CN108652010A - A kind of 3 quick-dissolving agent of omega and preparation method thereof - Google Patents
A kind of 3 quick-dissolving agent of omega and preparation method thereof Download PDFInfo
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- CN108652010A CN108652010A CN201810259661.4A CN201810259661A CN108652010A CN 108652010 A CN108652010 A CN 108652010A CN 201810259661 A CN201810259661 A CN 201810259661A CN 108652010 A CN108652010 A CN 108652010A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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Abstract
The invention discloses a kind of 3 quick-dissolving agents of omega and preparation method thereof.3 quick-dissolving agent of omega of the present invention is prepared by algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi, lipase, embedded material, auxiliary material；Wherein, algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi mass ratio be 1:1:1:1, fatty enzyme dosage be algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi gross mass 20 30%；When preparation, algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi and lipase are first subjected to ester exchange reaction, obtain enzymolysis product, then enzymolysis product and embedded material, auxiliary material, anion water are emulsified, homogeneous, embedding, lotion is obtained, then lotion is made by spray drying.3 quick-dissolving agent of omega of the present invention has the characteristics that good fluidity, in good taste, instant capacity is good, realizes good absorption, fast absorption, hypersorption of the human body to omega 3, improves bioavilability of the human tissue cell to product.
Description
Technical field
The present invention relates to a kind of 3 quick-dissolving agents of omega and preparation method thereof, belong to technical field of biology.
Background technology
Omega 3 is aliphatic acid necessary to universally acknowledged human life, health, and no omega 3 does not just have
Life.3 human body of omega cannot synthesize, and chemistry cannot synthesize, it is necessary to be supplemented from food, omega 3 cannot be stored in human body, must
It must supplement daily.World health organisation recommendations are grown up and need to absorb 600-1000mg from food daily, most long-lived auspicious in the world
Scholar, Japanese national daily intaking amount reach 700mg, and intake only has 47mg to China its people per capita.Scientific research proves omega 3
Lack has a direct correlation with the morbidity of 59 kinds of diseases such as cardiovascular and cerebrovascular diseases, tumour, compatriots' omega 3 there is a serious shortage of be compatriots
The one of the major reasons that cardiovascular and cerebrovascular diseases, tumour chronic diseases burst increase.The whole people supplement 3 aliphatic acid of omega, have been
Ensure the important measures of national health.
1, the World Health Organization（WHO）：During 3 aliphatic acid of omega can prevent thrombosis from carrying out cardioprotection while avoid
Wind, 3 replenishers of omega also have good effect.
2, European Union's food security office（EFSA）：3 unsaturated fatty acid of omega has reduction low-density lipoprotein and protection
Cardiovascular function.In Europe, the intakes of whole unsaturated fatty acids is generally within the scope of recommendation（The about 5- of energy
10%）.
3, the World Health Organization（) and FAO (Food and Agriculture Organization of the United Nation) WHO（FAQ)：1993, the World Health Organization（WHO）And connection
He Guo food and agricultural organizations（FAQ）It dispatches a joint document《About the opinion for requiring daily ration specialized to supplement omega 3》, opinion points out, in view of
The situation of the importance of omega 3 and the universal insufficiency of intake of the mankind determines worldwide special popularization omega 3, it is proposed that
Normal person should take in 600-1000 milligrams of omegas 3 daily.
4, U.S. sanitary nutrition department, American heart association：2003, U.S. sanitary nutrition department, American heart association
It is required that patients with coronary heart disease increases to 3 grams to the intake of omega 3 daily.
5, U.S. Food and Drug Administration（FDA）：U.S. Food and Drug Administration（FDA）Confirm omega 3
Coronary heart disease risk can be reduced, it is safe to daily intake 3 grams.
