CN108354867A

CN108354867A - A kind of preparation method of moisturizing de-etiolation facial mask

Info

Publication number: CN108354867A
Application number: CN201810341556.5A
Authority: CN
Inventors: 陈桂芳
Original assignee: Individual
Current assignee: Individual
Priority date: 2018-04-17
Filing date: 2018-04-17
Publication date: 2018-08-03

Abstract

The invention discloses a kind of preparation methods of moisturizing de-etiolation facial mask, include the following steps：(1) by propylene glycol, niacinamide, glycerine, glycosylglycerol, butanediol, beta glucan, Sodium Hyaluronate, panthenol, allantoin, hexylene glycol, EDETATE SODIUM, methyl hydroxybenzoate, ethyl hydroxy benzoate, hydroxyethyl cellulose, carbomer, deionized water, it is added in agitated kettle and is heated with stirring to 70 85 DEG C, stirring and dissolving is complete, and A phases are made；(2) glycerine polymethacrylates, hydrolysis Jojoba esters, 40 rilanit specials of PEG are added in agitated kettle and are heated with stirring to 70 85 DEG C, B phases are made；(3) it is slowly stirred down, B is added to A phases, is stirred evenly, is cooled to 40 55 DEG C, add Khotan jade superfine nano powder, Artemisia japonica extract, the gloomy polysaccharides of love, stir postcooling discharging.Facial mask prepared by the present invention can improve the problem of dark yellow colour of skin, dry skin well.

Description

A kind of preparation method of moisturizing de-etiolation facial mask

Technical field

The present invention relates to cosmetic fields, and in particular to a kind of preparation method of moisturizing de-etiolation facial mask.

Background technology

The dark yellow colour of skin refers to because a variety of causes causes skin surface aging, face yellowing, lusterless one kind skin to be asked Topic, it is the most commonly seen physiological aging phenomenon of Asia middle and aged women, and more seems serious with the increase at age, Show it has often been said that " yellow-faced woman-my wife " state.In recent years, with economic rapid growth, the accelerating rhythm of life, the work of people Make that pressure is also increasing, it is irregular along with rest, the problems such as environmental pollution, causes young women skin occur and cross early ageing It waits for a long time various skin problems, such as the long spot of skin, the colour of skin is obscure, jaundice.These skin problems seriously annoying people seeking beauty.

Currently, commercially available commonly have effects that the big multicomponent of the facial mask of de-etiolation is single, effect unobvious or it is added to a huge sum of money The chemical stimulations ingredients such as category, long term consumer use will produce side effect, generate the symptoms such as allergic reaction.

Invention content

In view of the deficiencies of the prior art, the purpose of the present invention is to provide a kind of preparation methods of moisturizing de-etiolation facial mask.

In order to reach the purpose of the present invention, adopt the following technical scheme that：

A kind of preparation method of moisturizing de-etiolation facial mask, includes the following steps：

(1) by 5-15% propylene glycol, 0.01-0.05% niacinamide, 5-10% glycerine, 1-5% glycosylglycerols, 10- 20% butanediol, 1-5% beta glucans, 0.05-0.1% Sodium Hyaluronates, 0.02-0.1% panthenols, 0.1-0.5% allantoins, 0.1-1% hexylene glycols, 0.1-0.5%EDTA disodiums, 0.02-0.2% methyl hydroxybenzoates, 0.02-0.2% ethyl hydroxy benzoates, 0.1- 0.5% hydroxyethyl cellulose, 0.1-0.3% carbomers, deionized water are added in agitated kettle and are heated with stirring to 70-85 DEG C, stirring Dissolving is complete, and A phases are made；

(2) by 0.1-0.5% glycerine polymethacrylates, 0.2-0.8% hydrolysis Jojobas esters, 0.1-0.5% Cremophor RH40 is added in agitated kettle and is heated with stirring to 70-85 DEG C, and B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 40-55 DEG C, adds 0.1-8% Khotan jades Superfine nano powder, 0.1-6% Artemisia japonica extracts, 0.1-8% like gloomy polysaccharides, stir postcooling discharging.

