CN108567669A - Anti-oxidant reparation facial mask of one kind and preparation method thereof - Google Patents
Anti-oxidant reparation facial mask of one kind and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/9783—Angiosperms [Magnoliophyta]
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Abstract
The present invention relates to a kind of anti-oxidant reparation facial masks and preparation method thereof, belong to cosmetic technical field.The present invention utilizes the Efficient antibacterial performance of oxidized sodium alginate, achieve the purpose that killing bacteria, suitable environment is supplied for neonatal cell, promote new collagen elastin laminin to generate with collagen, conducive to cell growth, reach the reparation of inflammatory aged skin, layer protecting film is formed in cell surface, reduce skin surface moisture evaporation, moisture is enabled to be freely spread to cuticula, to the function of effectively skin-moisturizing, skin and protection cell membrane, layer protecting film is formed in extracellular matrix, reduce the evaporation of skin surface moisture, the effect of to realize skin-moisturizing, skin, when intensive ultraviolet, special protective film is formed in cell surface, it avoids tanning severely, reduce melanin deposition, it is effectively pre- anti-aging, alleviate the local inflammation reaction of therapy of facial hormone dependent dermatitis, it is uncomfortable to improve sufferer face, sufferer skin of face barrier function is set slowly to restore.
Description
Technical field
The present invention relates to a kind of anti-oxidant reparation facial masks and preparation method thereof, belong to cosmetic technical field.
Background technology
Facial mask is a kind of carrier of face beautifying health keeping product, apply at 15~30 minutes on the face, when skin care products nutrient slowly by
After skin absorbs, that is, the film unloaded down, that the material of facial mask has that powder reconciles, kaolin, non-woven fabrics and silk mask, at present
Highest science and technology, carrier are careful, be easy to be inhaled by skin is silk mask, and general active ingredient is 2.5-22% or so.With society
The development of meeting, the raising of quality of life, people especially women are increasingly particular about the beauty and skin care of face, then just generate
Miscellaneous facial mask.Different facial masks can reach different skin effects, there is whitening, moisturizing, pore cleanser etc.
Deng.All kinds of facial masks currently on the market are although varied, but there are with single nutrient component, and effect is not comprehensive and skin absorbs
The factors such as effect difference, it is difficult to play the role of beauty and skin care.And the method complicated difficult prepared causes a large amount of cost to operate
It is lost in.
The problem of skin care has become a knowledge in the modern times, and present people increasingly pay attention to skin care, facial mask is at us
Prodigious effect is also functioned to during skin care.It is well known that the basis of skin care is moisturizing, water shortage is that all skin problems are formed
Root.Temperature change and pressure and skin aging that air-conditioning, environmental pollution, Seasonal conversion are brought, metabolism slow down etc. because
Element can all cause skin moisture loss, enable skin it is coarse, it is dim it is mute, form dry line, cause many skin problems.Permanent water shortage
The immunity degradation of skin itself can gradually lose self-repairing capability.Therefore, it is flesh for each likes to be beautiful Ms
Skin moisturizing so that it constantly carries out itself reparation and is very important for skin care.
Night is that physiological function is restrained oneself the rest period nursed, and what is at this time needed most is exactly to nourish skin, accelerates cell
Metabolism, the damage that maintenance skin is subject to daytime supplements the nutrients, skin is allowed to become more flexible, finer and smoother.Sleep surface
Film is different according to its formula, and the attainable skin effect of institute is just different, such as whitening, moisturizing, anti-aging function.Existing nutrition
Also there are many face mask of traditional Chinese medicine, and various face mask of traditional Chinese medicine Various Functions in facial mask, but these facial masks are added with various chemistry mostly
Drug, although quick, dependence is strong so that skin self-regeneration function is destroyed.