6, American Cancer Society：American Cancer Society recommend cancer first choice therapeutic scheme be：Patient receive radiotherapy and
When chemotherapy, doctor doses a patient with doses omega 3, on the one hand protects normal cell from infringement, inhibits cell mobilization
Property variation, and cancer metastasis and incidence of recurrences can be reduced！
7, Canadian government：The Canadian government most proximad 25-79 Sui national omega 3 for suggesting that 1.5 grams should be taken daily, it is special
Do not emphasize that 3 polybasic unsaturated fatty acid of omega is the necessary nutriment to maintaining health, normal development！
8, White House Management and Budget Office writes the Ministry of Agriculture, health and Human Services：（On May 27th, 2003, Hua Sheng
Pause and interrogates）White House's Management and Budget Office Wednesday writes the Ministry of Agriculture, health urges them to change existing standard with Human Services
Then, the people of the United States are instructed to consume beneficial 3 aliphatic acid of omega, because it can reduce the risk of heart disease and a variety of diseases.
9, French：More food of the food rich in 3 unsaturated fatty acid of omega, to prevent relieving convulsion contraction and cardiovascular and cerebrovascular disease
Deng.--- published by the famous doctor Shi Leibei of France《Rehabilitation》One book；" omega 3 is actually a variety of same type unsaturated lipids
The general name of fat acid, including fatty acid materials such as EPA and DHA.Some research institutions point out, are rich in 3 aliphatic acid of omega
Food contributes to brain cell to keep soft flexible, reduces the risk of developing cardiovascular diseases and apoplexy, while this group food exists
Cardioprotection, effect is also very big in terms of preventing myocardial infarction.”——《Science and future》Magazine；" 3 content of fatty acid of omega
When higher, the radiotherapy of cancer patient can be made to achieve good results.Animal experiments show that under the premise of absorbing enough DHA,
After receiving radiotherapy 12 days, cancer volume can reduce 60%." --- the scientist of French National Health ＆ Medical Inst., and Pasteur's Institute is most
Closely also publish thesis.
In recent years, conditional only a few crowd is from fish oil soft capsule dietary supplementation omega 3 in compatriots, but due to seawater
Chemical contamination, heavy metal pollution, nuclear pollution be on the rise, government is not recommended.Meanwhile fish oil is in pollution deodorization work of dispelling
The activity of omega 3 is compromised in skill, and ALA is free of in fish oil.
Also there are a small number of crowds from linseed oil dietary supplementation omega 3, but linseed in toxic removing, is removed containing micro- poison such as erucic acid
Also compromise the activity of omega 3 in smelly technique, and linseed oil without human body there is a serious shortage of EPA and DHA；Meanwhile passing through
Edible oil supplements omega 3, and edible oil oil enters human body, and acidic materials of the omega 3 in by gastric juice, intestinal juice destroy, and human body needs
It wants liver enzyme, bile enzyme to degrade oil, needs liver enzyme to be digested, small intestine pancreatic lipase is hydrolyzed into after aliphatic acid just through small
Intestinal absorption, this mode are increased to gall-bladder, liver function metabolic damage.
Invention content
The object of the present invention is to provide a kind of burdens neither influencing liver and gall internal organs to be metabolized damage, and is conducive to absorption of human body
With 3 quick-dissolving agent of omega and preparation method thereof for improving human bioavailability.
Technical scheme is as follows：A kind of 3 quick-dissolving agent of omega, by algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, U.S.
It is prepared by rattan fruit oil, lipase, embedded material, auxiliary material；Wherein, the quality of algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi
Than being 1:1:1:1, fatty enzyme dosage is the 20-30% of algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi gross mass；It prepares
When, algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi and lipase are first subjected to ester exchange reaction, obtain enzymolysis product,
Enzymolysis product and embedded material, auxiliary material, anion water are emulsified again, homogeneous, embedding, obtain lotion, then lotion is passed through
3 quick-dissolving agent of omega is made in spray drying.
The embedded material is one or both of resistant starch, corn sugar, and dosage is enzymolysis product quality
2-4 times；The auxiliary material is emulsifier, stabilizer, food flavor.
The emulsifier is one or both of single double glyceride, casein sodium, and stabilizer is dikalium phosphate.
The ester exchange reaction condition is：45 DEG C -55 DEG C of reaction temperature, reaction time 12-20 hour.
