CN108578531A - Intestinal cancer healing liquid and its production technology - Google Patents
Intestinal cancer healing liquid and its production technology Download PDFInfo
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- CN108578531A CN108578531A CN201810250968.8A CN201810250968A CN108578531A CN 108578531 A CN108578531 A CN 108578531A CN 201810250968 A CN201810250968 A CN 201810250968A CN 108578531 A CN108578531 A CN 108578531A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0014—Skin, i.e. galenical aspects of topical compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0087—Galenical forms not covered by A61K9/02 - A61K9/7023
- A61K9/0095—Drinks; Beverages; Syrups; Compositions for reconstitution thereof, e.g. powders or tablets to be dispersed in a glass of water; Veterinary drenches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
Abstract
The invention discloses a kind of intestinal cancer healing liquid and its production technologies.Intestinal cancer healing liquid of the present invention is formed by Lowiaceae plant extraction concentrate and active ionic water physics compound, and wherein the weight ratio of Lowiaceae plant extraction concentrate and active ionic water is 1:5.Intestinal cancer healing liquid of the present invention is easy to use, both it can smear, drink-service use can also be dripped, while supplying abundant nutrition to human body cell, there is repair to systemic cell, acid-base balance improves the microenvironment of cell growth, enhancing cell biological electric field promotes cell metabolism ability, to the various trace elements needed for sertoli cell, promote the synthesis of elastomer and collagen, strength repairs various skin injuries, in addition there is adjustment effect to human immune system so that human body is got well.
Description
Technical field
The present invention relates to a kind of intestinal cancer healing liquid and its production technologies.
Background technology
The disease of human body be as caused by immune system defect, such as blood disease, disease of digestive tract, cardiovascular and cerebrovascular disease,
Cardio-pulmonary function disease and gynaecology's functional disease and various anaphylactias, foster appearance, beauty treatment, psoriasis etc..Human body
Immune system existing defects in a certain respect, can influence the various aspects of human body for a long time.It is presently used for treatment and health care is made
Promote the health products that human immune system repairs to have a single function mostly, the defect of single aspect can only be repaired, no
The function of the immune system of energy General Promotion human body.And effect is weaker, and effect is slow, needs long term that could generate effect
Fruit.
Intestinal cancer refers to betiding the carninomatosis class disease of enteron aisle, is malignant tumour common in gastrointestinal tract, and incidence is only second to
Stomach and the cancer of the esophagus are the most common parts of colorectal cancer.
Intestinal cancer mainly has following symptom:
1. intestinal cancer initial stage, based on having blood in stool, followed by bowel habit changes, and defecation is felt not to the utmost, tenesmus etc., additionally
Easily cause to block phenomenon, generates enteron aisle irritation etc..
2. the typical performance that bowel habit change is intestinal cancer middle and advanced stage can due to rectal mass and its secretion of generation
Enteron aisle irritation is generated, causes patient the symptoms such as awareness of defecation is frequent, defecation is felt, is tenesmus not to the utmost occur, but effluent is mostly
Mucus purulence blood shape object, at this time excrement shape also changed, stool it is more and more thinner.
3. since cancerous swelling is infiltrated around intestinal wall week diameter, make stenosis of bowel, especially in proctosigmoid intersection, mostly stenotic type
Inocarcinoma easily causes to block phenomenon.Advanced rectal cancer patient, since disease long-term chronic consumes, it may appear that some whole body cancerations
Sick matter.
4. intestinal cancer often invades surrounding tissue organ, such as bladder and prostate adjacent tissue to late period, cause frequent micturition, urgent urination
And dysuria.It invades and presacral plexus, sacrum tail and flank pain occurs.The carcinoma of the rectum can also distally be transferred to liver, draw
Play hepatomegaly, the performances such as ascites, jaundice or even dyscrasia.
Invention content
Purpose of the present invention is to what is be achieved through the following technical solutions:
Technical problem to be solved by the invention is to provide a kind of intestinal cancer healing liquids.
Intestinal cancer healing liquid of the present invention, is made of Lowiaceae plant extraction concentrate and water, and wherein Lowiaceae plant extraction is dense
The weight ratio for the liquid sum that contracts is 1:(5-20).Water is preferably active ionic water.
In some embodiments of the invention, the Lowiaceae plant extraction concentrate is prepared by the following preparation method:
(1) 30-50g banana barks are added in 60-200g boiling water and are scalded 3-8 minutes, surface moisture is drained, then by 20-
40g bananas bark, 25-50g Banana trees stem, 10-20g bananas leaf are 6-12 hours dry at 40-60 DEG C, by banana bark, perfume (or spice)
Any of several broadleaf plants tree stem, banana leaf smash it through 20-50 mesh sieve respectively, are uniformly mixed that obtain mixture spare;
(2) 12-36g mixtures are taken, the sodium chloride that 40-80g mass fractions are 3-10%, temperature is 35-55 DEG C is added to
In aqueous solution, ultrasonic extraction 35-65 minutes under the conditions of power is 200-800W, frequency is 40-50KHz, with 4000-10000
Rev/min rotating speed centrifuge 20-60 minute, take centrifugation after supernatant liquid, cross 100-500 mesh sieve, reservation filtrate to get Lowiaceae
Plant extraction concentrate.
