CN108402104A - A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter and preparation method thereof - Google Patents
A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter and preparation method thereof Download PDFInfo
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- CN108402104A CN108402104A CN201810126055.5A CN201810126055A CN108402104A CN 108402104 A CN108402104 A CN 108402104A CN 201810126055 A CN201810126055 A CN 201810126055A CN 108402104 A CN108402104 A CN 108402104A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
- A01N33/18—Nitro compounds
- A01N33/20—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group
- A01N33/22—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group having at least one oxygen or sulfur atom and at least one nitro group directly attached to the same aromatic ring system
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- A—HUMAN NECESSITIES
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- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/04—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/10—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings with sulfur as the ring hetero atom
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- A—HUMAN NECESSITIES
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A—HUMAN NECESSITIES
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- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/22—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/10—Apiaceae or Umbelliferae [Carrot family], e.g. parsley, caraway, dill, lovage, fennel or snakebed
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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Abstract
The invention discloses steady broad-spectrum plant insecticides of a kind of environment-friendly high-efficiency matter and preparation method thereof, include the raw material of following parts by weight：Mix 20 30 parts of Chinese medicine, 15 25 parts of Chinese medicine of sterilization, 12 parts of nicotine, 12 parts of matrine, 0.5 1 parts of nimbin, 0.5 0.7 parts of toosendanin, 12 parts of alkaloid, 0.4 0.6 parts of xanthoxlin, 0.5 0.9 parts of Celastrus angulatus, 20 30 parts of Controlled-release filler, 0.6 0.8 parts of bleeding agent, 12 parts of stabilizer, 0.05 0.09 parts of growth regulator, 68 parts of water.The present invention has the excellent effect killed pest and inhibit worm's ovum growth, there is preferable preventive and therapeutic effect to pests such as aphid, trialeurodes vaporariorum, the oblique mosquito noctuid of scale insect, leaf folders, in addition there are certain sterilizing functions, it is not only non-hazardous to plant, but also to human body without any murder by poisoning and side effect, product had good sustained release effect, long action time, preparation method provided by the invention simultaneously, production cost is relatively low, technique is concise, has higher practical value and good application prospect.
Description
Technical field
The present invention relates to gardens Pesticidal technology fields, and in particular to a kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter and
Preparation method.
Background technology
Currently, artificial synthesized chemical pesticide about more than 500 is planted, these pesticides are widely used, and not only cause the tight of environment
Heavily contaminated, while causing damages to health, pesticide is mainly entered by three approach in human body：When accidentally a large amount of contacts,
Such as eat by mistake；Second is that a certain amount of pesticide of Long Term Contact, such as the worker of insecticide factory, surrounding resident and the peasant for using pesticide；Third,
Remains of pesticide in daily life contact environment and food, cosmetics, the latter are main original of a large amount of crowds by pollution by pesticides
Cause, a large amount of remains of pesticide can eventually enter into human body, danger of the pesticide to human body by food chain warp bioconcentration in environment
Evil is mainly shown as three kinds of forms：Acute poisoning, chronic hazard and " three cause " harm.
Further, since pesticide developing cost is higher and higher, the target of exploitation is mainly for cereal crops and industrial crops, very
It is less the special-purpose insecticide for protecting target specifically for ornamental plant, the protection of ornamental plant is mainly also with reference to agricultural insecticide
Drug use administration with people apart from nearest plant, become people and beautify life cycle however, ornamental plant belongs to ornamental plant
The part in border pollutes living environment if drug toxicity is too big or smell is more unpleasant, can cause to use than agricultural to people
The health risk of medicine bigger, thus for ornamental plant be protection target, exploitation low toxicity, free from extraneous odour, low-residual plant source kill
Worm agent is very important, and also complies with the requirement of the increasingly stronger security needs of people.
