CN108552249A - A kind of fungicide and preparation method thereof of prevention apple anthracnose - Google Patents
A kind of fungicide and preparation method thereof of prevention apple anthracnose Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/30—Polygonaceae [Buckwheat family], e.g. red-knees or rhubarb
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
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Abstract
The invention discloses a kind of fungicide and preparation method thereof of prevention apple anthracnose, belong to pest and disease control of fruit trees technical field.The fungicide of the prevention apple anthracnose of the present invention, is made of the following raw material：Bunge pricklyash leaf, Radix Salviae Miltiorrhizae, granatum, folium artemisiae argyi, polygoni cuspidati,radix, Celastrus angulatus, the root bark of Chinese wolf-berry, psoralea corylifolia, apple polyphenol extract, acetobacter xylinum, saccharomycete.The present invention integrates disease control and weed control, does not need additional use herbicide, has not only saved use cost, but also can greatly improve the control rate and weed control rate of disease, played the effect killed two birds with one stone.Fungicide bactericidal effect prepared by the present invention is good, and the more conventional processing of sterilizing rate improves 18.7~22.3 percentage points, and anthracnose control rate is 91.7~94.6%, weed control rate 95.7%~97.7%, 3800~3870kg/ mus of yield, volume increase 26.7%~29.0%, remarkable in economical benefits.
Description
Technical field
The invention belongs to pest and disease control of fruit trees technical fields, and in particular to it is a kind of prevention apple anthracnose fungicide and
Preparation method.
Background technology
Apple anthracnose is also known as bitter rot, late blight, is one of fruit disease important on apple, China's major part apple
There is generation in producing region, is particularly acute in summer high temperature, rainy, humid region morbidity.Main harm fruit can also endanger branch
With fruit platform etc..Occur filbert small round spot on initial stage fruit face, expand rapidly, brown or dark brown, surface depressions, pulp rot
In infundibulate, rotten can have bitter taste to core, it is apparent with good pulp boundary.Under warm conditions, germ can be weak or have wound
Ulceration, mostly irregular shape are formed on 1~2 year raw branch, is gradually expanded, is cracked to later stage disease epidermis, causes xylem exposed,
Scab surface also generates black small grain point.The sick above branch in portion is withered.The aggrieved sprawling from top to bottom of fruit platform is in dark brown, causes fruit platform
It can not take out the withered death of sublateral shoot.
Through the literature search of existing technologies, China Patent Publication No. CN106719865A, publication date 2017 05
The patent application on the moon 31 discloses a kind of biological pesticide and preparation method of prevention apple anthracnose, which is by group
Part A, component B, surfactant, cosolvent compounding are made, and wherein component A is by Chinese herbal medicine hypericum japonicum, dichrocephala, fortune holly fern rhizome, the wing
First grass is made.The invention mainly uses Chinese herbal medicine and 80% difoltan wettable powder to carry out compounding for preventing apple anthrax
Disease, although achieving certain bacteriostatic and disease prevention effect, it is simple chemical control, also has the pesticide residue of part.
If we coordinate some extracts using Chinese herbal medicine and some useful strains prepare a kind of fungicide, can either diseases prevention it is antibacterial,
The use of pesticide can be reduced again, but also with preferably effect, is effectively protected ecological environment, this fungicide becomes
The problem of we currently focus on solving.
Invention content
It is antibacterial that the purpose of the present invention is to provide preventable diseases, reduces or do not use pesticide, can utmostly improve apple production
The fungicide and preparation method thereof for preventing apple anthracnose of amount, effective protection ecological environment.
