CN108457082A - The processing method for improving damp crosslink finishing color-woven fabric easy-care properties - Google Patents
The processing method for improving damp crosslink finishing color-woven fabric easy-care properties Download PDFInfo
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- CN108457082A CN108457082A CN201810268889.XA CN201810268889A CN108457082A CN 108457082 A CN108457082 A CN 108457082A CN 201810268889 A CN201810268889 A CN 201810268889A CN 108457082 A CN108457082 A CN 108457082A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
- D06M11/61—Liquid ammonia
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Treatment Of Fiber Materials (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention belongs to textile dyeing and finishing technical fields, are specifically related to a kind of processing method improving damp crosslink finishing color-woven fabric easy-care properties.Technological process be singe → primary washing → secondary washing → tentering → finished product tests dress to desizing → mercerising → liquefied ammonia → pre- soft → tide crosslinking is rolled material → moist crosslinking → and baked →；It wherein bakes and is carried out on baker, baking temperature is 120~140 DEG C, bakes 3~5min of time.The present invention creatively using being crosslinked twice, more stablize, and saves shrinking processes, reduces the production cost of fabric by the contracting of fabric water, pyrocondensation；Process will be baked to be introduced into damp crosslink finishing processing flow, shorten damp crosslink finishing stacking time 6~12 hours, more traditional tide crosslinking process reduces 20%~50% resin and catalyst amount；0.2 0.5 grades of the color-woven fabric easy-care properties of damp crosslink finishing are improved, washable 50 times, easy-care properties are at 4.0 grades or more.
Description
Technical field
The invention belongs to textile dyeing and finishing technical fields, are specifically related to a kind of damp crosslink finishing color-woven fabric easy-care properties of raising
Processing method.
Background technology
The dosage of damp crosslinked resin is high in general tide crosslink finishing processing technology and fabric needs clot to bank up 24 hours, face
The high processing costs of material, stacking time is long, and feel is partially sliding, partially hard, and sewing is not easy bonding when rolling lining secured；Traditional tide crosslink finishing
Fabric is because being that damp state is crosslinked next time, and dry anti-wrinkle effect is poor, and the present invention carries out the crosslinked technique of above-mentioned tide creative improvement,
To improve easy-care properties.
Invention content
The purpose of the present invention is overcome the deficiencies of the prior art and provide a kind of damp crosslink finishing color-woven fabric easy-care properties of raising
Processing method.This method is reliable and stable, and non-ironing rank is high, good hand touch, and more traditional tide crosslinking process reduces resin and catalyst
Dosage reduces fabric production cost.
The processing method of the present invention for improving damp crosslink finishing color-woven fabric easy-care properties, technological process are to singe → move back
Slurry → mercerising → liquefied ammonia → pre- soft → damp crosslinking is rolled material → moist crosslinking → and baked → primary washing → secondary washing → tentering
→ finished product tests dress；It wherein bakes and is carried out on baker, baking temperature is 120~140 DEG C, bakes 3~5min of time.
Wherein：
Pre- softening step carries out on stenter, and adjuvant used and dosage is：15~30g/ of water imbibition softening agent SEH-02
l；Stenter drying room temperature is 90~110 DEG C, and speed is 50~70 ms/min.
Tide crosslinking is rolled material process and is carried out on stenter, and drying room temperature is 70~110 DEG C, and cropping temperature and humidity are controlled respectively
System is between 32~40 DEG C and 6~8%；Material auxiliary agent is rolled in tide crosslinking used and dosage is：100~210g/l of Resin A MC, catalysis
Agent LRMC50~105g/l, 15~30g/l of fiber protection agent SF-P, 10~30g/l of softening agent CS-1 and bleeding agent WA-X 1
~3g/L.
Moist crosslinking process is that tide crosslinking carries out clot package when rolling material process cropping to fabric, is placed on 32~40 DEG C of perseverance
Moist crosslinking reacts 12~18 hours in warm environment.
Primary washing and secondary washing carry out on rinsing machine, and rinsing machine has 8 rinsing bowls, primary washing and secondary water
It is 60~90 DEG C to wash temperature, and when first wash, 10~25g/l of soda ash is added in first rinsing bowl.
Tentering process is adjuvant used and dosage is：20~30g/l of softening agent SMI-50；Cropping humid control is 2~5%
Between.
Singe, desizing process is moved back in burning and is carried out on combination machine, singeing fire hole is to cut burnings, and flame intensity is 12~14mbar,
Fabric carries out positive and negative and singes, positive after first reverse side；By the way of enzyme desizing, desizing enzyme dosage is 10~15g/L for desizing.
For mercerising using conventional mercerized finish, mercerising concentration of lye is 23~26 Baume degrees, the color-woven fabric pH after mercerising
Value is 6~7.