However, the problems such as operating pressure and environmental pollution, often bring prodigious influence.There is investigation to show, has more than one
Half adult lives through the puzzlement of insomnia, and various body ＆ mind diseases can be brought by having a sleepless night, and influence normal life.Pollution
Dry skin, microgroove can be caused to aggravate the problems such as such as air, water source.Computer radiation, ultraviolet light, light pollution etc. can cause human body
Interior free radical is excessive, and free-radical chemistry property is active, can be chemically reacted with carbohydrate, protein, lipid etc. in human body, mistake
More free radicals can cause that energy expenditure is excessive, damage and destruction of cell function, accelerate the process of human senescence.It is existing to sleep
Dormancy facial mask is using moisturizing as primary efficacy mostly, and oxidation resistance is insufficient, and if premised on without good sleep, face
The active ingredient of film cannot then be fully absorbed utilization, and ideal effect is not achieved.
Invention content
The technical problems to be solved by the invention：It is added with various chemicals mostly for existing facial mask, although taking effect
Soon, but dependence is strong so that the problem of skin self-regeneration function is by destroying, provide a kind of anti-oxidant reparation facial mask and
Preparation method.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of anti-oxidant reparation facial mask, the anti-oxidant reparation facial mask includes following weight parts raw material：
2~3 parts of oxidized sodium alginates, 1~2 part of polyvinyl alcohol, 0.3~0.5 part of xanthan gum, 0.2~0.3 part of carboxymethyl cellulose
Sodium, 3~5 parts of glycerine, 0.1~0.2 part of Tween-80,2~3 parts of the concentrated liquid of tradition Chinese medicine.
The oxidized sodium alginate is that ethylene glycol stirring is added with sodium periodate in sodium alginate after being protected from light place's oxidation reaction
Reaction, then be precipitated and precipitated with chlorination sodium ethoxide solution, filter residue is filtered to obtain, alcohol precipitation is precipitated and dries system after filter residue repetition is dissolved
.
Weight of material part in the oxidized sodium alginate preparation process is 5~6 parts of sodium alginates, 200~240 parts go from
Sub- water, 5~6 parts of mass fractions are 5% sodium periodate solution, 1.0~1.2 parts of ethylene glycol, 200~300 parts of 5% chlorinations of mass fraction
Sodium ethoxide solution.
The concentrated liquid of tradition Chinese medicine is to be fitted into flash extracter with glusulase after compound Chinese medicine powder is mixed with deionized water
Extraction, and concentrate and be made through flash inspissator.
In the compound Chinese medicine powder parts by weight of raw materials be 10~20 parts of indocalamus leafs, 6~8 portions of honeysuckles, 4~6 parts of Radix Astragalis, 8
~10 portions of Radix Glycyrrhizaes, 4~5 parts of Radix Salviae Miltiorrhizaes, 8~10 portions of purslanes, 3~5 portions of dandelions.
The compound Chinese medicine powder, deionized water, the parts by weight of glusulase be 20~40 parts of compound Chinese medicine powder, 400~
800 parts of deionized waters, 0.02~0.04 part of glusulase.
The Extracting temperature is 40~60 DEG C.
