Liliopsida (monocotyledons)
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- A61K36/8945—Dioscorea, e.g. yam, Chinese yam or water yam
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8966—Fritillaria, e.g. checker lily or mission bells
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Abstract
The invention belongs to health liquor technical field, and in particular to a kind of pueraria root health care liquor.The pueraria root health care liquor is prepared from by following mass parts raw material:66 70 parts of liquor made from sorghum, 20 25 parts of the root of kudzu vine, 6 10 parts of mulberries, 12 parts of ganoderma lucidum, 24 parts of felwort, 35 parts of schizonepeta, 25 parts of Chinese yam, 45 parts of the root of herbaceous peony, 35 parts of henry woodbetony root, 68 parts of fritillaria thunbergii.The pueraria root health care liquor of the application is limpid transparent, glossy, without precipitation or suspension;Medicine is fragrant, aroma is strong, coordinates, free from extraneous odour;Mouthfeel alcohol and, relax along coordinating, sour and sweet palatability, long aftertaste, and nutritious.Brought down a fever with analgesic, expelling pathogenic factors from muscles and skin, promoting eruption, promote the production of body fluid to quench thirst, Shengyang Zhixie, fill blood, strengthening the bones and muscles, strengthening the spleen and stomach, help digestion, reduce fat, reduction blood fat, nutrition skin, makes skin delicate and the various health care functions such as black hair, anti-aging, the immune, cancer-resisting of enhancing.
Description
Technical field
The invention belongs to health liquor technical field, and in particular to a kind of pueraria root health care liquor and preparation method thereof.
Background technology
The root of kudzu vine is the dry root of legume pueraria lobata, and fresh-cut into sheet or fritter is taken advantage of in autumn, the excavation of season in winter two;Dry.The root of kudzu vine
In it is cool in nature containing the material such as isoflavones, Dai, daidzin, Puerarin, Puerarin -7- xylosides, acrid-sweet flavor, with expelling pathogenic factors from muscles and skin
Bring down a fever, promoting eruption, promote the production of body fluid to quench thirst, Shengyang Zhixie, three high drop, beauty, the effects such as improve the health care of sleep, adjust mood.
Root of kudzu vine alcoholic is a kind of normal method of the edible root of kudzu vine among the people.But the mouthfeel of existing kudzuvine root wine is bad.
The content of the invention
In view of this, it is an object of the invention to provide a kind of pueraria root health care liquor, the pueraria root health care liquor it is in good taste.
To realize object above, the technical scheme is that:
A kind of pueraria root health care liquor, is prepared from by following mass parts raw material:Kaoliang spirit 66-70 parts, root of kudzu vine 20-25 parts, mulberry
Shen 6-10 parts, ganoderma lucidum 1-2 parts, felwort 2-4 parts, schizonepeta 3-5 parts, Chinese yam 2-5 parts, root of herbaceous peony 4-5 parts, henry woodbetony root 3-5 parts, Zhejiang shellfish
It is female 6-8 parts.
The liquor made from sorghum is the white wine being made with sorghum as primary raw material.
The root of kudzu vine is the dry root of legume pueraria lobata, and fresh-cut into sheet or fritter is taken advantage of in autumn, the excavation of season in winter two;Dry.
Contain the compositions such as daidzein, daidzin, Puerarin, epoxide Puerarin, allantoin, sophoradiol.The root of kudzu vine its acrid-sweet flavor, property
It is cool, brought down a fever with expelling pathogenic factors from muscles and skin, promoting eruption, promote the production of body fluid to quench thirst, Shengyang Zhixie the effects such as.
The mulberries also known as mulberry fruit, mulberry sugarcane, mulberry jujube, sorosis, mulberry bubble youngster, black mulberry etc., are the mellow fruit of moraceae plants mulberry
It is real, contain protein, fat, dietary fiber, carbohydrate, ash content, vitamin A, carrotene, thiamine, riboflavin, dimension
The compositions such as raw element E, potassium, calcium, phosphorus, potassium, sodium, iron, zinc, copper, selenium, manganese, tannic acid, malic acid, vitamin C and aliphatic acid.Mulberries into
It is in atropurpureus when ripe, succulence, taste is sweet, it is cold in nature, with reducing fat, reduction blood fat, prevent vascular sclerosis;Make hair become it is black and
It is glossy;Improve skin (including scalp) blood supply, nutrition skin makes skin delicate and the effect such as black hair, and can anti-aging;
Enhancing is immune;Cancer-resisting;Nourishing yin and nourishing blood, fluid dryness;Improving eyesight, the dry and astringent symptom of relieving eye strain;Supplement lacking for gastric juice
It is weary, promote the digestion of gastric juice, stimulate gastric mucosa, promote intestinal fluid secretion, promote gastrointestinal peristalsis.