In addition it is to ensure that ornamental plant from insect pest, makes ornamental plant quickly grow up healthy and sound, mostly uses the mode of spraying insecticide
Prevent ornamental plant insect pest.But pesticide contains toxicity more, is easily polluted to surrounding enviroment such as air, and anti-by spraying insecticide
Ornamental plant insect pest is controlled, can not only cause insect pest dead, will also kill useful animals, be unfavorable for environmental protection and the ecological balance.In addition, agriculture
Medicine is volatile after being sprayed on ornamental plant so that pesticide only has drug effect over a period to come, is unable to reach long-term, thoroughly anti-
Control the effect of insect pest.It also once attempted to administer insect pest using biological control mode as biotechnology develops, in industry, namely utilized
Biology and its metabolite prevention phytopathogen, pest and weeds.But current biological prevention is not yet ripe, control effect
It is bad, and the use of biological prevention need to introduce the biology that insect pest can be inhibited to grow in conjunction with environmental conditions such as weather, soil properties,
Enforcement difficulty is big, and has regional condition limitation, is not easy to popularize.
Invention content
In view of the drawbacks of the prior art, the object of the present invention is to provide a kind of steady broad-spectrum plant source desinsections of environment-friendly high-efficiency matter
Agent, the insecticide have kill pest and inhibit worm's ovum growth excellent effect, to aphid, trialeurodes vaporariorum, the oblique mosquito noctuid of scale insect,
The pests such as leaf folder have preferable preventive and therapeutic effect, not only non-hazardous to plant in addition there are certain sterilizing function but also right
Human body without any murder by poisoning and side effect, product had good sustained release effect, long action time, while preparation method provided by the invention,
Production cost is relatively low, technique is concise, has higher practical value and good application prospect.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention provides a kind of steady broad-spectrum plant insecticides of environment-friendly high-efficiency matter, include the raw material of following parts by weight：
Mix 20-30 parts of Chinese medicine, 15-25 parts of Chinese medicine of sterilization, 1-2 parts of nicotine, 1-2 parts of matrine, 0.5-1 parts of nimbin, melia toosendan
0.5-0.7 parts plain, 1-2 portions of alkaloid, 0.5-0.9 parts of Celastrus angulatus, 20-30 parts of Controlled-release filler, oozes 0.4-0.6 parts of xanthoxlin
Saturating 0.6-0.8 parts of agent, 1-2 parts of stabilizer, 0.05-0.09 parts of growth regulator, 6-8 parts of water.
Preferably, the steady broad-spectrum plant insecticide of the environment-friendly high-efficiency matter includes the raw material of following parts by weight：
Mix 25 parts of Chinese medicine, sterilization 20 parts of Chinese medicine, 1.5 parts of nicotine, 1.5 parts of matrine, 0.7 part of nimbin, 0.6 part of toosendanin,
1.5 parts of alkaloid, 0.5 part of xanthoxlin, 0.7 part of Celastrus angulatus, 25 parts of Controlled-release filler, 0.7 part of bleeding agent, 1.5 parts of stabilizer, life
0.07 part of long conditioning agent, 7 parts of water.
Preferably, which is characterized in that the mixing Chinese medicine includes the raw material of following parts by weight：4-8 parts of Eupatorium adenophorum, cnidium monnieri
2-4 parts sub-, 2-4 parts of folium artemisiae argyi, 1-3 parts of garlic, 1-3 parts of Folium Forsythia, 2-4 parts of Ophiorrhiza japonica, 1-3 parts of marigold, 1-2 parts of maidenhair,
1-2 parts of Ageratum conyzoides, 1-3 parts of cepehalotaxus fortunei, 2-4 parts of asparagus.
Preferably, the sterilization Chinese medicine is 7-9 parts of aloe, 2-4 parts of lemon, 1-3 parts of rose, 3-5 parts of China pink, lily of the valley 2-6
Part, 1-3 parts of crape myrtle, 2-4 parts of lilac.
Preferably, the binder is polyvinyl alcohol and sodium carboxymethylcellulose according to weight ratio 3:The mixture of 2 compositions.
Preferably, the Controlled-release filler is attapulgite, medical stone, bentonite, oyster shell whiting according to weight ratio 3:1:2:1 group
At mixture.
Preferably, the growth regulator is gibberellin, potassium dihydrogen phosphate, brassinosteroid, compound sodium nitrophenolate according to weight
Than 2:1:1:The mixture of 1 composition.
Preferably, the bleeding agent is sulfated castor oil, methyl-silicone oil, glycerine according to 2:2:The mixture of 1 composition；Institute
It is sodium sorbate, lead sulfate tribasic according to weight ratio 2 to state stabilizer:The mixture of 3 compositions.