A kind of anti-oxidant preparation method for repairing facial mask, the specific steps are：
（1）Chinese medicine dry powder and attrition grinding are measured by formula, 60 mesh sieve is crossed, obtains compound Chinese medicine powder；
（2）Compound Chinese medicine powder is disperseed in deionized water and is added glusulase, is uniformly mixed and is placed in flash extracter,
2~3min is extracted at 40~60 DEG C, then is transferred to centrifuge to be placed in flash inspissator in centrifuge and is concentrated into primary liquid
Long-pending 20~30%, obtain the concentrated liquid of tradition Chinese medicine；
（3）It takes sodium alginate to be added in deionized water to stir evenly, it is 5% sodium periodate solution to add mass fraction, and is being kept away
Oxidation reaction 20 at light~ethylene glycol is added afterwards for 24 hours is stirred to react, and obtains mixed liquor；
（4）By mixed liquor be added mass fraction be stood in 5% chlorination sodium ethoxide solution be precipitated after filter to obtain filter cake, by filter cake plus
Enter and precipitated with absolute ethyl alcohol after being dissolved in deionized water, stand and filtered after being precipitated, dry 8~10h, must aoxidize at 30~40 DEG C
Sodium alginate；
（5）Take oxidized sodium alginate, mass fraction be 10% poly-vinyl alcohol solution, xanthan gum, sodium carboxymethylcellulose addition go from
In sub- water, 20~30min is stirred at 80~90 DEG C, and is placed on 20~25min of irradiation under ultraviolet lamp, then uses mass fraction
10~15h of crosslinking, sol solutions are stood at 4~5 DEG C after adjusting pH to 5.0~6.5 for 5% sodium hydroxide solution；
（6）Glycerine, Tween-80, the concentrated liquid of tradition Chinese medicine are added into sol solutions, 30~40min of insulated and stirred, quiet at 70~80 DEG C
It is filtered after setting 10~12h, obtains anti-oxidant reparation facial mask.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention has the disease-resistant micro- life of original by configuring based on clearing heat and detoxicating eliminating dampness, dispelling wind and arresting itching, cool blood nourishing yin effect
Object, inhibition immune response, reduce inflammation damage, treats steroid dependent dermatitis, and clearing heat and promoting diuresis, sterilization detumescence can effectively mitigate
Red and swollen, warts, there is the effect of promoting blood circulation and removing blood stasis, anti-inflammatory analgetic, preferable to telangiectasis, pigmentation effect, can obviously subtract
Light scytitis alleviates hormone withrawal symptom, accelerates the effective component of chinese medicine of skin barrier function reparation, and is supported on oxidation sea
Anti-oxidant reparation facial mask is made in the composite crosslinking gel that mosanom is formed with polyvinyl alcohol, xanthan gum, sodium carboxymethylcellulose,
With good water absorbing properties, high expansion function, flexibility is good, has good biocompatibility and biological degradability；
（2）The present invention utilizes the Efficient antibacterial performance of oxidized sodium alginate, achievees the purpose that killing bacteria, is supplied for neonatal cell
Suitable environment promotees new collagen elastin laminin and is generated with collagen, is conducive to cell growth, reaches repairing for inflammatory aged skin
It is multiple, it can be efficiently entering and play its unique water replacement stress factor effect into the cell, one layer of protection can be formed in cell surface
Film reduces skin surface moisture evaporation, moisture is enabled to be freely spread to cuticula, thus effectively skin-moisturizing, skin and protection cell membrane
Function, form layer protecting film in extracellular matrix, the evaporation of skin surface moisture reduced, to realize the work(of skin-moisturizing, skin
Effect when intensive ultraviolet, forms special protective film in cell surface, avoids tanning severely, and reduces melanin deposition, effective pre- health care
Always, alleviate the local inflammation reaction of therapy of facial hormone dependent dermatitis, improve sufferer face discomfort, make sufferer skin of face barrier work(
Can slowly it restore.
Specific implementation mode
Take 10~20g indocalamus leafs, 6~8g honeysuckles, 4~6g Radix Astragalis, 8~10g Radix Glycyrrhizaes, 4~5g Radix Salviae Miltiorrhizaes, 8~10g dents
Amaranth, 3~5g dandelions, is fitted into pulverizer and crushes, and crosses 60 mesh sieve, obtains compound Chinese medicine powder, take 20~40g compound Chinese medicine powder