For liquid ammonia finishing using conventional liquid ammonia finishing method, speed is 40~55m/min.
The present invention creatively using being crosslinked twice, first, moist crosslinking can be such that resin reaction fills second is that dry state is crosslinked
Point, so that fabric is worn flatness effect under damp state, under dry state preferable；After being crosslinked twice, the contracting of fabric water, pyrocondensation are more
Stablize, saves shrinking processes, reduce the production cost of fabric.
Water imbibition softening agent SEH-02 used is the production of Zibo Lu Rui Fine Chemical Co., Ltd in pre- softening step, and tide is handed over
Connection rolls adjuvant used in material process：Resin A MC is high high chemical industry (China) Co., Ltd production, catalyst LRMC, fiber protection
Softening agent SMI-50 used etc. is the auspicious fine chemistry industry life in Shandong in agent SF-P, softening agent CS-1, bleeding agent WA-X and stentering forming
Production.
The invention has the advantages that：
(1) creatively using being crosslinked twice, first, moist crosslinking can make resin reaction second is that baking crosslinking under dry state
Fully, so that fabric is worn under damp state, under dry state, flatness effect is preferable, and the fabric after secondary cross-linking can be 50 times washable,
Easy-care properties are kept for 4 grades or more.
(2) process will be baked to be introduced into damp crosslink finishing processing flow, it is small to shorten damp crosslink finishing stacking time 6~12
When, more traditional tide crosslinking process reduces 20%~50% resin and catalyst amount.
(3) 0.2-0.5 grades of color-woven fabric easy-care properties for improving damp crosslink finishing, before fabric other mechanical performances qualification
It puts, easy-care properties reach current best level.
(4) it is crosslinked twice, the contracting of fabric water, pyrocondensation are more stablized, and are saved shrinking processes, are reduced the production cost of fabric.
(5) this method is reliable and stable, and non-ironing rank is high, good hand touch, and more traditional tide crosslinking process reduces resin and catalyst
Dosage reduces fabric production cost.
Specific implementation mode
The invention will be further described with reference to embodiments.
Embodiment 1
Spin color-woven fabric in blue Oxford：Two strands of pure cotton 80s are all made of through weft yarn, warp-wise density is 160 pieces/inch, latitude
It it is 72 pieces/inch to density.
Production procedure is：Singe → desizing → mercerising → liquefied ammonia → pre- is soft → tide crosslinking rolls material → moist crosslinking → and bakes
→ primary washing → secondary washing → tentering → finished product tests dress.
It singes, desizing process：It moves back in burning and is carried out on combination machine, used when singing and cut burning, flame intensity 14mbar, fabric
It carries out positive and negative to singe, positive after first reverse side, by the way of enzyme desizing, desizing enzyme dosage is 15g/L for desizing.
Mercerizing process：Using conventional mercerized finish, mercerising concentration of lye is 26 Baume degrees, the color-woven fabric pH after mercerising
Value is 6.9.
Liquefied ammonia process：Using conventional liquid ammonia finishing method, speed 40m/min.
Pre- softening step carries out on stenter, and softening agent SEH-02 dosages are 30g/l, eight drying room temperatures of stenter point
Wei not be 92 DEG C, 103 DEG C, 108 DEG C, 110 DEG C, 110 DEG C, 109 DEG C, 102 DEG C, 94 DEG C, speed is 51 ms/min.
Tide crosslinking is rolled material process and is carried out on stenter, eight drying room temperatures of stenter are respectively 81 DEG C, 93 DEG C, 109 DEG C,
110 DEG C, 110 DEG C, 108 DEG C, 101 DEG C, 79 DEG C, the control of cropping temperature is adjuvant used in 39.5 DEG C or so, humidity 7.9% or so
And dosage is：Resin A MC 210g/l, catalyst LRMC 105g/l, fiber protection agent SF-P 30g/l, the auspicious fine chemistry industry life in Shandong
Softening agent CS-1 25g/l and bleeding agent the WA-X 3g/L of production.
Moist crosslinking process is that tide crosslinking carries out clot package when rolling material process cropping to fabric, is placed on 40 DEG C of constant temperature ring
Moist crosslinking reacts 18 hours in border.
Tide crosslinking carries out baking dry state crosslinking after rolling material, moist crosslinking, bakes actual temperature between 139 ± 1 DEG C, bakes
Time 3min.
Primary washing and secondary washing carry out on rinsing machine, and rinsing machine has 8 rinsing bowls, primary washing and secondary water
It is 78~90 DEG C to wash temperature, and when first wash, soda ash 25g/l is added in first rinsing bowl.
Softening agent SMI-50 30g/l are added when stentering forming, cropping humid control is 4.5% or so.
