CN108261459A - Treat Chinese medicine composition of pet calculus and preparation method thereof - Google Patents

Treat Chinese medicine composition of pet calculus and preparation method thereof Download PDF

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Publication number
CN108261459A
CN108261459A CN201611268677.9A CN201611268677A CN108261459A CN 108261459 A CN108261459 A CN 108261459A CN 201611268677 A CN201611268677 A CN 201611268677A CN 108261459 A CN108261459 A CN 108261459A
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parts
chinese medicine
medicine composition
calculus
pet
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李迎梅
安同伟
孙建
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Tianjin Rebate Science and Technology Development Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/11—Pteridophyta or Filicophyta (ferns)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
    • A61K33/12—Magnesium silicate
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/02—Algae
    • A61K36/03—Phaeophycota or phaeophyta (brown algae), e.g. Fucus
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/484—Glycyrrhiza (licorice)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/59—Menispermaceae (Moonseed family), e.g. hyperbaena or coralbead
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/68—Plantaginaceae (Plantain Family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/75—Rutaceae (Rue family)
    • A61K36/752—Citrus, e.g. lime, orange or lemon
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50—Methods involving additional extraction steps
    • A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50—Methods involving additional extraction steps
    • A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

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Abstract

The present invention relates to a kind of Chinese medicine composition for treating pet calculus, the component and its ratio of weight and number of Chinese medicine composition are respectively：10 30 parts of stone reed；10 40 parts of desmodium；10 40 parts of talcum；10 40 parts of plantain seed；10 40 parts of chingma abutilon seed；5 20 parts of Fructus Aurantii；5 20 parts of stephanotis；5 20 parts of kelp；10 40 parts of Radix Glycyrrhizae.Inventive formulation composition is scientific and reasonable, and sluicing is dried, and defaecation is moisturized, broken product softening hard masses, is had no toxic side effect, will not be generated medicament residue, can effectively treat the illnesss such as pet lithangiuria, difficulty and pain in micturition, dry and hard excrement.

