CN108607077A - A kind of pulverizing medicinal materials method of anaesthetic pill - Google Patents

A kind of pulverizing medicinal materials method of anaesthetic pill Download PDF

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Publication number
CN108607077A
CN108607077A CN201611165227.7A CN201611165227A CN108607077A CN 108607077 A CN108607077 A CN 108607077A CN 201611165227 A CN201611165227 A CN 201611165227A CN 108607077 A CN108607077 A CN 108607077A
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medicinal materials
medicinal material
medicine
materials method
calcite
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佘宜寰
齐平
韩风雨
于秀玲
李洪泽
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INNER MONGOLIA TIANQI ZHONGMENG PHARMACEUTICAL Co Ltd
Inner Mongolia Boao Modern Mongolian Traditional Chinese Medicine Technology Research Co Ltd
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INNER MONGOLIA TIANQI ZHONGMENG PHARMACEUTICAL Co Ltd
Inner Mongolia Boao Modern Mongolian Traditional Chinese Medicine Technology Research Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • A61K36/716—Clematis (leather flower)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
    • A61K33/10—Carbonates; Bicarbonates
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/14—Alkali metal chlorides; Alkaline earth metal chlorides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/31—Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/45—Ericaceae or Vacciniaceae (Heath or Blueberry family), e.g. blueberry, cranberry or bilberry
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/67—Piperaceae (Pepper family), e.g. Jamaican pepper or kava
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8968—Ophiopogon (Lilyturf)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/906—Zingiberaceae (Ginger family)
    • A61K36/9068—Zingiber, e.g. garden ginger
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/20—Pills, tablets, discs, rods
    • A61K9/2004—Excipients; Inactive ingredients

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
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Abstract

The present invention relates to a kind of pulverizing medicinal materials method of anaesthetic pill, more particularly to a kind of pulverizing medicinal materials method of anaesthetic pill that treating colitis.The drug is made of following medicinal materials：Calcite, halite, Clematis aethusifolia, rhododendron micranthum, nutmeg, Fructus Coriandri sativi, rhizoma zingiberis, fructus piperis longi, Radix Ophiopogonis, Gu Yue, raphani,radix, white sand, HALITUM PURPUREUM, elecampane, nitre.This preparation medicinal material is used as medicine using original powder, and micropill preparation is made.Therefore the smashing fineness of the grinding mode of medicinal material, flour extraction, medicinal powder is studied, to retain medicinal material active ingredient to the greatest extent, improves medicinal material utilization rate, it is ensured that the effect of drug.

