CN108498355A - A kind of condensate film and preparation method thereof - Google Patents
A kind of condensate film and preparation method thereof Download PDFInfo
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- CN108498355A CN108498355A CN201810549545.6A CN201810549545A CN108498355A CN 108498355 A CN108498355 A CN 108498355A CN 201810549545 A CN201810549545 A CN 201810549545A CN 108498355 A CN108498355 A CN 108498355A
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- condensate film
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8176—Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention provides a kind of condensate films and preparation method thereof, the condensate film is gel-type vehicle using carrageenan and polyvinylpyrrolidone, mesoporous silicon oxide is added in cooperation, not only increases the gel strength of condensate film, also has good improvement result for the gas permeability of condensate film.
Description
Technical field
The present invention relates to a kind of facial mask, a kind of especially condensate film.
Background technology
Condensate film is that have a kind of facial mask made of the hydrogel material of beauty functions, it works as handle using water as decentralized medium
It when gel is attached on skin, is influenced by body temperature, the physical arrangement inside gel penetrates to the skin from solid state into liquid state
In.Therefore, effective as collagen, hyaluronic acid, ursin, niacinamide etc. is injected in the facial mask of base material using hydrogel
Ingredient can be made into the facial mask of multiple functions；It has the function of powerful agglutination moisture, then skin can be persistently given after docile skin
Moisturizing, meanwhile, both effectiveness raw material in being added in hydrogel facial mask wants cosmetic result, example so as to reach your
Such as：After ursin is added in toward hydrogel facial mask, which is exactly the facial mask for having white-skinned face function, compared to traditional material face
The g., jelly-like essential ingredient of film, water-soluble hydrogel is not easy to evaporate, dries, and the effect releived of bringing down a fever is to acute skin injury
(such as allergy, long acne, scratch) has good result.
But existing hydrogel facial mask often has poor intensity, needs extreme care in use, not so
It is easy to damage gel paster, and existing gel paster facial mask is also not satisfactory in gas permeability.
Invention content
In order to solve the problems in the existing technology, the present invention provides a kind of condensate film, which is pitched by angle
Dish glue and at least one hydrophilic polymer form；
Further, which contains inorganic additive, is selected from mesoporous silicon oxide；
Further, which contains active constituent, plasticizer, aromatic, moisturizer
Further, active constituent is selected from quinhydrones, ursin, kojic acid, azelaic acid, Tretinoin, tartaric acid, leukotrienes, sub- oil
It is acid, hydrolyzed pearl, fibroin, collagen, licorice, green-tea extract, aloe extract, hippophae rhamnoides, white
Any one or a few mixture in art extract dimension, Flos Nelumbinis extract, vitamin C and vitamin E and its derivative；
Further, the one kind or combination of plasticizer in glycerine, propylene glycol, polyethylene glycol；
Further, aromatic is selected from salvia officianlis oil, Rosa Damascana, refined jasmine oil, osmanthus essential oil, Salvia japonica essential oil, breast
In essential oil, chamomile essential oil, Lavender, tea tree ethereal oil, Bergamot, lemon, Sweet Almond Oil, Peppermint essential oil
Any one or a few mixture；
Further, moisturizer be selected from chondroitin sulfate, allantoin, elastin, lactic acid, hyaluronic acid, sodium alginate,
Any one or a few mixture in chitosan, chitin, casein, soybean protein, wheat gluten protein, lactalbumin；
Further, which includes following content (w/v) component：Carrageenan 10-20% polyvinylpyrrolidones
1-5%, mesoporous silicon oxide 0.1-1%, ursin 0.1-0.5%, glycerine 1-10%, Rosa Damascana 1-3%, allantoin 1-
3%；
The present invention also provides a kind of preparation methods of condensate film：Each raw material is weighed according to prescription, by ursin, rhodamine toner
Oil, allantoin, which are dissolved in glycerine, obtains solution A, and polyvinylpyrrolidone obtains solution B, carrageenan heating melting with appropriate water dissolution
Solution C, will solution A and solution B mix after be added in the solution C of stirring to obtain mixed liquor D, mixed liquor D is poured while hot
It builds on mold, stands cooling, shearing prepares hydrogel.
Advantageous effect
Condensate film of the present invention is gel-type vehicle using carrageenan and polyvinylpyrrolidone, and meso-porous titanium dioxide is added in cooperation
Silicon not only increases the gel strength of condensate film, also has good improvement result for the gas permeability of condensate film.
Specific implementation mode
It elaborates to the present invention with reference to embodiment.
Embodiment 1：It is carrageenan 15%, polyvinylpyrrolidone 5%, mesoporous silicon oxide 1%, ursin 0.5%, sweet
Oil 10%, Rosa Damascana 3%, allantoin 3%, excess water
Preparation method：Each raw material is weighed according to prescription, ursin, Rosa Damascana, allantoin are dissolved in glycerine and obtain solution
A, polyvinylpyrrolidone obtain solution B with appropriate water dissolution, and carrageenan heating melts to obtain solution C, solution A and solution B are mixed
It is added to after conjunction in the solution C of stirring and obtains mixed liquor D, mixed liquor D is poured on mold while hot, stand cooling, sheared,
Prepare hydrogel.
