CN113248310A - Polyglutamic acid, sugar alcohol calcium aqua and preparation method thereof - Google Patents
Polyglutamic acid, sugar alcohol calcium aqua and preparation method thereof Download PDFInfo
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- CN113248310A CN113248310A CN202110568800.3A CN202110568800A CN113248310A CN 113248310 A CN113248310 A CN 113248310A CN 202110568800 A CN202110568800 A CN 202110568800A CN 113248310 A CN113248310 A CN 113248310A
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- polyglutamic acid
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Cultivation Of Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a polyglutamic acid, sugar alcohol calcium aqua and a preparation method thereof, wherein the effective active ingredients are polyglutamic acid and sugar alcohol calcium, and the preparation method is characterized in that: the composition comprises the following components in parts by weight: 1-5 parts of polyglutamic acid; 45-70 parts of sugar alcohol calcium; 1-4 parts of an auxiliary agent; water to 100 parts by weight. The polyglutamic acid, sugar alcohol and calcium aqua can be used for economic crops such as fruit trees, vegetables and the like, can obviously regulate the growth of plants, preserve water and moisture, preserve flowers and fruits and improve the quality; compared with products in the market, the compound formula is added, the soil environment is improved, the operation process is simple, and the application is convenient.
Description
Technical Field
The invention relates to the technical field of agricultural fertilizers, in particular to a polyglutamic acid and sugar alcohol calcium aqua and a preparation method thereof.
Background
Polyglutamic acid (gamma-poly-glutamic acid, abbreviated as gamma-PGA), also known as natto gum and polyglutamic acid, is a water-soluble, biodegradable, nontoxic biopolymer prepared by using a microbial fermentation method. The polyglutamic acid is a homo-polyamino acid polymerized by glutamic acid monomers through amido bonds, has the advantages of excellent biodegradability, super-strong adsorption, no toxicity and the like, and can reduce the loss of fertilizer nutrients, improve the utilization rate of the fertilizer, regulate plant growth and the like when being added into the fertilizer. Has obvious application effect on economic crops such as fruit trees, vegetables and the like, and can obviously improve the crop yield.
The Eucarol AGE synergistic penetrant is a biological auxiliary agent and has excellent wetting and penetrating properties. Is a natural derivative, can be completely degraded and is environment-friendly. Can improve the speed of the liquid medicine permeating into the mesophyll, improve the control effect of the liquid medicine, promote the growth of crops, be used as a soil conditioner, be stable in water and be added into a water aqua to be used as a synergist.
The sugar alcohol calcium can stabilize cell membranes and cell walls, increase the hardness of fruits, enhance the toughness of fruit peels, and reduce fruit cracking, sunburn and pest damage. The yield is increased, the quality is improved, and the storage property of the fruits is improved; reducing the respiratory intensity, reducing the consumption of nutrients and delaying the aging speed of fruits; improve the resistance of crops, and improve the antifungal capability.
The crops lack calcium elements, the tip parts of the leaves are bent and yellow-whitened, the leaf edges are folded upwards or downwards, the veins of the young leaves are yellowed, the fruit peels are rotted and split, the roots supplement calcium, the calcium is easily fixed in the soil and is also easily precipitated in the crops, the utilization rate is not high, and therefore, the calcium is needed to be supplemented outside the roots. Sugar alcohol calcium is a novel fertilizer product created by supplementing calcium outside roots, and has the advantages that a pure natural sugar alcohol chelating agent is adopted, calcium ions can be carried to quickly permeate into leaves or fruit peels after spraying, and can be directly and quickly transported to fruit parts needing calcium through xylem and phloem, so that the problem of supplementing calcium outside the roots of crops is well solved. The preparation of the novel product by compounding is an important means for realizing sustainable, green and healthy development of agriculture.
At present, the compounding of polyglutamic acid and sugar alcohol calcium is not reported.
Disclosure of Invention
The invention aims to provide a polyglutamic acid and sugar alcohol calcium aqua which can be used for economic crops such as fruit trees, vegetables and the like, can obviously increase plant nutrition, promote crop growth, retain water and fertilizer, retain flowers and fruits, improve yield and improve quality.
The technical problem to be solved by the invention is realized by the following technical scheme:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
moreover, the preferable components and the weight portion ratio are as follows:
and the sugar alcohol is one or the combination of any two or more of xylitol calcium, lactitol calcium, sorbitol calcium, mannitol calcium, maltitol calcium and erythritol calcium. And the auxiliary agent is one or the combination of any two or more of Eucarol AGE synergistic penetrant, disodium coco-glucoside citrate and potassium tristyrylphenol polyoxyethylene ether phosphate.
A preparation method of polyglutamic acid and sugar alcohol calcium aqua is characterized by comprising the following steps: the method comprises the following steps:
(1) putting weighed polyglutamic acid into a stirring kettle, adding a certain amount of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting the weighed sugar alcohol calcium and the auxiliary agent into another stirring kettle, adding the balance of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
An application of polyglutamic acid and sugar alcohol calcium aqua in regulating the growth of fruit tree and vegetable crops is disclosed.