The present invention also provides a kind of preparation methods of the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter, include the following steps：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 8-10 times of its weight is added by step 2, is boiled rear small fire and is decocted 2-4
After hour, the water of 4-6 times of weight is added in filtering, filter residue, is decocted 1-3 hours after boiling, and filters, and merges filtrate twice, is concentrated to give
To mixing thing liquid A；
Step 3 will sterilize Chinese medicine and crush in the ethanol solution that addition weight is 4-6 times, be 40-50 DEG C, ultrasonic power in temperature
For 1-1.5kW ultrasonic extractions 30-40 minutes, solvent is evaporated, mixture B is obtained；
Step 4 heats the water to 40-50 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, bitter skin
Rattan element is added in blender, is stirred 15-25 minutes, speed of agitator 150-250r/min sequentially adds bleeding agent, stabilization
Agent, growth regulator continue stirring 20-30 minutes, obtain mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 10-20 minutes, speed of agitator 150-250r/min, Controlled-release filler is being added in speed of agitator 250-
350r/min continues stirring 30-40 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
Preferably, the preparation process of the steady broad-spectrum plant insecticide of the environment-friendly high-efficiency matter is：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 9 times of its weight is added by step 2, is boiled rear small fire and is decocted 3 hours
Afterwards, it filters, the water of 5 times of weight is added in filter residue, is decocted 2 hours after boiling, and filters, and merges filtrate twice, is concentrated to give mixture
Liquid A；
Step 3, will sterilize Chinese medicine and crushes and weight is added is in 5 times of ethanol solution, temperature is 45 DEG C, ultrasonic power is
1.2kW ultrasonic extractions 35 minutes evaporate solvent, obtain mixture B；
Step 4 heats the water to 45 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, Celastrus angulatus
Element is added in blender, is stirred 20 minutes, speed of agitator 200r/min sequentially adds bleeding agent, stabilizer, growth regulating
Agent continues stirring 25 minutes, obtains mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 15 minutes, speed of agitator 200r/min, continue in speed of agitator 300r/min Controlled-release filler is added
Stirring 35 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
Compared with prior art, the present invention has following advantageous effect：
（1）The mixing Chinese medicine added in a kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present invention, is carried by water so that
Insecticidal constituent in each component is precipitated, and on the one hand improves the effect of desinsection suppression ovum, is carried substantially increasing by multiple water in addition
The service efficiency of raw material, has saved resource.
（2）Ten thousand in each component in a kind of steady broad-spectrum plant insecticide addition mixing Chinese medicine of environment-friendly high-efficiency matter of the present invention
Contain a kind of nematicide active material in its root of longevity chrysanthemum, a- terthienyls (a-T) can kill hairworm etc., in the effect of light
Under, the photosensitive molecular of terthienyl absorbs luminous energy, is transformed into excitation state from ground state, biomembrane is made to aoxidize, and it is thin to destroy nematode
The structure and function of after birth finally results in nematode death；Peacock grass roots and leaf contain insecticidal activity object α-terthienyl and 5- (3-
- 1 alkynyl-α of J alkene, 2 '-Dithiophenes).Extract is diluted with water, and has toxic action to a variety of nematodes.
（3）A kind of desinsection synergistic agent of the steady broad-spectrum plant insecticide addition of environment-friendly high-efficiency matter of the present invention is mainly cigarette
Alkali, matrine, nimbin, toosendanin, chamaejasmine, a few person's substances not only have food refusal and stomach poison function, can also block nerves maincenter
Conduction destroys midgut tissue and various Chlorogenic Acids and respiratory metabolism, influences to digest and assimilate, and loses the sense of taste work(to food
Can, cause pest growth and development abnormal and dead with food refusal, has wide spectrum antivirus effect, the model of pest control can be expanded
It encloses, insecticide is enable to kill a greater variety of insect pests；Leaf Blades of Nerium Indicum water extract is to javanese root knot nematode, half puncture line larva
There is extremely strong cytotoxicity；Asparagus can generate the nematicidals substance such as aspartic acid and dihydro aspartic acid, prevent root burr
The breeding of nematode and other nematodes, controls occurrence injury, and other components have preferable insecticidal effect, do not go to live in the household of one's in-laws on getting married one by one herein
It states.