Preferably, the preparation method of 3 quick-dissolving agent of omega of the invention is as follows：
（1）Algal oil, Purple Perilla Seed Oil, lipase are mixed, ester exchange reaction is carried out, obtains enzymolysis product 1.；The lipase is used
Amount is the 10%-15% of algal oil and Purple Perilla Seed Oil gross mass, 45 DEG C -55 DEG C of reaction temperature, 16 hours reaction time；Algal oil,
The mass ratio of Purple Perilla Seed Oil is 1:1；
（2）Seed oil of Moringa oleigera, oil and fat of sacha inchi, lipase are subjected to ester exchange reaction, obtain enzymolysis product 2.；Fatty enzyme dosage is Moringa
The 10%-15% of seed oil and oil and fat of sacha inchi gross mass, 45 DEG C -55 DEG C of reaction temperature, 16 hours reaction time；Seed oil of Moringa oleigera and U.S. rattan
The mass ratio of fruit oil is 1:1；
（3）By enzymolysis product 1. 30 mass parts, embedded material 60-80 mass parts, auxiliary material 9-15 mass parts, 55-65 DEG C bear from
Sub- water 80-200 mass parts mixing is emulsified, homogeneous embedding under the conditions of closed cycle with homogenizer, obtains mixing liquid 1.；
Wherein, embedded material is resistant starch, and auxiliary material is emulsifier, stabilizer, food flavor；
（4）By enzymolysis product 2. 30 mass parts, embedded material 60-80 mass parts, auxiliary material 9-15 mass parts, 55-65 DEG C bear from
Sub- water 80-200 mass parts mixing is emulsified, homogeneous embedding under the conditions of closed cycle with homogenizer, obtains mixing liquid 2.,
Wherein embedded material is corn sugar, resistant starch, and corn sugar, resistant starch mass ratio are 4-6:1, auxiliary material is emulsification
Agent, stabilizer, food flavor；
（5）Corn grape in 1. mixing liquid being added to mixing liquid 2. continued emulsification with homogenizer homogeneous 40-50 minute
Matter embeds, and obtains lotion；
（6）Lotion is spray-dried, particle 90% crosses 16-20 mesh sieve, and the particle after drying falls into displacement container, through cooling down,
3 quick-dissolving agent of omega is made in filling storage.
It is further preferred that the emulsifier is one or both of double glyceride, casein sodium, stabilizer is phosphorus
Sour dipotassium.Preferably, step（3）、（4）The emulsifier, stabilizer, food flavor mass ratio are 1:1:1.The edible perfume (or spice)
Selected one or more of the food flavor product for meeting production requirement commonly used in the art, for adjust product odour,
Fragrance.
It is further preferred that in step（3）、（4）When emulsification, homogeneous embedding, enzymolysis product can be first emulsified, then emulsify embedding
Material, acquisition more preferably embed effect；The processing condition of use can be：Homogenization pressure 30-80MPa, homogenizing temperature 55-65
DEG C, homogenizing time 0.5-5h.
It is further preferred that the spray drying condition is：125 DEG C, vacuum degree 200-500Pa of drying tower temperature, steam
500 tons/h of evaporation capacity, 20 tons/h of mixed liquor spray amount, 38 meters of adjustable tower height；Emulsion particle with flow velocity 15-20 seconds from top to bottom
It is dried.
After 3 quick-dissolving agent of omega of the present invention can be used for mixing with maltodextrin, it is prepared into the glue for supplementing omega 3
The functional food of wafer, tablet, oral solution, bead dosage form, such as solid beverage, beverage.3 quick-dissolving agent of omega of the present invention is outstanding
It is suitable for people, Patients with geriatric cardiovascular and cerebrovascular diseases, tumour conditioning and treating patient that liver and gall have lesion, pregnant woman, infant, sub- strong is applied also for
Kang Renqun etc. needs or must be supplemented with many people of omega 3.