The ganoderma lucidum is also known as Lin Zhongling, fine jade treasure, red sesame, red sesame, red sesame, seocho, Ganoderma Lucidum, Ganoderma, 10000 years gill fungus, ganoderma lucidum
Grass etc., is the fructification of On Polyporaceae Ganodermataceae Ganoderma.Contain amino acid, polypeptide, protein, fungi bacteriolyze in ganoderma lucidum
Enzyme, and carbohydrate (reduced sugar and polysaccharide), ergosterol, triterpenes, coumarin glucoside, volatile oil, stearic acid, benzoic acid, biology
Alkali, vitamin B2 and C etc.;The compositions such as mannitol, trehalose.Ganoderma lucidum is sweet, mild-natured, and gas is special, and mildly bitter flavor is puckery, with tonifying Qi peace
It is refreshing, relieving cough and asthma, promote longevity, protecting liver and detoxication, treatment diabetes, improve blood sugar, glucose in urine, increase CF, improve the heart
Flesh microcirculation, the supply of the myocardium oxygen of enhancing and energy, crease-resistant, anti-inflammatory, removes color spot, protection skin, keeps and regulation skin water
Property, recover skin elasticity, make the succulence effect such as skin wet, exquisiteness.
The felwort also known as rough gentian, courage grass, careless rough gentian, mountain rough gentian, are Angiospermae Gentianaceae agueweed bar
Leaf rough gentian dries root and rhizome, spring, the excavation of season in autumn two, in cleaning, drying felwort containing gentiopicrin, swertiamarin, when
The compositions such as medicine glucoside, Amarogentin, Amaroswerin.Felwort bitter, it is cold in nature, with heat-clearing and damp-drying drug, purging the liver of pathogenic fire is calmed the frightened, promote stomach
The effects such as liquid secretion, lidan liver, diuresis, antibacterial, analgesia.
The schizonepeta alias perfume chaste tree shepherd's purse, line shepherd's purse, four rib bar wormwood artemisias, false Soviet Union etc., are Labiatae Nepeta perennial plant schizonepeta
Dry aerial parts, the summer, season in autumn two, the flowers are in blossom to top, fringe it is green when tap, remove impurity, dry.Contain protein, dimension in schizonepeta
The compositions such as raw element, aromatic oil.Schizonepeta taste is pungent, slightly warm in nature, with wind-dispelling, sweating, inducing diaphoresis, hemostasis, promoting eruption, throat, is subsided a swelling, is helped
Taste, the effects such as help digestion.
The Chinese yam alias Chinese yam, native potato, sweet potato Chinese yam, RHIIZOMA DIOSCOREAE from Henan of China, Chinese yam, white Chinese yam, mountain Chinese yam, numb Chinese yam, water Chinese yam, hair
Chinese yam, light yam etc., are Dioscoreaceae plant Chinese yam dry rhizome.Excavated after winter cauline leaf is withered, cut root head, cleaned, removed
Crust and fibrous root are removed, after being smoked with Sulfur, is dried;Also there is select hypertrophy straight to dry Chinese yam, put in clear water, be dipped into without the dry heart,
It is vexed, with Sulfur it is smoked after, trim two ends, be twisted into plank cylindric, dry, polishing, practise and claim " light yam ".The Chinese yam of the application
For the former.Contain thick protein, crude fibre, starch, sugar, amino acid, potassium, phosphorus, calcium, magnesium, ash content, iron, zinc, copper, manganese in Chinese yam
Deng Multiple components.Chinese yam is sweet, mild-natured, with tonifying spleen nourishing the stomach, engender liquid and benefic lung, the puckery essence of kidney tonifying, skin maintenance, hypotensive, drop blood
Sugar, enhancing is immune, improve memory, body-building, anti-aging, it is antitumor, promote epithelial growth, anti-inflammatory, it is antibacterial the effects such as.
The root of herbaceous peony also known as spend Chinese herbaceous peony, Chinese herbaceous peony, auricledleaf swallowwort root etc. in vain, be the dry root of Paeoniaceae Chinese herbaceous peony platymiscium.Summer, autumn two
Season excavates, and cleans, and removes end to end and radicula, putting and boiled again after removing crust or peeling after boil in boiling water, dries.Contain egg in the root of herbaceous peony
It is white matter, sugar, starch, amino acid, Paeoniflorin, paeonol, paeoniflorin, benzoic acid, volatile oil, fat oil, resin, tannin, viscous
The compositions such as liquid matter, manganese, iron, copper.Root of herbaceous peony bitter acid, cold nature is exempted from smooth liver and relieve pain, nourishing blood for regulating menstruation, astringing YIN to stop sweating, raising
The effects such as epidemic disease, anti-inflammatory, analgesic, liver protection, solution spasm, resisting stress.
