CN108560253A - A kind of Chinese medicine health-care leather shell material and application thereof - Google Patents
A kind of Chinese medicine health-care leather shell material and application thereof Download PDFInfo
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- CN108560253A CN108560253A CN201810355291.4A CN201810355291A CN108560253A CN 108560253 A CN108560253 A CN 108560253A CN 201810355291 A CN201810355291 A CN 201810355291A CN 108560253 A CN108560253 A CN 108560253A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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Abstract
The present invention relates to a kind of Chinese medicine health-care leather shell materials and application thereof, are made by following steps,（1）Effective antimicrobial component extraction：It is spare to extract Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii, centella, cloves, the antimicrobial component of Jasmine；（2）Nano controlled-release processing：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；（3）Heat treatment：Nature Fibre Textile finished product and antimicrobial nano particle aqueous solution are heat-treated in 40 50 DEG C of rollers；（4）It is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.The present invention selects part Chinese medicinal plant to carry out function improvement to natural fibers such as cotton, fiber crops, bamboos, so that these fabrics is had antibacterial, faint scent, health-care effect, has protective effect to human skin.The processing technology of the present invention is simple, easy to operate, is suitble to craft and mechanization production, application field demand is big, and environment protection health is environmentally safe.
Description
Technical field
The present invention relates to a kind of Chinese medicine health-care leather shell materials and application thereof, belong to anti-bacterial fibre field.
Background technology
Health is current project of greatest concern with environmental protection.In recent years, it is worldwide advocate nature, green consumption tide
Under, various countries' textile industry is all good for the environment in active development, the functional textile product of health, is proposed many tools successively
There are health care, the health of medical functions, environment-friendly products, such as summer and autumn clothes, labour protection articles for use, parasols tourism supplies, storehouse
Multiple industry classes such as storage and all kinds of temporary building materials, decorating cloth, accumulate and educate very wide market.At present more
It is fine with the synthesis of nanoscale anti-biotic material containing silver zeolite that ripe and oneself realization industrialized production anti-bacterial fibre has two major classes one to be
Dimension be representative inorganic antibacterial system anti-bacterial fibre, this fiber it is safe to the human body it is harmless, durability is good.Second is that with organic antibacterial agent
The serial anti-bacterial fibre developed by blending method.With the development of nano industrial and antimicrobial technology, anti-bacterial fibre extensive use
Bad smell of perspiration, bacteria breed and infection can be effectively solved in the clothing that every field is made with anti-bacterial fibre, reduces the generation of infectious disease,
Create own health environment.Anti-bacterial fibre has played important function to creating clean, health environment.But it is asked there are following
Topic：One, silver ion chemical property is more active, more sensitive to light and heat, especially the meeting after ultraviolet light irradiates for a long time, is reduced to
The elemental silver of black significantly limits its application to influence the appearance of white or light-colored product.Ring is used due to fabric
Most of border in the sweat of the compound containing chlorion, especially human body all in the presence of a large amount of sodium chloride is contained, in the environment
In any silver compound can all be reacted with chlorion generate silver nitride precipitation.Since the light reaction of silver chlorate is stronger, can
Silver ion is reduced into the non-ionic metallic silver of brown under light-exposed irradiation.Two in addition to the biology of nano silver antibacterial fabric
Toxicity, safety in utilization also need further to be studied.
Invention content
The present invention provides a kind of Chinese medicine health-care leather shell material and application thereof, it is easy to change to solve existing antibacterial fabric, antibacterial
The problems such as effect is bad.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of Chinese medicine health-care leather shell material, it is characterised in that：It is made by following steps,
(1) according to the purposes of Chinese medicine health-care leather shell material, corresponding Chinese medicine is selected, effective antimicrobial component is extracted and carries；
(2) nano controlled-release is handled：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
(3) it is heat-treated：Nature Fibre Textile finished product or cladding and mass concentration are that 15% antimicrobial nano particle aqueous solution exists
It is heat-treated in 40-50 DEG C of roller；
(4) it is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
Chinese medicine in the present invention can choose corresponding Chinese medicine according to the purposes of fabric, extract effective ingredient, as sleeping is strong
Kang Peifang：The draft such as selection lavender, sweet basil, Chinese juniper, Radix Polygalae, sweet tea wild marjoram and Flos Albiziae are proportionally fabricated to sleeping and match
Side.It equally can also choose the antifatigue formula of inducing resuscitation：The book on Chinese herbal medicine such as peppermint, Jasmine, sweet basil, cloves, camphor is selected proportionally to prepare
At the antifatigue formula of inducing resuscitation；The fragrance formula of soothing the spirit can also be chosen：Rose, sweet osmanthus, cloves, peppermint etc. book on Chinese herbal medicine petal according to than
Example is configured to the fragrance formula of soothing the spirit.
