CN104624923A - Casting uniform mixing agent and manufacturing method - Google Patents
Casting uniform mixing agent and manufacturing method Download PDFInfo
- Publication number
- CN104624923A CN104624923A CN201510092341.0A CN201510092341A CN104624923A CN 104624923 A CN104624923 A CN 104624923A CN 201510092341 A CN201510092341 A CN 201510092341A CN 104624923 A CN104624923 A CN 104624923A
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- CN
- China
- Prior art keywords
- parts
- casting
- rotating speed
- uniform mixing
- mixing agent
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000005266 casting Methods 0.000 title claims abstract description 24
- 238000002156 mixing Methods 0.000 title abstract description 6
- 238000004519 manufacturing process Methods 0.000 title description 6
- 238000003756 stirring Methods 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 11
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 11
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 11
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 18
- 239000000463 material Substances 0.000 claims description 11
- 238000012856 packing Methods 0.000 claims description 10
- 241001272567 Hominoidea Species 0.000 claims description 9
- PRPAGESBURMWTI-UHFFFAOYSA-N [C].[F] Chemical compound [C].[F] PRPAGESBURMWTI-UHFFFAOYSA-N 0.000 claims description 9
- 239000004094 surface-active agent Substances 0.000 claims description 9
- 229920001617 Vinyon Polymers 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 230000003068 static effect Effects 0.000 claims description 6
- 239000000843 powder Substances 0.000 abstract description 27
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 16
- 239000011812 mixed powder Substances 0.000 abstract description 9
- 239000005350 fused silica glass Substances 0.000 abstract description 8
- 239000011248 coating agent Substances 0.000 abstract description 7
- 238000000576 coating method Methods 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 7
- 239000004576 sand Substances 0.000 abstract description 7
- 239000002344 surface layer Substances 0.000 abstract description 3
- 239000003795 chemical substances by application Substances 0.000 abstract 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 abstract 2
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 abstract 2
- 239000002736 nonionic surfactant Substances 0.000 abstract 2
- -1 polyoxyethylene Polymers 0.000 abstract 2
- 239000008213 purified water Substances 0.000 abstract 2
- 229910052845 zircon Inorganic materials 0.000 abstract 2
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 abstract 2
- 238000004806 packaging method and process Methods 0.000 abstract 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 18
- 229910052726 zirconium Inorganic materials 0.000 description 18
- 238000004140 cleaning Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 235000013312 flour Nutrition 0.000 description 3
- 230000008676 import Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000011819 refractory material Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 1
- 238000005058 metal casting Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22C—FOUNDRY MOULDING
- B22C3/00—Selection of compositions for coating the surfaces of moulds, cores, or patterns
Abstract
The invention discloses a casting uniform mixing agent. The casting uniform mixing agent comprises the following components in parts by weight: 100 parts of purified water, 5-10 parts of polyaluminum silicate chloride, 1-5 parts of polyacrylamide, 5-10 parts of organobentonite, 1-5 parts of polyethylene glycol, 1-2 parts of fluorocarbon non-ionic surfactants, and 0.5-1 percent of alkylphenol polyoxyethylene. A preparation method of the casting uniform mixing agent comprises the following steps: pouring the purified water into a clean chemical reaction kettle; heating to reach 50-60 DEG C and starting a stirrer again; slowly adding polyacrylamide and polyaluminum silicate chloride and stirring for 15-20 minutes; continuously adding the organobentonite and polyethylene glycol and stirring for 30-40 minutes; continuously adding the fluorocarbon non-ionic surfactants and alkylphenol polyoxyethylene and stirring for 60-120 minutes and stopping heating; and standing for 1-2 hours and sub-packaging. The casting uniform mixing agent is added into a mixture of fused quartz powder and zircon power to prepare a surface layer coating and a mixed powder process can reach or exceed a full zircon power process; moreover, the casting cost is reduced, and the sand clearing difficulty is reduced.
Description
Technical field
The present invention is mainly used in model casting industry, relates to equal mixture of shell surface layer coating and preparation method thereof.
Background technology
Model casting industry, shell is the prerequisite obtaining premium casting, and the investment precoat of shell is then crucial especially.
Traditional investment precoat adopts full zirconium English powder to make Main Refractory, the metal casting excellent surface quality of its technique cast, but it is large also to there is cost of manufacture, and resource is petered out, the defect that sand removal difficulty is large.