The henry woodbetony root alias wind catching arrow, cock flower root, mutual leaf henry woodbetony root, phoenix tail resupinate woodbetony leaf or root etc., are Scrophulariaceae resupinate woodbetony leaf or root
The dry root of platymiscium south of the River resupinate woodbetony leaf or root.Autumn excavates, and cleans and dries.Henry woodbetony root is sweet, slight bitter, warm in nature, with filling blood, lead to
Channels and collaterals, relieving cough and asthma, strengthening the bones and muscles, strengthening the spleen and stomach, the effects such as help digestion.
The fritillaria thunbergii alias Zhejiang shellfish, great Bei, Bulbus Fritillariae Thunbergii, BULBUS FRITILLARIAE THUNBERGII, pearl shellfish etc., are Liliaceae Fritillaria Linn fritillaria thunbergii
Dry bulb.Excavated when early summer plant is withered, cleaned.Size is separated, and big person removes coring bud, is practised and is claimed " great Bei ";Small person not coring
Bud, practises and claims " pearl shellfish ".Wiping is hit respectively, crust is removed, the oyster shell whiting to forge is mixed, the juice for clashing is sucked, and is dried;Or take squama
Stem, size is separate, cleans, and except coring bud, takes advantage of fresh-cut into sheet, cleaning, drying, practises and claiming in " Zhejiang shellfish piece ".Contain Zhejiang in fritillaria thunbergii
The compositions such as peimine, peiminine, Zhebeinine, zhebeirine.Fritillaria thunbergii bitter, it is cold in nature, stop with heat-clearing dissipating bind, resolving sputum
The effects such as coughing, detoxify, being depressured.
Further, the alcoholic strength of the liquor made from sorghum is 28-38%vol.
Preparation method the present invention also aims to protect the pueraria root health care liquor, comprises the following steps:
A. root of kudzu vine pretreatment:The root of kudzu vine of above-mentioned mass parts is taken, cleaning, peeling, crushing add ethanol solution, be placed in ultrasound
Extracted in ripple washer, cooled down, centrifugation, centrifuged deposit is added ethanol solution, is placed in ultrasonic cleaner and is carried
Take, the supernatant that merging is extracted twice, concentration obtains medicinal extract;
B. mulberries pretreatment:The mulberries for taking above-mentioned mass parts break into slurry, filtering, remove filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum, henry woodbetony root and the fritillaria thunbergii of above-mentioned mass parts are taken, is crushed, plus
Enter alcohol solution dipping 30-45min, then in backflow extraction 8-10h is carried out under 63-67 DEG C of bath temperature, filter;
D. felwort, schizonepeta, Chinese yam and the root of herbaceous peony pretreatment:Felwort, schizonepeta, Chinese yam and the root of herbaceous peony of above-mentioned mass parts are taken,
Pulverize, of length no more than 5cm of Chinese medicine each component, be placed in water immersion 30-45min, then decoct to boiling with high heat, then with
10-15min is cooked by slow fire, is filtered, remove filter residue;
E. the preparation of pueraria root health care liquor:Obtained to the medicinal extract, step B that add step A to obtain in the kaoliang spirit of above-mentioned mass parts
To the filtrate for obtaining, the filtrate that obtains of the filtrates for obtaining that obtain of step C and step D, stirring adds activated carbon, stands 2-3
My god, filtering is sterilized by filtrate, obtains final product the pueraria root health care liquor.
The intense fire refers to more violent fire during culinary art, is also called big fire, very hot oven, very hot oven, temperature >=100 DEG C, column of flame meeting
A pot side is stretched out, flame is high and stable, heat color is in blue and white, temperature is pressing.
The slow fire of stating is also called small fire or warm fire, refers to boiling small and slow fire used during thing, and temperature is 40-50
℃.The column of flame will not stretch out a pot side, flame it is small and when it is high when it is low, flame is in blue orange, and luminosity is dark and temperature is relatively low.
Further, the degree crushed described in step A is to be crushed to more than 90% grain diameter≤2.5 μm.
The particle diameter refer to certain physical characteristic or physical behavio(u)r and a certain diameter when tested particle homogenous spheres (or
Combination) it is most close when, just using the diameter of the spheroid (or combination) as the equivalent grain size (or size distribution) for being tested particle.
Further, ethanol solution described in step A is that volume fraction is the ethanol solution of 50-60%, the consumption of ethanol solution
It is 17-21 times of root of kudzu vine quality.
Further, during ultrasonic wave extraction described in step A, the power of ultrasonic wave is 130-145W, and the time is 20-
25min。
The ultrasonic wave extraction is extracted using ultrasonic assistant solvent, and sound wave produces cavitation effect at a high speed, strong
Should and stirring action, destroy the cell of vegetable drug, make solvent penetration in crude drug cell, shorten extraction time, improve and extract
Rate.
