CN108576820A - A kind of algae oil DHA composite particles and preparation method thereof - Google Patents
A kind of algae oil DHA composite particles and preparation method thereof Download PDFInfo
- Publication number
- CN108576820A CN108576820A CN201810279991.XA CN201810279991A CN108576820A CN 108576820 A CN108576820 A CN 108576820A CN 201810279991 A CN201810279991 A CN 201810279991A CN 108576820 A CN108576820 A CN 108576820A
- Authority
- CN
- China
- Prior art keywords
- algae oil
- oil dha
- composite particles
- dha
- lecithin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000195493 Cryptophyta Species 0.000 title claims abstract description 46
- 239000011246 composite particle Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims description 13
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims abstract description 19
- 239000008101 lactose Substances 0.000 claims abstract description 19
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims abstract description 12
- 239000000787 lecithin Substances 0.000 claims abstract description 12
- 229940067606 lecithin Drugs 0.000 claims abstract description 12
- 235000010445 lecithin Nutrition 0.000 claims abstract description 12
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims abstract description 7
- 235000008452 baby food Nutrition 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- 239000006210 lotion Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 7
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 6
- 229940083466 soybean lecithin Drugs 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims 1
- 239000003595 mist Substances 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 8
- 239000004615 ingredient Substances 0.000 abstract description 3
- 230000003647 oxidation Effects 0.000 abstract description 3
- 238000007254 oxidation reaction Methods 0.000 abstract description 3
- 230000006866 deterioration Effects 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 30
- JQWAHKMIYCERGA-UHFFFAOYSA-N (2-nonanoyloxy-3-octadeca-9,12-dienoyloxypropoxy)-[2-(trimethylazaniumyl)ethyl]phosphinate Chemical compound CCCCCCCCC(=O)OC(COP([O-])(=O)CC[N+](C)(C)C)COC(=O)CCCCCCCC=CCC=CCCCCC JQWAHKMIYCERGA-UHFFFAOYSA-N 0.000 description 7
- 239000000839 emulsion Substances 0.000 description 5
- 238000004108 freeze drying Methods 0.000 description 5
- 210000004556 brain Anatomy 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000035790 physiological processes and functions Effects 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 230000019240 optic nerve development Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001507 sample dispersion Methods 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
- A23L33/12—Fatty acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Molecular Biology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of algae oil DHA composite particles, are 1~3 it includes weight ratio:0.2~0.4:10 oligomeric lactose, lecithin, algae oil DHA, algae oil DHA composite particles disclosed in this invention, ingredient is simple, it forms oligomeric lactose and lecithin is commonly applied to infant food, only accounting for smaller proportion and need not add other materials can be with good stability, long-term at room temperature to store not oxidation deterioration.
Description
Technical field
The present invention relates to a kind of algae oil DHA composite particles and preparation method thereof.
Background technology
Algae oil DHA is the DHA extracted from microalgae, there is brain tonic and intelligence development, promote optic nerve development, anticancer, anti-aging etc.
A variety of important physiological functions.DHA can ensure that infantile health is developed, and promote developing infant brain, usually be applied to baby children
In youngster's food or health products.But there are many problems, such as double bond of DHA easily to be aoxidized by the oxygen in air for DHA directly applications,
It is exposed to high temperature for a long time, it is oxidizable rotten in damp and hot environment, it is serious to produce to influence the physiological function of DHA
Raw negative effect.
Currently, mainly taking the measures such as microcapsules and/or addition antioxidant for preventing Oxidation of Fat and Oils, such as
The patents such as CN201310536076.1, CN201611259563.8 improve algae oil by preparing the algae oil DHA of microencapsulation
The stability of DHA, but all there is the problems such as wall material constituent is complicated, and accounting is high, infant food is applied to for algae oil DHA
Or there are certain adverse effects for health products.
Invention content
The technical problem to be solved in the present invention is to provide a kind of ingredients simply, adds less, the algae oil that algae oil DHA content is high
DHA composite particles.
