CN108296427A - A kind of face layer anti-cracking agent and preparation method thereof - Google Patents
A kind of face layer anti-cracking agent and preparation method thereof Download PDFInfo
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- CN108296427A CN108296427A CN201810042273.0A CN201810042273A CN108296427A CN 108296427 A CN108296427 A CN 108296427A CN 201810042273 A CN201810042273 A CN 201810042273A CN 108296427 A CN108296427 A CN 108296427A
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- layer anti
- cracking agent
- face layer
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- cracking
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22C—FOUNDRY MOULDING
- B22C3/00—Selection of compositions for coating the surfaces of moulds, cores, or patterns
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Abstract
The present invention relates to a kind of face layer anti-cracking agents and preparation method thereof.The face layer anti-cracking agent of the present invention, including following components:Polyacrylamide 0.02 1.0%, polyethylene glycol 0.1 2%, ethylene glycol 10 30%, polyether antifoam agent 0.1 0.3%, surfactant 2 8%, pure water surplus.The face layer anti-cracking agent of the present invention is suitable for being investment precision casting technology, can add in investment precoat, can also add in by coating;The face layer anti-cracking agent of the present invention is suitable for the various powders of essence casting industry, such as zircon sand powder, white alundum powder, brown alundum powder, silica flour, mullite powder;The face layer anti-cracking agent of the present invention is colourless no obvious irritation liquid, is long placed in not stratified;The face layer anti-cracking agent of the present invention is neutrality, on the stability of investment precoat, quality, service life without influence;The face layer anti-cracking agent of this present invention does not influence to cast postprocessing working procedures and workpiece surface quality.
Description
Technical field
The present invention relates to a kind of face layer anti-cracking agents and preparation method thereof.
Background technology
Face layer anti-cracking agent is the compatibility chemicals for adding the normal temperature strength in investment precoat for improving shell, is belonged to
Environmentally friendly formulation product is mainly used for process for making shell in precision-investment casting industry.By the external factor such as humidity and material
Expect the factors such as the coefficient of expansion, the casting of precision-investment casting is usually cracking, scaling and the problems such as surface cracking.Temperature compared with
When low, the humidity in air is relatively low, is deep hole part, the larger workpiece of specific surface area or larger heavier casting for precision castings,
In the drying process of process for making shell, because drying time is long, shell is susceptible to cracking.In the north, humid control is bad to be caused
Shell cracking degree can reach 60%-70%.Precision-investment casting investment precoat main component is zircon sand powder, white alundum powder, palm fibre
Schmigel, silica flour, mullite powder etc., are mainly derived from ore, wherein containing certain impurity, because of the place of production of ore, processing work
Skill is different, and impurity content difference is larger, and different material coefficient of expansion when heated is different, to make shell in steam dewaxing
Face layer is cracked, so as to cause surface quality of continuous castings problem.
Currently, the face layer anti-cracking agent effect type of commercial type is seldom, it is such as poly- substantially to add single polymer
Ethylene glycol etc. increases the normal temperature strength of shell.Polymer belongs to polymer substance, and dissolving is more difficult, and has certain viscosity,
It is added in investment precoat, leads to the poor fluidity of investment precoat, influence mucilage;Meanwhile because investment precoat viscosity becomes larger, stablize
Property be deteriorated, coating it is apt to deteriorate.Therefore it is smaller in actual production process application.In addition, shell goes out in drying process in order to prevent
Existing cracking, water or installation humidifier often spread on the ground in precision-investment casting factory, with the humidity for keeping drying plant certain.This
Method has certain effect to surface cracking, but drying time is longer, and production efficiency reduces, and electricity consumption is big, causes to produce
Cost increases.
Invention content
In view of the deficiencies of the prior art, the object of the present invention is to provide a kind of face layer anti-cracking agents and preparation method thereof.This hair
Bright face layer anti-cracking agent is suitable for investment precision casting technology, can add in investment precoat, can also add in by coating.
The face layer anti-cracking agent of the present invention is neutrality, on the stability of investment precoat, quality and service life without influence, and after not influencing casting
Treatment process and workpiece surface quality.
The present invention is achieved by the following technical solutions:
A kind of face layer anti-cracking agent, including following components:
A kind of face layer anti-cracking agent, including following components:
A kind of face layer anti-cracking agent, including following components:
Preferably, the surfactant is isopropanol polyoxyethylene ether.