Further, a preferred embodiment of the present invention is：The Chinese medicine health-care leather shell material be antibacterial health-care fabric, by with
Lower step is made,
(1) effectively antimicrobial component extraction：In parts by weight, 20-30 parts of Rumex madaio, 10-15 parts of the tuber of stemona, kuh-seng 5- are extracted
10 parts, 10-15 parts of frutus cnidii, 10-15 parts of centella, 5-10 parts of cloves, the antimicrobial component of 10-15 parts of Jasmine it is spare；
(2) nano controlled-release is handled：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
(3) it is heat-treated：Nature Fibre Textile finished product and mass concentration are 15% antimicrobial nano particle aqueous solution at 40-50 DEG C
It is heat-treated in roller；
(4) it is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
Further, a preferred embodiment of the present invention is：Effective antimicrobial component extraction is specific as follows：
(1) Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii, the extraction of centella active ingredient：By Rumex madaio, the tuber of stemona, kuh-seng, cnidium monnieri
Son, centella add 80-90% ethyl alcohol, 40-50 DEG C of temperature, time 6-12h, filtering according to the ratio of solid-liquid ratio 3-5g/ml respectively
Filtrate is obtained, filtrate removes ethyl alcohol, obtains the first liquid,
(2) cloves, the extraction of Jasmine active ingredient：Cloves, Jasmine first pass through supercritical CO respectively2Extraction, obtains essence
Oil, the part after then extracting uses 90% ethyl alcohol, according to solid-liquid ratio 1g:10ml, temperature 60 C, extraction time 2h, filtering
Filtrate is obtained, filtrate removes ethyl alcohol, obtains the second liquid；
(3) the first liquid, essential oil and the second liquid are uniformly mixed, both obtain antimicrobial component stoste.
Further, a preferred embodiment of the present invention is：The nanometered disposal is：
(1) antimicrobial component stoste is mixed with cornstarch and is divided equally, ultrasonic wave dispersion is divided equally, and then dry, grinding obtains
Mixture；
(2) sodium alginate is dissolved in alkaline solution, obtains the sodium alginate soln of a concentration of 1mol/L；
(3) sodium alginate soln for being added to the mixture that step (1) obtains mixes at least 20min, through centrifuging,
Antimicrobial component nano controlled-release ball is obtained after washing, ultrasonic disperse；
(4) CaCl for the antimicrobial component nano controlled-release ball and a concentration of 0.125mol/L for obtaining step (3)2The bodies such as solution
After solidification, the antimicrobial component nano controlled-release ball powder of a diameter of 200nm~300nm is obtained after centrifugation, washing, drying for product mixing
Shape object.
Further, a preferred embodiment of the present invention is：The weight ratio of the antimicrobial component stoste and cornstarch is
1:1~2.
Further, a preferred embodiment of the present invention is：The mixing of the antimicrobial component stoste and sodium alginate soln
Temperature is 20 DEG C~40 DEG C.
Further, a preferred embodiment of the present invention is：The weight ratio of the antimicrobial component stoste and cornstarch is
1:1~2.
Further, a preferred embodiment of the present invention is：The antimicrobial component nano controlled-release ball and CaCl2The mixing of solution
Time 10min~20min.
Further, a preferred embodiment of the present invention is：The time of the heat treatment is 1-3h.
Further, a preferred embodiment of the present invention is：The Nature Fibre Textile product are cotton fiber textile, silk fibre
Tie up textile or flaxen fiber textile.
The Chinese medicine health-care leather shell material of the present invention is in clothes, footwear material, household material, automotive trim, special medical mat material
Purposes.
Beneficial effects of the present invention：
The present invention selects part Chinese medicinal plant to carry out function improvement to natural fibers such as cotton, fiber crops, bamboos, these fabrics is made to have
Antibacterial, faint scent, health-care effect have protective effect to human skin.The processing technology of the present invention is simple, easy to operate, is suitble to hand
Work and mechanization production, application field demand is big, and environment protection health is environmentally safe.
