CN107216948A - A kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil and its application - Google Patents
A kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil and its application Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/43—Addition of vegetable fats or oils; Addition of non-meat animal fats or oils; Addition of fatty acids
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Abstract
It is Albatrellus dispansus (Lloyd) Canf. ＆ Gilb method of extraction of essential oil present invention firstly discloses a kind of edible mushroom, processing including raw material, Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder is extracted using supercritical fluid extraction, and the reception of extraction product, one kind is finally given to give off a strong fragrance, it is bright, the essential oil with anti-oxidant and reduction natrium nitrosum active function Albatrellus dispansus (Lloyd) Canf. ＆ Gilb local flavor.The Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil obtained by supercritical liquid extraction technique is different from the essential oil that conventional method such as solvent extraction method is extracted, without dissolvent residual, purity is higher and quality better, fragrance is stronger, new preservative and natural flavouring can be used as, it is added to meat products or a ball is made, develops new product.Meanwhile, because Albatrellus dispansus (Lloyd) Canf. ＆ Gilb have it is anti-oxidant, improve immunity the effects such as, Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil can also be promoted as health products, met the green and healthy food idea that modern is pursued, reached limited resources high-value-use.
Description
Technical field
The present invention relates to extraction of essential oil technical field, the extracting method of more particularly to a kind of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil and its should
With.
Background technology
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb, also referred to as Sarcodon imbricatus (L. Ex Franch.) Karst, belong to fungus circle, Basidiomycota, agaric guiding principle, lead fungi mesh, slope Salmonella section.It is wild
The decorative pattern of the raw Albatrellus dispansus (Lloyd) Canf. ＆ Gilb fine hair very thin because its outward appearance uniqueness, uncovered stockless, phage surface have and black, exactly like the tiger palm thus obtain
Name.Albatrellus dispansus (Lloyd) Canf. ＆ Gilb can substantially be divided into HEIHUZHANG fungus, Polyporus ellissi (yellow Albatrellus dispansus (Lloyd) Canf. ＆ Gilb), Albatrellus dispansus (Lloyd) Canf. ＆ Gilb.China be mainly distributed on Sichuan,
The ground such as Yunnan, Gansu.There are Chuxiong, Lijing etc. in the main place of production in Yunnan.Because its harvesting is difficult, and yield is few, therefore more precious.China
The traditional Chinese medical science thinks that Albatrellus dispansus (Lloyd) Canf. ＆ Gilb is good Chinese medicine, its flat property and sweet taste, dehumidifying of dispeling cold, promoting blood circulation and removing blood stasis, supplementing qi and nourishing yin, ease constipation simply
The effects such as defaecation.Albatrellus dispansus (Lloyd) Canf. ＆ Gilb can also reduce Blood Cholesterol, cancer-preventing health etc..Research shows wild Albatrellus dispansus (Lloyd) Canf. ＆ Gilb to small white mouse meat
The inhibiting rate of knurl 180 is up to 96.8%.Modern medicine thinks that it can improve immune function of human body simultaneously, low fat, low cholesterol,
The advantages of low heat value, becomes one of natural diet food and preferable health food.
Essential oil, in being the flower from plant, leaf, stem, root or fruit, passes through steam distillation, extrusion, cold-maceration or molten
Agent extraction method refines the volatile flavor of extraction.Essential oil has lipophilicity, it is easy to be dissolved in grease.Essential oil is by terpenes
The chemical moleculars such as class, aldehydes, esters, alcohols are constituted.
Supercritical liquid extraction technique, is one and have developed rapidly, using very wide practicality new technology, especially from natural
Some valuable bioactive substances are extracted in animals and plants, big advantage is shown.It is easy to separate with product, safety
Nontoxic, operation does not gently destroy active ingredient.The technology has been used successfully to the flavor substances such as essential oil in hops extraction, plant
The extraction of matter, various aliphatic acid are extracted from animal oil, medicinal ingredient is extracted from natural products, extract total from soil the inside
Hydrocarbon, organic matter etc. is extracted from soil the inside.Fragrance can be not only efficiently extracted with supercritical fluid extraction extraction spices
Component, but also product purity can be improved, its natural flavor can be kept, such as from sweet osmanthus, Jasmine, chrysanthemum, plum blossom, Milan
Flower, extract extrait in rose, spice extracted from pepper, Chinese cassia tree, peppermint, from celery seed, ginger, tabernaemontanus bulrush ginger seed, Miao Xiang,
Essential oil is extracted in the raw materials such as fructus amomi, anise, cumin, flavoring is served not only as, and some essential oils are also with higher
Medical value.
