CN108658675A - A kind of high-content sugar alcohol calcium boron clear liquid fertilizer and preparation method thereof - Google Patents
A kind of high-content sugar alcohol calcium boron clear liquid fertilizer and preparation method thereof Download PDFInfo
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- CN108658675A CN108658675A CN201810738103.6A CN201810738103A CN108658675A CN 108658675 A CN108658675 A CN 108658675A CN 201810738103 A CN201810738103 A CN 201810738103A CN 108658675 A CN108658675 A CN 108658675A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C5/00—Fertilisers containing other nitrates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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Abstract
The invention discloses a kind of high-content sugar alcohol calcium boron clear liquid fertilizer and preparation method thereof, the fertilizer includes calcium compound, boron compound, magnesium compound, compound sugar alcohol, surfactant and cosolvent etc., utilize sugar alcohol chelating technology, clear liquid type calcium boron foliar fertilizer obtaining water white transparency, stablizing, calcium content is 120 ~ 140g/L, boron content is 20 ~ 30g/L, and the mass ratio of content of magnesium 10g/L, compound sugar alcohol are more than 15%.The calcium boron chelated using sugar alcohol, product stability is good, compound sugar alcohol has huge synergistic effect to absorption, the transhipment of calcium and boron, it can not only prevent from causing bitter pit, shepherd's purse maize ear rot and black red spot disease etc. because of calcium deficiency and boron, in terms of improving fruit quality, fruit appearance luster can be made good, hardness is high, resistance to storage, it is in good taste, it increases economic efficiency from quality.
Description
Technical field
The invention belongs to the technical field of agriculture composite calcium and boron, be related to a kind of high-content sugar alcohol calcium boron clear liquid fertilizer and its
Preparation method.
Background technology
Physiological disease is related with calcium deficiency there are many having now been found that in fruit tree, such as apple bitter pit, bitter pit, internal collapse
Disease, carbuncle spot disease, cork pinta, water core, brown boiling hot disease, suberification spot disease, hole skin ruin disease, pears black heart, mango it is soft
Nose disease etc..These physiological diseases seriously affect fruit quality and storing property.The prediction of Fruit physiology imbalance is often passed through at present
The content of calcium in front vane and fruit is adopted to carry out.It is reported that calcium content can predict the life of fruit in storage before being adopted according to apple
Disease incidence is managed, when being more than 3mg per 100g fresh weight calcics, substantially disease-free generation；When calcium content is less than 1.5mg, hair
Sick rate is more than 15%.It is reported that the enforcement of Calcium in Plants semiotic function depends on intracellular Ca2+Library is to the release of calcium ion or by born of the same parents
Outer Ca2+The Ca that library is inwardly transported2+The increase of stream, cytoplasm Ca2+The moment of concentration improves, and stimulates a series of biochemical reaction.Calcium
When insufficient, Ca is generated2+Signal dysfunction, Ca2+Library can not supplement intracellular Ca2+Library, Ca2+Deficiency make cell loss to the external world
The respond of environmental stimulus, to make fruit generate physiological disease.Cause cellular level Ca2+Any nutrition condition lacked is such as
High antagonism ION Mg2+, K+Fruit physiology disease can be caused, if calcium/magnesium is than low susceptible bitter pit, high potassium/calcium is than susceptible
Bitter pit.
Boron deficiency causes Fruit physiology imbalance just to be had been reported early in the 60's.It is reported that the bolt of the fruits such as apple, citrus
It is related with the shortage of boron to change disease, cracked fruit and bitter pit, symptom mitigates or completely disappears after spraying boron, improves the quality of fruit.
It may be the metabolic disorders such as nucleic acid, protein since the hormonal balance of cell destroys that boron deficiency, which causes the mechanism of Fruit physiology disease,
Aldehydes matter and accumulated active oxygen, fruit tissue necrosis；On the other hand, since boron deficiency makes conducting tissue seriously be destroyed.Boron
Calcium reciprocal effects significantly affect the physiological metabolism of fruit.GranelliG etc. (1989) thinks that the bitter pit for spraying boron mitigation apple is
Boron calcium interaction as a result, because the calcium content of fruit significantly improves after spray boron.B/Ca ratios appropriate can reduce the suberification disease of apple
And bitter pit.Experiment points out that citrus leaves, effective B/ Ca ratios of pericarp and Cracking fruit are in notable and extremely notable positive respectively
It closes.