（4）The sterilization Chinese medicine of the steady broad-spectrum plant insecticide addition of a kind of environment-friendly high-efficiency matter of the present invention, to all kinds of threats
Plant growth bacterium and mould have preferable bactericidal effect, while fully being extracted active ingredient by the way of ultrasonic extraction
Out, extraction liquid impurity is few, and active ingredient is easily isolated, while operating cost is relatively low, and recovery rate is higher.
（5）The nicotine of environment-friendly high-efficiency matter steady broad-spectrum plant insecticide addition of the present invention a kind of, matrine, nimbin,
Toosendanin, alkaloid, xanthoxlin, Celastrus angulatus, a few person's compound actions can form intense stimulus to insect pest and reach and drive worm
Evil, additionally it is possible to make the digestive system function of insect pest fail, reach best pest control effect, while active ingredient is naturalization
Object is closed, there is the degradation pathway of its nature, it is free from environmental pollution, natural enemy is not killed, is not developed immunity to drugs, to the nontoxic spy of people
Point.
（6）A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present invention, which has, kills pest and inhibition worm's ovum growth
Excellent effect, to the pests such as aphid, trialeurodes vaporariorum, the oblique mosquito noctuid of scale insect, leaf folder have preferable preventive and therapeutic effect, additionally
There is certain sterilizing function, it is not only non-hazardous to plant, but also to human body without any murder by poisoning and side effect, product slow release effect
It is good, long action time, while preparation method provided by the invention, production cost is relatively low, technique is concise, has higher practicality
Value and good application prospect.
Specific implementation mode
With reference to specific embodiment, technical scheme in the embodiment of the invention is clearly and completely described, shows
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1.
A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present embodiment, includes the raw material of following parts by weight：
Mix 20 parts of Chinese medicine, 15 parts of Chinese medicine of sterilization, 1 part of nicotine, 1 part of matrine, 0.5 part of nimbin, 0.5 part of toosendanin, biology
1 part of alkali, 0.4 part of xanthoxlin, 0.5 part of Celastrus angulatus, 20 parts of Controlled-release filler, 0.6 part of bleeding agent, 1 part of stabilizer, growth regulator
0.05 part, 6 parts of water.
Mixing Chinese medicine in the present embodiment includes the raw material of following parts by weight：4 parts of Eupatorium adenophorum, 2 parts of frutus cnidii, folium artemisiae argyi 2
Part, 1 part of garlic, 1 part of Folium Forsythia, 2 parts of Ophiorrhiza japonica, 1 part of marigold, 1 part of maidenhair, 1 part of Ageratum conyzoides, 1 part of cepehalotaxus fortunei, asparagus
2 parts.
Sterilization Chinese medicine in the present embodiment is 7 parts of aloe, 2 parts of lemon, 1 part of rose, 3 parts of China pink, 2 parts of the lily of the valley, crape myrtle 1
Part, 2 parts of lilac.
Binder in the present embodiment is polyvinyl alcohol and sodium carboxymethylcellulose according to weight ratio 3:The mixing of 2 compositions
Object.
Controlled-release filler in the present embodiment is attapulgite, medical stone, bentonite, oyster shell whiting according to weight ratio 3:1:2:1
The mixture of composition.
Growth regulator in the present embodiment is gibberellin, potassium dihydrogen phosphate, brassinosteroid, compound sodium nitrophenolate according to weight
Than 2:1:1:The mixture of 1 composition.
Bleeding agent in the present embodiment is sulfated castor oil, methyl-silicone oil, glycerine according to 2:2:The mixture of 1 composition；
The stabilizer is sodium sorbate, lead sulfate tribasic according to weight ratio 2:The mixture of 3 compositions.
A kind of preparation method of the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 8 times of its weight is added by step 2, is boiled rear small fire and is decocted 2 hours
Afterwards, it filters, the water of 4 times of weight is added in filter residue, is decocted 1 hour after boiling, and filters, and merges filtrate twice, is concentrated to give mixture
Liquid A；
Step 3, will sterilize Chinese medicine and crushes and weight is added is in 4 times of ethanol solution, temperature be 40 DEG C, ultrasonic power 1kW
Ultrasonic extraction 30 minutes evaporates solvent, obtains mixture B；
Step 4 heats the water to 40 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, Celastrus angulatus
Element is added in blender, is stirred 15 minutes, speed of agitator 150r/min sequentially adds bleeding agent, stabilizer, growth regulating
Agent continues stirring 20 minutes, obtains mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 10 minutes, speed of agitator 150r/min, continue in speed of agitator 250r/min Controlled-release filler is added
Stirring 30 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
Embodiment 2.