The preparation method of above-mentioned face layer anti-cracking agent, includes the following steps:
(1) polyacrylamide, polyethylene glycol are uniformly mixed, obtain mixture A;
(2) mixture A is added in ethylene glycol under stirring condition, obtains mixture B after mixing;
(3) it feeds the mixture into pure water inlet, stirring obtains compound C to being uniformly mixed;
(4) surfactant is added in mixture C, stirring obtains compound D to being uniformly mixed;
(5) polyether antifoam agent is added in compound D, stirring is to uniformly mixed to get face layer anti-cracking agent.
Preferably, the time stirred in step (3) is not less than 24 hours.
Beneficial effects of the present invention:
(1) layer anti-cracking agent in face of the invention is suitable for as investment precision casting technology (Ludox, waterglass or mixing work
Skill) it can add in investment precoat, it can also add in by coating;
(2) layer anti-cracking agent in face of the invention is suitable for the various powders of essence casting industry, such as zircon sand powder, white alundum powder, Brown Alundum
Powder, silica flour, mullite powder etc.;
(3) layer anti-cracking agent in face of the invention is colourless no obvious irritation liquid, is long placed in not stratified;
(4) layer anti-cracking agent in face of the invention is neutrality, on the stability of investment precoat, quality, service life without influence;
(5) the face layer anti-cracking agent of this present invention does not influence to cast postprocessing working procedures and workpiece surface quality.
Specific implementation mode
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
A kind of face layer anti-cracking agent, including following components:
The preparation method of above-mentioned face layer anti-cracking agent, includes the following steps:
(1) polyacrylamide, polyethylene glycol are uniformly mixed, obtain mixture A;
(2) mixture A is added in ethylene glycol under stirring condition, obtains mixture B after mixing;
(3) it feeds the mixture into pure water inlet, stirring obtains compound C in 24 hours to being uniformly mixed;
(4) isopropanol polyoxyethylene ether is added in mixture C, stirring obtains compound D to being uniformly mixed;
(5) polyether antifoam agent antifoaming agent is added in compound D, stirring is to uniformly mixed to get face layer anti-cracking agent.
Embodiment 2
A kind of face layer anti-cracking agent, including following components:
The preparation method of above-mentioned face layer anti-cracking agent, includes the following steps:
(1) polyacrylamide, polyethylene glycol are uniformly mixed, obtain mixture A;
(2) mixture A is added in ethylene glycol under stirring condition, obtains mixture B after mixing;
(3) it feeds the mixture into pure water inlet, stirring obtains compound C in 26 hours to being uniformly mixed;
(4) isopropanol polyoxyethylene ether is added in mixture C, stirring obtains compound D to being uniformly mixed;
(5) polyether antifoam agent antifoaming agent is added in compound D, stirring is to uniformly mixed to get face layer anti-cracking agent.
Embodiment 3
A kind of face layer anti-cracking agent, including following components:
The preparation method of above-mentioned face layer anti-cracking agent, includes the following steps:
(1) polyacrylamide, polyethylene glycol are uniformly mixed, obtain mixture A;
(2) mixture A is added in ethylene glycol under stirring condition, obtains mixture B after mixing;
(3) it feeds the mixture into pure water inlet, stirring obtains compound C in 25 hours to being uniformly mixed;
(4) isopropanol polyoxyethylene ether is added in mixture C, stirring obtains compound D to being uniformly mixed;
(5) polyether antifoam agent is added in compound D, stirring is to uniformly mixed to get face layer anti-cracking agent.
Claims (6)
1. a kind of face layer anti-cracking agent, which is characterized in that including following components:
2. layer anti-cracking agent in face according to claim 1, which is characterized in that including following components:
3. layer anti-cracking agent in face according to claim 2, which is characterized in that including following components:
4. layer anti-cracking agent in face according to any one of claim 1-3, which is characterized in that the surfactant is isopropyl
Alcohol polyoxyethylene ether.