In recent years, the application of calcium, boron on fruit tree is very extensive, they have fruit quality and keeping quality important
It influences.And calcium boron fertilizer on the market has the disadvantages that：1, calcium boron fertilizer is mostly based on composite fertilizer；2, its calcium boron of calcic boron foliar fertilizer
Content is relatively low；3, its boron content of high calcium content calcium boron fertilizer is insufficient, and calcium boron is than unreasonable；4, do not have and promote the collaboration increasing that calcium boron absorbs
Imitate substance.
And the present invention has the following advantages：1, clear liquid shape foliar fertilizer is made in the present invention, and complete water-soluble, foliage-spray effect is fast；
2, it is chelated using sugar alcohol, quickly can be absorbed by plants and transport, utilization rate is high；3, in the case of high calcium content, have high boron and contain
Amount, it is ensured that calcium boron is the same as benefit；4, it can be directed to the ratio of different crop demand adjustment transformation calcium boron and sugar alcohol, carried with maximum limit
High usage and fertilizer efficiency.
About the foliar fertilizer that calcium boron shares, Chinese patent《A kind of calcium-boron composite type foliage fertilizer and preparation method thereof》（Application
Number：200810029157）Apply for that a kind of calcium-boron composite type foliage fertilizer and preparation method thereof, the solvent used are a contracting second two
Alcohol, cosolvent are glycerine.Chinese patent《A kind of amino acid calcium boron chelated foliar fertilizer and preparation method thereof》（Application number：
201110306688）It is related to amino acid chelated calcium boron foliar fertilizer, calcium boron content is relatively low.The content that the above patent is included all with
The present invention does not obviously contact.
In conclusion in order to realize that calcium boron with mending, improves crop absorption and transport improvement effect, invention is this for improving fruit
Real quality those high in calcium boron foliar fertilizer is very necessary.
Invention content
Present invention aims to overcome that the Antagonism of calcium boron in chemistry, a kind of high-content is developed using suitable cosolvent
Calcium boron foliar fertilizer adds synergistic substance sugar alcohol, promotes calcium boron to absorb, increase operation rate, can be directed to Different Crop demand into
Row adjusts the ratio of calcium boron and sugar alcohol, and addition magnesium elements ensure to supplement magnesium elements while fruit supplement calcium boron, improve fruit product
Matter prevents the various illnesss because of calcium deficiency boron from occurring.
The above-mentioned purpose of the present invention is achieved through the following technical solutions：
A kind of high-content sugar alcohol calcium boron clear liquid fertilizer, is calcium containing compound, boron compound, magnesium compound, compound sugar alcohol, surface-active
Agent and cosolvent etc., calcium content are 120 ~ 140g/L, and boron content is 20 ~ 30g/L, content of magnesium 10g/L, the matter of compound sugar alcohol
Amount is than being more than 15%.
High-content sugar alcohol calcium boron clear liquid fertilizer, the calcium containing compound is calcium nitrate and calcium chloride, and boron-containing compound is boron
Acid, magnesium-containing compound are magnesium nitrate, and the surfactant is empgen BB, and the cosolvent is ethanol amine.
High-content sugar alcohol calcium boron clear liquid fertilizer, based on mass fraction, the compound sugar alcohol includes 7 ~ 10% glycerine, 4 ~ 7%
Sorbierite, 2 ~ 5% mannitol.
High-content sugar alcohol calcium boron clear liquid fertilizer, based on mass fraction, the empgen BB is 2%, the ethyl alcohol
Amine is 4.5 ~ 6.5%.
Compared with prior art, it is an advantage of the invention that：
1, the Antagonism of calcium boron in chemistry is overcome, the calcium boron of high-content is enable to be dissolved in same system altogether.
2, flexible modulation calcium boron ratio can be needed according to crop.
3, it can cross and adapt to different natural temperature weathers, there is higher product stability.
4, using sugar alcohol chelating technology, make calcium boron that there is high absorption and transfer efficiency.
5, magnesium elements are added, fruit quality is also of crucial importance.
6, it is added to surfactant, blade face is improved and opens up, improve utilization rate of fertilizer.
