CN108245657A - A kind of anti-corona fragrant spray and preparation method thereof - Google Patents

A kind of anti-corona fragrant spray and preparation method thereof Download PDF

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Publication number
CN108245657A
CN108245657A CN201810145979.XA CN201810145979A CN108245657A CN 108245657 A CN108245657 A CN 108245657A CN 201810145979 A CN201810145979 A CN 201810145979A CN 108245657 A CN108245657 A CN 108245657A
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CN
China
Prior art keywords
corona
hyoscine
fragrant
spray
oil
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Pending
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CN201810145979.XA
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Chinese (zh)
Inventor
黄惠明
吴水金
李海明
李跃森
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Institute Of Subtropical Agriculture Fujian Academy Of Agricultural Sciences Sugarcane And Hemp Research Center Fujian Academy Of Agricultural Sciences
Original Assignee
Institute Of Subtropical Agriculture Fujian Academy Of Agricultural Sciences Sugarcane And Hemp Research Center Fujian Academy Of Agricultural Sciences
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Priority to CN201810145979.XA priority Critical patent/CN108245657A/en
Publication of CN108245657A publication Critical patent/CN108245657A/en
Pending legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/906—Zingiberaceae (Ginger family)
    • A61K36/9068—Zingiber, e.g. garden ginger
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/10—Alcohols; Phenols; Salts thereof, e.g. glycerol; Polyethylene glycols [PEG]; Poloxamers; PEG/POE alkyl ethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0012—Galenical forms characterised by the site of application
    • A61K9/007—Pulmonary tract; Aromatherapy
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/10—Dispersions; Emulsions
    • A61K9/12—Aerosols; Foams
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
    • A61K31/46—8-Azabicyclo [3.2.1] octane; Derivatives thereof, e.g. atropine, cocaine

Abstract

The invention discloses a kind of anti-corona fragrant spray and preparation method thereof, the anti-corona fragrant spray formulations are as follows：Hyoscine 8 10%, Rosemary Oil 6 10%, solubilizer 0.8 1.2%, ethyl alcohol 18 22%, surplus are pure water in Rhizoma Zingiberis Recens volatile oil 5 8%, datura flower, and each raw material total amount is 100%.The anti-corona fragrant spray of the present invention can be used the mode for inhaling and smelling and spraying and use, and significant effect plays anti-corona effect of refreshing oneself, and safety is without side-effects, while environment can be kept pure and fresh.