The invention has the advantages and beneficial effects that:
1. the polyglutamic acid, sugar alcohol and calcium aqua can be used for economic crops such as fruit trees, vegetables and the like, can obviously increase plant nutrition, preserve water and fertilizer, preserve flowers and fruits, improve yield and improve quality.
2. According to the polyglutamic acid and sugar alcohol calcium aqua, the efficient synergistic auxiliary agent is added, so that the effect and the effect of the agents are synergistic, the preparation method is simple, and the raw materials are convenient and wide in source; the application method is simple, labor-saving and time-saving, and accords with the concept of sustainable, green and healthy development of modern agriculture.
Detailed Description
The present invention is further described in the following by specific examples, which are only illustrative and are not intended to limit the scope of the present invention.
First, an embodiment
Example 1:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) putting 1g of polyglutamic acid into a stirring kettle, adding 20g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting 45g of weighed calcium mannitol and 1g of eucanol AGE synergistic penetrating agent into another stirring kettle, adding 33g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable economic crops.
Example 2:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) placing 5g of weighed polyglutamic acid in a stirring kettle, adding 6g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting 70g of weighed calcium lactitol and 4g of disodium coco-glucoside citrate into another stirring kettle, adding 15g of water, and fully stirring to dissolve to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable economic crops.
Example 3:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) placing 2g of weighed polyglutamic acid in a stirring kettle, adding 20g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) placing 24g of xylitol calcium, 24g of maltitol calcium and 2g of Eucanol AGE synergistic penetrant in another stirring kettle, adding 28g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Example 4:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) putting 1g of weighed polyglutamic acid into a stirring kettle, adding 10g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting 45g of weighed calcium sorbitol, 1g of eucanol AGE synergistic penetrating agent and 1g of disodium coco-glucoside citrate into another stirring kettle, adding 42g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable economic crops.
Example 5:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) placing 5g of weighed polyglutamic acid in a stirring kettle, adding 20g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting 48g of weighed calcium sorbitol and 3g of potassium tristyrylphenol polyoxyethylene ether phosphate into another stirring kettle, adding 21g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Example 6:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) placing 5g of weighed polyglutamic acid in a stirring kettle, adding 15g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) placing 65g of weighed calcium mannitol, 1g of potassium tristyrylphenol polyoxyethylene ether phosphate and 2g of Eucarol AGE synergistic penetrant into another stirring kettle, adding 12g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Example 7:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) placing 5g of weighed polyglutamic acid in a stirring kettle, adding 17g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) placing 56g of weighed xylitol calcium, 1g of disodium coco-glucoside citrate III and 1g of styrylphenol polyoxyethylene ether phosphate potassium salt in another stirring kettle, adding 20g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Example 8:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) putting 4g of weighed polyglutamic acid into a stirring kettle, adding 17g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting 48g of weighed calcium sorbitol, 1g of disodium coco-glucoside citrate and 1g of potassium tristyrylphenol polyoxyethylene ether phosphate into another stirring kettle, adding 30g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Example 9:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) putting 3g of weighed polyglutamic acid into a stirring kettle, adding 14g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) placing 50g of the weighed calcium erythritol, 1g of the Eucarol AGE synergistic penetrant, 1g of the disodium coco-glucoside citrate and 1g of the potassium tristyrylphenol polyoxyethylene ether phosphate ester in another stirring kettle, adding 30g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Example 10:
a polyglutamic acid, sugar alcohol calcium aqua, characterized by that: the composite material comprises the following components in parts by weight:
the preparation method of the polyglutamic acid and sugar alcohol calcium aqua comprises the following steps: the method comprises the following steps;
(1) putting 3g of weighed polyglutamic acid into a stirring kettle, adding 10g of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) placing 15g of weighed calcium lactitol, 50g of calcium erythritol and 2g of potassium tristyrylphenol polyoxyethylene ether phosphate into another stirring kettle, adding 20g of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
The polyglutamic acid and sugar alcohol calcium aqua is applied to plant growth regulation of fruit trees and vegetable commercial crops.
Second, field verification test
1. Test for verifying influence of germination rate of rape seeds by using polyglutamic acid, sugar alcohol and calcium water aqua
The invention employs a total of 13 treatments, examples 1-10 of the invention; control 180g/L sugar alcohol calcium aqua (control 1); 3% aqueous polyglutamic acid (control 2); and a clear water control (control 3). Rape seeds (Jade Red oil No. 2) are selected as experimental materials in the experiment, the germination rate of the seeds is tested by simultaneously selecting three different dilution times, 10 seeds are taken from each group, 3 seeds are treated from each group, the rape seeds are immersed in treatment liquid, the seeds are immersed for 16 hours and sowed into a culture dish padded with wetting filter paper, the one-day germination rate after the seeds are immersed is recorded, and the specific test results are shown in Table 1.