The test result of finished fabric is：Easy-care properties (AATCC124 methods) are improved by 3.7 grades of former conventional damp crosslinking process
To 4.2 grades, 4 grades of easy-care properties after washing 50 times；Creasy recovery angle is improved by 247 ° of former conventional damp crosslinking process to 263.0 °；Contracting
For water in 0~-1.2%, difference is little；Ultimate strength, Tear strength, color are little with common process difference；Fabric hand
Sense is with common process ratio, and thick and solid fluffy sense is slightly good, and less sliding, skin-friendly is good；It is secured that fitting lining tests more conventional technique.
Embodiment 2
The thin Blue Streak plain weave color-woven fabric of white background：Warp-wise uses pure cotton 40s yarns, broadwise to use pure cotton 30s yarns, and warp-wise density is
120 pieces/inch, latitudinal density is 65 pieces/inch.
Production procedure is：Singe → desizing → mercerising → liquefied ammonia → pre- is soft → tide crosslinking rolls material → moist crosslinking → and bakes
→ primary washing → secondary washing → tentering → finished product tests dress.
It singes, desizing process：It moves back in burning and is carried out on combination machine, used when singing and cut burning, flame intensity 12mbar, fabric
It carries out positive and negative to singe, positive after first reverse side, by the way of enzyme desizing, desizing enzyme dosage is 10g/L for desizing.
Mercerizing process：Using conventional mercerized finish, mercerising concentration of lye is 24 Baume degrees, the color-woven fabric pH after mercerising
Value is 6.1.
Liquefied ammonia process：Using conventional liquid ammonia finishing method, speed 55m/min.
Pre- softening step carries out on stenter, and softening agent SEH-02 dosages are 15g/l, and eight drying room temperatures of stenter are
90 DEG C, 101 DEG C, 105 DEG C, 107 DEG C, 110 DEG C, 106 DEG C, 100 DEG C, 91 DEG C, speed is 70 ms/min.
Tide crosslinking is rolled material process and is carried out on stenter, eight drying room temperatures of stenter are respectively 70 DEG C, 83 DEG C, 100 DEG C,
105 DEG C, 105 DEG C, 101 DEG C, 95 DEG C, 74 DEG C, cropping temperature is controlled in 32.3 DEG C, humidity 6%, and adjuvant used and dosage is：Tree
The softening agent that fat AMC 100g/l, catalyst LRMC 50g/l, fiber protection agent SF-P 15g/l, the auspicious fine chemistry industry in Shandong produce
CS-110g/l and bleeding agent WA-X 1g/L.
Moist crosslinking process is that tide crosslinking carries out clot package when rolling material process cropping to fabric, is placed on 32.5 DEG C of constant temperature
Moist crosslinking reacts 12 hours in environment.
Tide crosslinking roll material, moist crosslinking after baked, bake actual temperature be 120 DEG C between, bake time 5min.
Primary washing and secondary washing carry out on rinsing machine, and rinsing machine has 8 rinsing bowls, primary washing and secondary water
It is 60~85 DEG C to wash temperature, and when first wash, soda ash 10g/l is added in first rinsing bowl.
Softening agent SMI-50 20g/l are added when stentering forming, cropping humid control is 2% or so.
The test result of finished fabric is：Easy-care properties (AATCC124 methods) are improved by 3.5 grades of former conventional damp crosslinking process
To 4.0 grades, 4 grades are still kept after 50 washings；Creasy recovery angle is improved by 239 ° of former conventional damp crosslinking process to 247.0 °；Contracting
For water in 0~-0.8%, difference is little；Ultimate strength, Tear strength, color are little with common process difference；Fabric hand
Sense is with common process ratio, and less sliding, pliability, skin-friendly are good, and it is secured to glue lining.
Embodiment 3
2/1 twill color-woven fabric of small purple grid：Warp-wise uses pure cotton 50s yarns, broadwise to use two stock yarns of pure cotton 100s, warp
It it is 140 pieces/inch to density, latitudinal density is 90 pieces/inch.
Production procedure is：Singe → desizing → mercerising → liquefied ammonia → pre- is soft → tide crosslinking rolls material → moist crosslinking → and bakes
→ primary washing → secondary washing → tentering → finished product tests dress.
It singes, desizing process：It moves back in burning and is carried out on combination machine, used when singing and cut burning, flame intensity 13mbar, fabric
It carries out positive and negative to singe, positive after first reverse side, by the way of enzyme desizing, desizing enzyme dosage is 12g/L for desizing.
Mercerizing process：Using conventional mercerized finish, mercerising concentration of lye is 23 Baume degrees, the color-woven fabric pH after mercerising
Value is 6.3.
Liquefied ammonia process：Using conventional liquid ammonia finishing method, speed 50m/min.