To solve the above problems, the present invention adopts the following technical scheme that：
A kind of fungicide of prevention apple anthracnose, is composed of the following raw materials in parts by weight：42~61 parts of bunge pricklyash leaf, Radix Salviae Miltiorrhizae
40~53 parts, 37.5~46.5 parts of granatum, 33~41 parts of folium artemisiae argyi, 27~36 parts of polygoni cuspidati,radix, 27~36 parts of Celastrus angulatus, the root bark of Chinese wolf-berry
23~35 parts, 20~31 parts of psoralea corylifolia, 14~20 parts of apple polyphenol extract, 10~14 parts of acetobacter xylinum, saccharomycete 9~12
Part；
The fungicide and preparation method thereof of the prevention apple anthracnose, includes the following steps：
1) acetobacter xylinum and saccharomycete at -15 DEG C~-8 DEG C are dried to bacterium powder, bacterium powder A must be mixed, and be dissolved in mixing
In the glycerine of 0.8~1.2 times of bacterium powder A weight, bacterium solution X is formed, it is spare；
2) fresh bunge pricklyash leaf is taken to be crushed to 40 mesh, 95% alcohol reflux that 4~7 times of weight is added extracts 3~4 times, preceding
30~40min, last time extract 15~20min every time twice, filter out bunge pricklyash leaf residue, merge extracting solution, obtain extract
Radix Salviae Miltiorrhizae, polygoni cuspidati,radix, Celastrus angulatus are shredded, are then added in bunge pricklyash leaf ethanol extract, are heated to 45~50 DEG C, are slowly stirred by M
1~2 hour, impurity screening, concentration and recovery ethyl alcohol obtained extract R；
3) add the distilled water of 4~10 times of amounts to be placed in pottery the three taste medicinal material such as granatum, folium artemisiae argyi, root bark of Chinese wolf-berry and heat decoction
2 times, every time 15~25min, and open agitating device and be stirred, it often heats 5min and stirs 1 time, filtration obtains filter residue F, then
Psoralea corylifolia is added thereto and 1.4~2.2 times of psoralea corylifolia weight, 70% ethyl alcohol of amount carry out refluxing extractions, obtains extract Q, it is spare；
4) bacterium solution X is placed in container and adds extract M, extract R, filter residue F, extract Q, apple polyphenol extract
Enter wherein temperature be 50~65 DEG C at dissolving 10~13min after, be added volumetric concentration be 40% ammonium hydroxide be stirred to react after
To the fungicide of prevention apple anthracnose.
Further, the fungicide of the prevention apple anthracnose, is composed of the following raw materials in parts by weight：Bunge pricklyash leaf 53
Part, 46 parts of Radix Salviae Miltiorrhizae, 42 parts of granatum, 37 parts of folium artemisiae argyi, 33 parts of polygoni cuspidati,radix, 33 parts of Celastrus angulatus, 29 parts of the root bark of Chinese wolf-berry, 27 parts of psoralea corylifolia,
17 parts of apple polyphenol extract, 12 parts of acetobacter xylinum, 11 parts of saccharomycete.
Compared with prior art, the beneficial effects of the present invention are：
1) the present invention overcomes excessive Pesticide uses to cause drug remaining defect in crop body, effectively raises
The yield of crop, and ensure that apple has higher quality requirements.
2) present invention integrates disease control and weed control, does not need additional use herbicide, both having saved makes
With cost, and the control rate and weed control rate of disease can be greatly improved, play the effect killed two birds with one stone.
3) strain is dried to bacterium powder by the present invention, is formed bacterium solution, the multi-level utilization of strain is realized, for apple anthrax
The control effect of disease can be improved 3.5~4.6 percentage points.
4) the fungicide bactericidal effect that prepared by the present invention is good, and the more conventional processing of sterilizing rate improves 18.7~22.3 percentages
Point, anthracnose control rate are 91.7%~94.6%, weed control rate 95.7%~97.7%, 3800~3870kg/ mus of yield
The 3000kg/ mus of volume increase 26.7%~29.0% of more conventional processing per mu yield, remarkable in economical benefits.
Specific implementation mode
Below by specific embodiment, technical scheme of the present invention is further illustrated.It should be appreciated that this hair
Bright embodiment is not limited to the following examples, and accommodation and/or change in any form made for the present invention all will
Fall into protection scope of the present invention.
Embodiment 1
A kind of fungicide of prevention apple anthracnose, is composed of the following raw materials in parts by weight：42 parts of bunge pricklyash leaf, Radix Salviae Miltiorrhizae 40
Part, 37.5 parts of granatum, 33 parts of folium artemisiae argyi, 27 parts of polygoni cuspidati,radix, 27 parts of Celastrus angulatus, 23 parts of the root bark of Chinese wolf-berry, 20 parts of psoralea corylifolia, apple polyphenol
14 parts of extract, 10 parts of acetobacter xylinum, 9 parts of saccharomycete；
The fungicide and preparation method thereof of the prevention apple anthracnose, includes the following steps：
1) acetobacter xylinum and saccharomycete at -15 DEG C are dried to bacterium powder, bacterium powder A must be mixed, and be dissolved in mixing bacterium powder A weights
In 0.8 times of glycerine of amount, bacterium solution X is formed, it is spare；
2) fresh bunge pricklyash leaf is taken to be crushed to 40 mesh, 95% alcohol reflux that 4 times of weight is added extracts 3 times, preceding every twice
Secondary 30min, last time extract 15min, filter out bunge pricklyash leaf residue, merge extracting solution, extract M are obtained, by Radix Salviae Miltiorrhizae, giant knotweed
Root, Celastrus angulatus chopping, are then added in bunge pricklyash leaf ethanol extract, are heated to 45 DEG C, are slowly stirred 1 hour, impurity screening is dense
It retracts and receives ethyl alcohol, obtain extract R；
3) add the distilled water of 4 times of amounts to be placed in heating in pottery the three taste medicinal material such as granatum, folium artemisiae argyi, root bark of Chinese wolf-berry to decoct 2 times,
Each 15min, and open agitating device and be stirred, it often heats 5min and stirs 1 time, filtration obtains filter residue F, then adds thereto
Enter psoralea corylifolia and 1.4 times of psoralea corylifolia weight, 70% ethyl alcohol of amount carry out refluxing extractions, obtains extract Q, it is spare；
4) bacterium solution X is placed in container and adds extract M, extract R, filter residue F, extract Q, apple polyphenol extract
Enter wherein temperature be 50 DEG C at dissolving 10min after, be added volumetric concentration be 40% ammonium hydroxide be stirred to react after obtain prevention apple
The fungicide of fruit anthracnose.