The present invention is by that will derive from different plant components（Behen-nut oil, oil and fat of sacha inchi, Purple Perilla Seed Oil, algal oil）'s
N-3 type aliphatic acid（Medium chain fatty acid）It by the transesterification technology of lipase, is incorporated on the same oil molecule, forms structured lipid
Matter；It is formed by structured lipid its fatty acid structure and is distributed as polyunsaturated fatty acid, wherein sn-2 are monoglyceride
PUFA, Sn-1,3 are MCFA.The present invention, which is formed by structured lipid, can give full play to different aliphatic acid compositions and position point
Advantage of the cloth in metabolism, absorption, has special physique and unique nutrition, Physiological Properties, has wide
Application prospect.
The preparation process of the present invention, by the preparation of quick-dissolving agent and the primary completion of sterilization, its bacterium colony of the quick-dissolving agent product of acquisition
Total 50-200CFU/g meets production and relevant criterion requirement.
The preparation process step of the present invention（5）By mixing liquid 1., mixing liquid 2. pass through homogeneous, continue to embed, finally
4 tunic shape forms are presented, high unsaturated fatty acid then protects algae oil, outer layer corn Portugal in innermost layer, the resistant starch of internal layer
Grape monosaccharide provides guarantee while protecting seed oil of Moringa oleigera, oil and fat of sacha inchi, and for realization is instant.
Further, the preparation method of 3 quick-dissolving agent of omega of the invention is being used to prepare for consumptive, nephrosis
It, can be by adjusting resistant starch and corn sugar ratio, to meet consumptive when with the product of tumour sufferer, nephrosis and swollen
Difference of the tumor sufferer to product in dissolubility, Physiological Properties, absorption characteristic etc. requires.It is described as follows：
Mostly it is only to consider embedding rate and stability, table when preparing the product containing omega 3 using existing common microcapsule technology
The problem of face oil content, does not consider whether product is effective to being played the role of in user's body, and the thing of product whether can
The problems such as really playing.By taking the preparation of high unsaturated fatty acid fish oil micro-capsule as an example：From product stability, it can only wrap
The fat for burying 30%, in its preparation process, to make surface oil content reduce, using secondary embedding fluidized bed-type；From embedding
On material, stability cost, smell, shelf-life are only considered.Compared with the prior art, the present invention can be directed to different crowd's tune
The dosage of embedded material therein is saved, the product of acquisition is in use, with more preferably technique effect.
For example, being directed to tumour sufferer, is supported for clinical tumor sufferer rehabilitation nutrition, energy can be used（Enzymolysis product）With
Carbohydrate（Embedded material）1:1 formula is considering cost, stability, shelf-life, surface oil using present invention process
Under the premise of the problem above such as content, takes release energy omega 3, DHA after application into consideration and play a role and whether meet
Interim sufferer demand, instant capacity mouthfeel is if appropriate for the compliance of urgent patient and nasal feeding, the requirement of tube feed；For lungs disease
Patient, it is main to consider lungs sufferer in application product of the present invention, respiratory quotient is reduced to lung ventilator demand to reducing sufferer, is carried
High lung function, it is main in terms of dispensing to consider to change pulmonary surfactant ingredient, reduce late period morning low blood caused by endotoxin
Pressure reduces bacterium infection risk, energy can be used（Enzymolysis product）30%, carbohydrate（Embedded material）40%, casein 10%
Formula, prepared；For the standard of Kidney Dialysis patient high-energy and low-carb, and meet dialysis sufferer pair
The needs of energy nutrient and the requirement for reducing protein susceptibility, then can be used energy（Enzymolysis product）30%, carbohydrate（Packet
Bury material）50%, the formula of casein 10%, is prepared.