Specific implementation mode
A kind of high-content sugar alcohol calcium boron clear liquid foliar fertilizer of present invention offer and preparation method thereof, sprays the blade face with crop,
By chelating fertilizer to promote to absorb, practice use shows with obvious effects.It is illustrated with the following example, but following implementations
Example is only preferred examples of the present invention, and is not intended to limit the present invention, all any modifications within the principle of the present invention, made and
Variation, within protection scope of the present invention.
A kind of high-content sugar alcohol calcium boron clear liquid clear liquid fertilizer, be calcium containing compound, boron compound, magnesium compound, compound sugar alcohol,
Surfactant and cosolvent etc., but Different Crop calcium is different from the demand of boron, and the type and ratio of sugar alcohol are also different, contain
Amount ratio is：Calcium content is 120 ~ 140g/L, and boron content is 20 ~ 30g/L, content of magnesium 10g/L；The mass ratio of compound sugar alcohol is big
In 15%, be respectively 7 ~ 10% glycerine, 4 ~ 9% sorbierite, 2 ~ 5% mannitol；The surfactant is the 12 of 2%
Alkyl betaine, the ethanol amine that the cosolvent is 4.5 ~ 6.5%.
In above-mentioned fertilizer, the species content distribution for the content ratio and sugar alcohol of Different Crop calcium and boron can root
It is matched according to the demand of crop.And the interpretation of result provided according to farmer for many years, propose the calcium of Different Crop and boron and
The demand of sugar alcohol matches, and specific proportioning is specific as shown in table 1.
1 Different Crop of table matches table to calcium and boron demand
| Crop title | Calcium（g/L） | Boron（g/L） | Glycerine（%） | Sorbierite（%） | Mannitol（%） |
| Citrus（Southern Fruit Trees） | 120 | 30 | 10 | 7 | 3 |
| Apple（Northern fruit tree） | 130 | 30 | 8 | 7 | 2 |
| Banana（Musa） | 130 | 20 | 7 | 5 | 5 |
| Capsicum（Solanaceous vegetables） | 140 | 30 | 7 | 4 | 4 |
| Corn（Unifacial leaf） | 120 | 20 | 8 | 5 | 5 |
And the proportioning of the preparation process and each component for fertilizer, it is illustrated below by embodiment.
Embodiment 1
A kind of preparation method for the high-content sugar alcohol calcium boron clear liquid fertilizer improving fruit quality, includes the following steps：
（1）Based on mass fraction, by 26.5 parts of water, 6.5 parts of ethanol amine（Cosolvent）, 12.5 parts of boric acid, by successively suitable
Sequence is added in reaction kettle, stirs 30 minutes, boric acid is completely dissolved to water white transparency, obtains B solution；
（2）Based on mass fraction, 10 parts of glycerine, 7 parts of sorbierite, 3 parts of mannitol, stirring to sugar are added in B solution
Alcohol obtains sugar alcohol B solution after being completely dissolved；
（3）Based on mass fraction, 25 parts of calcium chloride, 7.5 parts of magnesium nitrate are added in sugar alcohol B solution, it is small persistently to stir 3
When sugar alcohol chelating calcium B solution is obtained after calcium, magnesium compound are completely dissolved；
（4）Based on mass fraction, 2 parts of surfactant is added in sugar alcohol chelating calcium B solution, stirs 20 minutes, obtains height
Content sugar alcohol calcium boron clear liquid fertilizer, then dispenses.
Embodiment 2
A kind of preparation method for the high-content sugar alcohol calcium boron clear liquid fertilizer improving fruit quality, includes the following steps：
（1）Based on mass fraction, by 23 parts of water, 6 parts of ethanol amine（Cosolvent）, 12.5 parts of boric acid sequentially adds
It is added in reaction kettle, stirs 30 minutes, boric acid is completely dissolved to water white transparency, obtains B solution；
（2）Based on mass fraction, 8 parts of glycerine, 7 parts of sorbierite, 2 parts of mannitol, stirring to sugar are added in B solution
Alcohol obtains sugar alcohol B solution after being completely dissolved；
（3）Based on mass fraction, 10 parts of calcium nitrate, 22 parts of calcium chloride, 7.5 parts of nitric acid are added in sugar alcohol B solution
Magnesium persistently stirs 3 hours and obtains sugar alcohol chelating calcium B solution after calcium, magnesium compound are completely dissolved；
（4）Based on mass fraction, 2 parts of surfactant is added in sugar alcohol chelating calcium B solution, stirs 20 minutes, obtains height
Content sugar alcohol calcium boron clear liquid fertilizer, then dispenses.