Rumex madaio has stronger inhibiting effect to trichophyton purpureatum, finger-type trichophyte, for staphylococcus aureus and
Escherichia coli etc. also have good inhibiting effect, to the antibacterial action unobvious of aspergillus niger and Candida albicans.
The tuber of stemona is to meningococcus, staphylococcus aureus, staphylococcus albus, tubercle bacillus, shigella dysenteriae, typhoid fever bar
Bacterium, paratyphosum Bacterium, Escherichia coli, proteus, corynebacterium diphtheriae, pneumobacillus, yersinia pestis, bacillus anthracis, Pseudomonas aeruginosa
Deng there is a different degrees of antibacterial action, and bacteriostasis is more stable persistently.
Frutus cnidii is to Escherichia coli, golden yellow Portugal bacterium, bacillus subtilis, candida tropicalis, aspergillus flavus, penicillium chrysogenum etc.
Inhibiting effect is all had, the effect of bacterium is inhibited to be better than yeast and mould
Kuh-seng is the root of legume kuh-seng, to Escherichia coli, shigella dysenteriae, staphylococcus albus, Staphylococcus aureus
The bacteriums such as bacterium, proteus, Pseudomonas aeruginosa, paratyphoid bacillus A, pneumobacillus are inhibited.
Cloves is used for always in food production processing, as a kind of spice to improve the flavor mouth of food for a long time
Feel, some active constituents contained in cloves have stronger sterilizing ability.To Hansenula anomala, mould, aspergillus niger, golden yellow
Staphylococcus, bacillus subtilis, Escherichia coli have very strong bacteriostasis, and cloves anti-corrosion relatively stablizes heat, within 100 DEG C
It remains to keep bacteriostasis；Meanwhile cloves inhibitory effect is strong, has a broad antifungal spectrum, both can inhibit bacterium, and can inhibit yeast and mould
Functions on common pollutant bacteria have broad-spectrum antibacterial effect, minimal inhibitory concentration is low, especially inhibits fungi effect strong.
Centella has antibacterial and antivirus action, has bacteriostasis to staphylococcus aureus and proteus, to green
Purulence bacillus, Escherichia coli, paracolon, S. sonnei, shigella flexneri and bacillus anthracis are without bacteriostasis.Product
Snow grass shows stronger antibacterial activity to various drug-resistant bacterias, includes staphylococcus aureus (MRSA), the form staph of methicillin-resistant
(MRSE), the escherichia coli etc. of resistance to 5 kinds of aminoglycoside antibiotics, the enterococcus faecalis for producing inactive enzyme, production beta-lactamase.
Jasmine, which is the bacteriums such as Escherichia coli, staphylococcus aureus, hay bacillus, apparent bacteriostasis, especially right
Staphylococcus aureus inhibiting effect is the most notable；And to saccharomycete, mould without obvious inhibiting effect.Cream jasmin france oil is fragrance
Industrial important source material, the fragrant matter reconciliation of it and other flowers give the fragrance of numerous types to provide graceful and moist quality.
As antibiotic, synthesis and semi-synthetic antibacterials are in clinical extensive use, make many serious infectious diseases
Disease is effectively controlled.However, due to the abuse of antibiotic, clinically bacterial resistance getting worse.Reduce bacterial resistance and resistance to
The generation of medicine bacterial strain is the important topic that Medical interface is faced.Chinese medicine is that the health of Chinese has made great tribute for thousands of years
It offers, positive effect has also been played in terms of the modern times prevent and control bacterial infection disease.Due to the particularity of Chinese medicine, bacterium compared with
It is few that drug resistance is generated to Chinese medicine.The present invention chooses different Chinese medicine as antimicrobial component, and using different through a large number of experiments
Method extract the antimicrobial component of Chinese medicine, give full play to the different bacteriostasis of each Chinese medicine, Rumex madaio mainly inhibits fungi,
The tuber of stemona and kuh-seng mainly inhibit bacterium, cloves to inhibit bacterium and fungi, and frutus cnidii, centella and Jasmine are for coordinating other three
Kind Chinese medicine, improves synergistic effect, improves bacteriostasis antibiosis effect.