Description

A kind of anti-corona fragrant spray and preparation method thereof
Technical field
The present invention relates to pharmaceutical technology fields, and in particular to a kind of anti-corona fragrant spray and preparation method.
Background technology
" carsick, airsick, seasick " is three kinds of cardinal symptoms of motion sickness.It is the vibration due to the vehicles, makes human body certainly Nervous disorder is restrained, the Lymphatic Circulation of inner ear is affected, and leads to para-equlibrium, patient is in ride-on vehicles/aircraft/ship The different degrees of symptom such as dizziness, nausea, cold perspiration, vomiting can be generated in the process, and patient's journey safety and physical and mental health are made Influence big Cheng Dangxiang.
Have very much, such as acupoint massage for the control method of motion sickness, but due to understanding of the people to human acupoint It is and few, it is difficult to accurately hold, so acupoint massage is not easy to promote.
Drug preventing and controlling method, it is long-distance by bus when, can take medicine prevents the generation of cinetosis symptom, but can be complete there is presently no drug This disease is effected a radical cure entirely, has certain mitigation, but use slowly effect to carsickness there are also drug, and often have certain Side effect.
Invention content
The purpose of the present invention is to provide a kind of significant effect, safety anti-corona fragrant spray without side-effects and its preparation sides Method.
To achieve the above object, the present invention uses following technical scheme：
A kind of anti-corona fragrant spray, is made of the raw material of following weight percent：
Rhizoma Zingiberis Recens volatile oil 5-8%；
Hyoscine 8-10% in datura flower；
Rosemary Oil 6-10%；
Solubilizer 0.8-1.2%；
Ethyl alcohol 18-22%；
Surplus is pure water, and each raw material total amount is 100%.
Further, the anti-corona fragrant spray is made of the raw material of following weight ratio percentage：
Rhizoma Zingiberis Recens volatile oil 5%；
Hyoscine 10% in datura flower；
Rosemary Oil 8%；
Solubilizer 1%；
Ethyl alcohol 20%；
Surplus is pure water, and each raw material total amount is 100%.
The solubilizer is solubilizer SE3.
The Rhizoma Zingiberis Recens volatile oil is prepared by following methods：Ginger is dried in the shade, is crushed, according to solid-to-liquid ratio 1g: 8- 12ml adds in ethyl alcohol, and 80-100 min are extracted under the conditions of 50-60 DEG C, and filtering removal filter residue obtains Rhizoma Zingiberis Recens volatile oil, yield is 7-8%。
The volume fraction of the ethyl alcohol is 75-80%.
Hyoscine is prepared by following methods in the datura flower：Datura flower fresh flower is dried in the shade, is crushed, according to solid Liquor ratio 1g: 8-12ml adds in the hydrochloric acid solution ultrasonic extraction 25-35min of concentration 1.5-2mol/L, is then shaken with chloroform Extraction, recycling design, according to mass ratio 1: 250-300, by residue water dissolution, obtain hyoscine in datura flower, obtain to doing Rate is 0.33-0.40%.
The ultrasonic extraction conditions are：Power 240-260W, frequency 35-45kHz.
The Rosemary Oil is prepared by following method：It by rosemary, dries in the shade, cuts off, according to solid-to-liquid ratio 1g: 8- 12ml adds in solvent, and 3.5-4.5h is extracted using steam distillation, collects volatile matter, as Rosemary Oil, yield for 2.0~ 3.0%。
The preparation method of the anti-corona fragrant spray of the present invention is as follows：By hyoscine, rosemary in Rhizoma Zingiberis Recens volatile oil, datura flower Essential oil, solubilizer, ethyl alcohol and pure water are placed in container, are stirred evenly, then filling, obtain the anti-corona fragrant spray, should Spray is a kind of colourless transparent liquid, has apparent strong characteristic aromatic odor.
Appliance device used is both needed to disinfection processing in fragrant spray preparation process.
The present invention is main using hyoscine, Rosemary Oil in Rhizoma Zingiberis Recens volatile oil, datura flower using above technical scheme Raw material prepares anti-corona fragrant spray, and raw material has safety, odor type can by gained is screened in traditional Chinese medicine medicinal herbs most in use The features such as acceptance.