Embodiment 3
A kind of preparation method for the high-content sugar alcohol calcium boron clear liquid fertilizer improving fruit quality, includes the following steps：
（1）Based on mass fraction, by 25 parts of water, 5 parts of ethanol amine（Cosolvent）, 8.5 parts of boric acid sequentially adds
Into reaction kettle, stir 30 minutes, boric acid is completely dissolved to water white transparency, obtains B solution；
（2）Based on mass fraction, 7 parts of glycerine, 5 parts of sorbierite, 5 parts of mannitol, stirring to sugar are added in B solution
Alcohol obtains sugar alcohol B solution after being completely dissolved；
（3）Based on mass fraction, 15 parts of calcium nitrate, 20 parts of calcium chloride, 7.5 parts of nitric acid are added in sugar alcohol B solution
Magnesium persistently stirs 3 hours and obtains sugar alcohol chelating calcium B solution after calcium, magnesium compound are completely dissolved；
（4）Based on mass fraction, 2 parts of surfactant is added in sugar alcohol chelating calcium B solution, stirs 20 minutes, obtains height
Content sugar alcohol calcium boron clear liquid fertilizer, then dispenses.
Embodiment 4
A kind of preparation method for the high-content sugar alcohol calcium boron clear liquid fertilizer improving fruit quality, includes the following steps：
（1）Based on mass fraction, by 23 parts of water, 6 parts of ethanol amine（Cosolvent）, 12.5 parts of boric acid sequentially adds
It is added in reaction kettle, stirs 30 minutes, boric acid is completely dissolved to water white transparency, obtains B solution；
（2）Based on mass fraction, 7 parts of glycerine, 4 parts of sorbierite, 4 parts of mannitol, stirring to sugar are added in B solution
Alcohol obtains sugar alcohol B solution after being completely dissolved；
（3）Based on mass fraction, 10 parts of calcium nitrate, 24 parts of calcium chloride, 7.5 parts of nitric acid are added in sugar alcohol B solution
Magnesium persistently stirs 3 hours and obtains sugar alcohol chelating calcium B solution after calcium, magnesium compound are completely dissolved；
（4）Based on mass fraction, 2 parts of surfactant is added in sugar alcohol chelating calcium B solution, stirs 20 minutes, obtains height
Content sugar alcohol calcium boron clear liquid fertilizer, then dispenses.
Embodiment 5
A kind of preparation method for the high-content sugar alcohol calcium boron clear liquid fertilizer improving fruit quality, includes the following steps：
（1）Based on mass fraction, by 24.5 parts of water, 4.5 parts of ethanol amine（Cosolvent）, 8.5 parts of boric acid, sequentially
It is added in reaction kettle, stirs 30 minutes, boric acid is completely dissolved to water white transparency, obtains B solution；
（2）Based on mass fraction, 8 parts of glycerine, 5 parts of sorbierite, 5 parts of mannitol, stirring to sugar are added in B solution
Alcohol obtains sugar alcohol B solution after being completely dissolved；
（3）Based on mass fraction, 20 parts of calcium nitrate, 15 parts of calcium chloride, 7.5 parts of nitric acid are added in sugar alcohol B solution
Magnesium persistently stirs 3 hours and obtains sugar alcohol chelating calcium B solution after calcium, magnesium compound are completely dissolved；
（4）Based on mass fraction, 2 parts of surfactant is added in sugar alcohol chelating calcium B solution, stirs 20 minutes, obtains height
Content sugar alcohol calcium boron clear liquid fertilizer, then dispenses.
Claims (9)
1. a kind of high-content sugar alcohol calcium boron clear liquid fertilizer, which is characterized in that calcium containing compound, boron compound, magnesium compound, glycoconjugate
Alcohol, surfactant and cosolvent etc., calcium content be 120 ~ 140g/L, boron content be 20 ~ 30g/L, content of magnesium 10g/L,
The mass ratio of compound sugar alcohol is more than 15%.
2. high-content sugar alcohol calcium boron clear liquid fertilizer as described in claim 1, which is characterized in that the calcium containing compound is nitric acid
Calcium and calcium chloride, boron-containing compound are boric acid, and magnesium-containing compound is magnesium nitrate, and the surfactant is dodecyl beet
Alkali, the cosolvent are ethanol amine.
