CN108157940A - The preparation method of Periostracum cicadae pulvis - Google Patents

The preparation method of Periostracum cicadae pulvis Download PDF

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Publication number
CN108157940A
CN108157940A CN201810016129.XA CN201810016129A CN108157940A CN 108157940 A CN108157940 A CN 108157940A CN 201810016129 A CN201810016129 A CN 201810016129A CN 108157940 A CN108157940 A CN 108157940A
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China
Prior art keywords
powder
periostracum cicadae
weight
preparation
pulvis
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CN201810016129.XA
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Chinese (zh)
Inventor
陈相波
雷鸣
田朋飞
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Hangzhou Rong Biotechnology Co Ltd
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Hangzhou Rong Biotechnology Co Ltd
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Priority to CN201810016129.XA priority Critical patent/CN108157940A/en
Publication of CN108157940A publication Critical patent/CN108157940A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L31/00Edible extracts or preparations of fungi; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00Shaping or working of foodstuffs characterised by the products
    • A23P10/40Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mycology (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Microbiology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention discloses a kind of preparation methods of Periostracum cicadae pulvis to include the following steps:By the raw material powder of each component;Powder other than donkey-hide gelatin is mixed;The powder that donkey-hide gelatin and remaining component mix is mixed to form powder to be punched;Powder to be punched is placed in mold, progress is once stamped and formed out powder agglomates;Water mist is sprayed to powder agglomates;Tile is formed to having the powder agglomates of default moisture content to carry out two times punch;Tile is crushed using pulverizer;Substance after crushing is filtered to detach thick material and thin substance;Separating twice is carried out to thick material;Thin material mixing after thick material after separating twice and filtering is formed into mixture, carrying out rough lapping to mixture forms coarse powder;Fine lapping is carried out to coarse powder and forms fine powder;Ultrasonic vibration is carried out using ultrasonic vibration device to fine powder.The invention has the beneficial effects that provide a kind of preparation method of the Periostracum cicadae pulvis with compound health properties.

Description

The preparation method of Periostracum cicadae pulvis
Technical field
The present invention relates to a kind of preparation methods of pulvis, and in particular to a kind of preparation method of Periostracum cicadae pulvis.
Background technology
Periostracum cicadae for artificial cultivation golden cicada spend, be commonly called as big cordyceps sinensis, belong to entomogenous fungi, in the whole world it has been found that In 504 kinds of cordyceps sinensis, Periostracum cicadae, cordyceps sinensis are only two kinds therein;It is that a kind of shape has " animal " and " plant " shape The marvellous biology of state feature, root are the larva bodies of cicada, and flower grows out from single or 2-3 cicada larva head, about one It is very little how long, from top, branch is bloomed, and pollen is also referred to as milk yellow " cicada fungus conidia powder ", be exactly briefly " seed ", have Breeding function.Its forming process is that the larva of cicada is infected by Cordyceps Militaris before cicada sprouts wings, is parasitic, when climatic environment suitable for when, inhale The nutrition for receiving polypide is converted to mycelium, and final polypide accounts for tool by mycelium and only remains next body completely.During all things on earth recovery Section, mycelium gradates again from the vegetative phase has breeding function for the perfect stage " cicada fungus conidia powder ", gradually from top point Branch " germination " likeness in form flower, so also referred to as cicada fungus.It is distributed in Sichuan, Jiangsu, Zhejiang, Fujian, Anhui, the Yunnan Province of China. The effective ingredient of Periostracum cicadae has:Cordycepin, Cordyceps sinensis polysaccharide, cordycepic acid.Periostracum cicadae have high immunity, improve renal function, Antifatigue, reducing blood lipid, antitumor, improving eyesight, improves sleep, radioresistance, analgesia, calmness at hypoglycemic, blood pressure lowering.
So far, yet there are no in the market can effectively play the powder product i.e. preparation method of Periostracum cicadae effect, alternatively, Ingredient is more single, affects the health properties of product.