Wherein, Rhizoma Zingiberis Recens volatile oil is shogaol extract, the piquancy component in ginger alcohol extract play stimulation temperature, adjust by The effect of body, effect of stimulation influence gastric juice and choleresis by reflex, further excite stomach intestines liver the internal organs such as pancreas Hyperfunction, this alcohol extract can enhance the defence capability of stomach lining, play by adjusting nervous centralis and autonomic nervous function Anti-vomiting effect.
Hyoscine in datura flower, effect is similar to atropine, and atropine is compared in mydriasis and inhibition glandular secretion effect By force, have excitation to respiratory center, but have apparent inhibiting effect to cerebral cortex, in addition with expansion capillary, change The effects that kind microcirculation and carsick anti-blooming ship.
Rosemary Oil stimulates smell to achieve the purpose that strengthen physiology and mental functioning, rosemary be normal by essential oil The aromatic and inducing resuscitation substance seen is contacted with the hippocampus of Schistosomiasis control memory, participates in adjusting ability of learning and memory, stimulation smell can carry The ability of learning and memory of high normal subjects.
Anti-corona fragrant spray provided by the invention, can be used the mode for inhaling and smelling and spraying and uses, significant effect is played and refreshed oneself Anti-corona effect, safety is without side-effects, while environment space can be kept pure and fresh, has the characteristics that safety, odor type are acceptable, Use easy to spread.
Specific embodiment
A kind of anti-corona fragrant spray, is made of the raw material of following weight percent：
Hyoscine 8-10%, Rosemary Oil 6-10%, solubilizer SE30.8-1.2%, second in Rhizoma Zingiberis Recens volatile oil 5-8%, datura flower Alcohol 18-22%, surplus are pure water, and each raw material total amount is 100%.
Further, the anti-corona fragrant spray is made of the raw material of following weight ratio percentage：Rhizoma Zingiberis Recens volatile oil 5%, ocean gold It is pure water to spend middle hyoscine 10%, Rosemary Oil 8%, solubilizer SE31%, ethyl alcohol 20%, surplus, and each raw material total amount is 100%。
Wherein, Rhizoma Zingiberis Recens volatile oil is prepared by following methods：Ginger is dried in the shade, is crushed, according to solid-to-liquid ratio 1g: 8- 12ml adds in the ethyl alcohol of volume fraction 75-80%, and 80-100 min are extracted under the conditions of 50-60 DEG C, and filtering removal filter residue obtains Rhizoma Zingiberis Recens volatile oil, yield 7-8%.
Hyoscine is prepared by following methods in datura flower：Datura flower fresh flower is dried in the shade, is crushed, according to solid-to-liquid ratio 1g: 8-12ml adds in the hydrochloric acid solution ultrasonic extraction 25-35min of concentration 1.5-2mol/L（Power 240-260W, frequency 35- 45kHz）, then with chloroform shaking out, recycling design is to dry, according to mass ratio 1: 250-300, by residue with water-soluble Solution, obtains hyoscine in datura flower, yield 0.33-0.40%.
Rosemary Oil is prepared by following method：It by rosemary, dries in the shade, cuts off, add according to solid-to-liquid ratio 1g: 8-12ml Enter solvent, 3.5-4.5h is extracted using steam distillation, collect volatile matter, as Rosemary Oil, yield is 2.0~3.0%.
The preparation method of anti-corona fragrance spray is as follows：By hyoscine in Rhizoma Zingiberis Recens volatile oil, datura flower, Rosemary Oil, Solubilizer, ethyl alcohol and pure water are placed in container, are stirred evenly, then filling, obtain the anti-corona fragrant spray.
Embodiment 1
A kind of preparation method of anti-corona fragrant spray：
1）Prepare Rhizoma Zingiberis Recens volatile oil：Ginger is dried in the shade, is crushed, the ethyl alcohol of volume fraction 75% is added according to solid-to-liquid ratio 1g: 10ml, 90 min are extracted under the conditions of 55 DEG C, filtering removal filter residue obtains Rhizoma Zingiberis Recens volatile oil；
2）Prepare hyoscine in datura flower：Datura flower fresh flower is dried in the shade, is crushed, concentration is added according to solid-to-liquid ratio 1g: 10ml The hydrochloric acid solution ultrasonic extraction 30min of 1.8mol/L（Power 250W, frequency 40kHz）, then with chloroform shaking out, return Solvent is received to doing, according to mass ratio 1: 275, by residue water dissolution, obtains hyoscine in datura flower；