Further, the degree for being concentrated described in step A is 1.13-1.17 to be concentrated into relative density.The concentration is to instigate
The process of solvent evaporation solution concentration increase in solution.The relative density refers to the density of material and the density of water in 4 DEG C of temperature
The ratio between under degree.
Further, the water that slurry is directed in mulberries add 6-8 times of its quality is worn into described in step B, slurry is worn into.
Further, ethanol solution described in step C is that volume fraction is the ethanol solution of 65-70%, the consumption of ethanol solution
It is 10-13 times of ganoderma lucidum, henry woodbetony root and fritillaria thunbergii gross mass.
Further, the degree of the crushing described in step C is to be crushed to more than 80% grain diameter≤3 μm.
Further, the consumption of water described in step D is 4-7 times of felwort, schizonepeta, Chinese yam and root of herbaceous peony gross mass.
Further, the sterilization described in step E is realized by pasteurize.
Further, the consumption of activated carbon described in step E is the 0.015-0.018% of mixture quality after stirring.
The beneficial effects of the present invention are:
The pueraria root health care liquor of the application is limpid transparent, glossy, without precipitation or suspension;Medicine is fragrant, aroma is strong, coordinates,
Free from extraneous odour;Mouthfeel alcohol and, relax along coordinating, sour and sweet palatability, long aftertaste, and nutritious.With analgesic, expelling pathogenic factors from muscles and skin bring down a fever, promoting eruption,
Promote the production of body fluid to quench thirst, Shengyang Zhixie, fill blood, strengthening the bones and muscles, strengthening the spleen and stomach, help digestion, reduce fat, reduction blood fat, nutrition skin makes skin
The various health care functions such as delicate and black hair, anti-aging, the immune, cancer-resisting of enhancing.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.It is unreceipted in preferred embodiment
The experimental technique of actual conditions, generally according to normal condition.
Embodiment 1
A kind of pueraria root health care liquor, is prepared from the following materials:Alcoholic strength is kaoliang spirit 70kg, the root of kudzu vine of 38%vol
25kg, mulberries 10kg, ganoderma lucidum 1kg, felwort 4kg, schizonepeta 5kg, Chinese yam 5kg, root of herbaceous peony 5kg, henry woodbetony root 5kg, fritillaria thunbergii 6kg.
The preparation method of the pueraria root health care liquor is:
A. root of kudzu vine pretreatment:Root of kudzu vine 25kg is taken, cleaned, removed the peel, being crushed to more than 90% grain diameter≤2.5 μm, added
Ethanol solution (volume fraction is 50%, and consumption is 21 times of root of kudzu vine quality), is placed in ultrasonic cleaner and is extracted (power
It is 145W, the time is 25min), cooling, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is carried
Take (power is 145W, and the time is 25min), the supernatant that merging is extracted twice, it is 1.13 to be concentrated into relative density, is soaked
Cream;
B. mulberries pretreatment:Take mulberries 10kg and break into slurry (consumption of water is 6 times of mulberries quality), filtering removes filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum 1kg, henry woodbetony root 5kg and fritillaria thunbergii 6kg are taken, 80% is crushed to
Above grain diameter≤3 μm, (volume fraction is 65%, and consumption is ganoderma lucidum, henry woodbetony root and fritillaria thunbergii gross mass to add ethanol solution
10 times) immersion 45min, then in carried out under 63 DEG C of bath temperatures backflow extraction 10h, filtering;
D. felwort, schizonepeta, Chinese yam and the root of herbaceous peony pretreatment:Felwort 4kg, schizonepeta 5kg, Chinese yam 5kg and root of herbaceous peony 5kg are taken,
Pulverize, of length no more than 5cm of Chinese medicine each component, (consumption is the 4 of felwort, schizonepeta, Chinese yam and root of herbaceous peony gross mass to be placed in water
Times) middle immersion 45min, then decoct to boiling with high heat, then to be cooked by slow fire 15min, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:It is the leaching for adding step A to obtain in the kaoliang spirit 70kg of 28%vol to alcoholic strength
The filtrate that the filtrate for obtaining and step D that the filtrate for obtaining that cream, step B are obtained, step C are obtained obtain, stirring adds activity
Charcoal (consumption is 0.015% of mixture quality after stirring), stands 2 days, and filtrate is carried out pasteurize by filtering, is obtained final product described
Pueraria root health care liquor.
Embodiment 2
A kind of pueraria root health care liquor, is prepared from the following materials:Alcoholic strength is kaoliang spirit 66kg, the root of kudzu vine of 38%vol
20kg, mulberries 6kg, ganoderma lucidum 2kg, felwort 2kg, schizonepeta 3kg, Chinese yam 2kg, root of herbaceous peony 4kg, henry woodbetony root 3kg, fritillaria thunbergii 8kg.