In addition, the advantageous effect of the present invention compared with the existing technology also resides in：
（1）3 quick-dissolving agent of omega of the present invention realizes the burden metabolism damage for neither influencing liver and gall internal organs, and is conducive to human body
Absorb and improve human bioavailability：The present invention 3 quick-dissolving agent of omega enter human body before just complete enzymolysis, hydrolysis,
It is emulsified into the process of aliphatic acid, without degrading in vivo to oil by liver enzyme, bile enzyme；3 speed of omega of the present invention
Solvent by digesting, hydrolyzing, being emulsified into aliphatic acid, forms small molecule structure lipid, the advantageous people of small molecule structure lipid in vitro
Fast absorption, the hypersorption of body, improve the bioavilability of tissue.3 quick-dissolving agent of omega of the present invention can further spread out
Series of products are born, are prevented for a variety of serious diseases；
（2）Four kinds of feedstock oils of its composition of 3 quick-dissolving agent of omega of the present invention all have height containing omega 3, DHA, are provided simultaneously with
No chemical contamination, heavy metal free pollute, without nuclear pollution, the quality nontoxic, odorless is pure natural；
（3）Existing " oily micro-capsule embedding pulverizing technology " is all made of following technique and prepares：Oily --- ingredients --- emulsification
Micro-capsule embeds --- sterilization --- spray drying；That there are stability is poor, oxidizable for above-mentioned technique, the shelf-life is short（Only 12 months）、
The deficiency of instant capacity difference；The preparation method of the present invention can extend shelf life of products and be up to 24 months, and product is through broken wall, ultra micro processing
Afterwards, be conducive to the high-selenium corn of tissue, good absorption, absorb soon, hypersorption, improve tissue to 3 biology profit of omega
Expenditure；
（4）The present invention solve it is existing it is edible after need small intestine pancreatic lipase to be hydrolyzed into aliphatic acid then just absorbable deficiency, subtract
The burden of courage liver is lacked.
Specific implementation mode
The present invention is described in further details below by embodiment, these embodiments are only used for illustrating the present invention, and
It does not limit the scope of the invention.The unmentioned technique of the present invention, formula can be by skilled person will appreciate that the technology hands known
Section is realized.
Embodiment 1 realizes the present invention using following steps：
（1）Algal oil, Purple Perilla Seed Oil, lipase are mixed, ester exchange reaction is carried out, obtains enzymolysis product 1.；The lipase is used
Amount is the 12% of algal oil and Purple Perilla Seed Oil gross mass, 45 DEG C -55 DEG C of reaction temperature, 16 hours reaction time；Algal oil, purple perilla
The mass ratio of seed oil is 1:1；
（2）Seed oil of Moringa oleigera, oil and fat of sacha inchi, lipase are subjected to ester exchange reaction, obtain enzymolysis product 2.；Fatty enzyme dosage is Moringa
Seed oil and the 12% of oil and fat of sacha inchi gross mass, 45 DEG C -55 DEG C of reaction temperature, 16 hours reaction time；Seed oil of Moringa oleigera and oil and fat of sacha inchi
Mass ratio be 1:1；
（3）By enzymolysis product 1. 30 mass parts, 70 mass parts of embedded material, 12 mass parts of auxiliary material, 55-65 DEG C of anion water
120 mass parts mix, and are emulsified under the conditions of closed cycle with homogenizer, homogeneous embedding, obtain mixing liquid 1.；Wherein, it wraps
It is resistant starch to bury material, and auxiliary material is emulsifier（Double glyceride, casein sodium）, stabilizer dikalium phosphate, food flavor；Institute
It is 1 to state emulsifier, stabilizer, food flavor mass ratio:1:1；Processing condition：Homogenization pressure 40MPa, homogenizing temperature 55-65
DEG C, homogenizing time 2.5h；
（4）By enzymolysis product 2. 30 mass parts, 70 mass parts of embedded material, 12 mass parts of auxiliary material, 55-65 DEG C of anion water
150 mass parts mix, and are emulsified under the conditions of closed cycle with homogenizer, homogeneous embedding, mixing liquid are obtained 2., wherein embedding
Material is corn sugar, resistant starch, and corn sugar, resistant starch mass ratio are 5.5:1, auxiliary material is emulsifier（It is double sweet
One or both of grease, casein sodium）, stabilizer dikalium phosphate, food flavor；The emulsifier, is eaten stabilizer
Essence mass ratio is 1:1:1；Processing condition：Homogenization pressure 50MPa, homogenizing temperature are 55-65 DEG C, homogenizing time 3.5h；
（5）Corn grape in 1. mixing liquid being added to mixing liquid 2. continued emulsifying homogeneous packet with homogenizer homogeneous 50 minutes
It buries, obtains lotion；
（6）Lotion is spray-dried, particle 90% crosses 16-20 mesh sieve, and the particle after drying falls into displacement container, through cooling down,
3 quick-dissolving agent of omega is made in filling storage；Spray drying condition is：125 DEG C, vacuum degree 200-500Pa of drying tower temperature is steamed
500 tons/h of steam raising amount, 20 tons/h of mixed liquor spray amount, 38 meters of adjustable tower height；Emulsion particle with flow velocity 15-20 seconds from upper and
It is lower to be dried.