End is added in 400~800mL deionized waters, stirs 20~30min with 300~400r/min, adds 0.02~0.04g snails
Ox enzyme is uniformly mixed and is placed in flash extracter, 2~3min is extracted at 40~60 DEG C, then be transferred in centrifuge, with 6000
~8000r/min centrifuge 15~20min, collect supernatant be placed in be concentrated into flash inspissator stoste volume 20~
30%, the concentrated liquid of tradition Chinese medicine is obtained, 5~6g sodium alginates are taken, is added in 200~240mL deionized waters, is stirred with 300~400r/min
10~15min, it is 5% sodium periodate solution to add 5~6g mass fractions, and in the place's of being protected from light oxidation reaction 20~be added afterwards for 24 hours
1.0~1.2g ethylene glycol continues to be stirred to react 10~15min, obtains mixed liquor, and 200~300g mass fractions are added in mixed liquor
For in 5% chlorination sodium ethoxide solution, 20~30min is stirred with 500~600r/min, standing filters to obtain filter cake after 1~2h is precipitated,
Filter cake is added in 200~300mL deionized waters and is stirred to being completely dissolved, absolute ethyl alcohol precipitation is added, stands mistake after being precipitated
Filter residue is filtered to obtain, filter residue is transferred in vacuum drying chamber, dry 8~10h, obtains oxidized sodium alginate, take 2~3g at 30~40 DEG C
Oxidized sodium alginate, 10~20g mass fractions are 10% poly-vinyl alcohol solution, 0.3~0.5g xanthan gums, 0.2~0.3g carboxymethyls
Sodium cellulosate is added in 80~100g deionized waters, stirs 20~30min at 80~90 DEG C with 300~400r/min, and put
20~25min of irradiation under ultraviolet lamp is set, it is that 5% sodium hydroxide solution adjusts pH to 5.0~6.5, then sets that mass fraction, which is used in combination,
10~15h of crosslinking is stood under 4~5 DEG C of waters bath with thermostatic control, 3~5g glycerine is added into sol solutions for sol solutions, and 0.1~0.2g is spat
Temperature -80,2~3g the concentrated liquid of tradition Chinese medicine, 30~40min of insulated and stirred at 70~80 DEG C filter after standing 10~12h, obtain antioxygen
Change and repairs facial mask.
Take 10g indocalamus leafs, 6g honeysuckles, 4g Radix Astragalis, 8g Radix Glycyrrhizaes, 4g Radix Salviae Miltiorrhizaes, 8g purslanes, 3g dandelions, loading pulverizer
Middle crushing crosses 60 mesh sieve, obtains compound Chinese medicine powder, take 20g compound Chinese medicine powder, is added in 400mL deionized waters, with 300r/
Min stirs 20min, adds 0.02g glusulases, is uniformly mixed and is placed in flash extracter, 2min is extracted at 40 DEG C, then
It is transferred in centrifuge, 15min is centrifuged with 6000r/min, collection supernatant, which is placed in flash inspissator, is concentrated into stoste
The 20% of volume, obtains the concentrated liquid of tradition Chinese medicine, takes 5g sodium alginates, is added in 200mL deionized waters, and 10min is stirred with 300r/min,
It is 5% sodium periodate solution to add 5g mass fractions, and 1.0g ethylene glycol is added after being protected from light place oxidation reaction 20h, continues to stir
Reaction 10min is mixed, mixed liquor is obtained, it is in 5% chlorination sodium ethoxide solution, with 500r/min that 200g mass fractions, which are added, in mixed liquor
20min is stirred, stands and filters to obtain filter cake after 1h is precipitated, filter cake is added in 200mL deionized waters and is stirred to being completely dissolved, then is added
Enter absolute ethyl alcohol precipitation, stand and filter to obtain filter residue after being precipitated, filter residue is transferred in vacuum drying chamber, dry 8h, obtains at 30 DEG C
Oxidized sodium alginate, it is 10% poly-vinyl alcohol solution, 0.3g xanthan gums, 0.2g carboxylics to take 2g oxidized sodium alginates, 10g mass fractions
Sodium carboxymethylcellulose pyce is added in 80g deionized waters, stirs 20min at 80 DEG C with 300r/min, and be placed under ultraviolet lamp
20min is irradiated, it is that 5% sodium hydroxide solution adjusts pH to 5.0, then is placed under 4 DEG C of waters bath with thermostatic control and stands crosslinking that mass fraction, which is used in combination,
3g glycerine, 0.1g Tween-80s, 2g the concentrated liquid of tradition Chinese medicine, the insulated and stirred at 70 DEG C are added into sol solutions for 10h, sol solutions
30min filters after standing 10h, obtains anti-oxidant reparation facial mask.
