CN108456592A - A kind of extracting method of Antrodia camphorata essential oil and its application in cosmetics - Google Patents
A kind of extracting method of Antrodia camphorata essential oil and its application in cosmetics Download PDFInfo
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- CN108456592A CN108456592A CN201810139671.4A CN201810139671A CN108456592A CN 108456592 A CN108456592 A CN 108456592A CN 201810139671 A CN201810139671 A CN 201810139671A CN 108456592 A CN108456592 A CN 108456592A
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- antrodia camphorata
- essential oil
- extracting method
- chinese medicine
- treatment fluid
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses a kind of extracting methods of Antrodia camphorata essential oil, first crush Antrodia camphorata by Universalpulverizer, are then impregnated with Chinese medicine treatment fluid, finally obtain essential oil using supercritical fluid extraction；The technique of the present invention is on traditional Process ba- sis, add the step of Chinese medicine treatment fluid impregnates, and process many experiments have chosen paper mulberry juice and two Chinese medicine of safflower is used cooperatively, the essential oil of preparation is applied in cosmetics, not only have and go acne, antipruritic and other effects, is also equipped with whitening, antianaphylactic effect.
Description
Technical field
The present invention relates to the extracting method of technical field of plant extraction more particularly to a kind of Antrodia camphorata essential oil and its making up
Application in product.
Background technology
Antrodia camphorata also known as cinnamomum kanahirai hay mushroom, belong to Aphyllophorales, Polyporaceae, antrodia karst, perennial gill fungus mushroom, and Latin is entitled
Antrodia camphorata are the novel species just delivered by biochemical boundary nineteen ninety.Growth region is TaiWan, China mountain area height above sea level
Between 450-2000 meters of mountain forests, it is only grown in the rotten heartwood inner wall of the cinnamomum kanehirai trunk of peculiar a century of TaiWan, China or more, camphor tree
Timber moist surface, because its acquisition is not easy, the social event of illegal mining Antrodia camphorata still when have what is heard.
Antrodia camphorata was the distinctive fungi of TaiWan, China in the past, was only grow in the distinctive cinnamomum kanehirai of TaiWan, China.Wild ox
Antrodia is the insular child care class seeds of TaiWan, China, and more than 100 strain oxen are given birth in the snow mountain hole Cinnamomum kanahirai hay protection zone in big Anxi upstream
Camphor tree forest.Antrodia camphorata is the unique weeping fungus found in cinnamomum kanehirai, but the parasitic pathogenic of Antrodia camphorata is not strong, therefore Cinnamomum kanahirai hay
Tree is seldom dead, can grow centuries.Wild Cinnamomum kanahirai hay ganoderma lucidum is uniquely rely, and the host to make a living ----TaiWan, China cinnamomum kanehirai is taken a broad view
The whole world, is only grown on the mountain area of 450 to 2000 meters of TaiWan, China height above sea level, and Cinnamomum kanahirai hay ganoderma lucidum is only grow on the rotten inner wall of cinnamomum kanehirai
Middle vacancy or the dark moist surface of the cinnamomum kanehirai fallen of withered volt, quantity is very rare, and the speed of growth is very slow, often
Year only several centimeters of growth thickness.Due to rare numbers, acquisition is not easy, and market price is up to the hundreds thousand of New Taiwan Currencies of every jin, value
It much outmatches on the rare medicinal herbs such as ganoderma lucidum, ginseng, cordyceps sinensis, the king being referred to as in the king in medicinal material.
The mystery of Cinnamomum kanahirai hay ganoderma lucidum is early be it is wide-spread in the aboriginal clan of TaiWan, China mountainous region, in early days by mountainous region aboriginal in
Wild Antrodia camphorata is found unintentionally, realizes that not only spirit and QI cleaning, spirit improve, feeling of fatigue disappears immediately after edible, muscle power
Enhancing is many, successively there are many magical witness is found with clansman, so for many years, Cinnamomum kanahirai hay ganoderma lucidum is considered as mysterious spirit handed down from one's ancestors
Medicine.