The preparation method of the pueraria root health care liquor is:
A. root of kudzu vine pretreatment:Root of kudzu vine 20kg is taken, cleaned, removed the peel, being crushed to more than 90% grain diameter≤2.5 μm, added
Ethanol solution (volume fraction is 60%, and consumption is 17 times of root of kudzu vine quality), is placed in ultrasonic cleaner and is extracted (power
It is 130W, the time is 20min), cooling, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is carried
Take (power is 130W, and the time is 20min), the supernatant that merging is extracted twice, it is 1.17 to be concentrated into relative density, is soaked
Cream;
B. mulberries pretreatment:Take mulberries 6kg and break into slurry (consumption of water is 8 times of mulberries quality), filtering removes filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum 2kg, henry woodbetony root 3kg and fritillaria thunbergii 8kg are taken, 80% is crushed to
Above grain diameter≤3 μm, (volume fraction is 70%, and consumption is ganoderma lucidum, henry woodbetony root and fritillaria thunbergii gross mass to add ethanol solution
13 times) immersion 30min, then in carried out under 67 DEG C of bath temperatures backflow extraction 8h, filtering;
D. felwort, schizonepeta, Chinese yam and the root of herbaceous peony pretreatment:Felwort 2kg, schizonepeta 3kg, Chinese yam 2kg and root of herbaceous peony 4kg are taken,
Pulverize, of length no more than 5cm of Chinese medicine each component, (consumption is the 7 of felwort, schizonepeta, Chinese yam and root of herbaceous peony gross mass to be placed in water
Times) middle immersion 30min, then decoct to boiling with high heat, then to be cooked by slow fire 10min, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:It is the leaching for adding step A to obtain in the kaoliang spirit 66kg of 38%vol to alcoholic strength
The filtrate that the filtrate for obtaining and step D that the filtrate for obtaining that cream, step B are obtained, step C are obtained obtain, stirring adds activity
Charcoal (consumption is 0.018% of mixture quality after stirring), stands 3 days, and filtrate is carried out pasteurize by filtering, is obtained final product described
Pueraria root health care liquor.
Embodiment 3
A kind of pueraria root health care liquor, is prepared from the following materials:Alcoholic strength is kaoliang spirit 68kg, the root of kudzu vine of 30%vol
21kg, mulberries 8kg, ganoderma lucidum 1.5kg, felwort 3kg, schizonepeta 4kg, Chinese yam 3kg, root of herbaceous peony 4.5kg, henry woodbetony root 4kg, fritillaria thunbergii
7kg。
The preparation method of the pueraria root health care liquor is:
A. root of kudzu vine pretreatment:Root of kudzu vine 21kg is taken, cleaned, removed the peel, being crushed to more than 90% grain diameter≤2.5 μm, added
Ethanol solution (volume fraction is 55%, and consumption is 18 times of root of kudzu vine quality), is placed in ultrasonic cleaner and is extracted (power
It is 140W, the time is 22min), cooling, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is carried
Take (power is 140W, and the time is 22min), the supernatant that merging is extracted twice, it is 1.15 to be concentrated into relative density, is soaked
Cream;
B. mulberries pretreatment:Take mulberries 8kg and break into slurry (consumption of water is 7 times of mulberries quality), filtering removes filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum 1.5kg, henry woodbetony root 4kg and fritillaria thunbergii 7kg are taken, is crushed to
More than 80% grain diameter≤3 μm., (volume fraction is 68%, and consumption is ganoderma lucidum, henry woodbetony root and fritillaria thunbergii to add ethanol solution
11 times of gross mass) immersion 37min, then in backflow extraction 9h is carried out under 64 DEG C of bath temperatures, filters;
D. felwort, schizonepeta, Chinese yam and the root of herbaceous peony pretreatment:Take felwort 3kg, schizonepeta 4kg, Chinese yam 3kg and the root of herbaceous peony
4.5kg, pulverizes, of length no more than 5cm of Chinese medicine each component, and (consumption is felwort, schizonepeta, Chinese yam and the total matter of the root of herbaceous peony to be placed in water
5 times of amount) middle immersion 36min, then decoct to boiling with high heat, then to be cooked by slow fire 12min, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:It is the leaching for adding step A to obtain in the kaoliang spirit 68kg of 30%vol to alcoholic strength
The filtrate that the filtrate for obtaining and step D that the filtrate for obtaining that cream, step B are obtained, step C are obtained obtain, stirring adds activity
Charcoal (consumption is 0.017% of mixture quality after stirring), stands 3 days, and filtrate is carried out pasteurize by filtering, is obtained final product described
Pueraria root health care liquor.