Wherein, in the step (3) diameter of Khotan jade superfine nano powder between 0.01 nanometer -100 nanometers.

Preferably, the preparation method of above-mentioned moisturizing de-etiolation facial mask, includes the following steps：

(1) by 7-13% propylene glycol, 0.02-0.04% niacinamide, 6-8% glycerine, 2-4% glycosylglycerols, 12-18% Butanediol, 2-4% beta glucans, 0.06-0.08% Sodium Hyaluronates, 0.05-0.08% panthenols, 0.2-0.4% allantoins, 0.2-0.8% hexylene glycols, 0.2-0.4%EDTA disodiums, 0.05-0.18% methyl hydroxybenzoates, 0.05-0.18% ethyl hydroxy benzoates, 0.2-0.4% hydroxyethyl celluloses, 0.15-0.25% carbomers, deionized water are added in agitated kettle and are heated with stirring to 75-85 DEG C, stirring and dissolving is complete, and A phases are made；

(2) by 0.2-0.4% glycerine polymethacrylates, 0.5-0.7% hydrolysis Jojobas esters, 0.2-0.4% Cremophor RH40 is added in agitated kettle and is heated with stirring to 75-85 DEG C, and B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 45-55 DEG C, adds 0.5-7% Khotan jades Superfine nano powder, 0.2-5% Artemisia japonica extracts, 0.5-7% like gloomy polysaccharides, stir postcooling discharging.

(1) by 10% propylene glycol, 0.03% niacinamide, 7% glycerine, 3% glycosylglycerol, 15% butanediol, the Portugals 3% β- Glycan, 0.07% Sodium Hyaluronate, 0.06% panthenol, 0.3% allantoin, 0.5% hexylene glycol, 0.3%EDTA disodiums, 0.1% Methyl hydroxybenzoate, 0.1% ethyl hydroxy benzoate, 0.3% hydroxyethyl cellulose, 0.2% carbomer, deionized water are added in agitated kettle and stir It mixes and is heated to 80-85 DEG C, stirring and dissolving is complete, and A phases are made；

(2) by 0.3% glycerine polymethacrylates, 0.6% hydrolysis Jojoba esters, 0.3%PEG-40 hydrogenated castors Oil is added in agitated kettle and is heated with stirring to 80-85 DEG C, and B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 50-55 DEG C, it is ultra-fine to add 4% Khotan jade Nano powder, 3% Artemisia japonica extract, the 3% gloomy polysaccharides of love, stir postcooling discharging.

Following introduce is made to the fractions in the present invention：

Khotan jade category dolomitic marble and intermediate acidity magmatic rock contact metasomatism and the metamorphic rock formed, Chinese Gem Studies are pointed out For nephrite mohs hardness between 6.0-6.5, the jade that tremolite composition accounts for 98% or more is all named as Khotan jade, includes sudden strain of a muscle More mineral aggregates such as stone, hornblend, actinolite.It is micro- containing 13 kinds of calcium, iron, manganese, zinc, copper etc. in the mineral composition of Khotan jade Secondary element, they are beneficial to human body, and ancient medicine is classical《The Yellow Emperor's Canon of Internal Medicine》、《Tang materia medica》、《Legendary god of farming's book on Chinese herbal medicine》、《Compendium of Materia Medica》 Claim Khotan jade can " enriching yin gas, invigorating kidney yang, except it is middle heat, solution be tired of depressed and discontented, embellish lung, help sound larynx, grow hair, support the five internal organs, peace soul, Dredge blood vessels, bright knowledge ".

