CN108395936A - 一种制备生物柴油的方法及系统 - Google Patents
一种制备生物柴油的方法及系统 Download PDFInfo
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- CN108395936A CN108395936A CN201710066663.7A CN201710066663A CN108395936A CN 108395936 A CN108395936 A CN 108395936A CN 201710066663 A CN201710066663 A CN 201710066663A CN 108395936 A CN108395936 A CN 108395936A
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- 238000000034 method Methods 0.000 title claims abstract description 33
- 239000003225 biodiesel Substances 0.000 title claims abstract description 23
- 238000002156 mixing Methods 0.000 claims abstract description 135
- 239000000463 material Substances 0.000 claims abstract description 37
- 239000000047 product Substances 0.000 claims abstract description 30
- 150000001298 alcohols Chemical class 0.000 claims abstract description 16
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 12
- 230000009471 action Effects 0.000 claims abstract description 9
- 238000005886 esterification reaction Methods 0.000 claims abstract description 9
- 230000032050 esterification Effects 0.000 claims abstract description 5
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 37
- 238000006243 chemical reaction Methods 0.000 claims description 24
- 230000000694 effects Effects 0.000 claims description 15
- 239000004519 grease Substances 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 15
- 239000003054 catalyst Substances 0.000 claims description 12
- 230000008859 change Effects 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 5
- 230000035484 reaction time Effects 0.000 claims description 5
- 238000007906 compression Methods 0.000 claims description 4
- 230000008676 import Effects 0.000 claims description 4
- 230000001133 acceleration Effects 0.000 claims description 3
- 230000006835 compression Effects 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 230000009466 transformation Effects 0.000 claims description 3
- 125000004122 cyclic group Chemical group 0.000 claims description 2
- 238000005381 potential energy Methods 0.000 claims description 2
- 230000002441 reversible effect Effects 0.000 claims description 2
- 238000013329 compounding Methods 0.000 claims 1
- 230000007774 longterm Effects 0.000 abstract description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 42
- 235000019441 ethanol Nutrition 0.000 description 17
- 239000012530 fluid Substances 0.000 description 10
- 238000002360 preparation method Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- -1 aliphatic ester Chemical class 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
- 239000000194 fatty acid Substances 0.000 description 5
- 150000004665 fatty acids Chemical class 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
- 239000003549 soybean oil Substances 0.000 description 5
- 235000012424 soybean oil Nutrition 0.000 description 5
- 235000012343 cottonseed oil Nutrition 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 230000035939 shock Effects 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 235000019482 Palm oil Nutrition 0.000 description 3
- 239000002385 cottonseed oil Substances 0.000 description 3
- 238000006073 displacement reaction Methods 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000019198 oils Nutrition 0.000 description 3