3）Prepare Rosemary Oil：It by rosemary, dries in the shade, cuts off, solvent is added according to solid-to-liquid ratio 1g: 10ml, using vapor Distillation extraction 4h, collects volatile matter, as Rosemary Oil；
4）Prepare anti-corona fragrant spray：It stocks up according to following weight percent：Hyoscine in Rhizoma Zingiberis Recens volatile oil 5%, datura flower 10%th, Rosemary Oil 8%, solubilizer SE3 1%, ethyl alcohol 20%, surplus are pure water, and each raw material total amount is 100%；
Hyoscine, Rosemary Oil, solubilizer and ethyl alcohol and pure water in Rhizoma Zingiberis Recens volatile oil, datura flower are placed in container, 50 DEG C and fully mixing material are heated to, are cooled to room temperature, pure water is added in and stirs and evenly mixs, liquid to be mixed is cooled to room temperature, and is filled Dress, sealing obtain the anti-corona fragrant spray.
Embodiment 2
A kind of preparation method of anti-corona fragrant spray, is made of the raw material of following weight percent：
1）Prepare Rhizoma Zingiberis Recens volatile oil：Ginger is dried in the shade, is crushed, the ethyl alcohol of volume fraction 75% is added according to solid-to-liquid ratio 1g: 8ml, 100 min are extracted under the conditions of 50 DEG C, filtering removal filter residue obtains Rhizoma Zingiberis Recens volatile oil；
2）Prepare hyoscine in datura flower：Datura flower fresh flower is dried in the shade, is crushed, concentration is added according to solid-to-liquid ratio 1g: 8ml The hydrochloric acid solution ultrasonic extraction 25-min of 1.5mol/L（Power 260W, frequency 45kHz）, then with chloroform shaking out, Recycling design, according to mass ratio 1: 250, by residue water dissolution, obtains hyoscine in datura flower to doing；
3）Prepare Rosemary Oil：It by rosemary, dries in the shade, cuts off, add in solvent according to solid-to-liquid ratio 1g: 8ml, steamed using vapor Extraction 3.5h is evaporated, collects volatile matter, as Rosemary Oil；
4）Prepare anti-corona fragrant spray：It stocks up according to following weight percent：Hyoscine in Rhizoma Zingiberis Recens volatile oil 5%, datura flower 10%th, Rosemary Oil 6%, solubilizer SE3 0.8%, ethyl alcohol 18%, surplus are pure water, and each raw material total amount is 100%；
Hyoscine, Rosemary Oil, solubilizer and ethyl alcohol and pure water in Rhizoma Zingiberis Recens volatile oil, datura flower are placed in container, 45 DEG C and fully mixing material are heated to, are cooled to room temperature, pure water is added in and stirs and evenly mixs, liquid to be mixed is cooled to room temperature, and is filled Dress, sealing obtain the anti-corona fragrant spray.
Embodiment 3
A kind of preparation method of anti-corona fragrant spray, is made of the raw material of following weight percent：
1）Prepare Rhizoma Zingiberis Recens volatile oil：Ginger is dried in the shade, is crushed, the ethyl alcohol of volume fraction 80% is added according to solid-to-liquid ratio 1g: 12ml, 100 min are extracted under the conditions of 60 DEG C, filtering removal filter residue obtains Rhizoma Zingiberis Recens volatile oil；
2）Prepare hyoscine in datura flower：Datura flower fresh flower is dried in the shade, is crushed, concentration is added according to solid-to-liquid ratio 1g: 12ml The hydrochloric acid solution ultrasonic extraction 35min of 2mol/L（Power 240W, frequency 35kHz）, then with chloroform shaking out, recycling Solvent, according to mass ratio 1: 300, by residue water dissolution, obtains hyoscine in datura flower to doing；
3）Prepare Rosemary Oil：It by rosemary, dries in the shade, cuts off, solvent is added according to solid-to-liquid ratio 1g: 12ml, using vapor Distillation extraction 4.5h, collects volatile matter, as Rosemary Oil；
4）Prepare anti-corona fragrant spray：It stocks up according to following weight percent：Hyoscine in Rhizoma Zingiberis Recens volatile oil 8%, datura flower 8%th, Rosemary Oil 10%, solubilizer SE31.2%, ethyl alcohol 22%, surplus are pure water, and each raw material total amount is 100%；
Hyoscine, Rosemary Oil, solubilizer and ethyl alcohol and pure water in Rhizoma Zingiberis Recens volatile oil, datura flower are placed in container, 55 DEG C and fully mixing material are heated to, are cooled to room temperature, pure water is added in and stirs and evenly mixs, liquid to be mixed is cooled to room temperature, and is filled Dress, sealing obtain the anti-corona fragrant spray.