In some embodiments of the invention, the Lowiaceae plant extraction concentrate is prepared by the following preparation method:
(1) 30-50g banana barks are added in 60-200g boiling water and are scalded 3-8 minutes, surface moisture is drained, then by 20-
40g bananas bark, 25-50g Banana trees stem, 10-20g bananas leaf are 6-12 hours dry at 40-60 DEG C, by banana bark, perfume (or spice)
Any of several broadleaf plants tree stem, banana leaf smash it through 20-50 mesh sieve respectively, are uniformly mixed and obtain mixture, by mixture at -45~-40 DEG C
Freezing 30-90 minutes, then with power is 300-500W, microwave heating that frequency is 2450-3000MHz 5-25 minutes, -35
~-30 DEG C freeze 20-60 minutes, then with 5-20 points of the microwave heating that power is 300-500W, frequency is 2450-3000MHz
Clock freezes 10-40 minutes at -25~-20 DEG C, is then added with the microwave that power is 300-500W, frequency is 2450-3000MHz
It is 3-15 minutes hot, it is then placed 30-90 minutes in 30-60 DEG C of insulating box, obtains pretreated mixture;
(2) 12-36g mixtures are taken, the sodium chloride that 40-80g mass fractions are 3-10%, temperature is 35-55 DEG C is added to
In aqueous solution, ultrasonic extraction 35-65 minutes under the conditions of power is 200-800W, frequency is 40-50KHz, with 4000-10000
Rev/min rotating speed centrifuge 20-60 minute, take centrifugation after supernatant liquid, cross 100-500 mesh sieve, reservation filtrate to get Lowiaceae
Plant extraction concentrate.
Commercially available active ionic water may be used in active ionic water, can also be obtained by homemade method.
Preferably, the preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 20-30 minutes, is obtained corona treatment liquid;
The operating condition of excitation device is:Operating voltage 0.42-0.6KV, operating current 10-30mA, working gas are
The mixed gas of 98% argon gas and 2% oxygen, gas flow 5-8mL/ minutes;
Activated carbon or the modification of corona treatment liquid weight 0.2%-0.3% is added into corona treatment liquid by S2
Activated carbon after being stirred 40-60 minutes with 180-250 revs/min of rotating speed, is stood 2-3 hours, collects supernatant, is obtained net
Change liquid;
S3 is by scavenging solution and anti-oxidation peptide with 1:(0.005-0.01) is uniformly mixed, and obtains the active ionic water.
Plasma excites will produce active oxygen and a small amount of hydrogen peroxide under water, plays sterilization, kills virus, promotes
The effect of microbial cell death.In addition, there is faintly acid using the activated carbon that tartaric acid is modified, with commercially available activated carbon phase
Than surface is modified and has gone up some weakly acidic organo-functional groups, improves absorbent charcoal material to harmful metal ion in water
Removal effect, while tartaric acid to human body have health and beauty.Therefore, pass through slightly acidic water obtained by the above method, pH
Between 4.0-6.5, the health care demand of people can be met.
In some technical solutions of the present invention, the preparation process of the modified activated carbon is:Activated carbon is washed with water,
The mass ratio of activated carbon and slurry is 1:(50-100) removes the impurity on surface, 50-80 minutes dry in 110-120 DEG C;
Dry activated carbon is immersed in the tartaric acid aqueous solution that molar concentration is 0.1-0.6mol/L, activated carbon and tartaric acid aqueous solution
Solid-liquid ratio is 1:(2-3) (g/mL) is uniformly mixed, obtains mixed liquor;By mixed liquor after 40-60 DEG C is heated 8-12 hours, in
20-25 DEG C stands 2-3 hours, takes bottom solid;Bottom solid is 12-20 hours dry in 30-40 DEG C, it obtains described modified living
Property charcoal.
In some technical solutions of the present invention, the preparation process of the modified activated carbon is:Activated carbon is washed with water,
The mass ratio of activated carbon and slurry is 1:(50-100) removes the impurity on surface, 50-80 minutes dry in 110-120 DEG C;
By dry activated carbon and tartaric acid with mass ratio 1:(0.2-0.3) is uniformly mixed, and obtains mixture;By mixture in 40-60 DEG C
After heating 8-12 hours, 2-3 hours are stood in 20-25 DEG C, obtains the modified activated carbon.
In the technical solution that above two prepares modified activated carbon, activated carbon can adsorb tartaric acid, but will not destroy fruit
The physical and chemical properties of acid, save the original property of tartaric acid.The effect of wherein the first modified activated carbon is more excellent, this may
It is to make the porous movement of activated carbon more active since in the preparation process of activated carbon, temperature increases, adsorption capacity enhancing,
Adsorption capacity increases, and also so that the movement of tartaric acid molecule and hydrone is more active, promotes the progress of absorption, accelerates absorption
Rate.
The tartaric acid is malic acid, citric acid, persimmon leaf tartaric acid, oleanolic acid, ursolic acid, one kind in olive tartaric acid or more
Kind.