Embodiment 2 realizes the present invention using following steps：
（1）Algal oil, Purple Perilla Seed Oil, lipase are mixed, ester exchange reaction is carried out, obtains enzymolysis product 1.；The lipase is used
Amount is the 15% of algal oil and Purple Perilla Seed Oil gross mass, 45 DEG C -55 DEG C of reaction temperature, 20 hours reaction time；Algal oil, purple perilla
The mass ratio of seed oil is 1:1；
（2）Seed oil of Moringa oleigera, oil and fat of sacha inchi, lipase are subjected to ester exchange reaction, obtain enzymolysis product 2.；Fatty enzyme dosage is Moringa
Seed oil and the 15% of oil and fat of sacha inchi gross mass, 45 DEG C -55 DEG C of reaction temperature, 20 hours reaction time；Seed oil of Moringa oleigera and oil and fat of sacha inchi
Mass ratio be 1:1；
（3）By enzymolysis product 1. 30 mass parts, 80 mass parts of embedded material, 15 mass parts of auxiliary material, 55-65 DEG C of anion water
80 mass parts mix, and are emulsified under the conditions of closed cycle with homogenizer, homogeneous embedding, obtain mixing liquid 1.；Wherein, it embeds
Material is resistant starch, and auxiliary material is emulsifier（Casein sodium）, stabilizer dikalium phosphate, food flavor；It is the emulsifier, steady
Determine agent, food flavor mass ratio is 1:1:1；Processing condition：Homogenization pressure 60MPa, homogenizing temperature are 55-65 DEG C, homogenizing time
4h；
（4）By enzymolysis product 2. 30 mass parts, 80 mass parts of embedded material, 15 mass parts of auxiliary material, 55-65 DEG C of anion water
140 mass parts mix, and are emulsified under the conditions of closed cycle with homogenizer, homogeneous embedding, mixing liquid are obtained 2., wherein embedding
Material is corn sugar, resistant starch, and corn sugar, resistant starch mass ratio are 4:1, auxiliary material is emulsifier（Casein
Sour sodium）, stabilizer dikalium phosphate, food flavor；The emulsifier, stabilizer, food flavor mass ratio are 1:1:1；Homogeneous item
Part：Homogenization pressure 80MPa, homogenizing temperature are 55-65 DEG C, homogenizing time 5h；
（5）Corn grape in 1. mixing liquid being added to mixing liquid 2. continued emulsification with homogenizer homogeneous 40-50 minute
Matter embeds, and obtains lotion；
（6）Lotion is spray-dried, particle 90% crosses 16-20 mesh sieve, and the particle after drying falls into displacement container, through cooling down,
3 quick-dissolving agent of omega is made in filling storage；Spray drying condition is：125 DEG C, vacuum degree 200-500Pa of drying tower temperature is steamed
500 tons/h of steam raising amount, 20 tons/h of mixed liquor spray amount, 38 meters of adjustable tower height；Emulsion particle with flow velocity 15-20 seconds from upper and
It is lower to be dried.
