CN108658803B - 一种n,n-二烷基二苯基丙酰胺的合成方法 - Google Patents
一种n,n-二烷基二苯基丙酰胺的合成方法 Download PDFInfo
- Publication number
- CN108658803B CN108658803B CN201810783085.3A CN201810783085A CN108658803B CN 108658803 B CN108658803 B CN 108658803B CN 201810783085 A CN201810783085 A CN 201810783085A CN 108658803 B CN108658803 B CN 108658803B
- Authority
- CN
- China
- Prior art keywords
- dialkyl
- diphenylpropanamide
- reaction
- benzophenone
- synthesizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810783085.3A CN108658803B (zh) | 2018-07-16 | 2018-07-16 | 一种n,n-二烷基二苯基丙酰胺的合成方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810783085.3A CN108658803B (zh) | 2018-07-16 | 2018-07-16 | 一种n,n-二烷基二苯基丙酰胺的合成方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN108658803A CN108658803A (zh) | 2018-10-16 |
CN108658803B true CN108658803B (zh) | 2020-11-24 |
Family
ID=63788380
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810783085.3A Active CN108658803B (zh) | 2018-07-16 | 2018-07-16 | 一种n,n-二烷基二苯基丙酰胺的合成方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN108658803B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110305016B (zh) * | 2019-08-13 | 2021-08-31 | 青岛科技大学 | 一步法制备4-羟苄基苯甲醛碳酸酯 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB796839A (en) * | 1955-06-23 | 1958-06-18 | Pharmacia Ab | N,n-disubstituted amides of aryl acetic acids |
CN106957323A (zh) * | 2017-04-06 | 2017-07-18 | 青岛科技大学 | 一种合成芝麻素前体的简易方法 |
CN108997158A (zh) * | 2018-07-16 | 2018-12-14 | 青岛科技大学 | 一种实现二取代酰胺与二苯基甲酮偶联的方法 |
-
2018
- 2018-07-16 CN CN201810783085.3A patent/CN108658803B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB796839A (en) * | 1955-06-23 | 1958-06-18 | Pharmacia Ab | N,n-disubstituted amides of aryl acetic acids |
CN106957323A (zh) * | 2017-04-06 | 2017-07-18 | 青岛科技大学 | 一种合成芝麻素前体的简易方法 |
CN108997158A (zh) * | 2018-07-16 | 2018-12-14 | 青岛科技大学 | 一种实现二取代酰胺与二苯基甲酮偶联的方法 |
Non-Patent Citations (2)
Title |
---|
New Generation Method for a Samarium(II) Equivalent: MegSiX;Noriyuki Akane,等;《J. Org. Chem.》;19941201;第59卷(第25期);全文 * |
Sm/I2体系促进芳酮和酰胺/腈的反应研究;李晶晶;《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》;20181015(第10期);第36页倒数第1段,第54页第3.3.1.1节,第58页第3.4节,第56页表3-2 * |
Also Published As
Publication number | Publication date |
---|---|
CN108658803A (zh) | 2018-10-16 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP6719527B2 (ja) | アゾキシストロビン中間体の調製方法 | |
CN108658803B (zh) | 一种n,n-二烷基二苯基丙酰胺的合成方法 | |
CN109096126B (zh) | 一种氘标记d9-盐酸克伦特罗的合成方法 | |
CN108997158B (zh) | 一种实现二取代酰胺与二苯基甲酮偶联的方法 | |
CN113831318A (zh) | 一种胡椒乙胺的合成方法 | |
CN114349674A (zh) | 一种硫脲类化合物及其制备方法 | |
CN110317132B (zh) | 一种苯丁酸钠的制备方法 | |
CN110698352A (zh) | 一种3-溴-5-氨基邻苯二酚二甲醚的合成方法 | |
CN1353686A (zh) | 制备(1r,2s,4r)-(-)-2-[(2′-{n,n-二甲基氨基}乙氧基)]-2-[苯基]-1,7,7-三[甲基]-二环[2.2.1]庚烷及其可药用酸加成盐的方法 | |
CN108383754B (zh) | 一类芳基肟脂化合物的制备方法和应用 | |
CN108689880B (zh) | 无溶剂法制备二苯基羟基丙腈 | |
CN111393338A (zh) | 一种多菲利特-d3药物及其制备方法 | |
CN111777520A (zh) | 多位取代的二甲氨基苯基乙酸类化合物的合成方法 | |
CN110615751A (zh) | 一种2-氧代硫代丙酰胺的制备方法 | |
CN104311456A (zh) | 一种愈创木酚磺酸钾的制备方法 | |
CN111732556B (zh) | 一种氘代的洛沙平药物及其制备方法 | |
CN111072476B (zh) | β-酮酸酯类化合物氧上高选择性一氟甲基化的方法 | |
CN109265352B (zh) | 芳基环丙基醚及其衍生物的制备方法 | |
CN108822060B (zh) | 一种3-芳基取代氧杂环丁烷及其制备方法 | |
CN114380661B (zh) | 一种(±)-薰衣草醇的合成方法 | |
CN108558750B (zh) | 无溶剂法合成3-硝基喹啉衍生物的工艺 | |
CN110305083B (zh) | 一种以果糖制备5-氯甲基糠醛的工艺 | |
CN112409186B (zh) | 一种在水中合成n-甲基苯胺的方法 | |
CN108840793B (zh) | 一种应用模拟移动床色谱制备γ-崖柏素的方法 | |
CN110498812B (zh) | 一种艾拉普林的中间体化合物的制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20220818 Address after: 230000 Room 203, building 2, phase I, e-commerce Park, Jinggang Road, Shushan Economic Development Zone, Hefei City, Anhui Province Patentee after: Hefei Jiuzhou Longteng scientific and technological achievement transformation Co.,Ltd. Address before: No. 53, Zhengzhou Road, North District, Qingdao, Shandong Patentee before: QINGDAO University OF SCIENCE AND TECHNOLOGY |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230403 Address after: 2401-022 (centralized office area), 193 Jiangshan Middle Road, Qingdao Area, China (Shandong) Pilot Free Trade Zone, Qingdao, Shandong 266000 Patentee after: Shandong Dejing Energy Technology Co.,Ltd. Address before: 230000 Room 203, building 2, phase I, e-commerce Park, Jinggang Road, Shushan Economic Development Zone, Hefei City, Anhui Province Patentee before: Hefei Jiuzhou Longteng scientific and technological achievement transformation Co.,Ltd. |
|
TR01 | Transfer of patent right |