Embodiment 2
A kind of fungicide of prevention apple anthracnose, is composed of the following raw materials in parts by weight：53 parts of bunge pricklyash leaf, Radix Salviae Miltiorrhizae 46
Part, 42 parts of granatum, 37 parts of folium artemisiae argyi, 33 parts of polygoni cuspidati,radix, 33 parts of Celastrus angulatus, 29 parts of the root bark of Chinese wolf-berry, 27 parts of psoralea corylifolia, apple polyphenol carry
Take 17 parts of object, 12 parts of acetobacter xylinum, 11 parts of saccharomycete；
The fungicide and preparation method thereof of the prevention apple anthracnose, includes the following steps：
1) acetobacter xylinum and saccharomycete at -10 DEG C are dried to bacterium powder, bacterium powder A must be mixed, and be dissolved in mixing bacterium powder A weights
In 0.9 times of glycerine of amount, bacterium solution X is formed, it is spare；
2) fresh bunge pricklyash leaf is taken to be crushed to 40 mesh, 95% alcohol reflux that 6 times of weight is added extracts 3 times, preceding every twice
Secondary 35min, last time extract 18min, filter out bunge pricklyash leaf residue, merge extracting solution, extract M are obtained, by Radix Salviae Miltiorrhizae, giant knotweed
Root, Celastrus angulatus chopping, are then added in bunge pricklyash leaf ethanol extract, are heated to 46 DEG C, are slowly stirred 1.5 hours, impurity screening,
Concentration and recovery ethyl alcohol obtains extract R；
3) add the distilled water of 7 times of amounts to be placed in heating in pottery the three taste medicinal material such as granatum, folium artemisiae argyi, root bark of Chinese wolf-berry to decoct 2 times,
Each 20min, and open agitating device and be stirred, it often heats 5min and stirs 1 time, filtration obtains filter residue F, then adds thereto
Enter psoralea corylifolia and 1.8 times of psoralea corylifolia weight, 70% ethyl alcohol of amount carry out refluxing extractions, obtains extract Q, it is spare；
4) bacterium solution X is placed in container and adds extract M, extract R, filter residue F, extract Q, apple polyphenol extract
Enter wherein temperature be 58 DEG C at dissolving 11min after, be added volumetric concentration be 40% ammonium hydroxide be stirred to react after obtain prevention apple
The fungicide of fruit anthracnose.
Embodiment 3
A kind of fungicide of prevention apple anthracnose, is composed of the following raw materials in parts by weight：61 parts of bunge pricklyash leaf, Radix Salviae Miltiorrhizae 53
Part, 46.5 parts of granatum, 41 parts of folium artemisiae argyi, 36 parts of polygoni cuspidati,radix, 36 parts of Celastrus angulatus, 35 parts of the root bark of Chinese wolf-berry, 31 parts of psoralea corylifolia, apple polyphenol
20 parts of extract, 14 parts of acetobacter xylinum, 12 parts of saccharomycete；
The fungicide and preparation method thereof of the prevention apple anthracnose, includes the following steps：
1) acetobacter xylinum and saccharomycete at -8 DEG C are dried to bacterium powder, bacterium powder A must be mixed, and be dissolved in mixing bacterium powder A weights
In 1.2 times of glycerine of amount, bacterium solution X is formed, it is spare；
2) fresh bunge pricklyash leaf is taken to be crushed to 40 mesh, 95% alcohol reflux that 4~7 times of weight are added extracts 4 times, it is preceding twice
Each 40min, last time extract 20min, filter out bunge pricklyash leaf residue, merge extracting solution, extract M are obtained, by Radix Salviae Miltiorrhizae, giant knotweed
Root, Celastrus angulatus chopping, are then added in bunge pricklyash leaf ethanol extract, are heated to 50 DEG C, are slowly stirred 2 hours, impurity screening is dense
It retracts and receives ethyl alcohol, obtain extract R；
3) add the distilled water of 10 times of amounts to be placed in heating in pottery the three taste medicinal material such as granatum, folium artemisiae argyi, root bark of Chinese wolf-berry and decoct 2
It is secondary, each 25min, and open agitating device and be stirred, it often heats 5min and stirs 1 time, filtration obtains filter residue F, then thereto
Psoralea corylifolia is added and 2.2 times of psoralea corylifolia weight, 70% ethyl alcohol of amount carry out refluxing extractions, obtains extract Q, it is spare；
4) bacterium solution X is placed in container and adds extract M, extract R, filter residue F, extract Q, apple polyphenol extract
Enter wherein temperature be 65 DEG C at dissolving 13min after, be added volumetric concentration be 40% ammonium hydroxide be stirred to react after obtain prevention apple
The fungicide of fruit anthracnose.