At present, any technology on being carried out extraction of essential oil using Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and exploitation one are not disclosed also both at home and abroad
Plant with anti-oxidant, removing nitrous, natural free of contamination essential oil product and the relevant report of application.
The content of the invention
In order to solve the above technical problems, the present invention provides a kind of unique flavor, extraction yield is high, purity height is pollution-free, and
And the extracting method with the pure natural Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil of function such as anti-oxidant and its application.
A kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, comprises the following steps：
(1) preparation of raw material：Select without mildew and rot dry tiger palm bacteria, the dust in Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and other magazine particles are removed
Go, crushed from high speed Universal pulverizer, cross 40 mesh sieves, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder, weighed with electronic balance, vacuum
It is standby after packaging；
(2) Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder is extracted using supercritical fluid extraction：
(3) reception of product is extracted：Take sample to carry out receiving extraction product with 50mL brown, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essence
Oil, volatilization is sealed against by sealed membrane.
It is preferred that, the extraction procedure in step (2) is as follows：
A, weigh Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder and be encased in the extraction kettle of equipment；
B, switch on power, set gradually extraction parameters, extracting pressure 25-35MPa, 50-60 DEG C of extraction temperature, separating pressure
5-10MPa and during 20-30 DEG C of separation temperature, according to flow, opens extraction kettle, the heater switch of separator at different levels, opens simultaneously
Refrigeration switch, adjusts respective temperature controller to designated value；
C, near 5-8 DEG C when refrigerator temps, and extraction kettle, separator at different levels temperature close to setting value and it is stable when,
Main pump is opened, the air in extract and separate system is removed and then boosts to extracting pressure, by adjusting extraction kettle and separator
Gases at high pressure choke valve, makes each kettle reach set point pressure and CO2Flow is reached close to setting value；
D, machine start automatic running, after certain time, obtain extracting product i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil；
E, shutdown, first close main pump, then the intake valve of extraction kettle is closed, and simultaneously close off various heat cycles switches,
Turn off in total power switch, kettle to be extracted after the pressure balance such as pressure and separators at different levels, closing separator return valve is opened
Vent valve carries out deflation release.
It is preferred that, described Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil can apply to ham or a local flavor ball.
It is preferred that, the method that described Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil is applied to ham comprises the following steps：Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil concentration is
6-8%, is uniformly applied to meat products surface, fully absorbs it, then carries out pickling air-dried drying, you can.
It is preferred that, the method that described Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil is applied to a local flavor ball comprises the following steps：Pork is diced and put
Enter to cut in cutmixer and mix, cut mix during add the auxiliary material containing Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil and cut and mix auxiliary agent, raw material is mixed and quiet
Postpone, be put into mould shape, boiling water and cook, you can.
Beneficial effects of the present invention are compared with prior art：It is Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essence present invention firstly discloses a kind of edible mushroom
Oil extract method, includes the processing of raw material, and Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder is extracted using supercritical fluid extraction, and extraction product
Reception, finally give one kind and give off a strong fragrance, it is bright, with it is anti-oxidant and reduction natrium nitrosum active function Albatrellus dispansus (Lloyd) Canf. ＆ Gilb
The essential oil of local flavor.The Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil obtained by supercritical liquid extraction technique is carried different from conventional method such as solvent extraction method
The essential oil taken, without dissolvent residual, purity is higher and quality better, and fragrance is stronger, can be as new preservative and natural
Flavor enhancement, is added to meat products or a ball is made, develop new product.Meanwhile, because there is Albatrellus dispansus (Lloyd) Canf. ＆ Gilb anti-oxidant, raising to exempt from
The effects such as epidemic disease power, Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil can also be promoted as health products.Meet the green and healthy food sight that modern is pursued
Read, reached limited resources high-value-use.
Embodiment
With reference to embodiment, the embodiment to the present invention is described in further detail.Following examples are used for
Illustrate the present invention, but be not limited to the scope of the present invention.