At present, the zirconium English powder overwhelming majority raw material needed for China's model casting all relies on from Australian import, and price constantly rises, and import channel is extremely not smooth, causes China's foundry enterprise to face great survival pressure.
In view of the foregoing, domestic foundry industry finds relative low price one after another, supply refractory material that is stable, Domestic Resources relative abundance replaces or part replaces zirconium English powder.
Current best bet is: the fused quartz powder abundant with Domestic Resources mixes with import zirconium English powder, then makes investment precoat with mixed powder, and technique makes shell routinely.Because the density difference of fused quartz powder and zirconium English powder is too large, so the investment precoat extremely unstable made, cause the casting quality of cast also unstable, quality requirement and the standard of full zirconium English powder craft cannot be reached, more cannot realize reducing production cost, alleviate the target of sand removal difficulty and refractory material production domesticization.
Summary of the invention
The technical problem to be solved in the present invention is: overcome the not good defect of casting quality adopting the mixed powder of fused quartz powder and zirconium English powder to make the unstability of investment precoat, cast, the equal mixture of a kind of casting is proposed, join in the mixture of fused quartz powder and zirconium English powder and make investment precoat, this mixed powder technique meets or exceeds full zirconium English powder craft, and makes the reduction of casting cost, the reduction of sand removal difficulty.
In order to solve the problems of the technologies described above, the present invention proposes following technical proposal: the equal mixture of a kind of casting, it is made up of the following component according to weight parts: pure water 100 parts, polysilicate aluminum chloride 5-10 part, polyacrylamide 1-5 part, organobentonite 5-10 part, polyethylene glycol 1-5 part, fluorine carbon non-ionic surface active agent 1-2 part, APES 0.5-1%.
In order to solve the problems of the technologies described above, the present invention proposes following technical proposal: the preparation method of the equal mixture of described casting, it comprises the following steps:
Step 1: pure water is put into clean chemical reaction still, then heat to 50-60 DEG C, restart agitator, its rotating speed controls at 50-100R/min;
Step 2: slowly add polyacrylamide, polysilicate aluminum chloride, rotating speed controls in 50-100R/min situation, stirs 15-20 minute;
Step 3: continue to add organobentonite, polyethylene glycol, rotating speed is adjusted to 100-150R/min, stirs 30-40 minute;
Step 4: continue to add fluorine carbon non-ionic surface active agent, APES, rotating speed is adjusted to 50-100R/min, stirs 60-120 minute, then stops heating, and temperature is controlled at 20-30 DEG C;
Step 5: static 1-2 hour, carries out packing, and packing material must be vinyon material and have the pail pack of sealing function.
The present invention compares conventional method and has following effect: significantly decrease the dependence to zirconium English powder, reduce production cost, and flour mixed with adulterants coating is stablized, and the foundry goods of its shell made, cast reaches the quality requirement of full zirconium English powder craft completely.Add the collapsibility of arenaceous shell, alleviate the cleaning difficulty of the residual sand of cast(ing) surface.
Detailed description of the invention
The present invention proposes the equal mixture of a kind of casting, add in the process of the mixture making investment precoat with fused quartz powder and zirconium English powder, this addition of casting equal mixture accounts for the 1.5-3% of whole investment precoat mass percent, other composition of flour mixed with adulterants coating is constant, preparation method is also constant, the casting quality of its cast meets or exceeds the requirement of full zirconium English powder craft, and cast(ing) surface residual sand cleaning difficulty significantly alleviates.
The equal mixture of above-mentioned casting, be made up of the following component according to weight parts: pure water 100 parts, polysilicate aluminum chloride 5-10 part, polyacrylamide 1-5 part, organobentonite 5-10 part, polyethylene glycol 1-5 part, fluorine carbon non-ionic surface active agent 1-2 part, APES 0.5-1%.
The preparation method of the equal mixture of described casting, comprises the following steps:
Step 1: pure water is put into clean chemical reaction still, then heat to 50-60 DEG C, restart agitator, its rotating speed controls at 50-100R/min;
Step 2: slowly add polyacrylamide, polysilicate aluminum chloride, rotating speed controls in 50-100R/min situation, stirs 15-20 minute;
Step 3: continue to add organobentonite, polyethylene glycol, rotating speed is adjusted to 100-150R/min, stirs 30-40 minute;
Step 4: continue to add fluorine carbon non-ionic surface active agent, APES, rotating speed is adjusted to 50-100R/min, stirs 60-120 minute, then stops heating, and temperature is controlled at 20-30 DEG C;
Step 5: static 1-2 hour, carries out packing, and packing material must be vinyon material and have the pail pack of sealing function.