Take 15g indocalamus leafs, 7g honeysuckles, 5g Radix Astragalis, 9g Radix Glycyrrhizaes, 4.5g Radix Salviae Miltiorrhizaes, 9g purslanes, 4g dandelions, loading crushing
It is crushed in machine, crosses 60 mesh sieve, obtain compound Chinese medicine powder, take 30g compound Chinese medicine powder, be added in 600mL deionized waters, with
350r/min stirs 25min, adds 0.03g glusulases, is uniformly mixed and is placed in flash extracter, is extracted at 50 DEG C
2min, then be transferred in centrifuge, 17min is centrifuged with 7000r/min, collection supernatant, which is placed in flash inspissator, to be concentrated
To the 25% of stoste volume, the concentrated liquid of tradition Chinese medicine is obtained, takes 5.5g sodium alginates, is added in 220mL deionized waters, is stirred with 350r/min
13min is mixed, it is 5% sodium periodate solution to add 5.5g mass fractions, and 1.1g second is added after being protected from light place oxidation reaction 22h
Glycol continues to be stirred to react 13min, obtains mixed liquor, by mixed liquor be added 250g mass fractions be 5% chlorination sodium ethoxide solution in,
25min is stirred with 550r/min, stands and filters to obtain filter cake after 1h is precipitated, filter cake is added in 250mL deionized waters and is stirred to complete
Fully dissolved adds absolute ethyl alcohol precipitation, stands and filters to obtain filter residue after being precipitated, filter residue is transferred in vacuum drying chamber, at 35 DEG C
Lower dry 9h, obtains oxidized sodium alginate, and it is 10% poly-vinyl alcohol solution, 0.4g to take 2.5g oxidized sodium alginates, 15g mass fractions
Xanthan gum, 0.25g sodium carboxymethylcelluloses are added in 90g deionized waters, stir 25min at 85 DEG C with 350r/min, and put
It sets and irradiates 23min under ultraviolet lamp, it is that 5% sodium hydroxide solution adjusts pH to 6.0, then is placed in 4 DEG C of constant temperature that mass fraction, which is used in combination,
It is stood under water-bath and is crosslinked 13h, sol solutions, the addition 4g glycerine into sol solutions, 0.15g Tween-80s, 2.5g the concentrated liquid of tradition Chinese medicine,
Insulated and stirred 35min at 75 DEG C filters after standing 11h, obtains anti-oxidant reparation facial mask.
Take 20g indocalamus leafs, 8g honeysuckles, 6g Radix Astragalis, 10g Radix Glycyrrhizaes, 5g Radix Salviae Miltiorrhizaes, 10g purslanes, 5g dandelions, loading crushing
It is crushed in machine, crosses 60 mesh sieve, obtain compound Chinese medicine powder, take 40g compound Chinese medicine powder, be added in 800mL deionized waters, with
400r/min stirs 30min, adds 0.04g glusulases, is uniformly mixed and is placed in flash extracter, is extracted at 60 DEG C
3min, then be transferred in centrifuge, 20min is centrifuged with 8000r/min, collection supernatant, which is placed in flash inspissator, to be concentrated
To the 30% of stoste volume, the concentrated liquid of tradition Chinese medicine is obtained, takes 6g sodium alginates, is added in 240mL deionized waters, is stirred with 400r/min
15min, it is 5% sodium periodate solution to add 6g mass fractions, and 1.2g ethylene glycol is added afterwards for 24 hours being protected from light place's oxidation reaction,
Continue to be stirred to react 15min, obtain mixed liquor, by mixed liquor be added 300g mass fractions be 5% chlorination sodium ethoxide solution in, with
600r/min stirs 30min, stands and filters to obtain filter cake after 2h is precipitated, filter cake is added in 300mL deionized waters and is stirred to complete
Dissolving adds absolute ethyl alcohol precipitation, stands and filters to obtain filter residue after being precipitated, filter residue is transferred in vacuum drying chamber, at 40 DEG C
Dry 10h, obtains oxidized sodium alginate, and it is 10% poly-vinyl alcohol solution, the life of the 0.5g Chinese to take 3g oxidized sodium alginates, 20g mass fractions
Glue, 0.3g sodium carboxymethylcelluloses are added in 100g deionized waters, stir 30min at 90 DEG C with 400r/min, and be placed on
25min is irradiated under ultraviolet lamp, it is that 5% sodium hydroxide solution adjusts pH to 6.5, then is placed in 5 DEG C of waters bath with thermostatic control that mass fraction, which is used in combination,
Lower standing is crosslinked 15h, and 5g glycerine, 0.2g Tween-80s are added into sol solutions for sol solutions, and 3g the concentrated liquid of tradition Chinese medicine is protected at 80 DEG C
Temperature stirring 40min, filters after standing 12h, obtains anti-oxidant reparation facial mask.
