CN108698972B - 在流反应器中制备(烷基)丙烯酸酯的方法 - Google Patents

在流反应器中制备(烷基)丙烯酸酯的方法 Download PDF

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Publication number
CN108698972B
CN108698972B CN201780013295.8A CN201780013295A CN108698972B CN 108698972 B CN108698972 B CN 108698972B CN 201780013295 A CN201780013295 A CN 201780013295A CN 108698972 B CN108698972 B CN 108698972B
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Prior art keywords
alkyl
halide
alcohol
addition port
acryloyl
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Chinese (zh)
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CN108698972A (zh
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鲁道夫·J·达姆斯
鲁迪·W·范坎彭豪特
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3M Innovative Properties Co
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3M Innovative Properties Co
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/14—Preparation of carboxylic acid esters from carboxylic acid halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201780013295.8A 2016-02-25 2017-02-21 在流反应器中制备(烷基)丙烯酸酯的方法 Active CN108698972B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201662299575P 2016-02-25 2016-02-25
US62/299,575 2016-02-25
PCT/US2017/018633 WO2017147040A1 (en) 2016-02-25 2017-02-21 Methods of making (alk)acrylic esters in flow reactors

Publications (2)

Publication Number Publication Date
CN108698972A CN108698972A (zh) 2018-10-23
CN108698972B true CN108698972B (zh) 2021-06-29

Family

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CN201780013295.8A Active CN108698972B (zh) 2016-02-25 2017-02-21 在流反应器中制备(烷基)丙烯酸酯的方法

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Country Link
US (1) US10308584B2 (https=)
EP (1) EP3419958B1 (https=)
JP (1) JP6909798B2 (https=)
CN (1) CN108698972B (https=)
WO (1) WO2017147040A1 (https=)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3638646A1 (en) * 2017-06-12 2020-04-22 3M Innovative Properties Company Methods of making benzophenonyl(alk)acrylic esters and substituted benzophenonyl(alk)acrylic esters in flow reactors
EP3502089B1 (en) 2017-12-20 2020-08-19 3M Innovative Properties Company Process for the manufacturing of a 3-halopropionyl halide in a flow reactor
EP3502088A1 (en) 2017-12-20 2019-06-26 3M Innovative Properties Company Process for the manufacturing of an acid halide in a flow reactor
EP3502090B1 (en) 2017-12-20 2020-08-19 3M Innovative Properties Company Process for the manufacturing of a compound comprising a (meth)acryloyl group
EP3524589A1 (en) 2018-02-09 2019-08-14 3M Innovative Properties Company Process for the manufacturing of a (meth)acrylic anhydride in a flow reactor
CN112189004B (zh) 2018-05-23 2023-12-15 赢创运营有限公司 制备酮基官能化的芳族(甲基)丙烯酸化产物的方法
SG11202100238TA (en) 2018-07-17 2021-02-25 Evonik Operations Gmbh Method for preparing c-h acidic (meth)acrylates
EP3599232A1 (de) 2018-07-26 2020-01-29 Evonik Operations GmbH Verfahren zur herstellung von n-methyl(meth)acrylamid
US10807063B1 (en) * 2019-12-31 2020-10-20 Industrial Technology Research Institute Device and method for continuously manufacturing acrylate compound
CN114409927A (zh) * 2022-01-24 2022-04-29 安徽省纳胜生物科技有限公司 万吨级高粘速溶超高分子量聚丙烯酸钠及其制备方法与应用
TWI913079B (zh) * 2024-12-31 2026-01-21 財團法人工業技術研究院 微通道反應器合成丙烯酸酯之方法

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US1951782A (en) * 1931-01-29 1934-03-20 Rohm & Haas Process for making esters of acrylic acid
JP2004285001A (ja) * 2003-03-24 2004-10-14 Sumitomo Chem Co Ltd 含酸素化合物の製造方法
CN1553889A (zh) * 2001-09-10 2004-12-08 �����ɷ� (甲基)丙烯酸酯的制备方法
JP2004345974A (ja) * 2003-05-20 2004-12-09 Asahi Kasei Chemicals Corp カルボン酸エステルの連続的製造方法
CN101993371A (zh) * 2010-12-01 2011-03-30 长春工业大学 丙烯酸烯丙酯的制备方法
CN104086415A (zh) * 2014-07-18 2014-10-08 南京工业大学 一种利用微反应装置制备乙酰柠檬酸三丁酯的方法
CN104447311A (zh) * 2014-10-31 2015-03-25 上海博康精细化工有限公司 1-甲基-环戊醇-丙烯酸酯及其制备方法

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JPS6263541A (ja) * 1984-12-18 1987-03-20 Nippon Shokubai Kagaku Kogyo Co Ltd アクリル酸またはメタクリル酸エステルの製造方法
JPS61215355A (ja) * 1985-03-20 1986-09-25 Nippon Shokubai Kagaku Kogyo Co Ltd アクリル酸またはメタクリル酸の含フツ素アルキルエステルの製法
DE69318188T3 (de) 1993-09-15 2003-05-28 Ciba Speciality Chemicals Water Treatments Ltd., Bradford Synthese von vinylestern
US5808148A (en) 1997-01-03 1998-09-15 Eastman Chemical Company Preparation of α,β-unsaturated carboxylic acids and esters
GB9723260D0 (en) * 1997-11-05 1998-01-07 British Nuclear Fuels Plc A method of performing a chemical reaction
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JP4080723B2 (ja) 2001-10-30 2008-04-23 三菱レイヨン株式会社 レジスト用モノマーの製造方法
AR038161A1 (es) 2002-01-24 2004-12-29 Basf Ag Procedimiento para separar acidos de mezclas de reaccion quimicas con la ayuda de liquidos ionicos
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US1951782A (en) * 1931-01-29 1934-03-20 Rohm & Haas Process for making esters of acrylic acid
CN1553889A (zh) * 2001-09-10 2004-12-08 �����ɷ� (甲基)丙烯酸酯的制备方法
JP2004285001A (ja) * 2003-03-24 2004-10-14 Sumitomo Chem Co Ltd 含酸素化合物の製造方法
JP2004345974A (ja) * 2003-05-20 2004-12-09 Asahi Kasei Chemicals Corp カルボン酸エステルの連続的製造方法
CN101993371A (zh) * 2010-12-01 2011-03-30 长春工业大学 丙烯酸烯丙酯的制备方法
CN104086415A (zh) * 2014-07-18 2014-10-08 南京工业大学 一种利用微反应装置制备乙酰柠檬酸三丁酯的方法
CN104447311A (zh) * 2014-10-31 2015-03-25 上海博康精细化工有限公司 1-甲基-环戊醇-丙烯酸酯及其制备方法

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Publication number Publication date
US10308584B2 (en) 2019-06-04
EP3419958B1 (en) 2020-04-29
JP2019506420A (ja) 2019-03-07
CN108698972A (zh) 2018-10-23
WO2017147040A1 (en) 2017-08-31
JP6909798B2 (ja) 2021-07-28
US20190062257A1 (en) 2019-02-28
EP3419958A1 (en) 2019-01-02

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