The present invention can be summarized with others without prejudice to the concrete form of the spirit or essential characteristics of the present invention.No matter from which
From the point of view of a bit, the embodiment above of the invention can only all be considered the description of the invention and cannot limit the present invention, right
Claim indicates the scope of the present invention, therefore, with the comparable meaning and scope of claims of the present invention in it is any
Change, is all considered as being included within Claims scope.
Claims (2)
1. a kind of fungicide of prevention apple anthracnose, it is characterised in that be composed of the following raw materials in parts by weight：Bunge pricklyash leaf 42~
61 parts, 40~53 parts of Radix Salviae Miltiorrhizae, 37.5~46.5 parts of granatum, 33~41 parts of folium artemisiae argyi, 27~36 parts of polygoni cuspidati,radix, Celastrus angulatus 27~36
Part, 23~35 parts of the root bark of Chinese wolf-berry, 20~31 parts of psoralea corylifolia, 14~20 parts of apple polyphenol extract, 10~14 parts of acetobacter xylinum, yeast
9~12 parts of bacterium；
The fungicide and preparation method thereof of the prevention apple anthracnose, includes the following steps：
1) acetobacter xylinum and saccharomycete at -15 DEG C~-8 DEG C are dried to bacterium powder, bacterium powder A must be mixed, and be dissolved in mixing bacterium powder A
In the glycerine that 0.8~1.2 times of weight, bacterium solution X is formed, it is spare；
2) fresh bunge pricklyash leaf is taken to be crushed to 40 mesh, 95% alcohol reflux that 4~7 times of weight are added extracts 3~4 times, it is preceding twice
30~40min every time, last time extract 15~20min, filter out bunge pricklyash leaf residue, merge extracting solution, obtain extract M, will
Radix Salviae Miltiorrhizae, polygoni cuspidati,radix, Celastrus angulatus chopping, are then added in bunge pricklyash leaf ethanol extract, are heated to 45~50 DEG C, are slowly stirred 1~2
Hour, impurity screening, concentration and recovery ethyl alcohol obtains extract R；
3) add the distilled water of 4~10 times of amounts to be placed in heating in pottery the three taste medicinal material such as granatum, folium artemisiae argyi, root bark of Chinese wolf-berry to decoct 2 times,
15~25min every time, and open agitating device and be stirred, it often heats 5min and stirs 1 time, filtration obtains filter residue F, then to it
Middle addition psoralea corylifolia and 1.4~2.2 times of psoralea corylifolia weight, 70% ethyl alcohol of amount carry out refluxing extractions, obtain extract Q, spare；
4) bacterium solution X is placed in container and it is added in extract M, extract R, filter residue F, extract Q, apple polyphenol extract
In temperature be 50~65 DEG C at dissolving 10~13min after, be added volumetric concentration be 40% ammonium hydroxide be stirred to react after prevented
Control the fungicide of apple anthracnose.
2. a kind of fungicide of prevention apple anthracnose according to claim 1, it is characterised in that by following parts by weight
Raw material forms：53 parts of bunge pricklyash leaf, 46 parts of Radix Salviae Miltiorrhizae, 42 parts of granatum, 37 parts of folium artemisiae argyi, 33 parts of polygoni cuspidati,radix, 33 parts of Celastrus angulatus, the root bark of Chinese wolf-berry
29 parts, 27 parts of psoralea corylifolia, 17 parts of apple polyphenol extract, 12 parts of acetobacter xylinum, 11 parts of saccharomycete.
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| CN109247342A (en) * | 2018-11-05 | 2019-01-22 | 运城学院 | A kind of botanical fungicide and preparation method thereof for preventing and treating apple anthracnose |
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| CN109247342A (en) * | 2018-11-05 | 2019-01-22 | 运城学院 | A kind of botanical fungicide and preparation method thereof for preventing and treating apple anthracnose |
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