Invention content
A kind of preparation method of Periostracum cicadae pulvis includes:6 to 12 parts by weight of cicada fungus, 5 to 10 parts by weight of cordyceps sinensis, mountain 0.3 to 0.7 parts by weight of short, bristly hair or beard, 0.4 to 0.7 parts by weight of the fruit of Chinese wolfberry, 0.2 to 0.5 parts by weight of sealwort, 0.6 to 3 parts by weight of mulberries, Ah 7 to 70 parts by weight of glue;Preparation method includes the following steps:By the raw material powder of each component;By the powder other than donkey-hide gelatin It is mixed;The powder that donkey-hide gelatin and remaining component mix is mixed to form powder to be punched;Powder to be punched is placed in mould Tool, progress are once stamped and formed out powder agglomates;Water mist is sprayed to powder agglomates;Piece is formed to having the powder agglomates of default moisture content to carry out two times punch Block;Tile is crushed using pulverizer;Substance after crushing is filtered to detach thick material and thin substance;To thick object Matter carries out separating twice;By after the thick material after separating twice and filtering thin material mixing formed mixture, to mixture into Row rough lapping forms coarse powder;Fine lapping is carried out to coarse powder and forms fine powder;Ultrasonic vibration is carried out using ultrasonic vibration device to fine powder.
Further, the powder of cicada fungus is the sclerotium of cicada fungus or/and the powder of coremium.
Further, the weight ratio of the powder of the powder and coremium of the sclerotium in the powder of cicada fungus is 3 to 7.
Further, the moisture content of the tile of Periostracum cicadae ranging from 7% to 12%.
Further, the particle size range of donkey-hide gelatin powder is 100 to 200 mesh.
Further, ultrasonic wave is applied to the container of mixing when being mixed to the powder other than donkey-hide gelatin.
Further, to 40 to 50 degrees Celsius of the value range of the temperature of powder agglomates sprinkling water mist.
Further, powder moisture content in the block is made to volatilize using the means of heating when carrying out two times punch.
Further, powder moisture content in the block is made to volatilize in the form of microwave is applied to powder agglomates.
Further, when carrying out two times punch different pressure is used in different strokes.
The invention has the beneficial effects that:
Provide a kind of preparation method of the Periostracum cicadae pulvis with compound health properties.
It can effectively make raw material powder that mutually fusion occur into tile the press fitting of raw material powder.Add water and then two into powder agglomates What secondary punching press can speed up donkey-hide gelatin and other raw material powders merges speed and degree.The tile formed to two times punch passes through powder Broken, grinding and ultrasonic vibration can make the pulvis that tile becomes the fine powdered for being more favorable for absorbing.Tile is first usually made again Become pulvis, ensure that donkey-hide gelatin is merged with the reliable of other raw material powders, the raw material powder compared to initial mixing is more favorable for human body It absorbs.
Description of the drawings
Fig. 1 is the step schematic diagram of a preferred embodiment of the pulvis of the Periostracum cicadae of the production present invention.
Specific embodiment
A kind of pulvis of Periostracum cicadae includes:6 to 12 parts by weight of cicada fungus, 5 to 10 parts by weight of cordyceps sinensis, hawthorn 0.3 to 0.7 parts by weight, 0.4 to 0.7 parts by weight of the fruit of Chinese wolfberry, 0.2 to 0.5 parts by weight of sealwort, 0.6 to 3 parts by weight of mulberries, donkey-hide gelatin 7 to 70 Parts by weight.
As a kind of scheme, the pulvis of Periostracum cicadae includes:8 to 10 parts by weight of cicada fungus, 7 to 9 parts by weight of cordyceps sinensis, mountain 0.5 to 0.6 parts by weight of short, bristly hair or beard, 0.55 to 0.65 parts by weight of the fruit of Chinese wolfberry, 0.35 to 0.41 parts by weight of sealwort, 1.7 to 3 weight of mulberries Part, 30 to 50 parts by weight of donkey-hide gelatin.Remaining is starch.
As a kind of specific scheme, the pulvis of Periostracum cicadae includes:9 parts by weight of cicada fungus, 8 parts by weight of cordyceps sinensis, mountain 0.55 parts by weight of short, bristly hair or beard, 0.6 parts by weight of the fruit of Chinese wolfberry, 0.4 parts by weight of sealwort, 2 parts by weight of mulberries, 40 parts by weight of donkey-hide gelatin.Remaining is forms sediment Powder.