The anti-oxidation peptide is kidney bean protein antioxidant peptide and/or milk casein anti-oxidation peptide.Preferably, described anti-oxidant
Peptide is the mixture of kidney bean protein antioxidant peptide and milk casein anti-oxidation peptide, wherein kidney bean protein antioxidant peptide and milk casein
The mass ratio of anti-oxidation peptide is (2-3):1.
The kidney bean protein antioxidant peptide both may be used commercially available kidney bean protein antioxidant peptide, and can also pass through self-control
Method obtain.
Commercially available milk casein anti-oxidation peptide had both may be used in the milk casein anti-oxidation peptide, can also referenced patent
Application No. is 201210315545.2 embodiments three to obtain.
Kidney bean is full of nutrition, very rich in protein, vitamin, Soluble Fiber, antioxidant and fat content
It is low, there is excellent health-care effect.The preparation method of the kidney bean protein peptides is:
S1 prepares kidney bean albumen:Kidney bean (using red kidney bean) is crushed, 40 mesh sieve is crossed, obtains kidney bean part;By kidney bean powder and
Water is with solid-liquid ratio 1:15 (g/mL) mix, use molar concentration 1mol/L sodium hydrate aqueous solution adjust mixed liquor pH for
10, it is extracted 2 hours in 50 DEG C, obtains extracting solution;Extracting solution is cooled to 30 DEG C, 15 points are centrifuged with 4000 revs/min of rotating speed
Clock collects supernatant;It for the salt acid for adjusting pH of 1mol/L is 4 that supernatant, which is used molar concentration, stands 30 minutes, and it is solid to abandon bottom
Body collects clear liquid;By clear liquid vacuum freeze drying, kidney bean albumen is obtained;The process conditions of wherein vacuum freeze drying are:Pre-freeze
- 30 DEG C of temperature, pre-freeze time 2 h, 25 DEG C of sublimation temperature, 40 DEG C, vacuum degree 0.09MPa of resolution temperature, vacuum drying time
16 hours;
S2 is digested:Kidney bean albumen is configured to the solution that mass fraction is 5% with water, after ten minutes in 90 DEG C of processing, is adopted
It is 10 to adjust pH with the sodium hydrate aqueous solution of molar concentration 1mol/L, is heated to 55 DEG C, adds according to the additive amount of 4000u/mL
Entering alkali protease, (alkali protease2709, food-grade, 1,200,000 U/g of enzyme activity believe the limited public affairs of chemical products purchased from Zhengzhou crowd
Department), in 55 DEG C of enzyme digestion reactions 2 hours;In 100 DEG C of enzyme deactivations 10 minutes;Enzyme deactivation liquid is adjusted using the hydrochloric acid of molar concentration 1mol/L
PH be 4.2, centrifuged 20 minutes with 3000 revs/min of rotating speed, collect supernatant;By supernatant vacuum freeze drying, obtain
Kidney bean protein antioxidant peptide;The process conditions of wherein vacuum freeze drying are:- 30 DEG C of pre-freezing temperature, pre-freeze time 2 h rise
25 DEG C of magnificent temperature, 40 DEG C, vacuum degree 0.09MPa of resolution temperature, vacuum drying time 16 hours;
S3 ultrafiltration:Kidney bean protein antioxidant peptide is configured to the ultrafiltration feed liquid that mass fraction is 10% with water, by ultrafiltration material
Liquid is detached using the ultrafiltration membrane of molecular cut off 5000Da, collects permeate;Liquid is will transmit through to continue to use molecular cut off
The ultrafiltration membrane of 3000Da is detached, and permeate is separated into molecular weight between 3000~5000Da and less than 3000Da two
A part;Permeate by molecular weight less than 3000Da continues to be detached with the ultrafiltration membrane of molecular cut off 1000Da, penetrates
Liquid is separated into molecular weight between 1000~3000Da and less than two parts 1000Da;Obtained ultrafiltration component is distinguished
Vacuum freeze drying, obtain molecular weight between 3000~5000Da, between 1000~3000Da and be less than tri- portions 1000Da
Divide kidney bean protein antioxidant peptide.
The second technical problem to be solved by the present invention is to provide a kind of production technology of intestinal cancer healing liquid.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and water are uniformly mixed to get described
Intestinal cancer healing liquid.
The intestinal cancer healing liquid dosage is daily 5-6 milliliters, can divide 2-8 times and use absorption.
Intestinal cancer healing liquid of the present invention is easy to use, can both smear, and can also drip drink-service use, be supplied to human body cell
While to abundant nutrition, there is repair, acid-base balance to improve the microenvironment of cell growth, enhancing cell systemic cell
Bio-electric field promotes cell metabolism ability, to the various trace elements needed for sertoli cell, promotes elastomer and collagen egg
Various skin injuries are strongly repaired in white synthesis, in addition have adjustment effect to human immune system so that human body restores strong
Health.
Specific implementation mode
Each raw material introduction in embodiment:
Banana bark, tree stem, leaf, Musaceae banana banana (Classification system:Musa nana Lour.) perfume (or spice)
Any of several broadleaf plants bark, tree stem, leaf, banana variety are Saigon any of several broadleaf plants, place of production Nanning.
Excitation device is provided by Inst. of Mechanics, CAS.
Activated carbon, food is special, 180-240 mesh, is purchased from Hong Chang water-purifying materials factory of Gongyi City.