Embodiment 1
A kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, comprises the following steps：
(1) preparation of raw material：Select without mildew and rot dry tiger palm bacteria, the dust in Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and other magazine particles are removed
Go, crushed from high speed Universal pulverizer, cross 40 mesh sieves, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder, weighed with electronic balance, vacuum
It is standby after packaging；
(2) extraction of supercritical fluid extraction machine：
A, the Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder for weighing 800g are encased in the extraction kettle of equipment
B, switch on power, set gradually extraction parameters, extracting pressure 30MPa, 55 DEG C of extraction temperature, separating pressure 8MPa and
During 25 DEG C of separation temperature, according to flow, extraction kettle, the heater switch of separator at different levels are opened, while opening refrigeration switch, regulation
Respective temperature controller is to designated value.
C, when near 6 DEG C or so of refrigerator temps, and extraction kettle, separator at different levels temperature close to setting value and stably
When, main pump is opened, the air in extract and separate system is removed and then boosts to extracting pressure, by adjusting extraction kettle and separator
Gases at high pressure choke valve, each kettle is reached set point pressure and CO2Flow is reached close to setting value.
D, machine start automatic running, after certain time, obtain extracting product i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil.
E, shutdown, first close main pump, then the intake valve of extraction kettle is closed, and simultaneously close off various heat cycles switches,
Turn off in total power switch, kettle to be extracted after the pressure balance such as pressure and separators at different levels, closing separator return valve is opened
Vent valve carries out deflation release.
(3) reception of product is extracted
Sample is taken to carry out receiving extraction product, i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil with 50mL brown.By sealed membrane sealed with
Volatilization prevention.
Embodiment 2
A kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, comprises the following steps：
(1) preparation of raw material：Select without mildew and rot dry tiger palm bacteria, the dust in Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and other magazine particles are removed
Go, crushed from high speed Universal pulverizer, cross 40 mesh sieves, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder, weighed with electronic balance, vacuum
It is standby after packaging；
(2) extraction of supercritical fluid extraction machine：
A, the Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder for weighing 800g are encased in the extraction kettle of equipment
B, switch on power, set gradually extraction parameters, extracting pressure 35MPa, 50 DEG C of extraction temperature, separating pressure 10MPa
And during 20 DEG C of separation temperature, according to flow, extraction kettle, the heater switch of separator at different levels are opened, while opening refrigeration switch, adjust
Respective temperature controller is saved to designated value.
C, when near 8 DEG C or so of refrigerator temps, and extraction kettle, separator at different levels temperature close to setting value and stably
When, main pump is opened, the air in extract and separate system is removed and then boosts to extracting pressure, by adjusting extraction kettle and separator
Gases at high pressure choke valve, each kettle is reached set point pressure and CO2Flow is reached close to setting value.
D, machine start automatic running, after certain time, obtain extracting product i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil.
E, shutdown, first close main pump, then the intake valve of extraction kettle is closed, and simultaneously close off various heat cycles switches,
Turn off in total power switch, kettle to be extracted after the pressure balance such as pressure and separators at different levels, closing separator return valve is opened
Vent valve carries out deflation release.
(3) reception of product is extracted
Sample is taken to carry out receiving extraction product, i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil with 50mL brown.By sealed membrane sealed with
Volatilization prevention.
Embodiment 3
A kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, comprises the following steps：
(1) preparation of raw material：Select without mildew and rot dry tiger palm bacteria, the dust in Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and other magazine particles are removed
Go, crushed from high speed Universal pulverizer, cross 40 mesh sieves, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder, weighed with electronic balance, vacuum
It is standby after packaging；
(2) extraction of supercritical fluid extraction machine：
A, the Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder for weighing 800g are encased in the extraction kettle of equipment
B, switch on power, set gradually extraction parameters, extracting pressure 25MPa, 60 DEG C of extraction temperature, separating pressure 6MPa and
During 30 DEG C of separation temperature, according to flow, extraction kettle, the heater switch of separator at different levels are opened, while opening refrigeration switch, regulation
Respective temperature controller is to designated value.