- 239000002540 palm oil Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000009527 percussion Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910000639 Spring steel Inorganic materials 0.000 description 1
- 238000007171 acid catalysis Methods 0.000 description 1
- 238000005815 base catalysis Methods 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
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- 238000006731 degradation reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
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- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000005431 greenhouse gas Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000010338 mechanical breakdown Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000009473 power blending Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Abstract
Description
Claims (14)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710066663.7A CN108395936B (zh) | 2017-02-07 | 2017-02-07 | 一种制备生物柴油的方法 |
Applications Claiming Priority (1)
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CN201710066663.7A CN108395936B (zh) | 2017-02-07 | 2017-02-07 | 一种制备生物柴油的方法 |
Publications (2)
Publication Number | Publication Date |
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CN108395936A true CN108395936A (zh) | 2018-08-14 |
CN108395936B CN108395936B (zh) | 2021-10-08 |
Family
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Family Applications (1)
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CN201710066663.7A Active CN108395936B (zh) | 2017-02-07 | 2017-02-07 | 一种制备生物柴油的方法 |
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Citations (42)
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CA1264264A (en) * | 1986-04-18 | 1990-01-09 | Jiri Giorgio Kazda | Orthopedic crutch making it possible to place only a controlled and adjustable part of the body weight on the injured lower limb during walking |
US5251595A (en) * | 1990-12-06 | 1993-10-12 | Shenzhen Aote Electrical Appliances Co. Ltd. | Rotor engine |
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CN1347961A (zh) * | 2000-10-10 | 2002-05-08 | 张晓林 | 用废弃塑料制备汽、柴油的专用装置 |
KR100299288B1 (ko) * | 1991-12-10 | 2002-06-20 | 브룬너 하인리히 페터 울리히 | 왕복연소기관용연료분사밸브 |
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CN101117587A (zh) * | 2007-09-12 | 2008-02-06 | 福建棱舒石油化工设备有限公司 | 移动式生物柴油生产设备及其工艺流程 |
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DE102008022483A1 (de) * | 2007-05-16 | 2008-12-04 | Afton Chemical Corp. | Schmiermittelzusammensetzung |
WO2009012214A1 (en) * | 2007-07-13 | 2009-01-22 | Dow Global Technologies Inc. | Viscosity index improver for lubricant compositions |
CN101484860A (zh) * | 2006-03-22 | 2009-07-15 | 约翰逊迪瓦西公司 | 用于稀释控制的装置和方法 |
CN101506339A (zh) * | 2005-05-06 | 2009-08-12 | 巴特勒能源同盟有限公司 | 用扩展气体溶剂制备生物柴油 |
CN101586041A (zh) * | 2009-06-25 | 2009-11-25 | 华东理工大学 | 一种连续制备生物柴油的装置及方法 |
CN101717696A (zh) * | 2009-11-03 | 2010-06-02 | 朱瑞林 | 用棕榈油制备生物柴油的工艺方法和设备 |
CN101812379A (zh) * | 2010-04-14 | 2010-08-25 | 河北工业大学 | 一种以萌发的油料作物种子为原料自催化制备生物柴油的方法 |
CN101899363A (zh) * | 2009-11-02 | 2010-12-01 | 朱瑞林 | 以菜子油生产生物柴油的工艺方法及设备 |
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CN201744346U (zh) * | 2010-02-09 | 2011-02-16 | 丰映科技股份有限公司 | 用于制造生质柴油的往复式管型连续式反应器 |
CN102010792A (zh) * | 2010-12-15 | 2011-04-13 | 东南大学 | 一种连续化生产生物柴油的方法 |