Kidney bean protein antioxidant peptide, molecular weight are 3000~5000Da.The preparation method of the kidney bean protein antioxidant peptide
For:
S1 prepares kidney bean albumen:Kidney bean (using red kidney bean) is crushed, 40 mesh sieve is crossed, obtains kidney bean part;By kidney bean powder and
Water is with solid-liquid ratio 1:15 (g/mL) mix, use molar concentration 1mol/L sodium hydrate aqueous solution adjust mixed liquor pH for
10, it is extracted 2 hours in 50 DEG C, obtains extracting solution;Extracting solution is cooled to 30 DEG C, 15 points are centrifuged with 4000 revs/min of rotating speed
Clock collects supernatant;It for the salt acid for adjusting pH of 1mol/L is 4 that supernatant, which is used molar concentration, stands 30 minutes, and it is solid to abandon bottom
Body collects clear liquid;By clear liquid vacuum freeze drying, kidney bean albumen is obtained;The process conditions of wherein vacuum freeze drying are:Pre-freeze
- 30 DEG C of temperature, pre-freeze time 2 h, 25 DEG C of sublimation temperature, 40 DEG C, vacuum degree 0.09MPa of resolution temperature, vacuum drying time
16 hours;
S2 is digested:Kidney bean albumen is configured to the solution that mass fraction is 5% with water, after ten minutes in 90 DEG C of processing, is adopted
It is 10 to adjust pH with the sodium hydrate aqueous solution of molar concentration 1mol/L, is heated to 55 DEG C, adds according to the additive amount of 4000u/mL
Entering alkali protease, (alkali protease2709, food-grade, 1,200,000 U/g of enzyme activity believe the limited public affairs of chemical products purchased from Zhengzhou crowd
Department), in 55 DEG C of enzyme digestion reactions 2 hours;In 100 DEG C of enzyme deactivations 10 minutes;Enzyme deactivation liquid is adjusted using the hydrochloric acid of molar concentration 1mol/L
PH be 4.2, centrifuged 20 minutes with 3000 revs/min of rotating speed, collect supernatant;By supernatant vacuum freeze drying, obtain
Kidney bean protein antioxidant peptide;The process conditions of wherein vacuum freeze drying are:- 30 DEG C of pre-freezing temperature, pre-freeze time 2 h rise
25 DEG C of magnificent temperature, 40 DEG C, vacuum degree 0.09MPa of resolution temperature, vacuum drying time 16 hours;
S3 ultrafiltration:Kidney bean protein antioxidant peptide is configured to the ultrafiltration feed liquid that mass fraction is 10% with water, by ultrafiltration material
Liquid is detached using the ultrafiltration membrane of molecular cut off 5000Da, collects permeate;Liquid is will transmit through to continue to use molecular cut off
The ultrafiltration membrane of 3000Da is detached, and permeate is separated into molecular weight between 3000~5000Da and less than 3000Da two
A part;Permeate by molecular weight less than 3000Da continues to be detached with the ultrafiltration membrane of molecular cut off 1000Da, penetrates
Liquid is separated into molecular weight between 1000~3000Da and less than two parts 1000Da;Obtained ultrafiltration component is distinguished
Vacuum freeze drying, obtain molecular weight between 3000~5000Da, between 1000~3000Da and be less than tri- portions 1000Da
Divide kidney bean protein antioxidant peptide.Using the kidney bean protein antioxidant that molecular weight is 3000~5000Da in the embodiment of the present invention
Peptide.
Milk casein anti-oxidation peptide, the embodiment three that referenced patent application number is 201210315545.2 obtain.
It is prepared by persimmon leaf tartaric acid, the embodiment two that referenced patent application number is 201210376846.6.With 5% persimmon leaf tartaric acid
Continuous gavage small white mouse 30 days has no that small white mouse internal organ have acute lesion.It is continuously bathed to small white mouse with 40% persimmon leaf tartaric acid
30 days, 1 time a day, 20 minutes every time, have no mouse skin and paratrichosis.This illustrates the persimmon leaf fruit that the present invention is prepared
Acid is nontoxic.
Embodiment 1
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and pure water, wherein Lowiaceae plant extraction concentrate and
The weight ratio of pure water is 1:5.