C, when near 5 DEG C or so of refrigerator temps, and extraction kettle, separator at different levels temperature close to setting value and stably
When, main pump is opened, the air in extract and separate system is removed and then boosts to extracting pressure, by adjusting extraction kettle and separator
Gases at high pressure choke valve, each kettle is reached set point pressure and CO2Flow is reached close to setting value.
D, machine start automatic running, after certain time, obtain extracting product i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil.
E, shutdown, first close main pump, then the intake valve of extraction kettle is closed, and simultaneously close off various heat cycles switches,
Turn off in total power switch, kettle to be extracted after the pressure balance such as pressure and separators at different levels, closing separator return valve is opened
Vent valve carries out deflation release.
(3) reception of product is extracted
Sample is taken to carry out receiving extraction product, i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil with 50mL brown.By sealed membrane sealed with
Volatilization prevention.
The sample of embodiment 1 is detected below：
1st, the measure of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil physicochemical property
(1) color and luster：With the sense organ color and luster description visually carried out；
(2) relative density：Determined with reference to GB/T5526-1985 bottle methods；
(3) refraction index：Determined with reference to GB/T5527-2010；
(4) acid number：Determined with reference to GB/T5509.229-2016；
(5) peroxide value：Determined with reference to GB/T5534-2008；
(6) saponification number：Determined with reference to GB/T5509.227-2016；
Experiment measures Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil in light yellow, relative density and refraction index national edible oil standard scope it
Interior, acid number 3.2mgKOH/g, peroxide value is 0.25meq/kg, and saponification number is up to 185.5mgKOH/g, shows supercritical fluid
Extraction conditions is suitable, and every physical and chemical index is good, and obtained Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil purity is higher, quality better.
2nd, oxidation resistance index determining
(1) DPPH free radicals are removed：It is respectively 20,50,100,150,200 μ g/mL to prepare mass concentration with absolute ethyl alcohol
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil solution, Vc solution, the BHT solution for preparing same mass concentration is used as control sample solution.Take 2mL samples molten
Liquid and the DPPH solution that 2mL concentration is 0.2mmol/L, room temperature dark reaction 30min after mixing, are returned to zero with 95% ethanol, determined
Absorbance A at 517nm wavelengthSample, the same suction determined after 2mL sample solutions are mixed with 2mL95% ethanol at 517nm wavelength
Luminosity AControl, then determine 2mL DPPH solution and absorbance A of the 2mL60% alcohol mixeding liquids at 517nm wavelengthBlank。
DPPH clearance rates=[1- (ASample-AControl)/ABlank] × 100%
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil has certain Scavenging activity, V to DPPH free radicalsC, BHT and Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil remove DPPH from
By the IC of base50Respectively 36,52,47 μ g/mL, it is seen that sample Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil is totally better than to DPPH radical scavenging activities
BHT, no Vc understand that ability is strong, and DPPH free radical scavenging activities are reached when Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil mass concentration is 0.012g/mL
81.13%.
(2) hydroxyl radical free radical is removed：It is respectively 20,50,100,150,200 μ g/mL to prepare mass concentration with absolute ethyl alcohol
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil solution, prepare the V of same mass concentrationCSolution, BHT solution are used as control sample solution.Take sample solution
2mL, sequentially adds 1mL0.01mol/L FeSO4, 1.5mL10%H2O2Solution, mixes and stands 10min, add 2mL
0.01mol/L salicylic acid solutions, react in 37 DEG C of thermostat water bath after mixing and survey its absorbance at 30min, 510nm wavelength.
The absorbance (being repeated 3 times) that hydrogen peroxide, 2mL absolute ethyl alcohols replace sample to be measured with method is replaced with 1.5mL distilled water respectively.