A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present embodiment, includes the raw material of following parts by weight：
Mix 30 parts of Chinese medicine, 25 parts of Chinese medicine of sterilization, 2 parts of nicotine, 2 parts of matrine, 1 part of nimbin, 0.7 part of toosendanin, alkaloid 2
Part, 0.6 part of xanthoxlin, 0.9 part of Celastrus angulatus, 30 parts of Controlled-release filler, 0.8 part of bleeding agent, 2 parts of stabilizer, growth regulator
0.09 part, 8 parts of water.
Mixing Chinese medicine in the present embodiment includes the raw material of following parts by weight：8 parts of Eupatorium adenophorum, 4 parts of frutus cnidii, folium artemisiae argyi 4
Part, 3 parts of garlic, 3 parts of Folium Forsythia, 4 parts of Ophiorrhiza japonica, 3 parts of marigold, 2 parts of maidenhair, 2 parts of Ageratum conyzoides, 3 parts of cepehalotaxus fortunei, asparagus
4 parts.
Sterilization Chinese medicine in the present embodiment is 9 parts of aloe, 4 parts of lemon, 3 parts of rose, 5 parts of China pink, 6 parts of the lily of the valley, crape myrtle 3
Part, 4 parts of lilac.
Binder in the present embodiment is polyvinyl alcohol and sodium carboxymethylcellulose according to weight ratio 3:The mixing of 2 compositions
Object.
Controlled-release filler in the present embodiment is attapulgite, medical stone, bentonite, oyster shell whiting according to weight ratio 3:1:2:1
The mixture of composition.
Growth regulator in the present embodiment is gibberellin, potassium dihydrogen phosphate, brassinosteroid, compound sodium nitrophenolate according to weight
Than 2:1:1:The mixture of 1 composition.
Bleeding agent in the present embodiment is sulfated castor oil, methyl-silicone oil, glycerine according to 2:2:The mixture of 1 composition；
The stabilizer is sodium sorbate, lead sulfate tribasic according to weight ratio 2:The mixture of 3 compositions.
A kind of preparation method of the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 10 times of its weight is added by step 2, is boiled rear small fire and is decocted 4 hours
Afterwards, it filters, the water of 6 times of weight is added in filter residue, is decocted 3 hours after boiling, and filters, and merges filtrate twice, is concentrated to give mixture
Liquid A；
Step 3, will sterilize Chinese medicine and crushes and weight is added is in 6 times of ethanol solution, temperature is 50 DEG C, ultrasonic power is
1.5kW ultrasonic extractions 40 minutes evaporate solvent, obtain mixture B；
Step 4 heats the water to 50 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, Celastrus angulatus
Element is added in blender, is stirred 25 minutes, speed of agitator 250r/min sequentially adds bleeding agent, stabilizer, growth regulating
Agent continues stirring 30 minutes, obtains mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 20 minutes, speed of agitator 250r/min, continue in speed of agitator 350r/min Controlled-release filler is added
Stirring 40 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
Embodiment 3.
A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present embodiment, includes the raw material of following parts by weight：
Mix 25 parts of Chinese medicine, sterilization 20 parts of Chinese medicine, 1.5 parts of nicotine, 1.5 parts of matrine, 0.7 part of nimbin, 0.6 part of toosendanin,
1.5 parts of alkaloid, 0.5 part of xanthoxlin, 0.7 part of Celastrus angulatus, 25 parts of Controlled-release filler, 0.7 part of bleeding agent, 1.5 parts of stabilizer, life
0.07 part of long conditioning agent, 7 parts of water.
Mixing Chinese medicine in the present embodiment includes the raw material of following parts by weight：6 parts of Eupatorium adenophorum, 3 parts of frutus cnidii, folium artemisiae argyi 3
Part, 2 parts of garlic, 2 parts of Folium Forsythia, 3 parts of Ophiorrhiza japonica, 2 parts of marigold, 1.5 parts of maidenhair, 1.5 parts of Ageratum conyzoides, 2 parts of cepehalotaxus fortunei, stone
3 parts of Diao Bai.