The production technology of the intestinal cancer healing liquid is:By Lowiaceae plant extraction concentrate and pure water be uniformly mixed to get
The intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed that obtain mixture spare;
(2) 12g mixtures are taken, are added in the sodium-chloride water solution that 60g mass fractions are 3%, temperature is 35 DEG C, in work(
Ultrasonic extraction 35 minutes under the conditions of rate is 200W, frequency is 40KHz is centrifuged 30 minutes with 4000 revs/min of rotating speed, takes centrifugation
Supernatant liquid afterwards crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
Embodiment 2
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed that obtain mixture spare;
(2) 12g mixtures are taken, are added in the sodium-chloride water solution that 60g mass fractions are 3%, temperature is 35 DEG C, in work(
Ultrasonic extraction 35 minutes under the conditions of rate is 200W, frequency is 40KHz is centrifuged 30 minutes with 4000 revs/min of rotating speed, takes centrifugation
Supernatant liquid afterwards crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 revs/min
Rotating speed stir 60 minutes, stand 3 hours, collect supernatant, be purified liquid;
S3 is by scavenging solution and kidney bean protein antioxidant peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
Embodiment 3
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture;Mixture is freezed 60 minutes at -40 DEG C, then be 500W with power, frequency is
The microwave heating of 2450MHz 10 minutes freezes 30 minutes at -30 DEG C, is then 500W with power, frequency is the micro- of 2450MHz
Wave heating 8 minutes, freezes 20 minutes at -25 DEG C, then with power is 500W, microwave heating that frequency is 2450MHz 5 minutes,
Then it is placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 revs/min
Rotating speed stir 60 minutes, stand 3 hours, collect supernatant, be purified liquid;
S3 is by scavenging solution and kidney bean protein antioxidant peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
Embodiment 4
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of Lowiaceae plant extraction concentrate, includes the following steps:
(1) will 30g banana barks be added 100g boiling water in scald 5 minutes, drain surface moisture, then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture, mixture progress is freezed 30 minutes at -45 DEG C, is then 500W with power, frequency
The microwave heating that rate is 2450MHz 8 minutes, freezes 20 minutes, then be 500W with power, frequency is 2450MHz's at -35 DEG C
Microwave heating 5 minutes freezes 10 minutes at -20 DEG C, is then divided with the microwave heating 3 that power is 500W, frequency is 2450MHz
Then clock is placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 revs/min
Rotating speed stir 60 minutes, stand 3 hours, collect supernatant, be purified liquid;
S3 is by scavenging solution and kidney bean protein antioxidant peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
Embodiment 5
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of Lowiaceae plant extraction concentrate, includes the following steps:
(1) will 30g banana barks be added 100g boiling water in scald 5 minutes, drain surface moisture, then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture, mixture progress is freezed 90 minutes at -40 DEG C, is then 500W with power, frequency
The microwave heating that rate is 2450MHz 25 minutes, freezes 60 minutes at -30 DEG C, is then 500W with power, frequency 2450MHz
Microwave heating 15 minutes, freezed at -25 DEG C 40 minutes, then with the microwave heating 5 that power is 500W, frequency is 2450MHz
Minute, it is then placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 revs/min
Rotating speed stir 60 minutes, stand 3 hours, collect supernatant, be purified liquid;
S3 is by scavenging solution and kidney bean protein antioxidant peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
Embodiment 6
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture;Mixture is freezed 60 minutes at -40 DEG C, then be 500W with power, frequency is
The microwave heating of 2450MHz 10 minutes freezes 30 minutes at -30 DEG C, is then 500W with power, frequency is the micro- of 2450MHz
Wave heating 8 minutes, freezes 20 minutes at -25 DEG C, then with power is 500W, microwave heating that frequency is 2450MHz 5 minutes,
Then it is placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The modified activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 turns/
The rotating speed of minute stirs 60 minutes, stands 3 hours, collects supernatant, is purified liquid;
S3 is by scavenging solution and kidney bean protein antioxidant peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
The preparation process of the modified activated carbon is:Activated carbon is washed with water, the mass ratio of activated carbon and slurry
It is 1:100, the impurity on surface is removed, it is 50 minutes dry in 110 DEG C;Dry activated carbon, which is immersed in molar concentration, is
In the persimmon leaf tartaric acid aqueous solution of 0.4mol/L, the solid-liquid ratio of activated carbon and persimmon leaf tartaric acid aqueous solution is 1:3 (g/mL), mixing are equal
It is even, obtain mixed liquor;By mixed liquor after 60 DEG C are heated 10 hours, 3 hours are stood in 25 DEG C, takes bottom solid;Bottom is consolidated
Body is 20 hours dry in 30 DEG C, obtains the modified activated carbon.
Embodiment 7
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture;Mixture is freezed 60 minutes at -40 DEG C, then be 500W with power, frequency is
The microwave heating of 2450MHz 10 minutes freezes 30 minutes at -30 DEG C, is then 500W with power, frequency is the micro- of 2450MHz
Wave heating 8 minutes, freezes 20 minutes at -25 DEG C, then with power is 500W, microwave heating that frequency is 2450MHz 5 minutes,
Then it is placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The modified activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 turns/
The rotating speed of minute stirs 60 minutes, stands 3 hours, collects supernatant, is purified liquid;
S3 is by scavenging solution and kidney bean protein antioxidant peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
The preparation process of the modified activated carbon is:Activated carbon is washed with water, the mass ratio of activated carbon and slurry
It is 1:100, the impurity on surface is removed, it is 50 minutes dry in 110 DEG C;By dry activated carbon and persimmon leaf tartaric acid with mass ratio 1:
0.3 is uniformly mixed, and obtains mixture;By mixture after 60 DEG C are heated 10 hours, 3 hours are stood in 25 DEG C, obtains described change
Property activated carbon.