Otherwise for the generation of bacterial drug resistance, for one aspect of the present invention by way of Chinese medicine compounding, antibacterial is polytropism
And multiple target point, so that bacterium is difficult to create antagonism simultaneously the multidrug resistants of a variety of antimicrobial components, therefore with preferably inhibiting and kill
It goes out the effect of bacterium, otherwise for existing drug-resistant bacteria, the present invention inhibits drug-resistant bacteria by adding centella so that this hair
Bright anti-biotic material long-time service not will produce drug resistance.
Chinese medicine with the special smell of Chinese herbal medicine, is not received generally by some, the taste of traditional Chinese medicine that different Chinese traditional medicine compositions generate
Also different, the present invention can be effectively by the way of addition Jasmine and cloves according to selected Chinese herbal main component
Shelter the special smells of special Chinese herbal medicine such as Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii and centella so that antibacterial material of the invention
Material has special pure and fresh soft fragrance.
The present invention plants Nature Fibre Textile product using treated as raw material, and by antimicrobial treatment, the Chinese medicine of the preparation made is anti-
There is flavonoids, alkaloids, organic acid, volatile oil, carbohydrate, saponins, Anthraquinones, terpene etc. inside bacterium ingredient, resist
Bacterium ingredient is complete, has broad-spectrum antimicrobial effect, and good anti-bacterial effect.According further to the property of raw material, antimicrobial component is carried out
Nano controlled-release processing so that antimicrobial component retention time is long, good anti-bacterial effect.
The present invention, as carrier material, passes through antimicrobial component stoste and cornstarch mixed powder and seaweed using sodium alginate
Acid sodium solution mixing method makes it preferably play antibacterial action to protect antimicrobial component；CaCl2 curing technologies are used simultaneously,
The concentration of CaCl2 solution is set in 0.125mol/L, and technological process operability is strong, is easy to batch production, by test, the present invention
Obtained antimicrobial component nano controlled-release ball powder particle size range is 200nm~300nm, has good sustained release performance and antibacterial
Effect.
Specific implementation mode
Below in conjunction with the specific embodiment of the invention, technical scheme of the present invention is clearly and completely described, is shown
So, described content is only one embodiment of the invention, instead of all the embodiments.Based on the implementation in the present invention
Example, the every other embodiment that those of ordinary skill in the art are obtained without creative efforts belong to
The scope of protection of the invention.
A kind of Chinese medicine health-care leather shell material, is made by following steps,
(1) according to the purposes of Chinese medicine health-care leather shell material, corresponding Chinese medicine is selected, effective antimicrobial component is extracted and carries；
(2) nano controlled-release is handled：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
(3) it is heat-treated：Nature Fibre Textile finished product or cladding and mass concentration are that 15% antimicrobial nano particle aqueous solution exists
It is heat-treated in 40-50 DEG C of roller；
(4) it is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
Chinese medicine in the present invention can choose corresponding Chinese medicine according to the purposes of fabric, extract effective ingredient, as sleeping is strong
Kang Peifang：The draft such as selection lavender, sweet basil, Chinese juniper, Radix Polygalae, sweet tea wild marjoram and Flos Albiziae are proportionally fabricated to sleeping and match
Side.It equally can also choose the antifatigue formula of inducing resuscitation：The book on Chinese herbal medicine such as peppermint, Jasmine, sweet basil, cloves, camphor is selected proportionally to prepare
At the antifatigue formula of inducing resuscitation；The fragrance formula of soothing the spirit can also be chosen：Rose, sweet osmanthus, cloves, peppermint etc. book on Chinese herbal medicine petal according to than
Example is configured to the fragrance formula of soothing the spirit.
Cladding prepare tangible tanning before, technique using the present invention handles cladding.