3. high-content sugar alcohol calcium boron clear liquid fertilizer as described in claim 1, which is characterized in that based on mass fraction, described answers
Close sugar alcohol include 7 ~ 10% glycerine, 4 ~ 7% sorbierite, 2 ~ 5% mannitol.
4. high-content sugar alcohol calcium boron clear liquid fertilizer as claimed in claim 2, which is characterized in that based on mass fraction, described ten
Dialkyl group glycine betaine is 2%, and the ethanol amine is 4.5 ~ 6.5%.
5. a kind of preparation method of high-content sugar alcohol calcium boron clear liquid fertilizer, which is characterized in that include the following steps：
(1) based on mass fraction, by 23 ~ 26.5 parts of water, 4.5 ~ 6.5 parts of cosolvent, 8.5 ~ 12.5 parts of boron compound,
Sequentially it is added in reaction kettle, stirs 30 minutes, boric acid is completely dissolved to water white transparency, obtains B solution；
(2) based on mass fraction, 15 ~ 20 parts of compound sugar alcohol is added in B solution, stirring obtains after being completely dissolved to sugar alcohol
Sugar alcohol B solution；
(3) based on mass fraction, 25 ~ 35 parts of calcium compound, 7.5 parts of magnesium compound are added in sugar alcohol B solution, continues
Stirring obtains sugar alcohol chelating calcium B solution in 3 hours after calcium, magnesium compound are completely dissolved；
(4) based on mass fraction, 2 parts of surfactant is added in sugar alcohol chelating calcium B solution, stirs 20 minutes, stand,
Filtering collects filtrate and obtains high-content sugar alcohol calcium boron clear liquid fertilizer.
6. the preparation method of high-content sugar alcohol calcium boron clear liquid fertilizer as claimed in claim 5, which is characterized in that the cosolvent
For ethanol amine, boron compound is boric acid.
7. the preparation method of high-content sugar alcohol calcium boron clear liquid fertilizer as claimed in claim 5, which is characterized in that the glycoconjugate
Alcohol include 7 ~ 10% glycerine, 4 ~ 7% sorbierite, 2 ~ 5% mannitol.
8. the preparation method of high-content sugar alcohol calcium boron clear liquid fertilizer as claimed in claim 5, which is characterized in that the calcification is closed
Object is calcium nitrate and calcium chloride, and magnesium compound is magnesium nitrate.
9. the preparation method of high-content sugar alcohol calcium boron clear liquid fertilizer as claimed in claim 5, which is characterized in that live on the surface
Property agent be empgen BB.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111470902A (en) * | 2020-04-17 | 2020-07-31 | 华南农业大学 | High-activity organic calcium boron liquid compound fertilizer and preparation method and application thereof |
| CN113248310A (en) * | 2021-05-28 | 2021-08-13 | 广西产研院生物制造技术研究所有限公司 | Polyglutamic acid, sugar alcohol calcium aqua and preparation method thereof |
| CN113443938A (en) * | 2021-07-28 | 2021-09-28 | 广西太美生物科技股份有限公司 | High-concentration phosphorus-potassium-boron-copper liquid fertilizer suitable for flying prevention crops and preparation method thereof |
| CN115215705A (en) * | 2022-08-19 | 2022-10-21 | 山西丰田肥业有限公司 | Calcium-magnesium-boron preparation foliar fertilizer containing astragalus polysaccharides and preparation method thereof |
| CN115568321A (en) * | 2022-09-16 | 2023-01-06 | 江苏省农业科学院 | Method for prolonging physiological function period of Sucui No. 1 pear leaves |
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| CN115215705A (en) * | 2022-08-19 | 2022-10-21 | 山西丰田肥业有限公司 | Calcium-magnesium-boron preparation foliar fertilizer containing astragalus polysaccharides and preparation method thereof |
| CN115568321A (en) * | 2022-09-16 | 2023-01-06 | 江苏省农业科学院 | Method for prolonging physiological function period of Sucui No. 1 pear leaves |
| CN115568321B (en) * | 2022-09-16 | 2024-04-02 | 江苏省农业科学院 | Method for prolonging physiological function period of leaf of Su Cui No. 1 pear |
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Application publication date: 20181016 |