5. the preparation method of the face layer anti-cracking agent described in any one of claim 1-4, which is characterized in that include the following steps:
(1) polyacrylamide, polyethylene glycol are uniformly mixed, obtain mixture A;
(2) mixture A is added in ethylene glycol under stirring condition, obtains mixture B after mixing;
(3) it feeds the mixture into pure water inlet, stirring obtains compound C to being uniformly mixed;
(4) surfactant is added in mixture C, stirring obtains compound D to being uniformly mixed;
(5) polyether antifoam agent is added in compound D, stirring is to uniformly mixed to get face layer anti-cracking agent.
6. the preparation method of layer anti-cracking agent in face according to claim 5, which is characterized in that the time stirred in step (3)
To be not less than 24 hours.
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CN201810042273.0A CN108296427B (en) | 2018-01-17 | 2018-01-17 | A kind of surface layer anti-cracking agent and preparation method thereof |
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CN108296427A true CN108296427A (en) | 2018-07-20 |
CN108296427B CN108296427B (en) | 2019-08-23 |
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Citations (10)
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CA1007004A (en) * | 1972-04-19 | 1977-03-22 | Vestshell Inc. | Composition and method for forming an improved shell mold |
JPS5365220A (en) * | 1976-11-25 | 1978-06-10 | Nippon Steel Corp | Mold paint for steel ingot casting |
SU685409A1 (en) * | 1978-01-31 | 1979-09-15 | Lebedeva Genrietta M | Burn-on preventing coating |
JPS5540100A (en) * | 1979-09-17 | 1980-03-21 | Nippon Steel Corp | Casting process of steel ingot for rolling |
JPS58119433A (en) * | 1982-01-07 | 1983-07-15 | Sumitomo Deyurezu Kk | Resin coated sand for shell mold |
CN101099988A (en) * | 2007-08-02 | 2008-01-09 | 哈尔滨工业大学 | Casting titanium and titanium-aluminide alloy ceramic type backing layer paint and its preparation method |
CN104624923A (en) * | 2015-03-02 | 2015-05-20 | 深圳市千里行新材料有限公司 | Casting uniform mixing agent and manufacturing method |
CN105798225A (en) * | 2014-12-27 | 2016-07-27 | 嘉兴市亚达特种钢铸造有限公司 | Anti-crack enhanced complexing agent for fired mold precision casting paint and application thereof |
CN107030250A (en) * | 2017-04-01 | 2017-08-11 | 东风精密铸造安徽有限公司 | A kind of process for making shell of model casting |
CN107052228A (en) * | 2017-03-30 | 2017-08-18 | 惠州市吉邦精密技术有限公司 | A kind of high-efficiency and precision casts shell coating quick dry agent processed |
-
2018
- 2018-01-17 CN CN201810042273.0A patent/CN108296427B/en active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA1007004A (en) * | 1972-04-19 | 1977-03-22 | Vestshell Inc. | Composition and method for forming an improved shell mold |
JPS5365220A (en) * | 1976-11-25 | 1978-06-10 | Nippon Steel Corp | Mold paint for steel ingot casting |
SU685409A1 (en) * | 1978-01-31 | 1979-09-15 | Lebedeva Genrietta M | Burn-on preventing coating |
JPS5540100A (en) * | 1979-09-17 | 1980-03-21 | Nippon Steel Corp | Casting process of steel ingot for rolling |
JPS58119433A (en) * | 1982-01-07 | 1983-07-15 | Sumitomo Deyurezu Kk | Resin coated sand for shell mold |
CN101099988A (en) * | 2007-08-02 | 2008-01-09 | 哈尔滨工业大学 | Casting titanium and titanium-aluminide alloy ceramic type backing layer paint and its preparation method |
CN105798225A (en) * | 2014-12-27 | 2016-07-27 | 嘉兴市亚达特种钢铸造有限公司 | Anti-crack enhanced complexing agent for fired mold precision casting paint and application thereof |
CN104624923A (en) * | 2015-03-02 | 2015-05-20 | 深圳市千里行新材料有限公司 | Casting uniform mixing agent and manufacturing method |
CN107052228A (en) * | 2017-03-30 | 2017-08-18 | 惠州市吉邦精密技术有限公司 | A kind of high-efficiency and precision casts shell coating quick dry agent processed |
CN107030250A (en) * | 2017-04-01 | 2017-08-11 | 东风精密铸造安徽有限公司 | A kind of process for making shell of model casting |
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