Below based on antibacterial fabric, specific embodiment is as follows：
Embodiment 1
A kind of Chinese medicine health-care leather shell material, is made by following steps,
(1) effectively antimicrobial component extraction：In parts by weight, 20 parts of Rumex madaio, 15 parts of the tuber of stemona, 5 parts of kuh-seng, cnidium monnieri are extracted
13 parts of son, 10 parts of centella, 5 parts of cloves, the antimicrobial component of 10 parts of Jasmine are spare；
(2) nano controlled-release is handled：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
(3) it is heat-treated：Nature Fibre Textile finished product and antimicrobial nano particle aqueous solution are heat-treated in 40 DEG C of rollers；
(4) it is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
Effective antimicrobial component extraction is specific as follows：
(1) Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii, the extraction of centella active ingredient：By Rumex madaio, the tuber of stemona, kuh-seng, cnidium monnieri
Son, centella add 80% ethyl alcohol, 40 DEG C of temperature, time 6h to filter to get filtrate according to the ratio of solid-liquid ratio 3g/ml respectively, filtrate
Ethyl alcohol is removed, the first liquid is obtained,
(2) cloves, the extraction of Jasmine active ingredient：Cloves, Jasmine first pass through supercritical CO respectively2Extraction, obtains essence
Oil, the part after then extracting uses 90% ethyl alcohol, according to solid-liquid ratio 1g:10ml, temperature 60 C, extraction time 2h, filtering
Filtrate is obtained, filtrate removes ethyl alcohol, obtains the second liquid；
(3) the first liquid, essential oil and the second liquid are uniformly mixed, both obtain antimicrobial component stoste.
The nanometered disposal is：(1) antimicrobial component stoste being mixed with cornstarch and is divided equally, ultrasonic wave dispersion is divided equally,
Then dry, grinding, obtains mixture；
(2) sodium alginate is dissolved in alkaline solution, obtains the sodium alginate soln of a concentration of 1mol/L；
(3) sodium alginate soln for being added to the antimicrobial component stoste that step (1) obtains mixes at least 20min,
Antimicrobial component nano controlled-release ball is obtained after centrifugation, washing, ultrasonic disperse；
(4) CaCl for the antimicrobial component nano controlled-release ball and a concentration of 0.125mol/L for obtaining step (3)2The bodies such as solution
After solidification, the antimicrobial component nano controlled-release ball powder of a diameter of 200nm~300nm is obtained after centrifugation, washing, drying for product mixing
Shape object.
The weight ratio of the antimicrobial component stoste and cornstarch is 1:1.
The mixing temperature of the antimicrobial component stoste and sodium alginate soln is 20 DEG C.
The antimicrobial component nano controlled-release ball and CaCl2The incorporation time 10min of solution.
Nature Fibre Textile product are cotton fiber textile.
Embodiment 2
A kind of Chinese medicine health-care leather shell material, is made by following steps,
(1) effectively antimicrobial component extraction：In parts by weight, 25 parts of Rumex madaio, 13 parts of the tuber of stemona, 7 parts of kuh-seng, cnidium monnieri are extracted
10 parts of son, 13 parts of centella, 8 parts of cloves, the antimicrobial component of 12 parts of Jasmine are spare；
(2) nano controlled-release is handled：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
(3) it is heat-treated：Nature Fibre Textile finished product and antimicrobial nano particle aqueous solution are heat-treated in 45 DEG C of rollers；
(4) it is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
Effective antimicrobial component extraction is specific as follows：
(1) Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii, the extraction of centella active ingredient：By Rumex madaio, the tuber of stemona, kuh-seng, cnidium monnieri
Son, centella add 90% ethyl alcohol, temperature 45 C, time 8h to filter to get filtrate according to the ratio of solid-liquid ratio 4g/ml respectively, filtrate
Ethyl alcohol is removed, the first liquid is obtained,
(2) cloves, the extraction of Jasmine active ingredient：Cloves, Jasmine first pass through supercritical CO respectively2Extraction, obtains essence
Oil, the part after then extracting uses 90% ethyl alcohol, according to solid-liquid ratio 1g:10ml, temperature 60 C, extraction time 2h, filtering
Filtrate is obtained, filtrate removes ethyl alcohol, obtains the second liquid；
(3) the first liquid, essential oil and the second liquid are uniformly mixed, both obtain antimicrobial component stoste.
The nanometered disposal is：(1) antimicrobial component stoste being mixed with cornstarch and is divided equally, ultrasonic wave dispersion is divided equally,
Then dry, grinding, obtains mixture；
(2) sodium alginate is dissolved in alkaline solution, obtains the sodium alginate soln of a concentration of 1mol/L；
(3) sodium alginate soln for being added to the antimicrobial component stoste that step (1) obtains mixes at least 20min,
Antimicrobial component nano controlled-release ball is obtained after centrifugation, washing, ultrasonic disperse；
(4) CaCl for the antimicrobial component nano controlled-release ball and a concentration of 0.125mol/L for obtaining step (3)2The bodies such as solution
After solidification, the antimicrobial component nano controlled-release ball powder of a diameter of 200nm~300nm is obtained after centrifugation, washing, drying for product mixing
Shape object.