In order to solve the above technical problems, the invention discloses a kind of algae oil DHA composite particles, the composite particles include weight
Amount is than being 1~3:0.2~0.4:10 oligomeric lactose, lecithin, algae oil DHA.
The lecithin is preferably soybean lecithin or egg yolk lecithin；The weight of oligomeric lactose, lecithin, algae oil DHA
Than being preferably 2:0.3:10.
Algae oil DHA composite particles disclosed in this invention can be made by the steps：A) oligomeric lactose is placed in water, molten
Solve clear aqueous solution；B) lecithin is added in step a) aqueous solutions, algae oil DHA is added after mixing, homogeneous obtains lotion；C) lotion
It is dry to get.
The temperature of water is 50~70 DEG C in preferred steps a)；When algae oil DHA being added in step b) solution temperature be down to 25~
35℃；Step c) is using spray drying or freeze-drying；All steps preferably carry out under the conditions of nitrogen charging.
Algae oil DHA composite particles disclosed in this invention are suitable for infant food and health products.
Algae oil DHA composite particles disclosed in this invention, ingredient is simple, forms oligomeric lactose and lecithin is often applied
In infant food, only accounting for smaller proportion and need not add other materials can be with good stability, grows at room temperature
Phase stores not oxidation deterioration.
Specific implementation mode
The above of the present invention is described in further detail again below by way of specific embodiment.But this should not be managed
Solution is limited only to embodiment below for the range of the above-mentioned theme of the present invention.The case where not departing from above-mentioned technological thought of the invention
Under, the various replacements or change made according to ordinary skill knowledge and customary means should all be included in the model of the present invention
In enclosing.
Embodiment 1
Prescription：
| Material forms | Prescription matches (g) |
| Algae oil DHA | 10.0 |
| Oligomeric lactose | 2.0 |
| Egg yolk lecithin | 10.0 |
Preparation method：
1) oligomeric lactose is placed in 60 DEG C of water, dissolves to obtain clear aqueous solution；
2) egg yolk lecithin is added in step 1) aqueous solution, algae oil DHA is added to 30 DEG C in mixing postcooling, high-pressure homogeneous
Obtain lotion；
3) emulsion spray drying (180 DEG C of inlet air temperature, 80 DEG C of leaving air temp) to get.
Embodiment 2
Prescription：
| Material forms | Prescription matches (g) |
| Algae oil DHA | 10.0 |
| Oligomeric lactose | 4.0 |
| Egg yolk lecithin | 30.0 |
Preparation method：
1) oligomeric lactose is placed in 50 DEG C of water, dissolves to obtain clear aqueous solution；
2) egg yolk lecithin is added in step 1) aqueous solution, algae oil DHA is added to 25 DEG C in mixing postcooling, high-pressure homogeneous
Obtain lotion；
3) emulsion freeze drying to get.
Embodiment 3
Prescription：
| Material forms | Prescription matches (g) |
| Algae oil DHA | 10.0 |
| Oligomeric lactose | 2.0 |
| Soybean lecithin | 30.0 |
Preparation method：(under the conditions of nitrogen charging)
1) oligomeric lactose is placed in 70 DEG C of water, dissolves to obtain clear aqueous solution；
2) soybean lecithin is added in step 1) aqueous solution, algae oil DHA is added to 35 DEG C in mixing postcooling, high-pressure homogeneous
Obtain lotion；
3) emulsion freeze drying to get.
Embodiment 4
Prescription：
| Material forms | Prescription matches (g) |
| Algae oil DHA | 10.0 |
| Oligomeric lactose | 3.0 |
| Soybean lecithin | 20.0 |
Preparation method：(under the conditions of nitrogen charging)
1) oligomeric lactose is placed in 70 DEG C of water, dissolves to obtain clear aqueous solution；
2) soybean lecithin is added in step 1) aqueous solution, algae oil DHA is added to 35 DEG C in mixing postcooling, high-pressure homogeneous
Obtain lotion；
3) emulsion freeze drying to get.