Embodiment 8
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture;Mixture is freezed 60 minutes at -40 DEG C, then be 500W with power, frequency is
The microwave heating of 2450MHz 10 minutes freezes 30 minutes at -30 DEG C, is then 500W with power, frequency is the micro- of 2450MHz
Wave heating 8 minutes, freezes 20 minutes at -25 DEG C, then with power is 500W, microwave heating that frequency is 2450MHz 5 minutes,
Then it is placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The modified activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 turns/
The rotating speed of minute stirs 60 minutes, stands 3 hours, collects supernatant, is purified liquid;
S3 is by scavenging solution and milk casein anti-oxidation peptide with 1:0.007 is uniformly mixed, and obtains the active ionic water.
The preparation process of the modified activated carbon is:Activated carbon is washed with water, the mass ratio of activated carbon and slurry
It is 1:100, the impurity on surface is removed, it is 50 minutes dry in 110 DEG C;Dry activated carbon, which is immersed in molar concentration, is
In the persimmon leaf tartaric acid aqueous solution of 0.4mol/L, the solid-liquid ratio of activated carbon and persimmon leaf tartaric acid aqueous solution is 1:3 (g/mL), mixing are equal
It is even, obtain mixed liquor;By mixed liquor after 60 DEG C are heated 10 hours, 3 hours are stood in 25 DEG C, takes bottom solid;Bottom is consolidated
Body is 20 hours dry in 30 DEG C, obtains the modified activated carbon.
Embodiment 9
Intestinal cancer healing liquid is made of Lowiaceae plant extraction concentrate and active ionic water, and wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and active ionic water is 1:5.
The production technology of the intestinal cancer healing liquid is:Lowiaceae plant extraction concentrate and active ionic water are uniformly mixed,
Up to the intestinal cancer healing liquid.
The production technology of the Lowiaceae plant extraction concentrate, includes the following steps:
(1) 30g banana barks are added in 100g boiling water and are scalded 5 minutes, drain surface moisture;Then by 20g bananas bark,
25g Banana trees stem, 10g bananas leaf are 8 hours dry at 50 DEG C, after banana bark, Banana tree stem, banana leaf are crushed respectively
20 mesh sieve is crossed, is uniformly mixed and obtains mixture;Mixture is freezed 60 minutes at -40 DEG C, then be 500W with power, frequency is
The microwave heating of 2450MHz 10 minutes freezes 30 minutes at -30 DEG C, is then 500W with power, frequency is the micro- of 2450MHz
Wave heating 8 minutes, freezes 20 minutes at -25 DEG C, then with power is 500W, microwave heating that frequency is 2450MHz 5 minutes,
Then it is placed 40 minutes in 30 DEG C of insulating box, obtains pretreated mixture;
(2) the pretreated mixtures of 12g are taken, the aqueous sodium chloride that 60g mass fractions are 3%, temperature is 35 DEG C is added to
In liquid, ultrasonic extraction 35 minutes under the conditions of power is 200W, frequency is 40KHz centrifuge 30 points with 4000 revs/min of rotating speed
Clock takes the supernatant liquid after centrifugation, crosses 200 mesh sieve, retains filtrate to get Lowiaceae plant extraction concentrate.
The preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42KV, operating current 30mA, working gas are 98% argon gas and 2%
The mixed gas of oxygen, gas flow 6mL/ minutes;
The modified activated carbon of corona treatment liquid weight 0.2% is added into corona treatment liquid by S2, with 180 turns/
The rotating speed of minute stirs 60 minutes, stands 3 hours, collects supernatant, is purified liquid;
S3 is by scavenging solution, kidney bean protein antioxidant peptide and milk casein anti-oxidation peptide with 1:0.005:0.002 is uniformly mixed,
Obtain the active ionic water.
The preparation process of the modified activated carbon is:Activated carbon is washed with water, the mass ratio of activated carbon and slurry
It is 1:100, the impurity on surface is removed, it is 50 minutes dry in 110 DEG C;Dry activated carbon, which is immersed in molar concentration, is
In the persimmon leaf tartaric acid aqueous solution of 0.4mol/L, the solid-liquid ratio of activated carbon and persimmon leaf tartaric acid aqueous solution is 1:3 (g/mL), mixing are equal
It is even, obtain mixed liquor;By mixed liquor after 60 DEG C are heated 10 hours, 3 hours are stood in 25 DEG C, takes bottom solid;Bottom is consolidated
Body is 20 hours dry in 30 DEG C, obtains the modified activated carbon.
Test case 1
The wound repairing effect of the intestinal cancer healing liquid of embodiment 1-9 is tested.Specific testing procedure is as follows:
(1) animal model is established:Using wistar rats, weight 190-220g, half male and half female, back preserved skin, away from backbone
3, the symmetrical wound mouth of cutting diameter 2cm at the 3.0cm of both sides, depth is from skin to muscle layer, and the thickness of wound is 0.3cm, with life
Normal saline washing wound is managed, it is spare.Per 50 wistar rats of group selection as research object.
(2) in wound model, blank group is covered with vaseline hospital gauze, treated wound sterile gauze packet
It pricks;Test group with intestinal cancer healing liquid film of the present invention in wound surface, the next day dressing.
(3) evaluation method:Observation rats in test groups occur secretion, wound hypohydrops, the edge necrosis of wound skin situation,
There is the ratio shared by the rat of the above situation in statistics.Meanwhile the 6th day at once after wound, wound area, every group of wound area are measured
It is averaged.