Preparation embodiment 1
Pure water 100 parts is put into clean chemical reaction still, then heats to 50-60 DEG C, restart agitator, its rotating speed controls at 50-100R/min;
Step 2: slowly add polyacrylamide 1 part, polysilicate aluminum chloride 8 parts, rotating speed controls in 50-100R/min situation, stirs 15-20 minute;
Step 3: continue to add organobentonite 5 parts, polyethylene glycol 3 parts, rotating speed is adjusted to 100-150R/min, stirs 30-40 minute;
Step 4: continue to add fluorine carbon non-ionic surface active agent 2 parts, APES 0.8%, rotating speed is adjusted to 50-100R/min, stirs 60-120 minute, then stops heating, and temperature is controlled at 20-30 DEG C;
Step 5: static 1-2 hour, carries out packing, and packing material must be vinyon material and have the pail pack of sealing function.
Preparation embodiment 2
Pure water 100 parts is put into clean chemical reaction still, then heats to 50-60 DEG C, restart agitator, its rotating speed controls at 50-100R/min;
Step 2: slowly add polyacrylamide 3 parts, polysilicate aluminum chloride 5 parts, rotating speed controls in 50-100R/min situation, stirs 15-20 minute;
Step 3: continue to add organobentonite 10 parts, polyethylene glycol 1 part, rotating speed is adjusted to 100-150R/min, stirs 30-40 minute;
Step 4: continue to add fluorine carbon non-ionic surface active agent 1.5 parts, APES 0.5%, rotating speed is adjusted to 50-100R/min, stirs 60-120 minute, then stops heating, and temperature is controlled at 20-30 DEG C;
Step 5: static 1-2 hour, carries out packing, and pail pack must be the pail pack having sealing function of vinyon material.
Preparation embodiment 3
Pure water 100 parts is put into clean chemical reaction still, then heats to 50-60 DEG C, restart agitator, its rotating speed controls at 50-100R/min;
Step 2: slowly add polyacrylamide 5 parts, polysilicate aluminum chloride 10 parts, rotating speed controls in 50-100R/min situation, stirs 15-20 minute;
Step 3: continue to add organobentonite 8 parts, polyethylene glycol 5 parts, rotating speed is adjusted to 100-150R/min, stirs 30-40 minute;
Step 4: continue to add fluorine carbon non-ionic surface active agent 1 part, APES 1%, rotating speed is adjusted to 50-100R/min, stirs 60-120 minute, then stops heating, and temperature is controlled at 20-30 DEG C;
Step 5: static 1-2 hour, carries out packing, and packing material must be vinyon material and have the pail pack of sealing function.
The related index parameter that the present invention casts equal mixture is as shown in the table:
Outward appearance | The sticky mixing material of colourless-light yellowish |
Density 25 DEG C, g/cm3 | 1.03-1.05 |
PH value, 25 DEG C | 7-8 |
Dissolubility in water | Soluble in water |
Kinematic viscosity, 25 DEG C | 250-300 centistoke |
Security | Do not fire not quick-fried, corrosion-free |
Flash-point | Nothing |
Solid content | 11.89-24.81% |
Adding the present invention, to cast the related index parameter of the surface layer mixed powder that equal mixture is made as shown in the table:
Coating forms | Zirconium English powder, fused quartz powder, Ludox, all mixture |
Mixed powder forms | Zirconium English powder 30-50%, fused quartz powder 50-70% |
The each component content of coating | Equal mixture 1.5-3%, mixed powder 24.5-26.5%, mixed powder 72.5-75.5% |
Dope viscosity (¢ 6.100ml) | 45-120 second |
Smear weight | 0.55-0.65g |
Liquid powder ratio | 1:(2.8—3.5) |
The full zirconium English powder craft of tradition with add the related index contrast table that the present invention casts the mixed powder technique that equal mixture is made:
The present invention compares conventional method and has following effect: significantly decrease the dependence to zirconium English powder, reduce production cost.Flour mixed with adulterants coating is stablized, and the foundry goods of its shell made, cast reaches the quality of full zirconium English powder craft completely.Add the collapsibility of arenaceous shell, alleviate the cleaning difficulty of the residual sand of cast(ing) surface.
