CN108609865B - 一种玻璃用防火液及其制备方法 - Google Patents
一种玻璃用防火液及其制备方法 Download PDFInfo
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- CN108609865B CN108609865B CN201810555719.XA CN201810555719A CN108609865B CN 108609865 B CN108609865 B CN 108609865B CN 201810555719 A CN201810555719 A CN 201810555719A CN 108609865 B CN108609865 B CN 108609865B
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- glass
- fireproof
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- liquid
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- 239000011521 glass Substances 0.000 title claims abstract description 259
- 239000007788 liquid Substances 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 42
- 238000003756 stirring Methods 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 29
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 21
- 235000010333 potassium nitrate Nutrition 0.000 claims description 21
- 239000004323 potassium nitrate Substances 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 16
- NLSCHDZTHVNDCP-UHFFFAOYSA-N caesium nitrate Chemical compound [Cs+].[O-][N+]([O-])=O NLSCHDZTHVNDCP-UHFFFAOYSA-N 0.000 claims description 16
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 12
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 8
- 239000003063 flame retardant Substances 0.000 claims description 8
- 235000019253 formic acid Nutrition 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 description 37
- 238000012360 testing method Methods 0.000 description 37
- 230000035882 stress Effects 0.000 description 36
- 239000005341 toughened glass Substances 0.000 description 34
- 230000009970 fire resistant effect Effects 0.000 description 22
- 238000001816 cooling Methods 0.000 description 17
- 238000010791 quenching Methods 0.000 description 14
- 230000000171 quenching effect Effects 0.000 description 14
- 238000004519 manufacturing process Methods 0.000 description 12
- 230000008569 process Effects 0.000 description 12
- 238000006243 chemical reaction Methods 0.000 description 11
- 238000001035 drying Methods 0.000 description 11
- 230000035939 shock Effects 0.000 description 11
- 238000004140 cleaning Methods 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 10
- 239000005329 float glass Substances 0.000 description 9
- 238000009413 insulation Methods 0.000 description 9
- 239000010410 layer Substances 0.000 description 9
- 239000000243 solution Substances 0.000 description 9
- 239000002131 composite material Substances 0.000 description 8
- 230000008901 benefit Effects 0.000 description 7
- 238000005342 ion exchange Methods 0.000 description 7
- 239000005336 safety glass Substances 0.000 description 7
- 238000005507 spraying Methods 0.000 description 7
- 238000005496 tempering Methods 0.000 description 7
- 230000001070 adhesive effect Effects 0.000 description 6
- 238000010276 construction Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 5
- 239000000853 adhesive Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 230000002265 prevention Effects 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000010959 steel Substances 0.000 description 5
- 229910052792 caesium Inorganic materials 0.000 description 4
- -1 cesium ions Chemical class 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 4
- 229910001414 potassium ion Inorganic materials 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 239000002344 surface layer Substances 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 238000005452 bending Methods 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000006073 displacement reaction Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000004927 fusion Effects 0.000 description 3
- 239000005457 ice water Substances 0.000 description 3
- 229910001425 magnesium ion Inorganic materials 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 239000002356 single layer Substances 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 229910001415 sodium ion Inorganic materials 0.000 description 3
- 238000002834 transmittance Methods 0.000 description 3
- QZRLETONGKUVFA-UHFFFAOYSA-N [K].[Cs] Chemical compound [K].[Cs] QZRLETONGKUVFA-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 239000006121 base glass Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000004134 energy conservation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 239000011229 interlayer Substances 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 238000005498 polishing Methods 0.000 description 2