As another scheme, the pulvis of Periostracum cicadae includes:6 to 8 parts by weight of cicada fungus, 5 to 6 weight of cordyceps sinensis Part, 0.3 to 0.4 parts by weight of hawthorn, 0.45 to 0.5 parts by weight of the fruit of Chinese wolfberry, 0.2 to 0.3 parts by weight of sealwort, 0.6 to 1 weight of mulberries Part, 7 to 10 parts by weight of donkey-hide gelatin.Remaining is starch.
As a kind of scheme having, the pulvis of Periostracum cicadae includes:7 parts by weight of cicada fungus, 7 parts by weight of cordyceps sinensis, mountain 0.5 parts by weight of short, bristly hair or beard, 0.5 parts by weight of the fruit of Chinese wolfberry, 0.25 parts by weight of sealwort, 0.7 parts by weight of mulberries, 10 parts by weight of donkey-hide gelatin.Remaining is Starch.
As another scheme, the pulvis of Periostracum cicadae includes:9 to 12 parts by weight of cicada fungus, 7 to 10 weight of cordyceps sinensis Part, 0.65 to 0.7 parts by weight of hawthorn, 0.65 to 0.7 parts by weight of the fruit of Chinese wolfberry, 0.45 to 0.5 parts by weight of sealwort, 2.5 to 3 weight of mulberries Measure part, 50 to 65 parts by weight of donkey-hide gelatin.Remaining is starch.
As a kind of specific scheme, the pulvis of Periostracum cicadae includes:12 parts by weight of cicada fungus, 10 parts by weight of cordyceps sinensis, 0.7 parts by weight of hawthorn, 0.7 parts by weight of the fruit of Chinese wolfberry, 0.5 parts by weight of sealwort, 3 parts by weight of mulberries, 65 parts by weight of donkey-hide gelatin.Remaining is forms sediment Powder.
Above ingredient makes the pulvis of the Periostracum cicadae of the present invention that there is compound healthcare function to be easy to be made as again simultaneously Pulvis.
As shown in Figure 1, preparation method of the present invention introduced below.
Specifically, cicada fungus is powder before pulvis is made.More specifically, the powder of cicada fungus is the sclerotium of cicada fungus Or/and the powder of coremium.The weight ratio of the powder of sclerotium in the powder of cicada fungus and the powder of coremium is 3 to 7.
Before pulvis is made, the sclerotium and coremium of cicada fungus are acquired respectively, carry out dusting processing respectively.Form granularity model It encloses for 150 mesh to the powder between 170 mesh.
Before pulvis is made, cordyceps sinensis is Cordyceps sinensis powder before pulvis is made.Equally use cordyceps sinensis Dusting processing is carried out, forms particle size range as 160 mesh to the powder between 200 mesh.
Specifically, hawthorn is haw pulp powder before pulvis is made.The fruit of Chinese wolfberry is matrimony vine before pulvis is made The powder of sub whole fruit.By haw pulp, whole fruit of the fruit of Chinese wolfberry air-dries, and particle size range 100 to 120 is made in then dusting Powder between mesh.
Sealwort and mulberries after weathering are subjected to dusting processing, form powder of the particle size range between 150 to 200 mesh End.
It should be noted that during dusting, the side that can will recycle dusting if granularity requirements are not achieved in dusting Formula meets granularity requirements.
Specifically, after first dusting, pulvis will be obtained and carry out sieving, the powder for not meeting granularity requirements is sent into powder Broken machine grinding.
After the powder of each component meets granularity requirements, the powder of the component other than donkey-hide gelatin is placed on mixed powder machine In blending tank in, and several mill balls are placed in blending tank, then starting mixed powder machine is filled the powder in grinding pot Point mixing, mixed powder machine can also be into being blending tank row rotations other than blending tank can be made to carry out around the revolution in a specified axle center.Make Mixed powder machine operates 20 hours, and then can opening, powder is overturned, and then recharges back blending tank, is again turned on mixed powder machine fortune Row 20 hours, can opening overturning again, so repeatedly several times.It should be noted that can be with the increase for overturning number, it can be with Reduce the time of mixed powder machine operating.
The solid that donkey-hide gelatin condenses is put into pulverizer and is crushed, the granularity requirements of crushing are 300 mesh.
It will be mixed through the mixed powder of overmulling powder machine with the powder of donkey-hide gelatin powder and remaining filler such as starch, dextrin It is placed in same blending tank and is mixed in mixed powder machine.The time of mixing is 2 two hours.