Sterilization Chinese medicine in the present embodiment is 8 parts of aloe, 3 parts of lemon, 2 parts of rose, 4 parts of China pink, 4 parts of the lily of the valley, crape myrtle 2
Part, 3 parts of lilac.
Binder in the present embodiment is polyvinyl alcohol and sodium carboxymethylcellulose according to weight ratio 3:The mixing of 2 compositions
Object.
Controlled-release filler in the present embodiment is attapulgite, medical stone, bentonite, oyster shell whiting according to weight ratio 3:1:2:1
The mixture of composition.
Growth regulator in the present embodiment is gibberellin, potassium dihydrogen phosphate, brassinosteroid, compound sodium nitrophenolate according to weight
Than 2:1:1:The mixture of 1 composition.
Bleeding agent in the present embodiment is sulfated castor oil, methyl-silicone oil, glycerine according to 2:2:The mixture of 1 composition；
The stabilizer is sodium sorbate, lead sulfate tribasic according to weight ratio 2:The mixture of 3 compositions.
A kind of preparation method of the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present embodiment, includes the following steps：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 9 times of its weight is added by step 2, is boiled rear small fire and is decocted 3 hours
Afterwards, it filters, the water of 5 times of weight is added in filter residue, is decocted 2 hours after boiling, and filters, and merges filtrate twice, is concentrated to give mixture
Liquid A；
Step 3, will sterilize Chinese medicine and crushes and weight is added is in 5 times of ethanol solution, temperature is 45 DEG C, ultrasonic power is
1.2kW ultrasonic extractions 35 minutes evaporate solvent, obtain mixture B；
Step 4 heats the water to 45 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, Celastrus angulatus
Element is added in blender, is stirred 20 minutes, speed of agitator 200r/min sequentially adds bleeding agent, stabilizer, growth regulating
Agent continues stirring 25 minutes, obtains mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 15 minutes, speed of agitator 200r/min, continue in speed of agitator 300r/min Controlled-release filler is added
Stirring 35 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
A kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter of the present invention, which has, to be killed pest and inhibits worm's ovum growth
Excellent effect has preferable preventive and therapeutic effect to pests such as aphid, trialeurodes vaporariorum, the oblique mosquito noctuid of scale insect, leaf folders, in addition there are
Certain sterilizing function, it is not only non-hazardous to plant, but also to human body without any murder by poisoning and side effect, product had good sustained release effect,
Long action time, while preparation method provided by the invention, production cost is relatively low, technique is concise, has higher practical valence
Value and good application prospect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (10)
1. a kind of steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter, which is characterized in that include the raw material of following parts by weight：
Mix 20-30 parts of Chinese medicine, 15-25 parts of Chinese medicine of sterilization, 1-2 parts of nicotine, 1-2 parts of matrine, 0.5-1 parts of nimbin, melia toosendan
0.5-0.7 parts plain, 1-2 portions of alkaloid, 0.5-0.9 parts of Celastrus angulatus, 20-30 parts of Controlled-release filler, oozes 0.4-0.6 parts of xanthoxlin
Saturating 0.6-0.8 parts of agent, 1-2 parts of stabilizer, 0.05-0.09 parts of growth regulator, 6-8 parts of water.
2. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1, which is characterized in that the environmental protection
The efficient steady broad-spectrum plant insecticide of matter includes the raw material of following parts by weight：
Mix 25 parts of Chinese medicine, sterilization 20 parts of Chinese medicine, 1.5 parts of nicotine, 1.5 parts of matrine, 0.7 part of nimbin, 0.6 part of toosendanin,
1.5 parts of alkaloid, 0.5 part of xanthoxlin, 0.7 part of Celastrus angulatus, 25 parts of Controlled-release filler, 0.7 part of bleeding agent, 1.5 parts of stabilizer, life
0.07 part of long conditioning agent, 7 parts of water.
3. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1 or 2, which is characterized in that described
Mixing Chinese medicine includes the raw material of following parts by weight：4-8 parts of Eupatorium adenophorum, 2-4 parts of folium artemisiae argyi, 1-3 parts of garlic, connects 2-4 parts of frutus cnidii
Stick up 1-3 parts of leaf, 2-4 parts of Ophiorrhiza japonica, 1-3 parts of marigold, 1-2 parts of maidenhair, 1-2 parts of Ageratum conyzoides, 1-3 parts of cepehalotaxus fortunei, asparagus
2-4 parts.
4. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1 or 2, which is characterized in that described
Sterilization Chinese medicine is 7-9 parts of aloe, 2-4 parts of lemon, 1-3 parts of rose, 3-5 parts of China pink, 2-6 parts of the lily of the valley, 1-3 parts of crape myrtle, lilac
2-4 parts.
5. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1 or 2, which is characterized in that described
Binder is polyvinyl alcohol and sodium carboxymethylcellulose according to weight ratio 3:The mixture of 2 compositions.
6. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1 or 2, which is characterized in that described
Controlled-release filler is attapulgite, medical stone, bentonite, oyster shell whiting according to weight ratio 3:1:2:The mixture of 1 composition.
7. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1 or 2, which is characterized in that described
Growth regulator is gibberellin, potassium dihydrogen phosphate, brassinosteroid, compound sodium nitrophenolate according to weight ratio 2:1:1:The mixing of 1 composition
Object.
8. the steady broad-spectrum plant insecticide of a kind of environment-friendly high-efficiency matter according to claim 1 or 2, which is characterized in that described
Bleeding agent is sulfated castor oil, methyl-silicone oil, glycerine according to 2:2:The mixture of 1 composition；The stabilizer is sorbic acid
Sodium, lead sulfate tribasic are according to weight ratio 2:The mixture of 3 compositions.
9. a kind of method preparing the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter as claimed in claim 1 or 2, feature exist
In including the following steps：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 8-10 times of its weight is added by step 2, is boiled rear small fire and is decocted 2-4
After hour, the water of 4-6 times of weight is added in filtering, filter residue, is decocted 1-3 hours after boiling, and filters, and merges filtrate twice, is concentrated to give
To mixing thing liquid A；
Step 3 will sterilize Chinese medicine and crush in the ethanol solution that addition weight is 4-6 times, be 40-50 DEG C, ultrasonic power in temperature
For 1-1.5kW ultrasonic extractions 30-40 minutes, solvent is evaporated, mixture B is obtained；
Step 4 heats the water to 40-50 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, bitter skin
Rattan element is added in blender, is stirred 15-25 minutes, speed of agitator 150-250r/min sequentially adds bleeding agent, stabilization
Agent, growth regulator continue stirring 20-30 minutes, obtain mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 10-20 minutes, speed of agitator 150-250r/min, Controlled-release filler is being added in speed of agitator 250-
350r/min continues stirring 30-40 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
10. a kind of preparation method of the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter according to claim 9, feature exist
In the step is：
Step 1 weighs prepare each component raw material as required；
Mixing Chinese medicine is crushed, is added in decoction pot, the water of 9 times of its weight is added by step 2, is boiled rear small fire and is decocted 3 hours
Afterwards, it filters, the water of 5 times of weight is added in filter residue, is decocted 2 hours after boiling, and filters, and merges filtrate twice, is concentrated to give mixture
Liquid A；
Step 3, will sterilize Chinese medicine and crushes and weight is added is in 5 times of ethanol solution, temperature is 45 DEG C, ultrasonic power is
1.2kW ultrasonic extractions 35 minutes evaporate solvent, obtain mixture B；
Step 4 heats the water to 45 DEG C, mixing nicotine, matrine, nimbin, toosendanin, alkaloid, xanthoxlin, Celastrus angulatus
Element is added in blender, is stirred 20 minutes, speed of agitator 200r/min sequentially adds bleeding agent, stabilizer, growth regulating
Agent continues stirring 25 minutes, obtains mixed liquor C；
Step 5 mixes mixed liquor C prepared by mixture B made from mixed liquor A made from step 2, step 3, step 4
It is added in blender and stirs 15 minutes, speed of agitator 200r/min, continue in speed of agitator 300r/min Controlled-release filler is added
Stirring 35 minutes, the steady broad-spectrum plant insecticide of environment-friendly high-efficiency matter invented.
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Application publication date: 20180817 |