Pre- softening step carries out on stenter, and softening agent SEH-02 dosages are 20g/l, and eight drying room temperatures of stenter are
93 DEG C, 102 DEG C, 105 DEG C, 106 DEG C, 108 DEG C, 108 DEG C, 102 DEG C, 92 DEG C, speed is 65 ms/min.
Tide crosslinking is rolled material process and is carried out on stenter, eight drying room temperatures of stenter are respectively 72 DEG C, 87 DEG C, 102 DEG C,
108 DEG C, 110 DEG C, 106 DEG C, 92 DEG C, 71 DEG C, cropping temperature is controlled in 35 DEG C, humidity 6.8%, and adjuvant used and dosage is：Tree
The softening agent that fat AMC 130g/l, catalyst LRMC 65g/l, fiber protection agent SF-P 20g/l, the auspicious fine chemistry industry in Shandong produce
CS-1 15g/l and bleeding agent WA-X 2g/L.
Moist crosslinking process is that tide crosslinking carries out clot package when rolling material process cropping to fabric, is placed on 35 DEG C of constant temperature ring
Moist crosslinking reacts 15 hours in border.
Tide crosslinking roll material, moist crosslinking after baked, bake actual temperature be 130 DEG C between, bake time 4min.
Primary washing and secondary washing carry out on rinsing machine, and rinsing machine has 8 rinsing bowls, primary washing and secondary water
It is 65~80 DEG C to wash temperature, and when first wash, soda ash 15g/l is added in first rinsing bowl.
Softening agent SMI-50 is added when stentering forming, dosage 25g/l, cropping humid control is 2.5% or so.
The test result of finished fabric is：Easy-care properties (AATCC124 methods) are improved by 3.8 grades of former conventional damp crosslinking process
To 4.0 grades, 4.0 grades are still kept after 50 washings；Creasy recovery angle is improved by 243 ° of former conventional damp crosslinking process to 251 °；Contracting
For water in 0~-1.2%, difference is little；Ultimate strength, Tear strength, color are little with common process difference；Fabric hand
Sense is with common process ratio, and less sliding, pliability and skin-friendly are good；It is secured that fitting lining tests more conventional technique.
Claims (6)
1. a kind of processing method improving damp crosslink finishing color-woven fabric easy-care properties, it is characterised in that：Technological process be singe →
Desizing → mercerising → liquefied ammonia → pre- soft → tide crosslinking rolls material → moist crosslinking → and bakes → once washing → secondary washing → drawing
Width → finished product tests dress；It wherein bakes and is carried out on baker, baking temperature is 120~140 DEG C, bakes 3~5min of time.
2. the processing method according to claim 1 for improving damp crosslink finishing color-woven fabric easy-care properties, it is characterised in that：In advance
Softening step carries out on stenter, and adjuvant used and dosage is：15~30g/l of water imbibition softening agent SEH-02；Stenter dries
Room temperature is 90~110 DEG C, and speed is 50~70 ms/min.
3. the processing method according to claim 1 for improving damp crosslink finishing color-woven fabric easy-care properties, it is characterised in that：Tide
Crosslinking is rolled material process and is carried out on stenter, and drying room temperature is 70~110 DEG C, and cropping temperature and humidity are controlled respectively 32~40
DEG C and 6~8% between；Material auxiliary agent is rolled in tide crosslinking used and dosage is：100~210g/l of Resin A MC, catalyst LRMC 50~
105g/l, 1~3g/L of 15~30g/l of fiber protection agent SF-P, 10~30g/l of softening agent CS-1 and bleeding agent WA-X.
4. the processing method according to claim 1 for improving damp crosslink finishing color-woven fabric easy-care properties, it is characterised in that：Tide
State cross-linking process step is that tide crosslinking carries out clot package when rolling material process cropping to fabric, is placed in 32~40 DEG C of isoperibol damp
State cross-linking reaction 12~18 hours.
5. the processing method according to claim 1 for improving damp crosslink finishing color-woven fabric easy-care properties, it is characterised in that：One
Secondary washing and secondary washing carry out on rinsing machine, and rinsing machine has 8 rinsing bowls, and primary washing and secondary washing temperature are
60~90 DEG C, when first wash, 10~25g/l of soda ash is added in first rinsing bowl.
6. the processing method according to claim 1 for improving damp crosslink finishing color-woven fabric easy-care properties, it is characterised in that：It draws
Width process is adjuvant used and dosage is：20~30g/l of softening agent SMI-50；Cropping humid control is between 2~5%.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112900074B (en) * | 2021-02-09 | 2023-01-31 | 广东溢达纺织有限公司 | Non-ironing cotton fabric and preparation method and application thereof |
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| CN113235292A (en) * | 2021-06-28 | 2021-08-10 | 江南大学 | Delayed baking non-ironing finishing process for cotton fabric |
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