Description

Treat Chinese medicine composition of pet calculus and preparation method thereof
Technical field
The invention belongs to field of veterinary, especially a kind of Chinese medicine composition for treating pet calculus and preparation method thereof.
Background technology
The most common type of pet calculus has struvite calculus, calcinm oxalate calculus, urate calculi, cystine stone etc.. Wherein struvite calculus is more universal, wherein canine, quantity of falling ill 85% for bitch, have it is larger it is a risk that：Beijing breathe out Dog, short-leg Dachshund, mini Xue Narui, dalmatian, bulldag, Wales dog, beagling beagle, basset and Dandie dinmont etc..Cat class, illness as struvite calculus are commonplace with queen cat.Distinctive with male cat is bird Coprolite urethral obstruction.The small calculus of general diameter can interfere its urine in the urethra of male cat, so as to cause life danger.If One cat can not urine, it is necessary to the rescue of animal doctor.The present invention starts with from pathogenic factor, shortens illness pet recovery time Calculus can be inherently eliminated.
Invention content
The purpose of the present invention is to provide a kind of Chinese medicine composition for treating pet calculus, Chinese medicine composition sluicing is gone Wet, defaecation is moisturized, broken product softening hard masses, is had no toxic side effect, will not be generated medicament residue, can effectively treat pet lithangiuria, urine The illnesss such as puckery pain, dry and hard excrement.
It is another object of the present invention to provide a kind of preparation methods for the Chinese medicine composition for treating pet calculus.
The present invention is achieved by the following technical solutions：
A kind of Chinese medicine composition for treating pet calculus, the component and its ratio of weight and number of Chinese medicine composition are respectively：
10-30 parts of stone reed；
10-40 parts of desmodium；
10-40 parts of talcum；
10-40 parts of plantain seed；
10-40 parts of chingma abutilon seed；
5-20 parts of Fructus Aurantii；
5-20 parts of stephanotis；
5-20 parts of kelp；
10-40 parts of Radix Glycyrrhizae.
A kind of preparation method for the Chinese medicine composition for treating pet calculus, its step are as follows：
(1) stone reed, desmodium, talcum, plantain seed, Fructus Aurantii, stephanotis, kelp, Radix Glycyrrhizae are weighed by weight ratio, after mixing, 8 times of amounts of mixture weight, 6 times of amount water is added to decoct twice, 1 hour every time, decocting liquid obtained A decocting liquids after merging, spare；
(2) chingma abutilon seed is weighed according to weight proportion, added water to cook after crushing 3 times, 2 hours for the first time, second and third Secondary each 1 hour, merge decoction liquor, filtration, filtrate is concentrated into relative density and is 1.20~1.25 and adds in 2mol/L at 60 DEG C Hydrochloric acid solution adjusts pH value to 1.0~2.0, keeps the temperature 1 hour, stands 12 hours, filtration is precipitated, and 6~8 are added into precipitation Times amount water, formed mixed liquor, with 40% sodium hydroxide solution tune pH value to 7.0, then add with mixed liquor in equal volume it is a concentration of 95% ethanol solution, is stirred to dissolve, and filtration, filtrate 2mol/L hydrochloric acid solution tune pH value to 2.0 is protected at 50~60 DEG C Temperature 20~30 minutes stands 12 hours, and filtration, precipitation is washed till pH value to 7.0 with ethyl alcohol, after waving most ethyl alcohol, with institute in step (1) A decocting liquids merge, be concentrated into density and reach 1.20g/ml and obtain B decocting liquids, it is spare；
(3), by the spray-dried device of B decocting liquids obtained by step (2), under the conditions of 120 DEG C, fine powder is spray dried to get controlling Treat the Chinese medicine composition finished product of pet calculus.
Advantages of the present invention and advantageous effect are：
1st, the stone reed in the Chinese medicine composition of this treatment pet calculus, desmodium, talcum, plantain seed, Fructus Aurantii, stephanotis, Kelp, Radix Glycyrrhizae there is good sluicing to dry, defaecation is moisturized, broken the effect of product softening hard masses, nontoxic secondary work as natural traditional Chinese medicine composition With, medicament residue will not be generated, it is easy to use.
2nd, the invention by after the extracted process of Chinese medicine composition, using spray drying device by extracting solution It quickly dusts, changes previous conventional drying processes, greatly reduce production time and production cost, protect traditional Chinese medicine extraction Active ingredient in object will not go bad at high temperature.The high-speed rotating nozzle of the spray-dried device of Chinese medicine extract need not after spraying It crushes, is dried to micropowders rapidly, absorbed conducive to pet body, dosage and time of administration can be greatly reduced, reduce cultivation Cost.
Specific embodiment
The present invention is described in further detail by following embodiment.It should be noted that：Following embodiments are illustrative, are not It is limited, it is impossible to limit protection scope of the present invention with following embodiments.
Stone reed, desmodium, chingma abutilon seed, talcum, plantain seed, Fructus Aurantii, stephanotis, kelp, Radix Glycyrrhizae in the present invention can be with It is commercially available on the market.
Embodiment 1
A kind of Chinese medicine composition for treating pet calculus, its composition component and its weight are respectively：Stone reed 10kg；Money Careless 10kg, talcum 10kg, plantain seed 10kg, chingma abutilon seed 10kg, Fructus Aurantii 5kg, stephanotis 5kg, kelp 5kg, Radix Glycyrrhizae 10kg.
A kind of preparation method for the Chinese medicine composition for treating pet calculus, its step are as follows：
(1) stone reed, desmodium, talcum, plantain seed, Fructus Aurantii, stephanotis, kelp, Radix Glycyrrhizae are weighed by weight ratio, after mixing, 8 times of amounts of mixture weight, 6 times of amount water is added to decoct twice, 1 hour every time, decocting liquid obtained A decocting liquids after merging, spare；
(2) chingma abutilon seed is weighed according to weight proportion, added water to cook after crushing 3 times, 2 hours for the first time, second and third Secondary each 1 hour, merge decoction liquor, filtration, filtrate is concentrated into relative density and is 1.20~1.25 and adds in 2mol/L at 60 DEG C Hydrochloric acid solution adjusts pH value to 1.0~2.0, keeps the temperature 1 hour, stands 12 hours, filtration is precipitated, and 6~8 are added into precipitation Times amount water, formed mixed liquor, with 40% sodium hydroxide solution tune pH value to 7.0, then add with mixed liquor in equal volume it is a concentration of 95% ethanol solution, is stirred to dissolve, and filtration, filtrate 2mol/L hydrochloric acid solution tune pH value to 2.0 is protected at 50~60 DEG C Temperature 20~30 minutes stands 12 hours, and filtration, precipitation is washed till pH value to 7.0 with ethyl alcohol, after waving most ethyl alcohol, with institute in step (1) A decocting liquids merge, be concentrated into density and reach 1.20g/ml and obtain B decocting liquids, it is spare；
(3), by the spray-dried device of B decocting liquids obtained by step (2), under the conditions of 120 DEG C, fine powder is spray dried to get controlling Treat the Chinese medicine composition finished product of pet calculus.
Embodiment 2
A kind of Chinese medicine composition for treating pet calculus, its composition component and its weight are respectively：Stone reed 30g；Money Careless 40g, talcum 40g, plantain seed 40g, chingma abutilon seed 40g, Fructus Aurantii 20g, stephanotis 20g, kelp 20g, Radix Glycyrrhizae 40g.
The step of preparation method, is the same as embodiment 1.
10-30 parts of stone reed；10-40 parts of desmodium；10-40 parts of talcum；10-40 parts of plantain seed；10-40 parts of chingma abutilon seed；Trifoliate orange 5-20 parts of shell；5-20 parts of stephanotis；5-20 parts of kelp；10-40 parts of Radix Glycyrrhizae.
Embodiment 3
A kind of Chinese medicine composition for treating pet calculus, its composition component and its weight are respectively：Stone reed 20kg；Stone reed 20g；Desmodium 30g, talcum 30g, plantain seed 30g, chingma abutilon seed 30g, Fructus Aurantii 10g, stephanotis 10g, kelp 10g, Radix Glycyrrhizae 30g.
The step of preparation method, is the same as embodiment 1.
The present invention can be admixed directly in dog cat drinking-water, and dosage presses dog 6g/kg weight；Cat 3g/kg batheroom scales, 5 days are one A course for the treatment of.
Clinical practice is tested
1st, test method
Treatment (its of the present invention is carried out with calculus ox head stalk to third time in Qingdao pet clinic in June, 2014 It is preceding to use operative treatment twice), tracking statistics treatment results.
2nd, result of the test
Symptom before treatment：The ox head Terrier with kidney stone is made a definite diagnosis by clapping X-ray, some exceptions occurs in urinary system There is frequent micturition in symptom, oliguresis, urination have the symptoms such as feeling of pain, hematuria.
Using present invention administration 3 days, though there is microlith discharge successively, frequency symptoms mitigated, no blood urine；Present invention treatment 5 After it, urodynamic symptom completely disappears.