Comparative example 1
A kind of pueraria root health care liquor, is prepared from the following materials:Alcoholic strength is kaoliang spirit 69kg, the root of kudzu vine of 35%vol
24kg, mulberries 9kg, ganoderma lucidum 3kg, felwort 2kg, schizonepeta 5kg, Chinese yam 4kg, root of herbaceous peony 4kg, henry woodbetony root 3kg, fritillaria thunbergii 4kg.
The preparation method of the pueraria root health care liquor is:
A. root of kudzu vine pretreatment:Root of kudzu vine 24kg is taken, cleaned, removed the peel, being crushed to more than 90% grain diameter≤2.5 μm, added
Ethanol solution (volume fraction is 54%, and consumption is 18 times of root of kudzu vine quality), is placed in ultrasonic cleaner and is extracted (power
It is 138W, the time is 23min), cooling, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is carried
Take (power is 133W, and the time is 24min), the supernatant that merging is extracted twice, it is 1.16 to be concentrated into relative density, is soaked
Cream;
B. mulberries pretreatment:Take mulberries 9kg and break into slurry (consumption of water is 8 times of mulberries quality), filtering removes filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum 3kg, henry woodbetony root 3kg and fritillaria thunbergii 4kg are taken, 80% is crushed to
Above grain diameter≤3 μm, (volume fraction is 67%, and consumption is ganoderma lucidum, henry woodbetony root and fritillaria thunbergii gross mass to add ethanol solution
12 times) immersion 37min, then in carried out under 66 DEG C of bath temperatures backflow extraction 8h, filtering;
D. felwort, schizonepeta, Chinese yam and the root of herbaceous peony pretreatment:Felwort 2kg, schizonepeta 5kg, Chinese yam 4kg and root of herbaceous peony 4kg are taken,
Pulverize, of length no more than 5cm of Chinese medicine each component, (consumption is the 6 of felwort, schizonepeta, Chinese yam and root of herbaceous peony gross mass to be placed in water
Times) middle immersion 38min, then decoct to boiling with high heat, then to be cooked by slow fire 14min, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:It is the leaching for adding step A to obtain in the kaoliang spirit 69kg of 35%vol to alcoholic strength
The filtrate that the filtrate for obtaining and step D that the filtrate for obtaining that cream, step B are obtained, step C are obtained obtain, stirring adds activity
Charcoal (consumption is 0.017% of mixture quality after stirring), stands 2 days, and filtrate is carried out pasteurize by filtering, is obtained final product described
Pueraria root health care liquor.
Comparative example 2
A kind of pueraria root health care liquor, is prepared from the following materials:Alcoholic strength is kaoliang spirit 70kg, the root of kudzu vine of 37%vol
20kg, mulberries 7kg, ganoderma lucidum 2kg, felwort 4kg, schizonepeta 4kg, Chinese yam 5kg, henry woodbetony root 3kg, fritillaria thunbergii 6kg.
The preparation method of the pueraria root health care liquor is:
A. root of kudzu vine pretreatment:Root of kudzu vine 20kg is taken, cleaned, removed the peel, being crushed to more than 90% grain diameter≤2.5 μm, added
Ethanol solution (volume fraction is 50%, and consumption is 18 times of root of kudzu vine quality), is placed in ultrasonic cleaner and is extracted (power
It is 142W, the time is 21min), cooling, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is carried
Take (power is 130W, and the time is 25min), the supernatant that merging is extracted twice, it is 1.15 to be concentrated into relative density, is soaked
Cream;
B. mulberries pretreatment:Take mulberries 7kg and break into slurry (consumption of water is 7 times of mulberries quality), filtering removes filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum 2kg, henry woodbetony root 3kg and fritillaria thunbergii 6kg are taken, 80% is crushed to
Above grain diameter≤3 μm, (volume fraction is 65%, and consumption is ganoderma lucidum, henry woodbetony root and fritillaria thunbergii gross mass to add ethanol solution
11 times) immersion 30min, then in carried out under 63 DEG C of bath temperatures backflow extraction 8h, filtering;
D. felwort, schizonepeta and Chinese yam pretreatment:Felwort 4kg, schizonepeta 4kg and Chinese yam 5kg are taken, is pulverized, Chinese medicine each group
The of length no more than 5cm for dividing, is placed in immersion 45min in water (consumption is 6 times of felwort, schizonepeta, Chinese yam and root of herbaceous peony gross mass),
Then decoct to boiling with high heat, then to be cooked by slow fire 14min, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:It is the leaching for adding step A to obtain in the kaoliang spirit 70kg of 37%vol to alcoholic strength
The filtrate that the filtrate for obtaining and step D that the filtrate for obtaining that cream, step B are obtained, step C are obtained obtain, stirring adds activity
Charcoal (consumption is 0.018% of mixture quality after stirring), stands 3 days, and filtrate is carried out pasteurize by filtering, is obtained final product described
Pueraria root health care liquor.