The facial mask of anti-oxidant reparation facial mask and the production of Guangdong company prepared by the present invention is detected, specific detection knot
Fruit such as following table table 1：
This experiment uses volunteer women（Generally there is hormone face puzzlement person）20.Embodiment 1-3 and commercially available is used every night
Example is primary, uses one month/15 days altogether.
Effective evaluation standard is effective：Test event：The soft degree of skin, wrinkle depth（Crows feet area）, skin elasticity.
1 anti-oxidant repair surface film properties of table characterize
The anti-oxidant reparation facial mask that as shown in Table 1 prepared by the present invention, improves significantly to the sophistication and facial wrinkles of skin
It acts on, and repair skin barrier to have remarkable effect.With extremely vast market prospect and application value.
Claims (8)
1. a kind of anti-oxidant reparation facial mask, which is characterized in that the anti-oxidant reparation facial mask includes following weight parts raw material：
2~3 parts of oxidized sodium alginates, 1~2 part of polyvinyl alcohol, 0.3~0.5 part of xanthan gum, 0.2~0.3 part of carboxymethyl cellulose
Sodium, 3~5 parts of glycerine, 0.1~0.2 part of Tween-80,2~3 parts of the concentrated liquid of tradition Chinese medicine.
2. a kind of anti-oxidant reparation facial mask as described in claim 1, which is characterized in that the oxidized sodium alginate is alginic acid
Sodium is added ethylene glycol after the place's of being protected from light oxidation reaction with sodium periodate and is stirred to react, then is precipitated and is precipitated with chlorination sodium ethoxide solution,
Filter residue is filtered to obtain, alcohol precipitation is precipitated and dries and is made after filter residue repetition is dissolved.
3. a kind of anti-oxidant reparation facial mask as described in claim 1, which is characterized in that the oxidized sodium alginate preparation process
In weight of material part be 5~6 parts of sodium alginates, 200~240 parts of deionized waters, 5~6 parts of mass fractions are 5% sodium periodate
Solution, 1.0~1.2 parts of ethylene glycol, 200~300 parts of 5% chlorination sodium ethoxide solutions of mass fraction.
4. a kind of anti-oxidant reparation facial mask as described in claim 1, which is characterized in that the concentrated liquid of tradition Chinese medicine is compound Chinese medicine
Powder is fitted into flash extracter with glusulase after being mixed with deionized water and extracts, and concentrates and be made through flash inspissator.
5. a kind of anti-oxidant reparation facial mask as claimed in claim 4, which is characterized in that raw material weight in the compound Chinese medicine powder
Amount part is 10~20 parts of indocalamus leafs, 6~8 portions of honeysuckles, 4~6 parts of Radix Astragalis, 8~10 portions of Radix Glycyrrhizaes, 4~5 parts of Radix Salviae Miltiorrhizaes, 8~10 parts of dents
Amaranth, 3~5 portions of dandelions.
6. a kind of anti-oxidant reparation facial mask as claimed in claim 4, which is characterized in that the compound Chinese medicine powder, deionization
Water, glusulase parts by weight be 20~40 parts of compound Chinese medicine powder, 400~800 parts of deionized waters, 0.02~0.04 part of snail
Enzyme.