Claims (9)

1. a kind of anti-corona fragrant spray, it is characterised in that：Its raw material by following weight percent forms：
Rhizoma Zingiberis Recens volatile oil 5-8%；
Hyoscine 8-10% in datura flower；
Rosemary Oil 6-10%；
Solubilizer 0.8-1.2%；
Ethyl alcohol 18-22%；
Surplus is pure water, and each raw material total amount is 100%.
2. the anti-corona fragrant spray of one kind according to claim 1, it is characterised in that：Its original by following weight ratio percentage Material composition：
Rhizoma Zingiberis Recens volatile oil 5%；
Hyoscine 10% in datura flower；
Rosemary Oil 8%；
Solubilizer 1%；
Ethyl alcohol 20%；
Surplus is pure water, and each raw material total amount is 100%.
3. the anti-corona fragrant spray of one kind according to claim 1, it is characterised in that：The solubilizer is solubilizer SE3.
4. the anti-corona fragrant spray of one kind according to claim 1, it is characterised in that：The Rhizoma Zingiberis Recens volatile oil is by with lower section Method is prepared：Ginger is dried in the shade, is crushed, ethyl alcohol is added according to solid-to-liquid ratio 1g: 8-12ml, 80-100 is extracted at 50-60 DEG C Min, filtering removal filter residue, obtains Rhizoma Zingiberis Recens volatile oil.
5. the anti-corona fragrant spray of one kind according to claim 4, it is characterised in that：The volume fraction of the ethyl alcohol is 75- 80%。
6. the anti-corona fragrant spray of one kind according to claim 1, it is characterised in that：In the datura flower hyoscine be by Following methods are prepared：Datura flower fresh flower is dried in the shade, is crushed, concentration 1.5-2mol/L is added according to solid-to-liquid ratio 1g: 8-12ml Hydrochloric acid solution ultrasonic extraction 25-35min, then with chloroform shaking out, recycling design is to dry, according to mass ratio 1: 250-300 by residue water dissolution, obtains hyoscine in datura flower.
7. the anti-corona fragrant spray of one kind according to claim 6, it is characterised in that：The ultrasonic extraction conditions are：Power 240-260W, frequency 35-45kHz.
8. the anti-corona fragrant spray of one kind according to claim 1, it is characterised in that：The Rosemary Oil is by with laxative remedy It is prepared：It by rosemary, dries in the shade, cuts off, add in solvent according to solid-to-liquid ratio 1g: 8-12ml, extracted using steam distillation 3.5-4.5h collects volatile matter, as Rosemary Oil.
9. a kind of preparation method of anti-corona fragrant spray as described in one of claim 1-8, it is characterised in that：Ginger is volatilized Hyoscine, Rosemary Oil, solubilizer, ethyl alcohol and pure water are placed in container in oil, datura flower, are stirred evenly, are then filled Dress obtains the anti-corona fragrant spray.
CN201810145979.XA 2018-02-12 2018-02-12 A kind of anti-corona fragrant spray and preparation method thereof Pending CN108245657A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1150909A (en) * 1996-08-12 1997-06-04 陈述坤 Carsickness plaster and carsickness drug
US20020100185A1 (en) * 2000-09-24 2002-08-01 Sitz Richard G. Drying method for selectively removing volatile components from wet coatings
CN101780061A (en) * 2010-03-24 2010-07-21 朱秀青 Nasal spray
CN103585662A (en) * 2013-11-13 2014-02-19 东莞市日友汽车用品有限公司 Perfume and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1150909A (en) * 1996-08-12 1997-06-04 陈述坤 Carsickness plaster and carsickness drug
US20020100185A1 (en) * 2000-09-24 2002-08-01 Sitz Richard G. Drying method for selectively removing volatile components from wet coatings
CN101780061A (en) * 2010-03-24 2010-07-21 朱秀青 Nasal spray
CN103585662A (en) * 2013-11-13 2014-02-19 东莞市日友汽车用品有限公司 Perfume and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
侯建萍 等: "中西药联合应用防治晕船", 《现代中西医结合杂志》 *
郭琪 等: "干姜及其提取物的抗晕动病作用研究", 《实用药物与临床》 *

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Application publication date: 20180706