Antrodia camphorata is grown on the moist surface of the rotten hollow inside of cinnamomum kanehirai dry rot or the trunk that lodges.Wild Antrodia camphorata is grown
Aged cinnamomum kanehirai, sporophore shape changeableization have plate, clock shape, horse-hof shape or tower-like；Nascent cerise is gradually long to become
It is white, reddish tan, filbert or khaki.Antrodia camphorata gas fragranced is arduous, flat.There is wind-dispelling promoting the circulation of qi, change become silted up promoting blood circulation, middle benefit gas
Disappear knot, removing toxicity for detumescence, sedation-analgesia, antibacterial, antiviral and antitumor, promoted immunity of organisms the benefits of；For treatment stomach and intestine pain
Bitterly, diarrhea and vomiting, food poisoning, mushroom poisoning, diabetes, alcoholic liver, fatty liver, hepatic sclerosis, liver cancer etc. are even more to have unique work(
Energy.Antrodia camphorata be there are many physiologically active ingredient, such as polysaccharide body, triterpene compound, Sudismase, adenosine, protein
(containing immune protein), vitamin, trace element, nucleic acid, agglutinin, amino acid, solid liquor-saturated tired, cellulose, blood pressure stabilization substance etc..
With triterpene compound for most especially, up to 200 kinds or more, which are other mushrooms, to compare in the active ingredient of Antrodia camphorata,
More than 200 kinds of triterpene compound makes Antrodia camphorata have anticancer, liver protection and other effects.Due to antrodia TaiWan, China be considered as it is unique and
Precious medicinal fungi, therefore there is high research and commercial value, and the wild fungi of TaiWan, China most expensive at present.
Chinese invention patent CN104856925A disclose it is a kind of going acne essence rich in Antrodia camphorata extract, which exists
Vitamin C, tartaric acid and Rosa Damascana are added on the basis of Antrodia camphorata extract, to going acne to have good effect after use；But
This method is only extracted Antrodia camphorata using common hot extraction process, fails further to play work of the Antrodia camphorata in beauty
With；Therefore it is necessary to carry out deep extraction to Antrodia camphorata, to develop its new effect.
Invention content
Technical problems based on background technology, the present invention propose a kind of extracting method of Antrodia camphorata essential oil.
Technical scheme is as follows：
A kind of extracting method of Antrodia camphorata essential oil, includes the following steps：
A, it after Antrodia camphorata appearance being cleaned up and dried, is crushed, and is sieved by high speed Universal pulverizer, obtained
Bacterium powder；
B, bacterium powder is weighed, is put into Chinese medicine treatment fluid and impregnates 15-24h, then concentrated and be spray-dried, obtains pre- place
Manage powder；
C, the pretreatment powder weighed up is fitted into supercritical fluid extraction kettle, adjusts suitable extraction parameters, obtains Cinnamomum kanahirai hay
Sesame essential oil.
Preferably, in the step A, 325-800 mesh sieve is crossed.
Preferably, the traditional Chinese medicine ingredients of the Chinese medicine treatment fluid are paper mulberry juice and safflower.
Preferably, the safflower is the xanthorrhiza below safflower red column cap.
Preferably, the Chinese medicine treatment fluid, includes the ingredient of following weight percent：
Safflower 2-5%
Paper mulberry juice 3-8%
Water surplus.
Preferably, in the step B, the weight ratio of bacterium powder and Chinese medicine treatment fluid is 1：(10-25).
Preferably, the extraction parameters are：Extracting pressure is 35-45MPa, 45-55 DEG C of extraction temperature, and extraction time is
60-80min。
Paper mulberry juice, also known as small paper mulberry juice, Chinese medicine name.For the small paper mulberry Broussonetia kaempferi of moraceae plants
Sieb. myron.It is distributed in various regions and Shaanxi on the south the middle and lower reach of Yangtze River.With dispelling wind and arresting itching, it is clearing heat and detoxicating the effect of.For skin
Inflammation, mange, snakeworm dog sting.
Safron (scientific name：Crocus sativus L.) it is also known as safflower, west safflower, it is a kind of Iridaceae crocus
Flowering perennial and a kind of common fragrance.Perennial herb.The oblate spherical shape of bulb, about 3 centimetres of diameter, has yellowish-brown outside
The film quality of color is coated with.Phyllopodium gives birth to, 9-15 pieces, bar shaped, celadon, edge warp；Leafage base portion is surrounded by the sheath shape of 4-5 piece film quality
Leaf.Scape is very short, does not elevate above the soil；1-2, flower, light blue, reddish violet or white, savory, style is orange red, and column cap omits
Flat, top wedge shape has shallow tooth, the narrow spindle of ovary.Capsule ellipse, is about 3 centimetres.