7. a kind of anti-oxidant reparation facial mask as claimed in claim 4, which is characterized in that the Extracting temperature is 40~60 DEG C.
8. a kind of anti-oxidant preparation method for repairing facial mask as described in claim 1~7 any one, which is characterized in that tool
Body step is：
（1）Chinese medicine dry powder and attrition grinding are measured by formula, 60 mesh sieve is crossed, obtains compound Chinese medicine powder；
（2）Compound Chinese medicine powder is disperseed in deionized water and is added glusulase, is uniformly mixed and is placed in flash extracter,
2~3min is extracted at 40~60 DEG C, then is transferred to centrifuge to be placed in flash inspissator in centrifuge and is concentrated into primary liquid
Long-pending 20~30%, obtain the concentrated liquid of tradition Chinese medicine；
（3）It takes sodium alginate to be added in deionized water to stir evenly, it is 5% sodium periodate solution to add mass fraction, and is being kept away
Oxidation reaction 20 at light~ethylene glycol is added afterwards for 24 hours is stirred to react, and obtains mixed liquor；
（4）By mixed liquor be added mass fraction be stood in 5% chlorination sodium ethoxide solution be precipitated after filter to obtain filter cake, by filter cake plus
Enter and precipitated with absolute ethyl alcohol after being dissolved in deionized water, stand and filtered after being precipitated, dry 8~10h, must aoxidize at 30~40 DEG C
Sodium alginate；
（5）Take oxidized sodium alginate, mass fraction be 10% poly-vinyl alcohol solution, xanthan gum, sodium carboxymethylcellulose addition go from
In sub- water, 20~30min is stirred at 80~90 DEG C, and is placed on 20~25min of irradiation under ultraviolet lamp, then uses mass fraction
10~15h of crosslinking, sol solutions are stood at 4~5 DEG C after adjusting pH to 5.0~6.5 for 5% sodium hydroxide solution；
（6）Glycerine, Tween-80, the concentrated liquid of tradition Chinese medicine are added into sol solutions, 30~40min of insulated and stirred, quiet at 70~80 DEG C
It is filtered after setting 10~12h, obtains anti-oxidant reparation facial mask.
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| CN201810758110.2A CN108567669A (en) | 2018-07-11 | 2018-07-11 | Anti-oxidant reparation facial mask of one kind and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109602667A (en) * | 2019-02-18 | 2019-04-12 | 山西农业大学 | A kind of bacteriostatic hand sanitizer and preparation method thereof |
| CN113855854B (en) * | 2021-10-20 | 2022-07-29 | 贵州医科大学附属医院 | Biological material with 4D construction performance and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1257701A (en) * | 1998-12-18 | 2000-06-28 | 杨波 | Film forming compsition and spot-removing mask thereof |
| CN105287339A (en) * | 2015-11-03 | 2016-02-03 | 刘爱红 | Goat colostrum fat-containing mask |
| CN106581734A (en) * | 2016-11-22 | 2017-04-26 | 孙祎 | Preparation method of highly antibacterial alginate dressing |
-
2018
- 2018-07-11 CN CN201810758110.2A patent/CN108567669A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1257701A (en) * | 1998-12-18 | 2000-06-28 | 杨波 | Film forming compsition and spot-removing mask thereof |
| CN105287339A (en) * | 2015-11-03 | 2016-02-03 | 刘爱红 | Goat colostrum fat-containing mask |
| CN106581734A (en) * | 2016-11-22 | 2017-04-26 | 孙祎 | Preparation method of highly antibacterial alginate dressing |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109602667A (en) * | 2019-02-18 | 2019-04-12 | 山西农业大学 | A kind of bacteriostatic hand sanitizer and preparation method thereof |
| CN109602667B (en) * | 2019-02-18 | 2021-12-24 | 山西农业大学 | Antibacterial hand sanitizer and preparation method thereof |
| CN113855854B (en) * | 2021-10-20 | 2022-07-29 | 贵州医科大学附属医院 | Biological material with 4D construction performance and preparation method and application thereof |
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Application publication date: 20180925 |