Description

A kind of pulverizing medicinal materials method of anaesthetic pill
Technical field
The present invention relates to anaesthetic preparation fields, and in particular to a kind of pulverizing medicinal materials method of anaesthetic pill.
Background technology
Pellet is more and more favored in recent years, has the following advantages：(1) after taking extensively, be evenly distributed in Gastrointestinal tract, on stomach and intestine surface, distribution area is big, to the stimulation for improving bioavilability, drug being reduced or eliminated to gastrointestinal tract； (2) micropill preparation is not influenced in the transhipment of gastrointestinal tract by the food conveying rhythm and pace of moving things, gastric emptying；(3) mobility is preferable, is conducive to preparation Packing or further molding；(4) stability for increasing drug, improves curative effect, is convenient for quality when reducing adverse reaction, and producing Control and assay；(5) have the advantages that patient is facilitated to carry and take.
The preparation process of we is according to ratio, physicochemical property and the effect of main flavour of a drug in this prescription, produce reality feelings Condition compares and formulates by testing, studying repeatedly, analyze, is now described below：
For Da Ge -15 by ten five tastes mongolian medicine prescription such as calcite, wherein Clematis aethusifolia, rhododendron micranthum is main ingredient in side, two Person is used as medicine in charcoal drug, and dosage is maximum in we, accounts for the 69% of prescription ratio altogether；Calcite, halite, nitre etc. are main in side It is respectively calcium carbonate, sodium chloride, potassium nitrate to want ingredient, also accounts for the 22.4% of prescription ratio；Ten taste such as nutmeg only accounts for prescription ratio The 8.6% of example；Based on charcoal drug in our prescription and mineral salts medicine, extraction, which is used as medicine relatively to be stranded, tests, and plans its exploitation and enters for pill Medicine.Because of the micromeritis distribution character of pellet, it is suitble to our the characteristics for the treatment of gastrointestinal disease, therefore we's exploitation is used as medicine for pellet. The kind is researched and developed to pushing the modernization development of Mongolia Medicine and improving the quality controllability of anaesthetic with certain meaning.
Invention content
The object of the present invention is to provide a kind of pulverizing medicinal materials methods of anaesthetic pill.
We are that anaesthetic tradition side is used as medicine using prescription taste of traditional Chinese medicine main component property as foundation using original powder, and will be measured less Fine powder facing-up hybrid technique prepared.
Clematis aethusifolia mainly contains saponins, flavonoids, lignanoids in side, includes additionally volatile oil, alkaloid, has Other compounds such as machine acids, alkane, flower, leaf are containing flavones ingredients such as Quercetin, Kaempferols；It is unsuitable because it is used as medicine to forge charcoal It is used as medicine mode using extraction, to ensure that ingredient does not lose in preparation process, and takes into account medication custom, be used as medicine using original powder.
Rhododendron micranthum is containing saponin, tannin, reducing substances, polysaccharide, flavones, grease and volatile oil etc. in side.Flavones in leaf Class has Quercetin, gossypetin, Kaempferol.The content of volatile oil is 0.27% (fresh leaf).Also contain 4 phenolic acid in leaf：P- hydroxyl Benzoic acid, protocatechuic acid, vanillic acid and syringic acid.Because it is used as medicine to forge charcoal, extraction should not be used to be used as medicine mode, for ensure at Divide and do not lost in preparation process, and take into account medication custom, is used as medicine using original powder.
Elecampane mainly contains volatile oil 0.3%~3.0%, saussurine, synanthrin in side, and main component is in elecampane in oil Ester, dihydroalantolacton, dihydroisoalantolactone, separately contains dammaradienyl acetate, elecampane at isoalantolactone Acid, alantol etc..To ensure that ingredient does not lose in preparation process, it is used as medicine using original powder.
Fructus Coriandri sativi contains volatile oil 1%~1.4%, fat 26% in side.Also contain glucose, fructose, sucrose and coriander sterol Glycosides etc..To ensure that ingredient does not lose in preparation process, it is used as medicine using original powder.
Rhizoma zingiberis mainly contains volatile oil and piquancy component two major classes in side.Mainly there are gingerol, salad oil in piquancy component With the phenols components such as zingiberone.To ensure that ingredient does not lose in preparation process, it is used as medicine using original powder.
Fructus piperis longi Piper longum fruits contain pipering, palmitic acid, tetrahydropiperic acid, 11 carbon -1- alkene -3,4- methylene dioxies in side Benzene, piperidines, volatile oil, the anti-4- amides of N- isobutyl groups decadinene-anti-2-, sesamin, fructus piperis longi nonadiene piperidines, 11 carbon three of fructus piperis longi Alkene piperidines, the bright peaceful alkali of fructus piperis longi, the bright peaceful alkali of dihydro fructus piperis longi, piperamide, Guinea's piperamide, 18 carbon -2,4- of N- isobutyl groups Diene amide, 20 carbon -2,4- diene amide of N- isobutyl groups etc..To ensure that ingredient does not lose in preparation process, using original powder It is used as medicine.
Radix Ophiopogonis contains a variety of steroid saponins：Ophiopogon saponin A, B, C, D, glucoside member are ruscogenin, separately contain ophiopogon saponin B ', C ', D ', glucoside member are diosgenin；It is to ensure that ingredient does not damage in preparation process still to contain a variety of flavone compound It loses, is used as medicine using original powder.
Gu Yue contains a variety of amides compounds, and contains volatile oil.To ensure that ingredient does not lose in preparation process, using original Powder is used as medicine.
Raphani,radix carbohydrate containing, organic acid, minerals, vitamin, mustard oil etc..
Nutmeg mainly contains the volatile oil components such as nopinene, γ-terpinene, methyl eugenol, myristic acid in side, is Ensure that ingredient does not lose in preparation process, is used as medicine using original powder.