TABLE 1 germination percentage of rape seeds 1 day after seed soaking
As can be seen from Table 1, the effect of the toothpicks was better when all the agents were diluted 2000 times, and the sprouting effect of the examples was significantly higher than that of the control agent. The application method of dilution by 2000 times is selected, and the test results are continuously observed, as shown in tables 2 and 3.
TABLE 2 germination percentage of rape seeds 2 days after seed soaking (dilution 2000 times, seed soaking 2 days)
TABLE 3 germination percentage 3 days after rape seed soaking (dilution 2000 times, soaking for 3 days)
Treatment of | Root number (number) | Rooting rate |
Example 1 | 21 | 70% |
Example 2 | 21 | 70% |
Example 3 | 22 | 73.3% |
Example 4 | 22 | 73.3% |
Example 5 | 23 | 76.7% |
Example 6 | 22 | 73.3% |
Example 7 | 24 | 80% |
Example 8 | 23 | 76.7% |
Example 9 | 23 | 76.7% |
Example 10 | 25 | 83.3% |
Control 1 | 20 | 66.7% |
Control 2 | 18 | 60% |
Control 3 | 15 | 50% |
As can be seen from the test data in tables 2 and 3, the products of examples 1-10 of the present invention have obvious growth promoting effect on the rape seeds, and the germination rate and rooting rate are both obviously higher than those of the control agents, wherein the effect is most obvious in example 10.
2. Test for verifying influence of germination rate of corn seeds by using polyglutamic acid, sugar alcohol and calcium aqua
The invention employs a total of 13 treatments, examples 1-10 of the invention; control 180g/L sugar alcohol calcium aqua (control 1); 3% aqueous polyglutamic acid (control 2); and a clear water control (control 3). Corn seeds (Zhengdan 958) are selected as experimental materials in the experiment, the germination rate of the seeds is tested by selecting 2000 times of dilution times, 10 seeds are taken from each group, 2 seeds are taken from each group, the corn seeds are immersed in treatment liquid, the seeds are immersed for 16 hours, the seeds are sowed in a culture dish padded with wetting filter paper, the germination rate of the seeds one day after the seeds are immersed is recorded, and the specific test results are shown in table 4.
TABLE 4 test results 1 day after corn seed soaking
As can be seen from table 4, the product of example 10 of the present invention performed best compared to the control three agents.
Claims (6)
1. A polyglutamic acid, sugar alcohol calcium aqua and its preparation method, characterized by that: the composite material comprises the following components in parts by weight: 1-5 parts of polyglutamic acid; 45-70 parts of sugar alcohol calcium; 1-4 parts of an auxiliary agent; and the purified water is complemented to 100 parts by weight.
2. The aqueous agent of polyglutamic acid and sugar alcohol calcium and the preparation method thereof according to claim 1, wherein the aqueous agent comprises: the preferable components and the weight portion ratio are as follows: 2-5 parts of polyglutamic acid; 48-65 parts of sugar alcohol calcium; 1-3 parts of an auxiliary agent; and the purified water is complemented to 100 parts by weight.
3. The aqueous polyglutamic acid and sugar alcohol calcium and the preparation method thereof according to claim 1 or 2, wherein the aqueous polyglutamic acid and sugar alcohol calcium is prepared by the following steps: the sugar alcohol calcium is one or the combination of any two or more than two of xylitol calcium, lactitol calcium, sorbitol calcium, mannitol calcium, maltitol calcium and erythritol calcium.
4. The aqueous polyglutamic acid and sugar alcohol calcium and the preparation method thereof according to claim 1 or 2, wherein the aqueous polyglutamic acid and sugar alcohol calcium is prepared by the following steps: the auxiliary agent is one or the combination of any two or more of a Eucaroleage synergistic penetrating agent, disodium coco-glucoside citrate and potassium tristyrylphenol polyoxyethylene ether phosphate.
5. A polyglutamic acid, sugar alcohol calcium aqua and its preparation method, characterized by that: the method comprises the following steps:
(1) putting weighed polyglutamic acid into a stirring kettle, adding a certain amount of water, and fully stirring until the polyglutamic acid is dissolved to obtain a solution A;
(2) putting the weighed sugar alcohol calcium and the auxiliary agent into another stirring kettle, adding the balance of water, and fully stirring and dissolving to obtain a solution B;
(3) and dropwise adding the solution A into the solution B while stirring, uniformly stirring, sampling, analyzing and detecting, and obtaining a finished product after the product is qualified.
6. An application of polyglutamic acid and sugar alcohol calcium aqua in regulating plant nutrition of fruit trees and vegetable commercial crops is disclosed.
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CN115349409A (en) * | 2022-09-05 | 2022-11-18 | 华南农业大学 | Method for improving quality of cabbage seedlings |
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CN115349409A (en) * | 2022-09-05 | 2022-11-18 | 华南农业大学 | Method for improving quality of cabbage seedlings |
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Application publication date: 20210813 |
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