It is Asia west and south initial species, earliest by Greek's artificial cultivation.It is mainly distributed on Europe, Mediterranean and Central Asia etc.
Ground, incoming China when the Ming Dynasty,《Compendium of Materia Medica》It is included in drug etc, there is plantation on the ground such as Zhejiang Province, China.It is a kind of rare
There is Chinese medicine powerful physiological activity, column cap as medicinal, to have calmness, eliminating the phlegm, spasmolysis, use in Asia and Europe
In the treatment of stomach trouble, menstruation regulating, measles, fever, jaundice, hepatosplenomegaly etc..
The present invention substitutes red column cap using the xanthorrhiza below safflower red column cap, several by repeatedly testing discovery
Can be with red column cap the effect of, is suitable, significantly reduces cost.
The invention has the beneficial effects that：The extracting method of the Antrodia camphorata essential oil of the present invention, passes through ten thousand by Antrodia camphorata first
Energy pulverizer crushes, and is then impregnated with Chinese medicine treatment fluid, finally obtains essential oil using supercritical fluid extraction；This
The technique of invention adds the step of Chinese medicine treatment fluid impregnates, and have chosen by many experiments on traditional Process ba- sis
Paper mulberry juice and two Chinese medicine of safflower are used cooperatively, and the essential oil of preparation is applied in cosmetics, are not only had and are removed the work(such as acne, antipruritic
Effect, is also equipped with whitening, antianaphylactic effect.
Specific implementation mode
Embodiment 1：
A kind of extracting method of Antrodia camphorata essential oil, includes the following steps：
A, it after Antrodia camphorata appearance being cleaned up and dried, is crushed, and is sieved by high speed Universal pulverizer, obtained
Bacterium powder；
B, bacterium powder is weighed, is put into Chinese medicine treatment fluid and impregnates 18h, then concentrated and be spray-dried, pre-processed
Powder；
C, the pretreatment powder weighed up is fitted into supercritical fluid extraction kettle, adjusts suitable extraction parameters, obtains Cinnamomum kanahirai hay
Sesame essential oil.
In the step A, 500 mesh sieve is crossed.
The traditional Chinese medicine ingredients of the Chinese medicine treatment fluid are paper mulberry juice and safflower.
The safflower is the xanthorrhiza below safflower red column cap.
The Chinese medicine treatment fluid, includes the ingredient of following weight percent：
Safflower 3%
Paper mulberry juice 5%
Water surplus.
In the step B, the weight ratio of bacterium powder and Chinese medicine treatment fluid is 1：15.
The extraction parameters are：Extracting pressure is 38MPa, 50 DEG C of extraction temperature, extraction time 75min.
Embodiment 2：
A kind of extracting method of Antrodia camphorata essential oil, includes the following steps：
A, it after Antrodia camphorata appearance being cleaned up and dried, is crushed, and is sieved by high speed Universal pulverizer, obtained
Bacterium powder；
B, bacterium powder is weighed, is put into Chinese medicine treatment fluid and impregnates 15h, then concentrated and be spray-dried, pre-processed
Powder；
C, the pretreatment powder weighed up is fitted into supercritical fluid extraction kettle, adjusts suitable extraction parameters, obtains Cinnamomum kanahirai hay
Sesame essential oil.
In the step A, 800 mesh sieve is crossed.
The traditional Chinese medicine ingredients of the Chinese medicine treatment fluid are paper mulberry juice and safflower.
The safflower is the xanthorrhiza below safflower red column cap.
The Chinese medicine treatment fluid, includes the ingredient of following weight percent：
Safflower 2%
Paper mulberry juice 8%
Water surplus.
In the step B, the weight ratio of bacterium powder and Chinese medicine treatment fluid is 1：10.
The extraction parameters are：Extracting pressure is 45MPa, 45 DEG C of extraction temperature, extraction time 80min.
Embodiment 3：
A kind of extracting method of Antrodia camphorata essential oil, includes the following steps：
A, it after Antrodia camphorata appearance being cleaned up and dried, is crushed, and is sieved by high speed Universal pulverizer, obtained
Bacterium powder；
B, bacterium powder is weighed, is put into Chinese medicine treatment fluid and impregnates 15-24h, then concentrated and be spray-dried, obtains pre- place
Manage powder；
C, the pretreatment powder weighed up is fitted into supercritical fluid extraction kettle, adjusts suitable extraction parameters, obtains Cinnamomum kanahirai hay
Sesame essential oil.