Calcite is carbonate mineral calcite race calcite, main calcium carbonate (CaCO in side3), for mine contained by guarantee Material composition does not lose, and takes into account medication custom, and independent crushing, original powder is taken to be used as medicine.
Halite is halogenation species halite race lake salt crystalline solid, main sodium chloride-containing (NaCl) in side.For mineral contained by guarantee Matter ingredient does not lose, and takes into account medication custom, and independent crushing, original powder is taken to be used as medicine.
White sand is halogenation species mineral sal ammoniac, main containing ammonium chloride (NH in side4Cl).Not for mineral composition contained by guarantee Loss, and medication custom is taken into account, take independent crushing, original powder to be used as medicine.
HALITUM PURPUREUM is halogenation species mineral stone salt, main sodium chloride-containing (NaCl) in side.Not for mineral composition contained by guarantee Loss, and medication custom is taken into account, take independent crushing, original powder to be used as medicine.
Nitre is Nitrates Na Jia stones race mineral niter in side.Main (the KNO containing potassium nitrate3).For mineral contained by guarantee Matter ingredient does not lose, and takes into account medication custom, and independent crushing, original powder is taken to be used as medicine.
This preparation of other side's Minerals medicinal material is quasi- to be used as medicine using individually crushing, because removing calcite, Clematis aethusifolia in side, according to mountain 12 taste such as ultrawhite nutmeg dosage in we is few, therefore carries out facing-up technique to its hybrid technique and examined with other techniques It examines, therefore the few medicinal material of the eight taste amounts such as nutmeg carries out group's powder when its crushing, measures big Clematis aethusifolia, two taste group's powder of rhododendron micranthum, And smashing fineness is provided.
Above-mentioned medicinal material is used as medicine with original powder.Medicinal material is processed before crushing.It is specific to process with disintegrating process such as Under：
1. the processing of medicinal material
Medicinal material used meets statutory standards in we, and is cleaned by method removing under each kind item, cutting.
Calcite is fumed to take net calcite, according to method of direct calcination (《Chinese Pharmacopoeia》Annex II D) it is calcined to white, put into water In quench shortcake, take out, dry.
Halite is fumed to take net halite, crushes.It sets in iron pan, slow boiling is fried about 4~6 minutes, is taken when until sending out the sound Go out.
Rhododendron micranthum fries charcoal and takes net rhododendron micranthum, is fried to appearance coke black with moderate heat, internal coke brown, still clearly discernible medicine It is taken out when object original shape.
Clematis aethusifolia fries charcoal and takes net Clematis aethusifolia, is fried to appearance coke black with moderate heat, internal coke brown, still can be clear It is taken out when clear discrimination drug original shape.
2. the crushing of medicinal material
This preparation is pellet, is used as medicine using original powder, therefore it is thin to have carried out pulverizing medicinal materials mode, flour extraction, the crushing of medicinal powder The research of degree.
The investigation of 2.1 independent grinding medicinal materials flour extractions
Since calcite, halite, white sand, HALITUM PURPUREUM, nitre are mineral medicinal material, it is all made of independent crushing.To ensure The accuracy of dosage respectively studies its flour extraction and smashing fineness.Precision weighs calcite, halite, white Nao Each 3 parts of sand, HALITUM PURPUREUM, nitre sample, each heavy 100g of every part of sample cross 120 mesh sieve.It the results are shown in Table 1,2,3,4,5.
1 calcite flour extraction of table is studied
2 halite flour extraction of table is studied
3 white sand flour extraction of table is studied
4 HALITUM PURPUREUM flour extraction of table is studied
5 nitre flour extraction of table is studied
Conclusion：The above independent grinding medicinal materials average yield of the five tastes is 98.66%, ensure that the accuracy to feed intake, is ground into The absorption of active ingredient in vivo is more advantageous to after impalpable powder.
The investigation of 2.2 groups of powder medicinal material flour extractions
2.2.1 Clematis aethusifolia, rhododendron micranthum crush
Three parts of medicinal material is weighed according to recipe quantity ratio：Clematis aethusifolia 500g, rhododendron micranthum 500g.Co-grinding crosses 100 mesh Sieve to get.It the results are shown in Table 6.
6 Clematis aethusifolia of table, rhododendron micranthum crush flour extraction research
2.2.2 eight taste such as nutmeg crushes
Three parts of medicinal material is weighed according to recipe quantity ratio：Nutmeg 100g, Fructus Coriandri sativi 100g, rhizoma zingiberis 100g, fructus piperis longi 100g, wheat Winter 100g, Gu Yue 100g, raphani,radix 100g, elecampane 100g.Co-grinding, sieve with 100 mesh sieve to get.It the results are shown in Table 7.
Eight tastes such as 7 nutmeg of table crush flour extraction research
The flour extraction average out to 97.90% of group's powder medicinal material.
In conclusion passing through the grinding mode investigation to medicinal material, it is possible to reduce the loss of medicinal material is accelerated, increases it in body Interior absorption, while its removing in vivo can also be accelerated, reduce accumulation in vivo.Again to body while guarantee curative effect Toxic side effect smaller.
Specific implementation mode
Embodiment
Calcite (system) 156.74, halite (system) 31.35, Clematis aethusifolia (charcoal) 313.48, rhododendron micranthum (charcoal) 313.48, nutmeg 7.84, Fructus Coriandri sativi 7.84, rhizoma zingiberis 7.84, fructus piperis longi 7.84, Radix Ophiopogonis 7.84, Gu Yue 7.84, raphani,radix 7.84, White sand 7.84, HALITUM PURPUREUM 7.84, elecampane 7.84, nitre 15.68.
Preparation method：Calcite, halite, white sand, HALITUM PURPUREUM, nitre are individually ground into impalpable powder；Parsley iron Line lotus, rhododendron micranthum are ground into fine powder；Eight taste such as remaining nutmeg is ground into fine powder；12 taste such as nutmeg and calcite, parsley Clematis, rhododendron micranthum powder facing-up, sieving, mixing.Be added appropriate amount of auxiliary materials, mixing, pill, it is dry to get.