Clearance rate=A0-(ASample-A1)/Ao × 100%
A0For the absorbance in blank control liquid
A1Not add the absorbance of hydrogenperoxide steam generator sample
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, VC, BHT obvious dose-effect relationship is presented to the Scavenging activity of hydroxy radical, as quality is dense
The Scavenging activity increase of the increase scavenging hydroxyl of degree；VC, BHT and Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil scavenging hydroxyl IC50 be respectively
54th, 82,71 μ g/mL, it is seen that Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil will be significantly stronger than V to the elimination effect of hydroxy radicalC.When Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil quality
76% has been reached to the clearance rate of hydroxy radical when concentration is 200 μ g/mL, has been better than the BHT of homogenous quantities concentration, less than Vc
(3)ABTS+Scavenging activity is determined：Prepare 2mmol/L ABTS solution, draw 50mL ABTS solution with
200mL70mmol/L K2S2O8Solution is mixed, and ABTS is obtained after room temperature avoid light place 12-16h+Solution.Use phosphate buffer
PH7.0-7.2 is by ABTS+It is 0.70 ± 0.02 that solution, which is diluted to the absorbance at 734nm wavelength,.Quality is prepared with absolute ethyl alcohol
Concentration is respectively 20,50,100,150,200 μ g/mL Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil solution, prepares the V of same mass concentrationCSolution, BHT
Solution is used as control sample solution.0.1mL sample solutions are taken, 1.9mL ABTS are added+Solution, its absorbance (weight is surveyed in 734nm
It is multiple 3 times).
Clearance rate=(A0-A)/A0× 100%
In formula：A0For ABTS+The absorbance of solution；A is to add the absorbance after Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil solution.
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil is to ABTS+Scavenging action be proportionate with its mass concentration, when Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil mass concentration
Clearance rate reaches 83% during for 200 μ g/mL, higher than the BHT (66%) of homogenous quantities concentration, less than the Vc of homogenous quantities concentration
(91%)；Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, BHT and VCRemove ABTS+IC50Respectively 61,72,49 μ g/mL, it is seen that Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil pair
ABTS+Scavenging action be better than BHT less than Vc.
The experiment of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil antioxidation activity in vitro shows Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil to DPPH free radicals, ABTS+It is free with hydroxyl
The IC of base50BHT is above less than VC, illustrate that Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil has stronger antioxidant activity in vitro, although antioxidation
Effect can be added in meat products oxidation resistant while the special local flavor of increase not as good as Vc.
It is application example below：
Application examples 1
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil prepared by the embodiment of the present invention 1 is added in ham, its production method, based on ham weight,
Salt 3.5%-5% is used, Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil concentration is that 6%-8% constitutes seasoning, and step is as follows：
(1) ham is pickled：The Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil got ready and salt are first mixed into seasoning, foundation in above ratio
The ham weight pickled takes the seasoning of corresponding amount, looks first at, the thick ham of meat by weight 8% take seasoning, meat is thin
Ham by weight 5.5% take seasoning, the relative ham in intermediate gauge of meat is by weight, suitable between 5.5%-8%
Close data and take seasoning；
(2) seasoning method on：Divide 3 times and smear the seasoning prepared, surface of ham is evenly coated in every time, is rubbed immediately, to assistant
In material immersion ham meat, then secondary upper seasoning is rubbed, and upper three seasonings are rubbed afterwards, and the water leached into straight ham meat overflows
Go out on surface；
(3) stack and pickle：Stacking is pickled at least 30 days, and the ham in stacking once, is pressed above by the turning of five days periods
Ham turning is moved up in lower floor, the gradually past of middle part, makes moisture extruding therein excessive；
(4) hang and air-dry：Tear heap open by stacking more than 30 days, it is air-dried in the workshop of ventilation by only hanging, wait to air-dry to
Ham, when weight at least reduces to the 70% of fresh ham weight, is transferred to fermentation plant；
(5) ferment：The air-dried ham that above-mentioned steps are obtained is in fermentation plant, ham salting technique routinely, it is desirable to phase
To humidity no more than 72%, fermentation turns into Albatrellus dispansus (Lloyd) Canf. ＆ Gilb local flavor ham after 3 months under the conditions of 13 DEG C -16 DEG C of temperature.
Ham is combined with Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, using the distinctive local flavor of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and corrosion-resistant effect, salt dosage is reduced, together
When can improve the sensory issues of ham, break through traditional ham processing technology, exploitation has Yunnan characteristic, wild mushroom and ham
The product being combined, lengthening manufacturing chain bar promotes the development of ham.