Embodiment 5
Prescription：
| Material forms | Prescription matches (g) |
| Algae oil DHA | 10.0 |
| Oligomeric lactose | 3.0 |
| Egg yolk lecithin | 20.0 |
Preparation method：(under the conditions of nitrogen charging)
1) oligomeric lactose is placed in 70 DEG C of water, dissolves to obtain clear aqueous solution；
2) egg yolk lecithin is added in step 1) aqueous solution, algae oil DHA is added to 25 DEG C in mixing postcooling, high-pressure homogeneous
Obtain lotion；
3) emulsion freeze drying to get.
The experimental test result of algae oil DHA composite particles prepared by above example of the present invention is as follows：
1) the obtained algae oil DHA composite particles of above example are white powder, and electron microscope scanning result is shown
Each embodiment sample dispersion is uniform, and primitive is the microballoon of about 10~20 microns of diameter.
2) the algae oil DHA composite particles prepared by embodiment are placed under the conditions of 25 DEG C of 60%RH and investigate its stability, real
The stability for applying example 1~5 is all preferable, can store for a long time to 24 months.Concrete outcome see the table below 1：
Table 1
Claims (9)
1. a kind of algae oil DHA composite particles, it is characterised in that：The composite particles include that weight ratio is 1~3:0.2~0.4:10
Oligomeric lactose, lecithin, algae oil DHA.
2. algae oil DHA composite particles as described in claim 1, it is characterised in that：The lecithin is soybean lecithin or egg
Yellow lecithin.
3. algae oil DHA composite particles as described in claim 1, it is characterised in that：The oligomeric lactose, lecithin, algae oil DHA
Weight ratio be 2：0.3：10.
4. the preparation method of algae oil DHA composite particles as described in claim 1, it is characterised in that：It comprises the following steps：
A) oligomeric lactose is placed in water, and dissolves to obtain clear aqueous solution；
B) lecithin is added in step a) aqueous solutions, algae oil DHA is added after mixing, homogeneous obtains lotion；
C) lotion drying to get.
5. the preparation method of algae oil DHA composite particles as claimed in claim 4, it is characterised in that：Water in the step a)
Temperature is 50~70 DEG C.
6. the preparation method of algae oil DHA composite particles as claimed in claim 5, it is characterised in that：It is added in the step b)
Solution temperature is down to 25~35 DEG C when algae oil DHA.
7. the preparation method of algae oil DHA composite particles as claimed in claim 4, it is characterised in that：The step c) is using spray
Mist is dry or is freeze-dried.
8. the preparation method of algae oil DHA composite particles as claimed in claim 4, it is characterised in that：The step is in nitrogen charging item
It is carried out under part.
9. application of the algae oil DHA composite particles as described in claim 1 in infant food and health products.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810279991.XA CN108576820A (en) | 2018-03-30 | 2018-03-30 | A kind of algae oil DHA composite particles and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810279991.XA CN108576820A (en) | 2018-03-30 | 2018-03-30 | A kind of algae oil DHA composite particles and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108576820A true CN108576820A (en) | 2018-09-28 |
Family
ID=63624103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810279991.XA Pending CN108576820A (en) | 2018-03-30 | 2018-03-30 | A kind of algae oil DHA composite particles and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108576820A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023067056A1 (en) | 2021-10-21 | 2023-04-27 | Frieslandcampina Nederland B.V. | Powdered compositions containing an edible oil and their use in food products |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101971984A (en) * | 2010-09-06 | 2011-02-16 | 南昌大学 | Preparation method of DHA microemulsion |
| CN105748416A (en) * | 2016-04-15 | 2016-07-13 | 国家海洋局第三海洋研究所 | DHA (docosahexaenoic acid) nanoemulsion freeze-dried powder and preparation method thereof |
| CN105832666A (en) * | 2016-04-15 | 2016-08-10 | 国家海洋局第三海洋研究所 | Preparation method for DHA algae oil nanoemulsion |