Embodiment 2：It is carrageenan 10%, polyvinylpyrrolidone 5%, mesoporous silicon oxide 1%, ursin 0.5%, sweet
Oil 10%, Rosa Damascana 3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1.
Embodiment 3：It is carrageenan 20%, polyvinylpyrrolidone 5%, mesoporous silicon oxide 1%, ursin 0.5%, sweet
Oil 10%, Rosa Damascana 3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1.
Embodiment 4：It is carrageenan 5%, polyvinylpyrrolidone 15%, mesoporous silicon oxide 1%, ursin 0.5%, sweet
Oil 10%, Rosa Damascana 3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1.
Embodiment 5：Carrageenan 15%, polyvinyl alcohol 5%, mesoporous silicon oxide 1%, ursin 0.5%, glycerine
10%, Rosa Damascana 3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1, unlike, change polyvinylpyrrolidone into polyvinyl alcohol.
Embodiment 6：Carrageenan 15%, gelatin 5%, mesoporous silicon oxide 1%, ursin 0.5%, glycerine 10%, rose
Rare essential oil 3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1, unlike, change polyvinylpyrrolidone into gelatin.
Embodiment 7：Carrageenan 20%, mesoporous silicon oxide 1%, ursin 0.5%, glycerine 10%, Rosa Damascana
3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1, unlike, eliminate polyvinylpyrrolidone.
Embodiment 8：Polyvinylpyrrolidone 20%, mesoporous silicon oxide 1%, ursin 0.5%, glycerine 10%, rose
Essential oil 3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1, unlike, eliminate carrageenan.
Embodiment 9：Carrageenan 15%, polyvinylpyrrolidone 5%, ursin 0.5%, glycerine 10%, Rosa Damascana
3%, allantoin 3%, excess water.
The preparation method is the same as that of Example 1, unlike, eliminate mesoporous silicon oxide.
The measurement of gel strength：
Gel strength measures at normal temperatures, measuring instrument instron5569, and measurement formula piece thickness is 5.0mm, a diameter of
10mm, each embodiment prepares 3 test pieces of the same area and measures, and when measurement, T-head speed is 10mm/min, is determined
Compressive strength when test piece 50% deforms is measurement result value.
Ventilation characteristic measuring：
The comparative approach of aeration is, among closed cylinder, hydrogel test piece and is supported in cylinder middle part
Non-woven fabrics is fixed together, and a side entrance of sealing installation, cylinder opens, and the other side is connected to vacuum pump, and forms vacuum, note
The vacuum values of instrument are recorded, every group of test piece is measured 5 times, averaged, and on the basis of embodiment 9, improvement rate of breathing freely is calculated, wherein in fact
The average value for applying the vacuum values of every group of measurement in a 1-8 is calculated as PX, the average value of the vacuum values of embodiment 9 is calculated as P0, breathing freely improves
Rate calculates as follows：
Ventilative improvement rate (%)=[(PX-P0)/P0] × 100%
The measurement result of each experimental group is as follows：
| Gel strength (mPa) | Ventilative improvement rate | |
| Embodiment 1 | 45 | 30% |
| Embodiment 2 | 37 | 27% |
| Embodiment 3 | 42 | 29% |
| Embodiment 4 | 20 | 22% |
| Embodiment 5 | 15 | 17% |
| Embodiment 6 | 13 | 11% |
| Embodiment 7 | 40 (can not restore to the original state) | 31% |
| Embodiment 8 | It is unable to reach 50% deformation | 21% |
| Embodiment 9 | 41 | 0 |
According to result above it is found that carrageenan has positive meaning as gel-type vehicle for gel strength, implement
Example 1 and embodiment 7 compare it is found that by the synergistic effect of carrageenan and polyvinylpyrrolidone, facial mask can be made to have
The gel strength more increased, although embodiment 7 also achieves good gel strength, its elasticity is poor, after deformation
It is difficult to restore to the original state, results in using upper inconvenience, the combination for other waterborne polymerics and carrageenan is simultaneously not implemented
Preferable gel strength；In addition, the addition of silica, significantly increases the gas permeability of facial mask, this is to use in the process to skin
Skin has positive meaning.
Claims (8)
1. a kind of condensate film, it is characterised in that：The condensate membrane matrix is made of carrageenan and at least one hydrophilic polymer.
2. condensate film as described in claim 1, it is characterised in that：The condensate film also contains inorganic additive.
3. such as the condensate film of claims 1 or 2, it is characterised in that：Hydrophilic polymer is selected from polyvinylpyrrolidone, polyethylene
One or more of alcohol, gelatin, hydroxypropyl methyl cellulose combine.