Application examples 2
Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil prepared by the embodiment of the present invention 1 is applied to a local flavor ball, its processing method, with the base of embodiment 1
This is identical, and its difference is：
(1) selection of raw material：Pig back leg lean meat, the fat meat for being chosen to remove connective tissue are cut into 2 × 2 × 2 centimetres of meat cubelets
It is stand-by；
(2) preparation of auxiliary material：By Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil 8%, 50mL, bad hematic acid sodium 0.2Kg, radix glycyrrhizae 0.25Kg, garlic 500g,
Cooking wine 20g, five-spice powder 20g, pepper powder 150g, salt 500g, sugar are a small amount of, auxiliary material mixing is made in oil consumption；
(3) preparation for mixing auxiliary agent is cut：Starch 10Kg, glycerin monostearate 40g, Sucrose Fatty Acid Ester acid esters 120g, modified soybean
Phosphatidase 2 00g, stearoyl lactate 200g；
(4) the lean meat block cut is put into cutmixer and carries out chopping system, chopped, 5min back cut side and add fat meat fourth and cut
Mix and auxiliary material is added after auxiliary agent, 2min, cut altogether and mix 10min or so, various raw materials are mixed, 2h is stood at 4 DEG C and obtains meat stuffing；
(5) upper mould：The muddy flesh after mixing will be cut to be put on ball screen tray, it is uniform in size consistent, put in 100 DEG C of boiling water
Enter to cook, you can obtain an Albatrellus dispansus (Lloyd) Canf. ＆ Gilb local flavor ball.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, some improvement and modification can also be made, these improvement and modification
Also it should be regarded as protection scope of the present invention.
Claims (5)
1. a kind of extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, it is characterised in that comprise the following steps：
(1) preparation of raw material：Select without mildew and rot dry tiger palm bacteria, the dust in Albatrellus dispansus (Lloyd) Canf. ＆ Gilb and other magazine particles are removed, choosing
Crushed with high speed Universal pulverizer, cross 40 mesh sieves, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder, weighed with electronic balance, be vacuum-packed
It is standby afterwards；
(2) Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder is extracted using supercritical fluid extraction：
(3) reception of product is extracted：Take sample to carry out receiving extraction product with 50mL brown, that is, obtain Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil, lead to
Cross sealed membrane and be sealed against volatilization.
2. the extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil as claimed in claim 1, it is characterised in that the extraction procedure in step (2) is such as
Under：
A, weigh Albatrellus dispansus (Lloyd) Canf. ＆ Gilb powder and be encased in the extraction kettle of equipment；
B, switch on power, set gradually extraction parameters, extracting pressure 25-35MPa, 50-60 DEG C of extraction temperature, separating pressure 5-
10MPa and during 20-30 DEG C of separation temperature, according to flow, opens extraction kettle, the heater switch of separator at different levels, while opening system
Cold switch, adjusts respective temperature controller to designated value；
C, near 5-8 DEG C when refrigerator temps, and extraction kettle, separator at different levels temperature close to setting value and it is stable when, open
Main pump, removes the air in extract and separate system and then boosts to extracting pressure, by the high pressure for adjusting extraction kettle and separator
Gas throttling valve, makes each kettle reach set point pressure and CO2Flow is reached close to setting value；
D, machine start automatic running, after certain time, obtain extracting product i.e. Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil；
E, shutdown, first close main pump, then the intake valve of extraction kettle is closed, and simultaneously close off various heat cycles switches, then close
Close in total power switch, kettle to be extracted after the pressure balance such as pressure and separators at different levels, closing separator return valve is opened and deflated
Valve carries out deflation release.
3. the extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil as claimed in claim 1, it is characterised in that described Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil can be answered
For ham or a local flavor ball.
4. the extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil as claimed in claim 3, it is characterised in that described Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil is applied to
The method of ham, comprises the following steps：Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil concentration is 6-8%, is uniformly applied to meat products surface, it is fully inhaled
Receive, then carry out pickling air-dried drying, you can.
5. the extracting method of Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil as claimed in claim 3, it is characterised in that described Albatrellus dispansus (Lloyd) Canf. ＆ Gilb essential oil is applied to
The method of a local flavor ball, comprises the following steps：Pork is diced to be put into cut in cutmixer and mixed, cut mix during add containing tiger
Slap the auxiliary material of bacterium essential oil and cut and mix auxiliary agent, after raw material is mixed and stood, be put into cooking in mould shape, boiling water, you can.
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