Embodiment 3 realizes the present invention using following steps：
（1）Algal oil, Purple Perilla Seed Oil, lipase are mixed, ester exchange reaction is carried out, obtains enzymolysis product 1.；The lipase is used
Amount is the 10% of algal oil and Purple Perilla Seed Oil gross mass, 45 DEG C -55 DEG C of reaction temperature, 12 hours reaction time；Algal oil, purple perilla
The mass ratio of seed oil is 1:1；
（2）Seed oil of Moringa oleigera, oil and fat of sacha inchi, lipase are subjected to ester exchange reaction, obtain enzymolysis product 2.；Fatty enzyme dosage is Moringa
Seed oil and the 10% of oil and fat of sacha inchi gross mass, 45 DEG C -55 DEG C of reaction temperature, 12 hours reaction time；Seed oil of Moringa oleigera and oil and fat of sacha inchi
Mass ratio be 1:1；
（3）By enzymolysis product 1. 30 mass parts, 60 mass parts of embedded material, 9 mass parts of auxiliary material, 55-65 DEG C of anion water
100 mass parts mix, and are emulsified under the conditions of closed cycle with homogenizer, homogeneous embedding, obtain mixing liquid 1.；Wherein, it wraps
It is resistant starch to bury material, and auxiliary material is emulsifier（Double glyceride, casein sodium）, stabilizer dikalium phosphate, food flavor；Institute
It is 1 to state emulsifier, stabilizer, food flavor mass ratio:1:1；Processing condition：Homogenization pressure 55MPa, homogenizing temperature 55-65
DEG C, homogenizing time 0.5h；
（4）By enzymolysis product 2. 30 mass parts, 60 mass parts of embedded material, 9 mass parts of auxiliary material, 55-65 DEG C of anion water 200
Mass parts mix, and are emulsified under the conditions of closed cycle with homogenizer, homogeneous embedding, mixing liquid are obtained 2., wherein embedding material
Material is corn sugar, resistant starch, and corn sugar, resistant starch mass ratio are 6:1, auxiliary material is emulsifier（Double glyceride,
Casein sodium）, stabilizer dikalium phosphate, food flavor；The emulsifier, stabilizer, food flavor mass ratio are 1:1:1；
Processing condition：Homogenization pressure 60MPa, homogenizing temperature are 55-65 DEG C, homogenizing time 5h；
（5）Corn grape in 1. mixing liquid being added to mixing liquid 2. continued emulsifying homogeneous packet with homogenizer homogeneous 40 minutes
It buries, obtains lotion；
（6）Lotion is spray-dried, particle 90% crosses 16-20 mesh sieve, and the particle after drying falls into displacement container, through cooling down,
3 quick-dissolving agent of omega is made in filling storage；Spray drying condition is：125 DEG C, vacuum degree 200-500Pa of drying tower temperature is steamed
500 tons/h of steam raising amount, 20 tons/h of mixed liquor spray amount, 38 meters of adjustable tower height；Emulsion particle with flow velocity 15-20 seconds from upper and
It is lower to be dried.
Claims (10)
1. a kind of 3 quick-dissolving agent of omega, which is characterized in that by algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi, fat
It is prepared by enzyme, embedded material, auxiliary material；Wherein, algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi mass ratio be 1:1:1:1,
Fatty enzyme dosage is the 20-30% of algal oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi gross mass；When preparation, first by seaweed
Oil, Purple Perilla Seed Oil, seed oil of Moringa oleigera, oil and fat of sacha inchi and lipase carry out ester exchange reaction, obtain enzymolysis product, then by enzymolysis product
Emulsified with embedded material, auxiliary material, anion water, homogeneous, embedding, obtain lotion, then by lotion through spray drying, be made
3 quick-dissolving agent of omega.
2. 3 quick-dissolving agent of omega according to claim 1, which is characterized in that the embedded material is resistant starch, corn
One or both of glucose, dosage are 2-4 times of enzymolysis product quality；The auxiliary material is emulsifier, stabilizer, eats
Essence.
3. 3 quick-dissolving agent of omega according to claim 1, which is characterized in that the emulsifier is single double glyceride, junket egg
One or both of white acid sodium, stabilizer are dikalium phosphate.