Claims (5)

1. a kind of pulverizing medicinal materials method of anaesthetic pill, which is characterized in that the preparation is made of following medicinal materials：Calcite, Halite, Clematis aethusifolia, rhododendron micranthum, nutmeg, Fructus Coriandri sativi, rhizoma zingiberis, fructus piperis longi, Radix Ophiopogonis, Gu Yue, raphani,radix, white sand, purple Nao Sand, elecampane, nitre.
2. pulverizing medicinal materials method according to claim 1, which is characterized in that other side's Minerals medicinal material is quasi- using individually crushing It is used as medicine.Mineral medicinal material includes：Calcite, halite, white sand, HALITUM PURPUREUM and nitre.Grinding particle size is 120 mesh.
3. pulverizing medicinal materials method according to claim 1, which is characterized in that Clematis aethusifolia and rhododendron micranthum carry out in other side Co-grinding, grinding particle size are 100 mesh.
4. pulverizing medicinal materials method according to claim 1, which is characterized in that nutmeg, Fructus Coriandri sativi, rhizoma zingiberis, Bi in other side The roots of grass, Radix Ophiopogonis, Gu Yue, raphani,radix, elecampane carry out co-grinding, and grinding particle size is 100 mesh.
5. pulverizing medicinal materials method according to claim 1, which is characterized in that the smaller medicinal material of the 12 taste dosage such as nutmeg Powder and calcite, Clematis aethusifolia, rhododendron micranthum medicinal powder carry out facing-up, sieving, mixing.
CN201611165227.7A 2016-12-09 2016-12-09 A kind of pulverizing medicinal materials method of anaesthetic pill Pending CN108607077A (en)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101590216A (en) * 2009-05-19 2009-12-02 赤峰天奇制药有限责任公司 A kind of medicine for the treatment of colitis

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101590216A (en) * 2009-05-19 2009-12-02 赤峰天奇制药有限责任公司 A kind of medicine for the treatment of colitis

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
侯秀英等: "《新编现代实用药剂学》", 31 July 2015, 西安交通大学出版社 *
娜仁图雅等: "十五味达哈布—满那格治疗胃病30例体会", 《中国民族民间医药》 *

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Application publication date: 20181002