Specific test result is shown in Table 1.Statistical analysis is carried out after each group, the results showed that P < 0.05, difference have system
Meter learns meaning.
Table 1:Curative effect test result table
As it can be seen from table 1 intestinal cancer healing liquid of the present invention has the effect of promoting Wound healing and repairs skin.With
Examples 1 to 2 directly to banana skin, cauline leaf spend it is dry after direct extraction phase ratio, embodiment 3-5 is to banana skin, stem, leaf, Hua Jin
Row freezing repeatedly, microwave heating treatment, improve the percentage of damage of cell, improve the leaching rate of cell inclusion, effect of extracting carries
Height, anti-oxidant, antimicrobial component can be extracted preferably in extract liquor.Conditions of the embodiment 3-5 to freezing, microwave heating treatment
It optimizes, the treatment conditions of embodiment 3 have superior technique effect.
Test case 2
Antioxidant effect test to the intestinal cancer healing liquid of embodiment 1-9, using assay NBT photoreduction, to the present invention
The intestinal cancer healing liquid tests the scavenging effect of ultra-oxygen anion free radical.Specific testing procedure is as follows:Draw intestinal cancer
What the Tris-HCL buffer solutions (pH 8.2) and 0.3mL of healing liquid 1mL, addition 4.5mL, 0.1mol/L preheated under the conditions of 25 DEG C
5mmol/L pyrogallol solution keeps the temperature 5 minutes after mixing under the conditions of 25 DEG C, adds the HCl solution 1mL of 10mol/L to terminate anti-
It answers, light absorption value is measured at 320nm wavelength, be denoted as Ai, blank control replaces intestinal cancer healing liquid with the water of same volume, is denoted as A0,
Every group of experiment is repeated 3 times, and is averaged.Clearance rate calculation formula:Clearance rate (%)=[(Ai-A0)/A0] × 100%.
Specific test result is shown in Table 2.
Table 2:Anti-oxidant test result table
Test case 3
The healthcare function of the intestinal cancer healing liquid of embodiment 9 of the present invention is tested.
20~30 years old beauty and health care persons respectively take 3 milliliters of intestinal cancer healing liquid of the present invention sooner or later daily, take 2 months
Afterwards, skin is obviously improved, full of vitality.
40~60 years old beauty and health care persons respectively take 3 milliliters of intestinal cancer healing liquid of the present invention sooner or later daily, take 6-8
After month, a large amount of collagens are supplemented, and skin becomes high resilience.
Test case 4
The treatment intestinal cancer effect of embodiment 1-9 intestinal cancer healing liquids is tested.
Colorectal cancer cell strain is suspended in PBS solution, preparing becomes 1 × 107The solution of/mL, then according to
The capacity of 0.1mL is transplanted to the right side of the BALB/c female mices (SPF grades, Guangzhou province medical experiment animal center provides) of 8 week old
Rib abdomen subcutaneous part.Reach about 100mm from gross tumor volume3When, continuous gavage intestinal cancer healing liquid of the present invention 4 weeks, given low
For 0.1mL/kg.After last time gastric infusion, next day weighs, and cuts open tumor after execution animal and weighs.
Every group of 20 animals of experimental group and control group.The physiological saline of control group gavage equivalent.
Tumor control rate is calculated according to the following formula:Tumor control rate=(control group average tumor weight-experimental group is average
Tumor weight)/control group average tumor weight × 100%.
Specific test result is shown in Table 3.Statistical analysis is carried out after each group, the results showed that P < 0.05, difference have system
Meter learns meaning.
Table 3:Treat intestinal cancer measure of merit result table
The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be in the protection domain being defined in the patent claims.
Claims (10)
1. intestinal cancer healing liquid, which is characterized in that be made of Lowiaceae plant extraction concentrate and water, wherein Lowiaceae plant extraction concentrates
The weight ratio of liquid and water is 1:(5-20).
2. intestinal cancer healing liquid according to claim 1, which is characterized in that the water is active ionic water.
3. intestinal cancer healing liquid according to claim 1, which is characterized in that the Lowiaceae plant extraction concentrate passes through following
Preparation method obtains:
(1) 30-50g banana barks are added in 60-200g boiling water and are scalded 3-8 minutes, drain surface moisture, then by 20-40g perfume
Any of several broadleaf plants bark, 25-50g Banana trees stem, 10-20g bananas leaf are 6-12 hours dry at 40-60 DEG C, by banana bark, Banana tree
Stem, banana leaf smash it through 20-50 mesh sieve respectively, are uniformly mixed that obtain mixture spare;
(2) 12-36g mixtures are taken, the aqueous sodium chloride that 40-80g mass fractions are 3-10%, temperature is 35-55 DEG C is added to
In liquid, ultrasonic extraction 35-65 minutes under the conditions of power is 200-800W, frequency is 40-50KHz, with 4000-10000 revs/min
The rotating speed of clock centrifuges 20-60 minutes, takes the supernatant liquid after centrifugation, crosses 100-500 mesh sieve, retains filtrate to get Lowiaceae plant
Extract concentrate.