As a kind of expansion scheme, during mixed powder is carried out above, the mixed powder tank mixed in powder machine can be applied super Sound wave, to improve mixed powder efficiency.
Powder after the completion of mixing is filled to mold, a punching press is then carried out, stamping of powder is molded, a punching press Pressure limit be 1.3 thousand Ns of 1.1 thousand wild marjoram.
By institute's molding powder agglomates merging humidity cabinet after a punching press, by spray system to powder agglomates spray water in humidity cabinet Mist, this water mist is all angles injection of powder agglomates, and water mist has certain temperature in itself.It should be noted that Powder agglomates sprinkling must be the steam of atomization rather than direct water spray, and principle and dress that similar humidifier generates water mist may be used Put the steam that atomization is generated in humidity cabinet.
By water mist, treated that powder agglomates contains certain moisture content, as a kind of expansion scheme, humidity cabinet can not spray Watering mist but the powder adhesive that has been atomized of sprinkling, it should be noted that used powder adhesive is can to eat at this time .
So, the part donkey-hide gelatin powder in surface can be combined in water, that is, is partly dissolved in water.
Powder agglomates Jing Guo atomization process is placed in final mold, by the mold for being loaded with powder agglomates be placed in microwave box into Row microwave treatment, while two times punch is carried out to powder agglomates, the certain time of two times punch is micro- when carrying out two times punch Wave case first with larger power output microwave, is then maintained at a lower-wattage output microwave for a period of time, then stops again Export microwave.In these three corresponding stages, in two times punch, when microwave is exported with relatively high power, controlling the pressure of punching press makes It is gradually increased, and in this stage, the 25% of entire punching press stroke is completed in punching press;It is defeated that a smaller power is maintained in microwave When going out, the 30% of entire stroke is completed in punching press;After stopping exporting microwave, the remainder of entire stroke is completed in punching press, i.e., whole The 45% of a stroke.
Above three phases are respectively defined as the first punching press stage, the second punching press stage and third punching press stage. Melting was collectively formed as the donkey-hide gelatin on the surface layer of powder agglomates of the output of microwave Jing Guo atomization process is combined with water in first punching press stage State substance, melt substance plays the role of bonding other powder in the state of punching press, in the first stage, with further punching Pressure and microwave are further compacted in powder agglomates while moisture content therein are further volatilized, reduce the water content of powder agglomates; In the third punching press stage, moisture content has met the requirements, and donkey-hide gelatin plays viscous effect due to heating by other in powder agglomates Together, complete entire stroke at this time makes powder agglomates become fine and close completion punching press so as to arrive required tile to powder bonding.It is specific and Speech, the moisture content ranging from 7% to 12% of the tile of final Periostracum cicadae.Tile is crushed using pulverizer.After crushing Substance be filtered to detach thick material and thin substance.Specifically, the substance after crushing was carried out using filter screen Filter.The substance leaked out across filter screen is the smaller thin substance of particle.The substance that cannot pass through filter screen is larger for particle Thick material.Thick material is needed further to crush, i.e. separating twice is to reduce the granular size of thick material.After separating twice Thick material and filtering after thin material mixing formed mixture.Rough lapping is carried out to mixture and forms coarse powder.Coarse powder is carried out Fine lapping forms fine powder.It can be good at reducing the size of powder by rough lapping and fine lapping.Ultrasonic vibration is used to fine powder Device carries out ultrasonic vibration, and the powder that can be good at mixing different material can be with.And make relatively large powder by super Sound rocking equipment can grind powder corner angle.Make powder convenient for absorbing.
Preferably, the pressure limit in the first punching press stage is 1.5 thousand Ns of 1,000 wild marjoram;The pressure in the second punching press stage Power ranging from 2,000 Ns of 1.5 thousand wild marjoram;The pressure limit in third punching press stage is 4,000 Ns of 3,000 wild marjoram.
As other preferred embodiment, using the means of refrigeration, the temperature of powder agglomates can be reduced in the third punching press stage, Wherein donkey-hide gelatin is made more effectively to condense other powder.
It alternatively, can be without using microwave treatment but real in a manner that the punch to punching press heats Now heat and make the effect of moisture evaporation.
For example, punch is made of metal, the in-built electrical heated filament so as to make punch that there is certain temperature inside punch.