The weight ratio of the antimicrobial component stoste and cornstarch is 1:2.
The mixing temperature of the antimicrobial component stoste and sodium alginate soln is 30 DEG C.
The antimicrobial component nano controlled-release ball and CaCl2The incorporation time 15min of solution.
Nature Fibre Textile product are flaxen fiber textile.
Embodiment 3
A kind of Chinese medicine health-care leather shell material, is made by following steps,
(1) effectively antimicrobial component extraction：In parts by weight, 30 parts of Rumex madaio, 10 parts of the tuber of stemona, 10 parts of kuh-seng, snake are extracted
15 parts of machine tool, 15 parts of centella, 10 parts of cloves, the antimicrobial component of 15 parts of Jasmine are spare；
(2) nano controlled-release is handled：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
(3) it is heat-treated：Nature Fibre Textile finished product and antimicrobial nano particle aqueous solution are heat-treated in 50 DEG C of rollers；
(4) it is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
Effective antimicrobial component extraction is specific as follows：
(1) Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii, the extraction of centella active ingredient：By Rumex madaio, the tuber of stemona, kuh-seng, cnidium monnieri
Son, centella add 90% ethyl alcohol, temperature 50 C, time 12h to filter to get filtrate according to the ratio of solid-liquid ratio 5g/ml respectively, filtrate
Ethyl alcohol is removed, the first liquid is obtained,
(2) cloves, the extraction of Jasmine active ingredient：Cloves, Jasmine first pass through supercritical CO respectively2Extraction, obtains essence
Oil, the part after then extracting uses 90% ethyl alcohol, according to solid-liquid ratio 1g:10ml, temperature 60 C, extraction time 2h, filtering
Filtrate is obtained, filtrate removes ethyl alcohol, obtains the second liquid；
(3) the first liquid, essential oil and the second liquid are uniformly mixed, both obtain antimicrobial component stoste.
The nanometered disposal is：(1) antimicrobial component stoste being mixed with cornstarch and is divided equally, ultrasonic wave dispersion is divided equally,
Then dry, grinding, obtains mixture；
(2) sodium alginate is dissolved in alkaline solution, obtains the sodium alginate soln of a concentration of 1mol/L；
(3) sodium alginate soln for being added to the antimicrobial component stoste that step (1) obtains mixes at least 20min,
Antimicrobial component nano controlled-release ball is obtained after centrifugation, washing, ultrasonic disperse；
(4) CaCl for the antimicrobial component nano controlled-release ball and a concentration of 0.125mol/L for obtaining step (3)2The bodies such as solution
After solidification, the antimicrobial component nano controlled-release ball powder of a diameter of 200nm~300nm is obtained after centrifugation, washing, drying for product mixing
Shape object.
The weight ratio of the antimicrobial component stoste and cornstarch is 1:2.
The mixing temperature of the antimicrobial component stoste and sodium alginate soln is 40 DEG C.
The antimicrobial component nano controlled-release ball and CaCl2The incorporation time 20min of solution.
Nature Fibre Textile product are cotton fiber textile.