Artemisia japonica (Artemisia japonica T) is composite family artemisia tarragon subgenus, and perennial herb is planted for medicine-food two-purpose Object, civil also known as native radix bupleuri (《Luchuan book on Chinese herbal medicine》), stomachache spirit, bear's paw grass, with all herbal medicine.With heat-clearing, cool blood, liver heat, solution Heat, stomach invigorating hemostasia effect.Artemisia japonica is containing abundant flavonoids, polysaccharide, Polyphenols, saponins, the compounds such as qinghaosu, volatile oil. And flavone compound remove with antibacterial, anti-inflammatory, anti-oxidant, anti-corrosive fresh-keeping, promote arteriole restoration of blood flow, reduce diastolic pressure, Activate blood circulation and disperse blood clots etc. outside medical function, also have anti-aging, it is wrinkle resistant increase from, gradually decompose and eliminate melanin, chloasma, freckle and powder The cosmetology functions such as thorn.

Like that gloomy polysaccharides can become the synthesis accelerant of hyaluronic acid in human body cell, promote the generation of hyaluronic acid, Allow a large amount of hyaluronic acid that skin can be helped to draw a large amount of moisture, skin has moisture, can keep elasticity and softness naturally. Enhance the prolonged water holding capacity of skin simultaneously, elastic fibers and collagen can be helped to be in the environment full of moisture, Skin is allowed to show more flexible.In addition, it is a kind of hyaluronidase inhibitor to like gloomy polysaccharides again, hyaluronic acid specificity is inhibited to split Enzyme is solved, the activity of inhibition can make hyaluronic acid not be decomposed, maintain normal physiological function.Like that gloomy polysaccharides have more significant resist Oxidability, such as to oxygen radical absorbability (ORAC), ABTS free radical scavenging abilities and reducing power, it is effectively improved skin Skin aging reduces wrinkle and relaxation.

Compared with prior art, the present invention has the advantages that：

(1) moisturizing de-etiolation facial mask prepared by the present invention, by Khotan jade superfine nano powder, Artemisia japonica extract and Ai Sen polysaccharides Reasonable compatibility is carried out, scientific matching makes different effective active compositions generate synergistic function, can improve the colour of skin well The problem of dark yellow, dry skin.

(2) the Khotan jade superfine nano powder in facial mask of the present invention has extremely strong activation, adsorption function, can improve micro- follow Ring accelerates skin metabolism, while its trace element being rich in can also be that skin supplements the nutrients, and conserve skin；Artemisia japonica is extracted Object and Ai Sen polysaccharides have anti-oxidant, moisturizing and other effects, can remove extra free radical, keep the moisture of skin, significantly slow Skin aging problem is solved, the barrier function of skin is repaired.

(3) the moisturizing de-etiolation facial mask that prepared by the present invention is mildly non-stimulated to skin, and preparation process is simple, adapts to industrialization Production.

Specific implementation mode

Below in conjunction with specific embodiment, the present invention is further elaborated.

A kind of formula of moisturizing de-etiolation facial mask prepared by 1-3 of the embodiment of the present invention see the table below 1：

Table 1

A kind of preparation methods of moisturizing de-etiolation facial mask of above-described embodiment 1-3 include the following steps：

(1) by propylene glycol, niacinamide, glycerine, glycosylglycerol, butanediol, beta glucan, Sodium Hyaluronate, panthenol, urine Stirring is added in Bursin, hexylene glycol, EDETATE SODIUM, methyl hydroxybenzoate, ethyl hydroxy benzoate, hydroxyethyl cellulose, carbomer, deionized water It is heated with stirring to 70-85 DEG C in pot, stirring and dissolving is complete, and A phases are made；

(2) glycerine polymethacrylates, hydrolysis Jojoba esters, Cremophor RH40 are added in agitated kettle and are stirred It mixes and is heated to 70-85 DEG C, B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 40-55 DEG C, add that Khotan jade is ultra-fine to be received Rice flour, Artemisia japonica extract, the gloomy polysaccharides of love, stir postcooling discharging.

Wherein, in above-mentioned steps (3) diameter of Khotan jade superfine nano powder between 0.01 nanometer -100 nanometers.

Comparative example 1

Difference with embodiment 1 is that Khotan jade superfine nano powder, other preparation conditions and method and 1 phase of embodiment are not added Together.

Comparative example 2

Difference with embodiment 1 is that Artemisia japonica extract is not added, other preparation conditions and method are same as Example 1.