In the step A, 325 mesh sieve is crossed.
The traditional Chinese medicine ingredients of the Chinese medicine treatment fluid are paper mulberry juice and safflower.
The safflower is the xanthorrhiza below safflower red column cap.
The Chinese medicine treatment fluid, includes the ingredient of following weight percent：
Safflower 5%
Paper mulberry juice 3%
Water surplus.
In the step B, the weight ratio of bacterium powder and Chinese medicine treatment fluid is 1：25.
The extraction parameters are：Extracting pressure is 35MPa, 55 DEG C of extraction temperature, extraction time 60min.
Comparative example 1
Safflower in embodiment 1 is replaced with into safflower red column cap.
Comparative example 2
Chinese medicine treatment fluid immersion in embodiment 1 is replaced with pure water to impregnate.
Application examples
The essential oil smaple of 1-3 of the embodiment of the present invention and comparative example 1-2 are carried out using test below, by the essential oil of the present invention
It is added in facial mask with 2% ratio, tests using effect.
Test method：Each embodiment selects face that there is the patient 25 of allergic symptom to test respectively, takes implementation
3 bags of facial mask obtained by example 1-3 and comparative example 1-2, the next day after early, evening is respectively washed one's face with warm water sample be applied to face
Portion 15min, then washed one's face with warm water, it repeats above operation.
Experiment is checked that statistics recovery from illness, effective, improvement, invalid sufferer number calculate its total effective rate after 20 days
(%).Curative effect determinate standard：1. fully recovering:Naked eyes regard allergy area recession >=90%；2. effective:Naked eyes regard allergy area and subside
>=60%；3. improving:Naked eyes regard allergy area recession >=30%；4. invalid:Naked eyes regard allergy area recession ＜ 30%.
Test result is shown in Table 1：
Table 1：Therapeutic effect of the essential oil smaple to autopath
By the above test data it is recognised that after the immersion of Chinese medicine treatment fluid, therapeutic effect is good very much, and uses safranine
Xanthorrhiza below premium color column cap and safflower red column cap, curative effect difference are little.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (8)
1. a kind of extracting method of Antrodia camphorata essential oil, which is characterized in that include the following steps：
A, it after Antrodia camphorata appearance being cleaned up and dried, is crushed, and is sieved by high speed Universal pulverizer, obtain bacterium
Powder；
B, bacterium powder is weighed, is put into Chinese medicine treatment fluid and impregnates 15-24h, then concentrated and be spray-dried, pre-processed
Powder；
C, the pretreatment powder weighed up is fitted into supercritical fluid extraction kettle, adjusts suitable extraction parameters, obtain Antrodia camphorata essence
Oil.
2. the extracting method of Antrodia camphorata essential oil as described in claim 1, which is characterized in that in the step A, cross 325-
800 mesh sieve.
3. the extracting method of Antrodia camphorata essential oil as described in claim 1, which is characterized in that the Chinese medicine of the Chinese medicine treatment fluid
Ingredient is paper mulberry juice and safflower.
4. the extracting method of Antrodia camphorata essential oil as claimed in claim 3, which is characterized in that the safflower is safranine premium
Xanthorrhiza below color column cap.
5. the extracting method of Antrodia camphorata essential oil as claimed in claim 3, which is characterized in that the Chinese medicine treatment fluid, including
The ingredient of following weight percent：
Safflower 2-5%
Paper mulberry juice 3-8%
Water surplus.
6. the extracting method of Antrodia camphorata essential oil as described in claim 1, which is characterized in that in the step B, bacterium powder is in
The weight ratio of medicine treatment fluid is 1: (10-25).
7. the extracting method of Antrodia camphorata essential oil as described in claim 1, which is characterized in that the extraction parameters are：Extraction
Pressure is 35-45MPa, 45-55 DEG C of extraction temperature, extraction time 60-80min.
8. the extracting method of Antrodia camphorata essential oil as described in claim 1, which is characterized in that the essential oil can be applied to cosmetics,
There are acne, antipruritic, whitening and antianaphylactic effect.
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| CN201810139671.4A CN108456592A (en) | 2018-02-09 | 2018-02-09 | A kind of extracting method of Antrodia camphorata essential oil and its application in cosmetics |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112322392A (en) * | 2020-10-29 | 2021-02-05 | 湖南观芝茬牛樟芝生物科技有限公司 | Method for extracting antrodia camphorata essential oil |
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