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CN102344857A (zh) * | 2010-08-06 | 2012-02-08 | 无锡市正洪生物柴油设备科技有限公司 | 移动式多组串连固定床固体酸生物柴油生产设备及工艺流程 |
CN102453561A (zh) * | 2010-10-27 | 2012-05-16 | 中国石油化工股份有限公司 | 一种柴油添加剂及其在低硫柴油中的应用 |
CN102533438A (zh) * | 2011-08-16 | 2012-07-04 | 中国海洋石油总公司 | 一种生物柴油粗产品的精制方法 |
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CN203061129U (zh) * | 2013-02-07 | 2013-07-17 | 汤树林 | 基于油气井的固液混配装置 |
CN103254997A (zh) * | 2012-02-16 | 2013-08-21 | 浙江中义达能源科技有限公司 | 连续生产振荡流酯化反应塔 |
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CN103666774A (zh) * | 2013-11-22 | 2014-03-26 | 清华大学 | 一种煤基甲醇与棕榈油超临界法制备生物柴油的方法和装置 |
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CN203655404U (zh) * | 2013-11-06 | 2014-06-18 | 西安永昌机械动力有限公司 | 柴油机 |
CN104263523A (zh) * | 2014-09-17 | 2015-01-07 | 江苏大学 | 一种制备生物柴油的空化器 |
CN105062696A (zh) * | 2015-04-16 | 2015-11-18 | 彭才文 | 一种单塔逆流超临界非催化连续的酯化工艺方法 |
CN205216720U (zh) * | 2015-12-04 | 2016-05-11 | 广东和平君乐药业有限公司 | 一种二维运动混合机 |
CN105647657A (zh) * | 2016-01-25 | 2016-06-08 | 山东岩海建设资源有限公司 | 一种生物柴油甲酯化装置及其生产工艺 |
CN205669018U (zh) * | 2016-06-16 | 2016-11-02 | 朱贵兴 | 一种用于生物柴油预处理脱酸装置 |
CN106215755A (zh) * | 2016-08-24 | 2016-12-14 | 杜杭华 | 一种食品加工用混合机 |
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2017
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CA1264264A (en) * | 1986-04-18 | 1990-01-09 | Jiri Giorgio Kazda | Orthopedic crutch making it possible to place only a controlled and adjustable part of the body weight on the injured lower limb during walking |
US5251595A (en) * | 1990-12-06 | 1993-10-12 | Shenzhen Aote Electrical Appliances Co. Ltd. | Rotor engine |
KR100299288B1 (ko) * | 1991-12-10 | 2002-06-20 | 브룬너 하인리히 페터 울리히 | 왕복연소기관용연료분사밸브 |
US7222614B2 (en) * | 1996-07-17 | 2007-05-29 | Bryant Clyde C | Internal combustion engine and working cycle |
CN2443967Y (zh) * | 2000-10-10 | 2001-08-22 | 张晓林 | 用废弃塑料制备汽、柴油的专用装置 |
CN1347961A (zh) * | 2000-10-10 | 2002-05-08 | 张晓林 | 用废弃塑料制备汽、柴油的专用装置 |
US20050142250A1 (en) * | 2002-06-03 | 2005-06-30 | Agb, Llc | Method of processing waste product into fuel |
CN2583378Y (zh) * | 2002-10-17 | 2003-10-29 | 陈宾 | 柴油机燃油喷射器 |
US20050023835A1 (en) * | 2003-07-30 | 2005-02-03 | Aisin Seiki Kabushiki Kaisha | Reciprocating engine type electric generator |
CN1982269A (zh) * | 2003-11-20 | 2007-06-20 | 索尔维公司 | 用于生产有机化合物的方法 |
CN101506339A (zh) * | 2005-05-06 | 2009-08-12 | 巴特勒能源同盟有限公司 | 用扩展气体溶剂制备生物柴油 |
CN101484860A (zh) * | 2006-03-22 | 2009-07-15 | 约翰逊迪瓦西公司 | 用于稀释控制的装置和方法 |
CN1844754A (zh) * | 2006-04-30 | 2006-10-11 | 何仁 | 一种生物质油燃烧灶具 |
CN101113354A (zh) * | 2006-07-27 | 2008-01-30 | 上海中油企业集团有限公司 | 一种环保型生物柴油的制备方法 |
CN101132157A (zh) * | 2007-03-09 | 2008-02-27 | 温天驰 | 磁能发动机 |
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CN201744346U (zh) * | 2010-02-09 | 2011-02-16 | 丰映科技股份有限公司 | 用于制造生质柴油的往复式管型连续式反应器 |
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CN102453561A (zh) * | 2010-10-27 | 2012-05-16 | 中国石油化工股份有限公司 | 一种柴油添加剂及其在低硫柴油中的应用 |
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CN205216720U (zh) * | 2015-12-04 | 2016-05-11 | 广东和平君乐药业有限公司 | 一种二维运动混合机 |
CN105647657A (zh) * | 2016-01-25 | 2016-06-08 | 山东岩海建设资源有限公司 | 一种生物柴油甲酯化装置及其生产工艺 |
CN205669018U (zh) * | 2016-06-16 | 2016-11-02 | 朱贵兴 | 一种用于生物柴油预处理脱酸装置 |
CN106215755A (zh) * | 2016-08-24 | 2016-12-14 | 杜杭华 | 一种食品加工用混合机 |
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