Comparative example 3

Difference with embodiment 1 is that the gloomy polysaccharides of love are not added, other preparation conditions and method are same as Example 1.

Comparative example 4

Difference with embodiment 1 is that Khotan jade superfine nano powder, Artemisia japonica extract, the gloomy polysaccharides of love, other systems are not added Standby condition and method are same as Example 1.

Embodiment 4

Human body patch test

Organize 30 volunteers according to《Cosmetics health specification》The human skin patch Experimental Standardization of (2007 editions) records, The moisturizing de-etiolation facial mask obtained by the embodiment of the present invention 1 is tested, as a result such as the following table 2：

Table 2

Embodiment 5

Efficacy assessment is tested

Research object：The trier of dark yellow, obscure, dry five kinds of skin problems of microgroove is selected, each problem skin is chosen 120 people are divided into 4 groups, 30 people of each group, the facial mask that group 1 is prepared with embodiment 1, the preparation of embodiment 2 of group 2 Facial mask, the facial mask that group 3 is prepared with embodiment 3, group 4 use facial mask prepared by comparative example 4 to use 3 weekly as blank control It is secondary, it is used continuously 3 months, records trier's skin.Experimental result is shown in the following table 3：

Table 3

Experimental result：

What dark yellow skin was obviously improved shows as：Skin is apparent pale bright.

What dark yellow skin symptom was alleviated shows as：Skin dark yellow subtracts light, slightly turns white.

Dark yellow skin is shown as without improvement：Skin is dark yellow, white also without intensification without turn.

What obscure skin was obviously improved shows as：Skin is apparent pale bright.

What obscure skin symptom was alleviated shows as：The obscure color of skin subtracts light, slightly turns white.

Obscure skin is shown as without improvement：Skin is dark yellow, white also without intensification without turn.

What dry skin was obviously improved shows as：Skin smooth water is tender.

Dry skin remission is shown as：Dry decortication phenomenon mitigates, and partial skin water is tender.

Dry skin is shown as without improvement：Dry decortication phenomenon is without mitigation also without deterioration.

What microgroove skin was obviously improved shows as：Microgroove disappears.

What microgroove skin symptom was alleviated shows as：Lines shoals.

Microgroove skin is shown as without improvement：Microgroove is without shoaling also without intensification.

The facial mask prepared using embodiment 1-3 it can be seen from upper table 3 is to dark yellow, obscure, microgroove and dry skin Problem has fine curative effect, adheres to being used for a long time, and effect can be more preferable more stable.

Embodiment 6

Effect contrast test

1, test object：The women that the selection age is 20-55 Sui, every group 50；

2, test equipment：VISA digital skins analyzer (U.S.), Aomei health moisture of skin tester (China) and Minolta CR300 colour difference meters (China)；

3, test zone：Face；

4, usage time：3 times a week, it persistently uses 2 months；

5, test event：Whitening, humidity of skin and skin delicacy degree.

The using effect of moisturizing de-etiolation facial mask prepared by moisturizing de-etiolation facial mask and comparative example 1-3 prepared by embodiment 1-3 is such as Shown in the following table 4：

Table 4

As can be seen from Table 4, the moisturizing for the facial mask that prepared by embodiment 1-3 and whitening effect are apparently higher than comparative example 1- 3 facial masks prepared illustrate Khotan jade superfine nano powder, Artemisia japonica extract, the gloomy polysaccharides three combination of love having synergy Effect is good more than single additive effect.

Above example only illustrates embodiment of the present invention, and there is no have limitation in any form to the present invention；Appoint What is engaged in professional and technical personnel, all has the ability to make some changes or modification using the technology contents disclosed, becomes equivalent The equivalent embodiment of variation carries out simple modification, equivalent change and modification to the present invention, belongs to according to the technology of the present invention essence In the range of technical solution of the present invention.