Claims (2)

1. a kind of Chinese medicine composition for treating pet calculus, it is characterised in that：The component and its parts by weight of the Chinese medicine composition Than being respectively：
10-30 parts of stone reed；
10-40 parts of desmodium；
10-40 parts of talcum；
10-40 parts of plantain seed；
10-40 parts of chingma abutilon seed；
5-20 parts of Fructus Aurantii；
5-20 parts of stephanotis；
5-20 parts of kelp；
10-40 parts of Radix Glycyrrhizae.
2. a kind of preparation method of the Chinese medicine composition for the treatment of pet calculus as described in claim 1, it is characterised in that：The system The step of Preparation Method is：
(1) stone reed, desmodium, talcum, plantain seed, Fructus Aurantii, stephanotis, kelp, Radix Glycyrrhizae are weighed by weight ratio, after mixing, are added mixed 8 times of amounts of polymer weight, 6 times of amount water decoct twice, and 1 hour every time, decocting liquid obtained A decocting liquids after merging, spare；
(2) chingma abutilon seed is weighed according to weight proportion, added water to cook after crushing 3 times, 2 hours for the first time, for the second time and third time was each 1 hour, merge decoction liquor, filtration, filtrate is concentrated into relative density as 1.20~1.25 and the addition 2mol/L hydrochloric acid at 60 DEG C Solution adjusts pH value to 1.0~2.0, keeps the temperature 1 hour, stands 12 hours, filtration is precipitated, and 6~8 times of amounts are added into precipitation Water forms mixed liquor, with 40% sodium hydroxide solution tune pH value to 7.0, then adds a concentration of 95% isometric with mixed liquor Ethanol solution is stirred to dissolve, filtration, filtrate 2mol/L hydrochloric acid solution tune pH value to 2.0, at 50~60 DEG C keep the temperature 20~ 30 minutes, 12 hours are stood, filtration, precipitation is washed till pH value to 7.0 with ethyl alcohol, after waving most ethyl alcohol, is decocted with gained A in step (1) Liquid merges, and is concentrated into density and reaches 1.20g/ml and obtains B decocting liquids, spare；
(3), by the spray-dried device of B decocting liquids obtained by step (2), under the conditions of 120 DEG C, it is spray dried to fine powder and dotes on to get treatment The Chinese medicine composition finished product of object calculus.
CN201611268677.9A 2016-12-31 2016-12-31 Treat Chinese medicine composition of pet calculus and preparation method thereof Pending CN108261459A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114452359A (en) * 2022-01-28 2022-05-10 北京爱宠族科技有限公司 Traditional Chinese medicine composition for preventing and treating pet urinary calculus and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103656021A (en) * 2012-09-24 2014-03-26 天津瑞贝特科技发展有限公司 Traditional Chinese medicinal composition for livestock with effects of relieving stagnant qi and dissipating swelling, and relaxing bowel, as well as preparation method of traditional Chinese medicinal composition
CN104784251A (en) * 2015-05-11 2015-07-22 李汶峰 Traditional Chinese medicine for treating urinary calculus

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103656021A (en) * 2012-09-24 2014-03-26 天津瑞贝特科技发展有限公司 Traditional Chinese medicinal composition for livestock with effects of relieving stagnant qi and dissipating swelling, and relaxing bowel, as well as preparation method of traditional Chinese medicinal composition
CN104784251A (en) * 2015-05-11 2015-07-22 李汶峰 Traditional Chinese medicine for treating urinary calculus

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
吴娅玲: "排石汤治疗泌尿系结石64例", 《实用中医药杂志》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114452359A (en) * 2022-01-28 2022-05-10 北京爱宠族科技有限公司 Traditional Chinese medicine composition for preventing and treating pet urinary calculus and preparation method thereof

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