| CN105901712A (en) * | 2016-04-26 | 2016-08-31 | 广西三椿生物科技有限公司 | Microemulsion for preventing constipation of diabetics and preparation method thereof |
| CN104719913B (en) * | 2015-03-09 | 2017-04-05 | 李宏 | A kind of algae oil DHA nanosuspension and its preparation method and application |
-
2018
- 2018-03-30 CN CN201810279991.XA patent/CN108576820A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101971984A (en) * | 2010-09-06 | 2011-02-16 | 南昌大学 | Preparation method of DHA microemulsion |
| CN104719913B (en) * | 2015-03-09 | 2017-04-05 | 李宏 | A kind of algae oil DHA nanosuspension and its preparation method and application |
| CN105748416A (en) * | 2016-04-15 | 2016-07-13 | 国家海洋局第三海洋研究所 | DHA (docosahexaenoic acid) nanoemulsion freeze-dried powder and preparation method thereof |
| CN105832666A (en) * | 2016-04-15 | 2016-08-10 | 国家海洋局第三海洋研究所 | Preparation method for DHA algae oil nanoemulsion |
| CN105901712A (en) * | 2016-04-26 | 2016-08-31 | 广西三椿生物科技有限公司 | Microemulsion for preventing constipation of diabetics and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023067056A1 (en) | 2021-10-21 | 2023-04-27 | Frieslandcampina Nederland B.V. | Powdered compositions containing an edible oil and their use in food products |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104206561A (en) | Preparation process of peony seed oil micro-capsule powder | |
| CN102427740B (en) | The microencapsulation of bioactivator and manufacture method thereof | |
| CN103948035A (en) | Peony seed oil microcapsules as well as preparation method and application thereof | |
| CN107518094A (en) | The preparation method and camellia seed oil capsule powders of a kind of camellia seed oil microscapsule powder | |
| WO2020233101A1 (en) | Colorful-jelly 4d printing method utilizing spontaneous color change of blueberry anthocyanins | |
| CN107550764A (en) | A kind of preparation method of the oil and fat of sacha inchi water profit Q hoodles of high stability | |
| CN111387291A (en) | Method for producing grease microcapsule by low-temperature electrostatic spray drying | |
| CN105124604A (en) | High-dispersion phytosterol ester microcapsule, as well as preparation method and application thereof | |
| CN102170790B (en) | Process for producing protein microparticles | |
| CN108142950A (en) | A kind of acer truncatum seed oil composite Nano microcapsule powder for improving brain neuroblastoma and preparation method thereof | |
| CN109380700A (en) | A kind of galic essential oil microcapsules and preparation method thereof | |
| CN114271499A (en) | Microcapsule powder with high embedding rate and preparation method thereof | |
| CN109953336A (en) | A kind of high instant microcapsule powder of carrying capacity polymethoxyflavone and preparation method thereof | |
| CN108576820A (en) | A kind of algae oil DHA composite particles and preparation method thereof | |
| CN105685933B (en) | egg milk paste essence and preparation method thereof | |
| Tolve et al. | Current advantages in the application of microencapsulation in functional bread development | |
| Panghal et al. | Microencapsulation for delivery of probiotic bacteria | |
| CN105852131B (en) | Method for preparing fish oil microcapsule meeting organic food processing standard | |
| CN105995978A (en) | Perilla oil composition and perilla oil microcapsule powder and preparation method thereof | |
| CN105326021B (en) | A kind of preparation process improving desugar egg-white powder emulsibility and emulsion stability | |
| CN106306114A (en) | Coixseed bran oil microcapsule and preparation method thereof | |
| CN101390588B (en) | Grease microcapsule prepared by high-pressure homogeneous modification rice starch and method thereof | |
| IT9021668A1 (en) | FOOD BASED ON FAT OILS CONTAINING CHLORELLA AND PROCEDURE TO PRODUCE IT | |
| CN109288030A (en) | A kind of plural gel fat substitute and low fat Egg Tarts fillings prepared therefrom | |
| CN105211883A (en) | A kind of food-grade Co-Q10 microcapsules and its preparation method and application |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180928 |
|
| RJ01 | Rejection of invention patent application after publication |