Comparative example 3
A kind of pueraria root health care liquor, is prepared from the following materials:Alcoholic strength is kaoliang spirit 68kg, the root of kudzu vine of 30%vol
24kg, mulberries 8kg, ganoderma lucidum 2kg, felwort 4kg, schizonepeta 4kg, Chinese yam 4kg, root of herbaceous peony 4kg, henry woodbetony root 4kg, fritillaria thunbergii 8kg.
The preparation method of the pueraria root health care liquor is:
A. root of kudzu vine pretreatment:Root of kudzu vine 24kg is taken, cleaned, removed the peel, being crushed to more than 90% grain diameter≤2.5 μm, added
Ethanol solution (volume fraction is 58%, and consumption is 20 times of root of kudzu vine quality), is placed in ultrasonic cleaner and is extracted (power
It is 138W, the time is 21min), cooling, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is carried
Take (power is 135W, and the time is 22min), the supernatant that merging is extracted twice, it is 1.16 to be concentrated into relative density, is soaked
Cream;
B. mulberries pretreatment:Take mulberries 8kg and break into slurry (consumption of water is 7 times of mulberries quality), filtering removes filter residue;
C. ganoderma lucidum, schizonepeta, henry woodbetony root and fritillaria thunbergii pretreatment:Take ganoderma lucidum 2kg, schizonepeta 4kg, henry woodbetony root 4kg and fritillaria thunbergii
8kg, is crushed to more than 80% grain diameter≤3 μm, add ethanol solution (volume fraction is 68%, consumption be ganoderma lucidum, schizonepeta,
12 times of henry woodbetony root and fritillaria thunbergii gross mass) immersion 36min, then in backflow extraction 9h is carried out under 66 DEG C of bath temperatures, filters;
D. felwort, Chinese yam and the root of herbaceous peony pretreatment:Felwort 4kg, Chinese yam 4kg and root of herbaceous peony 4kg are taken, is pulverized, Chinese medicine each group
The of length no more than 5cm for dividing, is placed in immersion 44min in water (consumption is 4 times of felwort, Chinese yam and root of herbaceous peony gross mass), then
Decoct to boiling with high heat, then to be cooked by slow fire 12min, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:It is the leaching for adding step A to obtain in the kaoliang spirit 68kg of 30%vol to alcoholic strength
The filtrate that the filtrate for obtaining and step D that the filtrate for obtaining that cream, step B are obtained, step C are obtained obtain, stirring adds activity
Charcoal (consumption is 0.015% of mixture quality after stirring), stands 2 days, and filtrate is carried out pasteurize by filtering, is obtained final product described
Pueraria root health care liquor.
Pueraria root health care liquor sensory evaluation
Selection 5 has the tasters of more than 3 years experiences of sampling wine, to embodiment 1-3 and root of kudzu vine guarantor obtained in comparative example 1-3
Strong wine carries out the sensory evaluation in terms of outward appearance, smell and mouthfeel (sensory evaluation standard is as shown in table 1).
The pueraria root health care liquor sensory evaluation standard of table 1
Wherein, the detection method of outward appearance is:Under suitable light (non-direct sunlight), glass post is grasped, cheered
Qi Mei, the color and luster of the wine that detects by an unaided eye, transparency, clarification degree, whether there is precipitation, suspension, as a result as shown in table 2;
The detection method of smell is:First apply one's nose under static state 3 times, then hold in both hands wineglass in the palm of shaking hands, make wine
Heating slightly, and wineglass is shaken, wine is distributed on glass wall in making cup.Wineglass of speaking slowly is placed in nostril lower section, smelling its Volatile Gas
Taste, differentiate medicine perfume, aroma, whether have peculiar smell, as a result as shown in table 2;
The method of inspection of mouthfeel is:A small amount of sample is drunk in mouth, gustatory area is uniformly distributed in as far as possible, carefully tasted, had
Under clear and definite impression posterior phraynx, then know from experience taste after mouthfeel, as a result as shown in table 2:
The pueraria root health care liquor Analyses Methods for Sensory Evaluation Results of table 2
Pueraria root health care liquor physical and chemical index is checked
To embodiment 1-3 and pueraria root health care liquor obtained in comparative example 1-3 carries out the survey of total reducing sugar, total acid, total ester, sugar-free extract
It is fixed.