Antibacterial effect measures
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Assay method | |
| Trichophyton rubrum bacterial reduction (%) | >99.95 | >99.96 | >99.95 | AATCC100-2012 |
| Staphylococcus aureus bacteriostasis rate (%) | 95 | 96 | 94 | GBT20944.3-2008 |
| Candida albicans bacteriostasis rate (%) | 96 | 98 | 98 | GBT20944.3-2008 |
The Chinese medicine health-care leather shell material of the present invention passes through 50 cleanings, is measured according to above-mentioned antibacterial effect assay method, right
It is maintained at 90% or more in Trichophyton rubrum bacterial reduction (%), staphylococcus aureus bacteriostasis rate (%) and white are read
Pearl bacterium bacteriostasis rate (%) is maintained at 85% or more.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (10)
1. a kind of Chinese medicine health-care leather shell material, it is characterised in that：It is made by following steps,
（1）According to the purposes of Chinese medicine health-care leather shell material, corresponding Chinese medicine is selected, extracts effective antimicrobial component；
（2）Nano controlled-release processing：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
（3）Heat treatment：Nature Fibre Textile finished product or cladding and mass concentration are 15% antimicrobial nano particle aqueous solution in 40-50
It is heat-treated in DEG C roller；
（4）It is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
2. a kind of Chinese medicine health-care leather shell material according to claim 1, it is characterised in that：The Chinese medicine health-care leather shell material is
Antibacterial health-care fabric is made by following steps,
（1）Effective antimicrobial component extraction：In parts by weight, 20-30 parts of Rumex madaio, 10-15 parts of the tuber of stemona, kuh-seng 5-10 are extracted
Part, 10-15 parts of frutus cnidii, 10-15 parts of centella, 5-10 parts of cloves, the antimicrobial component of 10-15 parts of Jasmine are spare；
（2）Nano controlled-release processing：Antimicrobial component is subjected to nano controlled-release processing, antimicrobial nano particle is made；
（3）Heat treatment：Nature Fibre Textile finished product or cladding and mass concentration are 15% antimicrobial nano particle aqueous solution in 40-50
It is heat-treated in DEG C roller；
（4）It is dehydrated, dried, shaped, both obtain Chinese medicine health-care leather shell material.
3. a kind of Chinese medicine health-care leather shell material according to claim 2, it is characterised in that：Effective antimicrobial component extraction
It is specific as follows：
（1）Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii, the extraction of centella active ingredient：By Rumex madaio, the tuber of stemona, kuh-seng, frutus cnidii,
Centella adds 80-90% ethyl alcohol, 40-50 DEG C of temperature, time 6-12h to filter to obtain filter according to the ratio of solid-liquid ratio 3-5g/ml respectively
Liquid, filtrate remove ethyl alcohol, obtain the first liquid,
（2）Cloves, the extraction of Jasmine active ingredient：Cloves, Jasmine first respectively by SCF-CO 2, obtain essential oil, so
Part after extracting afterwards uses 90% ethyl alcohol, according to solid-liquid ratio 1g:10ml, temperature 60 C, extraction time 2h filter to get filtrate,
Filtrate removes ethyl alcohol, obtains the second liquid；
（3）First liquid, essential oil and the second liquid are uniformly mixed, antimicrobial component stoste is both obtained.
4. a kind of Chinese medicine health-care leather shell material according to claim 1 or 2, it is characterised in that：The nanometered disposal is：
（1）Antimicrobial component stoste is mixed with cornstarch and is divided equally, ultrasonic wave dispersion is divided equally, and then dry, grinding is mixed
Object；
（2）Sodium alginate is dissolved in alkaline solution, the sodium alginate soln of a concentration of 1mol/L is obtained；
（3）By step（1）Sodium alginate soln that obtained antimicrobial component stoste is added to mixes at least 20min, through from
Antimicrobial component nano controlled-release ball is obtained after the heart, washing, ultrasonic disperse；
（4）By step（3）The CaCl of obtained antimicrobial component nano controlled-release ball and a concentration of 0.125mol/L2Solution is isometric
After solidification, the antimicrobial component nano controlled-release ball powdery of a diameter of 200nm~300nm is obtained after centrifugation, washing, drying for mixing
Object.
5. a kind of Chinese medicine health-care leather shell material according to claim 4, it is characterised in that：The antimicrobial component stoste and jade
The weight ratio of rice starch is 1:1~2.
6. a kind of Chinese medicine health-care leather shell material according to claim 4, it is characterised in that：The antimicrobial component stoste and sea
The mixing temperature of solution of sodium alginate is 20 DEG C~40 DEG C.
7. a kind of Chinese medicine health-care leather shell material according to claim 4, it is characterised in that：The antimicrobial component nano controlled-release ball
With CaCl2Incorporation time 10min~20min of solution.
8. according to a kind of Chinese medicine health-care leather shell material of claim 2 any one of them, it is characterised in that：The heat treatment when
Between be 1-3h.
9. according to a kind of Chinese medicine health-care leather shell material of claim 2 any one of them, it is characterised in that：The natural fiber is spun
Fabric is cotton fiber textile, silk fiber textile or flaxen fiber textile.
10. claim 1-9 any one of them Chinese medicine health-care leather shell materials are in clothes, footwear material, household material, automotive trim, spy
Purposes in different medical mat material.
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Application publication date: 20180921 |