Claims

1. a kind of preparation method of moisturizing de-etiolation facial mask, which is characterized in that include the following steps：

(1) by 5-15% propylene glycol, 0.01-0.05% niacinamide, 5-10% glycerine, 1-5% glycosylglycerols, 10-20% fourths Glycol, 1-5% beta glucans, 0.05-0.1% Sodium Hyaluronates, 0.02-0.1% panthenols, 0.1-0.5% allantoins, 0.1- 1% hexylene glycol, 0.1-0.5%EDTA disodiums, 0.02-0.2% methyl hydroxybenzoates, 0.02-0.2% ethyl hydroxy benzoates, 0.1-0.5% hydroxyls Ethyl cellulose, 0.1-0.3% carbomers, deionized water are added in agitated kettle and are heated with stirring to 70-85 DEG C, and stirring and dissolving is complete Entirely, A phases are made；

(2) by 0.1-0.5% glycerine polymethacrylates, 0.2-0.8% hydrolysis Jojobas esters, 0.1-0.5%PEG-40 Rilanit special is added in agitated kettle and is heated with stirring to 70-85 DEG C, and B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 40-55 DEG C, it is ultra-fine to add 0.1-8% Khotan jades Nano powder, 0.1-6% Artemisia japonica extracts, 0.1-8% like gloomy polysaccharides, stir postcooling discharging.

2. the preparation method of moisturizing de-etiolation facial mask as described in claim 1, which is characterized in that include the following steps：

(1) by 7-13% propylene glycol, 0.02-0.04% niacinamide, 6-8% glycerine, 2-4% glycosylglycerols, 12-18% fourths two Alcohol, 2-4% beta glucans, 0.06-0.08% Sodium Hyaluronates, 0.05-0.08% panthenols, 0.2-0.4% allantoins, 0.2- 0.8% hexylene glycol, 0.2-0.4%EDTA disodiums, 0.05-0.18% methyl hydroxybenzoates, 0.05-0.18% ethyl hydroxy benzoates, 0.2- 0.4% hydroxyethyl cellulose, 0.15-0.25% carbomers, deionized water are added in agitated kettle and are heated with stirring to 75-85 DEG C, stir It is complete to mix dissolving, A phases are made；

(2) by 0.2-0.4% glycerine polymethacrylates, 0.5-0.7% hydrolysis Jojobas esters, 0.2-0.4%PEG-40 Rilanit special is added in agitated kettle and is heated with stirring to 75-85 DEG C, and B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 45-55 DEG C, it is ultra-fine to add 0.5-7% Khotan jades Nano powder, 0.2-5% Artemisia japonica extracts, 0.5-7% like gloomy polysaccharides, stir postcooling discharging.

3. the preparation method of moisturizing de-etiolation facial mask as claimed in claim 2, which is characterized in that include the following steps：

(1) 10% propylene glycol, 0.03% niacinamide, 7% glycerine, 3% glycosylglycerol, 15% butanediol, the Portugals 3% β-are gathered Sugar, 0.07% Sodium Hyaluronate, 0.06% panthenol, 0.3% allantoin, 0.5% hexylene glycol, 0.3%EDTA disodiums, 0.1% hydroxyl Benzene methyl, 0.1% ethyl hydroxy benzoate, 0.3% hydroxyethyl cellulose, 0.2% carbomer, deionized water are added in agitated kettle and stir It is heated to 80-85 DEG C, stirring and dissolving is complete, and A phases are made；

(2) 0.3% glycerine polymethacrylates, 0.6% hydrolysis Jojoba esters, 0.3%PEG-40 rilanit specials are added Enter and be heated with stirring to 80-85 DEG C in agitated kettle, B phases are made；

(3) it is slowly stirred down, B is added to A phases, stirs evenly, is cooled to 50-55 DEG C, add 4% Khotan jade superfine nano Powder, 3% Artemisia japonica extract, the 3% gloomy polysaccharides of love, stir postcooling discharging.

4. the preparation method of moisturizing de-etiolation facial mask as described in claim any one of 1-3, which is characterized in that in the step (3) The diameter of Khotan jade superfine nano powder is between 0.01 nanometer -100 nanometers.