Wherein, total reducing sugar according to《GB/T45038-2006 grape wine fruit wine universaling analysis methods》Tested, as a result such as table 3
It is shown;
Total acid according to《GB/T45038-2006 grape wine fruit wine universaling analysis methods》Tested, as a result as shown in table 3;
Total ester according to《GB/T45038-2006 grape wine fruit wine universaling analysis methods》Tested, as a result as shown in table 3;
Sugar-free extract according to《GB/T45038-2006 grape wine fruit wine universaling analysis methods》Tested, as a result such as table 3
It is shown;
The pueraria root health care liquor physical and chemical index testing result of table 3
Pueraria root health care liquor efficacy validation
It is curative effect of the obtained pueraria root health care liquor of the checking present invention in terms of antimigraine is treated, where inventor circumferentially
Patients with 300 Cases is accepted in area for medical treatment altogether, is randomly divided into 6 groups.Every group of patient's daily morning 9:00th, afternoon 17:00 drinks embodiment respectively
1-3 and pueraria root health care liquor 1 time obtained in comparative example 1-3, each 20mL, Ganderwa is 3 months.Diagnosis and treatment evaluation criteria is:Fully recover from an illness
More, clinical symptom disappearance, disables half a year no relapse;Effectively, symptom mitigation, but do not take a turn for the better completely;Invalid, symptom is without substantially changing
Become.Test result is as shown in table 4:
The pueraria root health care liquor health-care effect of table 4
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to compared with
Good embodiment has been described in detail to the present invention, it will be understood by those within the art that, can be to skill of the invention
Art scheme is modified or equivalent, and without deviating from the objective and scope of technical solution of the present invention, it all should cover at this
In the middle of the right of invention.
Claims (10)
1. pueraria root health care liquor, it is characterised in that be prepared from by following mass parts raw material:Kaoliang spirit 66-70 parts, root of kudzu vine 20-25
Part, mulberries 6-10 parts, ganoderma lucidum 1-2 parts, felwort 2-4 parts, schizonepeta 3-5 parts, Chinese yam 2-5 parts, root of herbaceous peony 4-5 parts, henry woodbetony root 3-5
Part, fritillaria thunbergii 6-8 parts.
2. pueraria root health care liquor according to claim 1, it is characterised in that the alcoholic strength of the liquor made from sorghum is 28-38%
vol。
3. the preparation method of the pueraria root health care liquor described in claim 1, it is characterised in that comprise the following steps:
A. root of kudzu vine pretreatment:The root of kudzu vine of above-mentioned mass parts is taken, cleaning, peeling, crushing add ethanol solution, be placed in ultrasonic wave clear
Wash in device and extracted, cool down, centrifugation, centrifuged deposit adds ethanol solution, is placed in ultrasonic cleaner and is extracted, close
And the supernatant for extracting twice, concentration, obtain medicinal extract;
B. mulberries pretreatment:The mulberries for taking above-mentioned mass parts break into slurry, filtering, remove filter residue;
C. ganoderma lucidum, henry woodbetony root and fritillaria thunbergii pretreatment:Ganoderma lucidum, henry woodbetony root and the fritillaria thunbergii of above-mentioned mass parts are taken, is crushed, add second
Alcoholic solution soaks 30-45min, then in backflow extraction 8-10h is carried out under 63-67 DEG C of bath temperature, filters;
D. felwort, schizonepeta, Chinese yam and the root of herbaceous peony pretreatment:Felwort, schizonepeta, Chinese yam and the root of herbaceous peony of above-mentioned mass parts are taken, are pulverized,
Of length no more than 5cm of Chinese medicine each component, is placed in water immersion 30-45min, then decocts to boiling with high heat, then with slow fire
10-15min is decocted, filtering removes filter residue;
E. the preparation of pueraria root health care liquor:Obtained to the medicinal extract, step B that add step A to obtain in the kaoliang spirit of above-mentioned mass parts
The filtrate that the filtrate for obtaining and step D that the filtrate that obtains, step C are obtained obtain, stirring adds activated carbon, stands 2-3 days,
Filtering, filtrate is sterilized, obtain final product the pueraria root health care liquor.
4. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that the degree crushed described in step A
To be crushed to more than 90% grain diameter≤2.5 μm.
5. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that ethanol solution described in step A is
Volume fraction is the ethanol solution of 50-60%, and the consumption of ethanol solution is 17-21 times of root of kudzu vine quality.
6. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that ultrasonic wave extraction described in step A
During, the power of ultrasonic wave is 130-145W, and the time is 20-25min.
7. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that the degree concentrated described in step A
To be concentrated into relative density for 1.13-1.17.
8. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that ethanol solution described in step C is
Volume fraction is the ethanol solution of 65-70%, and the consumption of ethanol solution is the 10-13 of ganoderma lucidum, henry woodbetony root and fritillaria thunbergii gross mass
Times.
9. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that the sterilization described in step E is
Realized by pasteurize.
10. the preparation method of pueraria root health care liquor according to claim 3, it is characterised in that the use of activated carbon described in step E
It is the 0.015-0.018% of mixture quality after stirring to measure.
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