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 229910001427 strontium ion Inorganic materials 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000005337 ground glass Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000009863 impact test Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000005340 laminated glass Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000005649 metathesis reaction Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 235000003270 potassium fluoride Nutrition 0.000 description 1
- 239000011698 potassium fluoride Substances 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
- C03C17/008—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character comprising a mixture of materials covered by two or more of the groups C03C17/02, C03C17/06, C03C17/22 and C03C17/28
- C03C17/009—Mixtures of organic and inorganic materials, e.g. ormosils and ormocers
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C03C21/001—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
- C03C21/002—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions to perform ion-exchange between alkali ions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Composite Materials (AREA)
- Surface Treatment Of Glass (AREA)
Abstract
Description
表面应力(MPa) | |
防火玻璃1 | 237 |
防火玻璃2 | 243 |
防火玻璃3 | 249 |
钢化玻璃 | 96 |
玻璃原片 | 24 |
弯曲强度(MPa) | |
防火玻璃1 | ≥180 |
防火玻璃2 | ≥180 |
防火玻璃3 | ≥180 |
钢化玻璃 | ≥120 |
玻璃原片 | ≥50 |
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810555719.XA CN108609865B (zh) | 2018-05-31 | 2018-05-31 | 一种玻璃用防火液及其制备方法 |
Applications Claiming Priority (1)
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CN201810555719.XA CN108609865B (zh) | 2018-05-31 | 2018-05-31 | 一种玻璃用防火液及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN108609865A CN108609865A (zh) | 2018-10-02 |
CN108609865B true CN108609865B (zh) | 2021-01-15 |
Family
ID=63664668
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201810555719.XA Active CN108609865B (zh) | 2018-05-31 | 2018-05-31 | 一种玻璃用防火液及其制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN108609865B (zh) |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101092286B (zh) * | 2006-06-19 | 2011-02-16 | 福清市新福兴玻璃有限公司 | 防火玻璃的生产方法及生产专用设备 |
CN105271799A (zh) * | 2015-11-03 | 2016-01-27 | 江苏惠宇玻璃有限公司 | 一种钢化铯钾防火玻璃的制备方法 |
CN107954610A (zh) * | 2016-10-14 | 2018-04-24 | 北京华城耀强玻璃科技有限公司 | 玻璃防火液及其应用 |
-
2018
- 2018-05-31 CN CN201810555719.XA patent/CN108609865B/zh active Active
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Publication number | Publication date |
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CN108609865A (zh) | 2018-10-02 |
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PB01 | Publication | ||
PB01 | Publication | ||
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SE01 | Entry into force of request for substantive examination | ||
CB02 | Change of applicant information |
Address after: 350314 Yan Dou village, Yuan Hong Industrial Zone, Fuqing City, Fuzhou, Fujian Applicant after: Xinfuxing Glass Industry Group Co.,Ltd. Address before: 350315 Yan Dou village, Yuan Hong Industrial Zone, Fuqing City, Fuzhou, Fujian Applicant before: XINFUXING GLASS CO.,LTD. |
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CB02 | Change of applicant information | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210324 Address after: 350300 Yandou village, Yuanhong Industrial Zone, Fuqing City, Fuzhou City, Fujian Province Patentee after: Xinfuxing Glass Industry Group Co.,Ltd. Patentee after: FUZHOU XINFUXING GLASS Co.,Ltd. Patentee after: Fuzhou Xinfuxing Float Glass Co.,Ltd. Patentee after: Fujian Xinfuxing glass Intelligent Technology Co.,Ltd. Address before: 350314 Yandou village, Yuanhong Industrial Zone, Fuqing City, Fuzhou City, Fujian Province Patentee before: Xinfuxing Glass Industry Group Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
CP03 | Change of name, title or address |
Address after: 350300 Yandou village, Yuanhong Industrial Zone, Fuqing City, Fuzhou City, Fujian Province Patentee after: Xinfuxing Glass Industry Group Co.,Ltd. Country or region after: China Patentee after: FUZHOU XINFUXING GLASS Co.,Ltd. Patentee after: Fuzhou Xinfuxing Glass Technology Co.,Ltd. Patentee after: Fujian Xinfuxing glass Intelligent Technology Co.,Ltd. Address before: 350300 Yandou village, Yuanhong Industrial Zone, Fuqing City, Fuzhou City, Fujian Province Patentee before: Xinfuxing Glass Industry Group Co.,Ltd. Country or region before: China Patentee before: FUZHOU XINFUXING GLASS Co.,Ltd. Patentee before: Fuzhou Xinfuxing Float Glass Co.,Ltd. Patentee before: Fujian Xinfuxing glass Intelligent Technology Co.,Ltd. |
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CP03 | Change of name, title or address |