Method more than can make powder be effectively combined into fine and close pulvis, while again without using additional Additive but donkey-hide gelatin property in itself is utilized to realize the effect of bonding.Donkey-hide gelatin is both in itself active ingredient simultaneously and prepares The binding agent of molding effect can be played in pulvis.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should Understand, the invention is not limited in any way above-described embodiment, all to be obtained by the way of equivalent substitution or equivalent transformation Technical solution is all fallen in protection scope of the present invention.

Claims (10)

1. a kind of preparation method of Periostracum cicadae pulvis, it is characterised in that:The Periostracum cicadae pulvis includes:6 to 12 weight of cicada fungus Measure part, 5 to 10 parts by weight of cordyceps sinensis, 0.3 to 0.7 parts by weight of hawthorn, 0.4 to 0.7 parts by weight of the fruit of Chinese wolfberry, sealwort 0.2 to 0.5 Parts by weight, 0.6 to 3 parts by weight of mulberries, 7 to 70 parts by weight of donkey-hide gelatin;
The preparation method includes the following steps:
By the raw material powder of each component;
Powder other than donkey-hide gelatin is mixed;
The powder that donkey-hide gelatin and remaining component mix is mixed to form powder to be punched;
Powder to be punched is placed in mold, progress is once stamped and formed out powder agglomates;
Water mist is sprayed to powder agglomates;
Tile is formed to having the powder agglomates of default moisture content to carry out two times punch;
Tile is crushed using pulverizer;
Substance after crushing is filtered to detach thick material and thin substance;
Separating twice is carried out to thick material;
Thin material mixing after thick material after separating twice and filtering is formed into mixture, carrying out rough lapping to mixture forms Coarse powder;
Fine lapping is carried out to coarse powder and forms fine powder;
Ultrasonic vibration is carried out using ultrasonic vibration device to fine powder.
2. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:The powder of the cicada fungus is cicada Colored sclerotium or/and the powder of coremium.
3. the preparation method of Periostracum cicadae pulvis according to claim 2, it is characterised in that:In the powder of the cicada fungus The weight ratio of the powder of sclerotium and the powder of coremium is 3 to 7.
4. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:The tile of the Periostracum cicadae Moisture content ranging from 7% to 12%.
5. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:The granularity of the donkey-hide gelatin powder Ranging from 100 to 200 mesh.
6. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:To the powder other than donkey-hide gelatin Ultrasonic wave is applied to the container of mixing when end is mixed.
7. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:To the temperature of powder agglomates sprinkling water mist 40 to 50 degrees Celsius of the value range of degree.
8. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:When carrying out the two times punch Make powder moisture content volatilization in the block using the means of heating.
9. the preparation method of Periostracum cicadae pulvis according to claim 8, it is characterised in that:Apply using to the powder agglomates The form of microwave makes powder moisture content volatilization in the block.
10. the preparation method of Periostracum cicadae pulvis according to claim 1, it is characterised in that:When carrying out two times punch Different pressure is used in different strokes.
CN201810016129.XA 2018-01-08 2018-01-08 The preparation method of Periostracum cicadae pulvis Pending CN108157940A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103637281A (en) * 2013-11-21 2014-03-19 威海五谷怡健食品有限公司 Functional food for postpartum lactogenesis and lactation promotion and preparation method thereof
CN105497519A (en) * 2016-01-04 2016-04-20 环翠楼红参生物科技股份有限公司 Preparation method for radix ginseng rubra-colla corii asini cell-wall breaking superfine powder
CN107183676A (en) * 2017-04-17 2017-09-22 安徽虫草源生物科技有限公司 A kind of Periostracum cicadae lozenge and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103637281A (en) * 2013-11-21 2014-03-19 威海五谷怡健食品有限公司 Functional food for postpartum lactogenesis and lactation promotion and preparation method thereof
CN105497519A (en) * 2016-01-04 2016-04-20 环翠楼红参生物科技股份有限公司 Preparation method for radix ginseng rubra-colla corii asini cell-wall breaking superfine powder
CN107183676A (en) * 2017-04-17 2017-09-22 安徽虫草源生物科技有限公司 A kind of Periostracum cicadae lozenge and preparation method thereof

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* Cited by examiner, † Cited by third party
Title
王文章主编: "《阿胶》", 30 September 2013, 文化艺术出版社 *
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