Claims (2)
1. the equal mixture of casting, it is made up of the following component according to weight parts: pure water 100 parts, polysilicate aluminum chloride 5-10 part, polyacrylamide 1-5 part, organobentonite 5-10 part, polyethylene glycol 1-5 part, fluorine carbon non-ionic surface active agent 1-2 part, APES 0.5-1%.
2. the preparation method of the equal mixture of casting according to claim 1, it is characterized in that, it comprises the following steps:
Step 1: pure water is put into clean chemical reaction still, then heat to 50-60 DEG C, restart agitator, its rotating speed controls at 50-100R/min;
Step 2: slowly add polyacrylamide, polysilicate aluminum chloride, rotating speed controls in 50-100R/min situation, stirs 15-20 minute;
Step 3: continue to add organobentonite, polyethylene glycol, rotating speed is adjusted to 100-150R/min, stirs 30-40 minute;
Step 4: continue to add fluorine carbon non-ionic surface active agent, APES, rotating speed is adjusted to 50-100R/min, stirs 60-120 minute, then stops heating, and temperature is controlled at 20-30 DEG C;
Step 5: static 1-2 hour, carries out packing, and pail pack must be the pail pack having sealing function of vinyon material.
Priority Applications (1)
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CN201510092341.0A CN104624923B (en) | 2015-03-02 | 2015-03-02 | The equal mixture of a kind of casting and preparation method |
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CN201510092341.0A CN104624923B (en) | 2015-03-02 | 2015-03-02 | The equal mixture of a kind of casting and preparation method |
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CN104624923A true CN104624923A (en) | 2015-05-20 |
CN104624923B CN104624923B (en) | 2016-09-07 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108296427A (en) * | 2018-01-17 | 2018-07-20 | 江门市新灵科技有限公司 | A kind of face layer anti-cracking agent and preparation method thereof |
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CN101015850A (en) * | 2007-01-24 | 2007-08-15 | 中国重型汽车集团有限公司 | Water borne coating for metal mold casting and its prepn. |
CN102000762A (en) * | 2010-11-08 | 2011-04-06 | 上海市机械制造工艺研究所有限公司 | Combined coating layer process for large-scale steel casting water glass sand molds |
CN103586406A (en) * | 2013-11-27 | 2014-02-19 | 吴江市液铸液压件铸造有限公司 | Casting coating for stainless steel valve body and preparation method thereof |
CN103817290A (en) * | 2014-03-17 | 2014-05-28 | 中国科学院金属研究所 | Preparation method for precision casting of large-size thin-wall titanium alloy bucket body structure |
-
2015
- 2015-03-02 CN CN201510092341.0A patent/CN104624923B/en not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101015850A (en) * | 2007-01-24 | 2007-08-15 | 中国重型汽车集团有限公司 | Water borne coating for metal mold casting and its prepn. |
CN102000762A (en) * | 2010-11-08 | 2011-04-06 | 上海市机械制造工艺研究所有限公司 | Combined coating layer process for large-scale steel casting water glass sand molds |
CN103586406A (en) * | 2013-11-27 | 2014-02-19 | 吴江市液铸液压件铸造有限公司 | Casting coating for stainless steel valve body and preparation method thereof |
CN103817290A (en) * | 2014-03-17 | 2014-05-28 | 中国科学院金属研究所 | Preparation method for precision casting of large-size thin-wall titanium alloy bucket body structure |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108296427A (en) * | 2018-01-17 | 2018-07-20 | 江门市新灵科技有限公司 | A kind of face layer anti-cracking agent and preparation method thereof |
CN108296427B (en) * | 2018-01-17 | 2019-08-23 | 江门市新灵科技有限公司 | A kind of surface layer anti-cracking agent and preparation method thereof |
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CN104624923B (en) | 2016-09-07 |
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C53 | Correction of patent of invention or patent application | ||
CB03 | Change of inventor or designer information |
Inventor after: Wu Hao Inventor after: Wu Yaozu Inventor before: Wu Yaozu Inventor before: Wu Hao Inventor before: Xiong Shiyong Inventor before: Zhang Qingjiang Inventor before: Zong Rongfeng |
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COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: WU YAOZU WU HAO XIONG SHIYONG ZHANG QINGJIANG ZONG RONGFENG TO: WU HAO WU YAOZU |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160907 |
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