4. 3 quick-dissolving agent of omega according to claim 1, which is characterized in that the ester exchange reaction condition is：Reaction temperature
45 DEG C -55 DEG C of degree, reaction time 12-20 hour.
5. 3 quick-dissolving agent of omega according to claim 1, which is characterized in that preparation method is as follows：
（1）Algal oil, Purple Perilla Seed Oil, lipase are mixed, ester exchange reaction is carried out, obtains enzymolysis product 1.；The lipase is used
Amount is the 10%-15% of algal oil and Purple Perilla Seed Oil gross mass, 45 DEG C -55 DEG C of reaction temperature, 16 hours reaction time；Algal oil,
The mass ratio of Purple Perilla Seed Oil is 1:1；
（2）Seed oil of Moringa oleigera, oil and fat of sacha inchi, lipase are subjected to ester exchange reaction, obtain enzymolysis product 2.；Fatty enzyme dosage is Moringa
The 10%-15% of seed oil and oil and fat of sacha inchi gross mass, 45 DEG C -55 DEG C of reaction temperature, 16 hours reaction time；Seed oil of Moringa oleigera and U.S. rattan
The mass ratio of fruit oil is 1:1；
（3）By enzymolysis product 1. 30 mass parts, embedded material 60-80 mass parts, auxiliary material 9-15 mass parts, 55-65 DEG C bear from
Sub- water 80-200 mass parts mixing is emulsified, homogeneous embedding under the conditions of closed cycle with homogenizer, obtains mixing liquid 1.；
Wherein, embedded material is resistant starch, and auxiliary material is emulsifier, stabilizer, food flavor；
（4）By enzymolysis product 2. 30 mass parts, embedded material 60-80 mass parts, auxiliary material 9-15 mass parts, 55-65 DEG C bear from
Sub- water 80-200 mass parts mixing is emulsified, homogeneous embedding under the conditions of closed cycle with homogenizer, obtains mixing liquid 2.,
Wherein embedded material is corn sugar, resistant starch, and corn sugar, resistant starch mass ratio are 4-6:1, auxiliary material is emulsification
Agent, stabilizer, food flavor；
（5）In 1. mixing liquid being added to mixing liquid 2., with homogenizer homogeneous 40-50 minutes, continues emulsifying homogeneous embedding, obtain
Lotion；
（6）Lotion is spray-dried, particle 90% crosses 16-20 mesh sieve, and the particle after drying falls into displacement container, through cooling down,
3 quick-dissolving agent of omega is made in filling storage.
6. 3 quick-dissolving agent of omega according to claim 5, which is characterized in that step（3）、（4）The emulsifier, stabilization
Agent, food flavor mass ratio are 1:1:1.
7. 3 quick-dissolving agent of omega according to claim 5, which is characterized in that the step（3）、（4）Processing condition is：
Homogenization pressure 30-80MPa, homogenizing temperature are 55-65 DEG C, homogenizing time 0.5-5h.
8. 3 quick-dissolving agent of omega according to claim 5, which is characterized in that the emulsifier is double glyceride, casein
One or both of sour sodium, stabilizer are dikalium phosphate.
9. 3 quick-dissolving agent of omega according to claim 5, which is characterized in that stating spray drying condition is：Drying tower temperature
125 DEG C, vacuum degree 200-500Pa, 500 tons/h of steam raising amount, 20 tons/h of mixed liquor spray amount.
10. 3 quick-dissolving agent of omega according to any one of claim 1-9, it is characterised in that：By 3 quick-dissolving agent of omega
The functional food of capsule for supplementing omega 3, tablet, oral solution, bead dosage form is prepared by mixing into maltodextrin.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105995979A (en) * | 2016-05-20 | 2016-10-12 | 福建师范大学 | Sacha inchi oil composition, micro-capsule powder and method for preparing same |
| CN107549332A (en) * | 2017-09-11 | 2018-01-09 | 江南大学 | Strengthen method of baby's long-chain polyunsaturated fatty acid bioavailability and products thereof |
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2018
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105995979A (en) * | 2016-05-20 | 2016-10-12 | 福建师范大学 | Sacha inchi oil composition, micro-capsule powder and method for preparing same |
| CN107549332A (en) * | 2017-09-11 | 2018-01-09 | 江南大学 | Strengthen method of baby's long-chain polyunsaturated fatty acid bioavailability and products thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王慧敏编: "《植物油图鉴》", 30 April 2016, 山西科学技术出版社 * |
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