4. condensate film as claimed in claim 2 or claim 3, it is characterised in that：The inorganic additive is mesoporous silicon oxide.
5. condensate film as claimed in claim 1 or 2, it is characterised in that：The condensate film also contains active constituent, plasticizer, virtue
Pastil, moisturizer.
6. condensate film as claimed in claim 5, it is characterised in that：The active constituent is selected from quinhydrones, ursin, kojic acid, nonyl
Diacid, Tretinoin, tartaric acid, leukotrienes, linoleic acid, hydrolyzed pearl, fibroin, collagen, licorice, green tea extraction
In object, aloe extract, hippophae rhamnoides, Rhizoma Atractylodis Macrocephalae extract dimension, Flos Nelumbinis extract, vitamin C and vitamin E and its derivative
Any one or a few mixture；Plasticizer is selected from one or more of glycerine, propylene glycol, polyethylene glycol mixture；Virtue
Pastil is selected from salvia officianlis oil, Rosa Damascana, refined jasmine oil, osmanthus essential oil, Salvia japonica essential oil, frankincense essential oil, chamomile essential oil, smokes
Any one or a few mixing in clothing grass essential oil, tea tree ethereal oil, Bergamot, lemon, Sweet Almond Oil, Peppermint essential oil
Object；Moisturizer be selected from chondroitin sulfate, allantoin, elastin, lactic acid, hyaluronic acid, sodium alginate, chitosan, chitin,
Any one or a few mixture in casein, soybean protein, wheat gluten protein, lactalbumin.
7. condensate film as described in claim 1, it is characterised in that：The condensate film includes following content component (w/v)：Irish moss
Glue 10-20% polyvinylpyrrolidones 1-5%, mesoporous silicon oxide 0.1-1%, ursin 0.1-0.5%, glycerine 1-10%,
Rosa Damascana 1-3%, allantoin 1-3%.
8. a kind of preparation method of condensate film as claimed in claim 7, which is characterized in that comprise the following steps：According to prescription
Each raw material is weighed, ursin, Rosa Damascana, allantoin are dissolved in glycerine and obtain solution A, polyvinylpyrrolidone is used appropriate water-soluble
Solution B is solved, carrageenan heating melts to obtain solution C, is added in the solution C of stirring after solution A and solution B are mixed
Mixed liquor D is obtained, mixed liquor D is poured on mold while hot, stands cooling, shearing prepares hydrogel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810549545.6A CN108498355A (en) | 2018-05-31 | 2018-05-31 | A kind of condensate film and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810549545.6A CN108498355A (en) | 2018-05-31 | 2018-05-31 | A kind of condensate film and preparation method thereof |
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| Publication Number | Publication Date |
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| CN108498355A true CN108498355A (en) | 2018-09-07 |
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| CN201810549545.6A Withdrawn CN108498355A (en) | 2018-05-31 | 2018-05-31 | A kind of condensate film and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111956507A (en) * | 2020-08-24 | 2020-11-20 | 四川康养健生物科技有限公司 | Soluble bletilla striata facial mask and preparation method thereof |
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| JP2008088110A (en) * | 2006-10-02 | 2008-04-17 | Kao Corp | Hydrogel particle |
| CN103099777A (en) * | 2011-11-15 | 2013-05-15 | 上海高科生物工程有限公司 | Bio-enzyme hydrogel taking porous calcium carbonate as carrier and preparation method of bio-enzyme hydrogel |
| CN105310893A (en) * | 2015-12-03 | 2016-02-10 | 依莱恩(上海)实业有限公司 | Condensate water mask and production method thereof |
| CN110028270A (en) * | 2019-03-29 | 2019-07-19 | 深圳中天精装股份有限公司 | A kind of assembled architecture outer wall plastering mortar and preparation method thereof |
-
2018
- 2018-05-31 CN CN201810549545.6A patent/CN108498355A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008088110A (en) * | 2006-10-02 | 2008-04-17 | Kao Corp | Hydrogel particle |
| CN103099777A (en) * | 2011-11-15 | 2013-05-15 | 上海高科生物工程有限公司 | Bio-enzyme hydrogel taking porous calcium carbonate as carrier and preparation method of bio-enzyme hydrogel |
| CN105310893A (en) * | 2015-12-03 | 2016-02-10 | 依莱恩(上海)实业有限公司 | Condensate water mask and production method thereof |
| CN110028270A (en) * | 2019-03-29 | 2019-07-19 | 深圳中天精装股份有限公司 | A kind of assembled architecture outer wall plastering mortar and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 翟茂林等: "k-型卡拉胶/聚乙烯吡咯烷酮共混水凝胶的辐射合成", 《高分子学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111956507A (en) * | 2020-08-24 | 2020-11-20 | 四川康养健生物科技有限公司 | Soluble bletilla striata facial mask and preparation method thereof |
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Application publication date: 20180907 |