4. intestinal cancer healing liquid according to claim 1, which is characterized in that the Lowiaceae plant extraction concentrate passes through following
Preparation method obtains:
(1) 30-50g banana barks are added in 60-200g boiling water and are scalded 3-8 minutes, drain surface moisture, then by 20-40g perfume
Any of several broadleaf plants bark, 25-50g Banana trees stem, 10-20g bananas leaf are 6-12 hours dry at 40-60 DEG C, by banana bark, Banana tree
Stem, banana leaf smash it through 20-50 mesh sieve respectively, are uniformly mixed and obtain mixture, mixture is freezed at -45~-40 DEG C
30-90 minutes, then with power is 300-500W, microwave heating that frequency is 2450-3000MHz 5-25 minutes, -35~-
30 DEG C freeze 20-60 minutes, then with power is 300-500W, microwave heating that frequency is 2450-3000MHz 5-20 minutes,
It is freezed at -25~-20 DEG C 10-40 minutes, then with the microwave heating 3- that power is 300-500W, frequency is 2450-3000MHz
It 15 minutes, is then placed 30-90 minutes in 30-60 DEG C of insulating box, obtains pretreated mixture;
(2) 12-36g mixtures are taken, the aqueous sodium chloride that 40-80g mass fractions are 3-10%, temperature is 35-55 DEG C is added to
In liquid, ultrasonic extraction 35-65 minutes under the conditions of power is 200-800W, frequency is 40-50KHz, with 4000-10000 revs/min
The rotating speed of clock centrifuges 20-60 minutes, takes the supernatant liquid after centrifugation, crosses 100-500 mesh sieve, retains filtrate to get Lowiaceae plant
Extract concentrate.
5. intestinal cancer healing liquid according to claim 2, which is characterized in that the preparation method of the active ionic water is:
The nozzle of excitation device is immersed in the water by S1, is handled 20-30 minutes, is obtained corona treatment liquid;Deng from
The operating condition of daughter excitation apparatus is:Operating voltage 0.42-0.6KV, operating current 10-30mA, working gas are 98% argon
The mixed gas of gas and 2% oxygen, gas flow 5-8mL/ minutes;
The activated carbon or modified active of corona treatment liquid weight 0.2%-0.3% is added into corona treatment liquid by S2
Charcoal after being stirred 40-60 minutes with 180-250 revs/min of rotating speed, is stood 2-3 hours, collects supernatant, be purified liquid;
S3 is by scavenging solution and anti-oxidation peptide with 1:(0.005-0.01) is uniformly mixed, and obtains the active ionic water.
6. intestinal cancer healing liquid according to claim 5, which is characterized in that the preparation process of the modified activated carbon is:It will
Activated carbon is washed with water, and the mass ratio of activated carbon and slurry is 1:(50-100) removes the impurity on surface, in 110-120
DEG C dry 50-80 minutes;Dry activated carbon is immersed in the tartaric acid aqueous solution that molar concentration is 0.1-0.6mol/L, activity
The solid-liquid ratio of charcoal and tartaric acid aqueous solution is 1:(2-3) (g/mL) is uniformly mixed, obtains mixed liquor;Mixed liquor is added in 40-60 DEG C
After 8-12 hours hot, 2-3 hours are stood in 20-25 DEG C, takes bottom solid;Bottom solid is small in 30-40 DEG C of dry 12-20
When, obtain the modified activated carbon.
7. intestinal cancer healing liquid according to claim 5, which is characterized in that the preparation process of the modified activated carbon is:It will
Activated carbon is washed with water, and the mass ratio of activated carbon and slurry is 1:(50-100) removes the impurity on surface, in 110-120
DEG C dry 50-80 minutes;By dry activated carbon and tartaric acid with mass ratio 1:(0.2-0.3) is uniformly mixed, and obtains mixture;It will
Mixture stands 2-3 hours after 40-60 DEG C is heated 8-12 hours, in 20-25 DEG C, obtains the modified activated carbon.
8. the intestinal cancer healing liquid described according to claim 6 or 7, which is characterized in that the tartaric acid is malic acid, citric acid, persimmon
It is one or more in leaf fruit acid, oleanolic acid, ursolic acid, olive tartaric acid.
9. intestinal cancer healing liquid according to claim 5, which is characterized in that the anti-oxidation peptide is kidney bean protein antioxidant peptide
And/or milk casein anti-oxidation peptide.
10. the production technology of intestinal cancer healing liquid according to claim 1, which is characterized in that concentrate Lowiaceae plant extraction
Liquid and water are uniformly mixed to get the intestinal cancer healing liquid.
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CN109700900A (en) * | 2019-03-14 | 2019-05-03 | 北京康芬中医药研究院 | Health composition of the plant extraction liquid containing Lowiaceae and preparation method thereof |
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Address after: 530031 No. 8, East Branch Road, Guokai Avenue, Nanning City, Guangxi Zhuang Autonomous Region Applicant after: GUANGXI TIANYUANLV BIOTECHNOLOGY Co.,Ltd. Address before: 6-7 Floor, Phase I Office Building, No. 9 Jingxiu Software Park, Binhe Road, Nanning High-tech Zone, Guangxi Zhuang Autonomous Region, 530000 Applicant before: GUANGXI YUYANG LVZHOU BIOLOGICAL TECHNOLOGY CO.,LTD. |
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Application publication date: 20180928 |
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WW01 | Invention patent application withdrawn after publication |