CN108617763A - A kind of apple fresh-keeping agent and preparation method thereof - Google Patents

A kind of apple fresh-keeping agent and preparation method thereof Download PDF

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Publication number
CN108617763A
CN108617763A CN201810424727.0A CN201810424727A CN108617763A CN 108617763 A CN108617763 A CN 108617763A CN 201810424727 A CN201810424727 A CN 201810424727A CN 108617763 A CN108617763 A CN 108617763A
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CN
China
Prior art keywords
parts
preparation
keeping agent
sodium alginate
essential oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201810424727.0A
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Chinese (zh)
Inventor
武行峰
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Hefei Jintongwei Low-Temperature Technology Co Ltd
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Hefei Jintongwei Low-Temperature Technology Co Ltd
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Application filed by Hefei Jintongwei Low-Temperature Technology Co Ltd filed Critical Hefei Jintongwei Low-Temperature Technology Co Ltd
Priority to CN201810424727.0A priority Critical patent/CN108617763A/en
Publication of CN108617763A publication Critical patent/CN108617763A/en
Withdrawn legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/14Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
    • A23B7/153Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
    • A23B7/154Organic compounds; Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Storage Of Fruits Or Vegetables (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

A kind of apple fresh-keeping agent of present invention offer and preparation method thereof, is prepared by following component:Chitosan, modified sodium alginate, sodium citrate, plants essential oil, sucrose fatty ester, vitamin E, organic extractant and water.Preparation method of the present invention is simple, formula is reasonable, of low cost, and when use is easy to operate, of good preservation effect, and the problems such as the brown skin of dehydration wilting, brown stain will not occur for storage period fruit, appearance freshness is kept well.

Description

A kind of apple fresh-keeping agent and preparation method thereof
Technical field
The invention belongs to antistaling agent technical fields, and in particular to a kind of apple fresh-keeping agent and preparation method thereof.
Background technology
With the development of science and technology, people's living standard is gradually increased, the water that people produce different regions Various Seasonal The demand of fruit is gradually increased.So that people propose higher and higher want to the fresh-keeping and storing of the fruit of hardly possible storage and transport It asks.Existing fruit freshness preserving technology is usually to make preservative film, and preservative film is in room temperature or preservation by low temperature, long acting fresh-keeping, transport guarantor Fresh aspect has certain progress really.But there is also some shortcomings, and predominantly acquisition time is shorter, and preservation is uneven, it is difficult to protect Demonstrate,prove effect;Preparation method complexity is cumbersome;Cost of manufacture is higher, and raw material sources are narrow;Some raw material components are hazardous to the human body.
In summary, it is therefore desirable to a kind of better apple fresh-keeping agent, to improve the deficiencies in the prior art.
Invention content
The object of the present invention is to provide a kind of apple fresh-keeping agent and preparation method thereof, preparation method of the present invention is simple, is formulated Rationally, of low cost, when use, is easy to operate, of good preservation effect, and it is brown that dehydration wilting, brown stain will not occur in storage period fruit The problems such as skin, appearance freshness are kept well.
The present invention provides the following technical solutions:
A kind of apple fresh-keeping agent includes the raw material of following parts by weight:22-29 parts of chitosan, 18-26 parts of modified sodium alginate, lemon 13-19 parts of lemon acid sodium, 15-22 parts of plants essential oil, 14-23 parts of sucrose fatty ester, 7-25 parts of vitamin e1, organic extractant 12-18 parts and 12-17 parts of water.
Preferably, the antistaling agent includes the raw material of following parts by weight:22-26 parts of chitosan, modified sodium alginate 23-26 Part, 15-19 parts of sodium citrate, 15-20 parts of plants essential oil, 14-21 parts of sucrose fatty ester, 9-25 parts of vitamin e1, You Jicui Take 12-15 parts of 12-16 parts of agent and water.
Preferably, the antistaling agent includes the raw material of following parts by weight:23 parts of chitosan, 25 parts of modified sodium alginate, lemon 14 parts of 18 parts of lemon acid sodium, 20 parts of plants essential oil, 14 parts of sucrose fatty ester, 4 parts of vitamin E2,12 parts of organic extractant and water.
A kind of preparation method of apple fresh-keeping agent, including following preparation process:
A, chitosan, vitamin E and water are mixed, 20-25min is stirred at 55-60 DEG C and obtains solution one after cooling;
B, modified sodium alginate, sodium citrate and sucrose fatty ester are mixed, is imported in reaction kettle, at 65-70 DEG C, with The rotating speed of 120-160r/min stirs 30-40min, obtains material one;
C, plants essential oil is added into material one, after mixing, imports in mulser, stirring, emulsification obtain material two;
D, solution one, material two and organic extractant are mixed, imports in batch mixer, 10- is stirred at 50-55 DEG C 15min, after being cooled to room temperature, you can obtain finished product.
Preferably, the preparation method of the modified sodium alginate of the step b is:Sodium alginate is added in phosphate buffer It is stirred 1-2h, adds mixed solvent, reacts 2-3h at 70-80 DEG C, sodium cyanoborohydride is added and is stirred to react 25- 40min reuses methanol and carries out precipitation reaction, and sediment is soluble in water, progress dialysis is freeze-dried, you can be changed Property sodium alginate.
Preferably, the mixed solvent is by n-hexylamine and methanol in mass ratio 2:9 mix.
Preferably, the plants essential oil of the step c is Salvia japonica essential oil, Herba Origani Vulgaris quintessence oil and clove oil in mass ratio 3:5: 9 mix.
Preferably, the preparation method of the organic extractant of the step d is:By garlic and ginger mixed grinding at powder, The deionized water of 6-8 times of weight is added, extraction, filtering removal filter residue, you can obtain organic extractant are heated at 80-90 DEG C.
The beneficial effects of the invention are as follows:
Preparation method of the present invention is simple, formula is reasonable, of low cost, and when use is easy to operate, of good preservation effect, in storage period The problems such as dehydration wilting, brown stain brown skin, will not occur for fruit, and appearance freshness is kept well.
The compounding of the chitosan and vitamin E that are added in the present invention has preferable anti-corrosive properties, the finished product safety collar of preparation Protect taste that is degradable, and not influencing apple;The organic extractant of addition, the ingredient used all have for garlic and ginger Natural effective sterilization, bacteriostasis, then the compounding with modified sodium alginate, modified sodium alginate mix breast with other ingredients again After change, there is preferable film forming, may make sterilization, the volatilization of antibacterial active ingredient or rate of release to slow down, to extend Sterilization, antibacterial time improve the apple fresh-keeping effect of finished product, extend the apple fresh-keeping time.
Specific implementation mode
Embodiment 1
A kind of apple fresh-keeping agent includes the raw material of following parts by weight:29 parts of chitosan, 18 parts of modified sodium alginate, sodium citrate 17 parts of 19 parts, 15 parts of plants essential oil, 14 parts of sucrose fatty ester, 7 parts of vitamin e1,12 parts of organic extractant and water.
A kind of preparation method of apple fresh-keeping agent, including following preparation process:
A, chitosan, vitamin E and water are mixed, 20min is stirred at 60 DEG C and obtains solution one after cooling;
B, modified sodium alginate, sodium citrate and sucrose fatty ester are mixed, is imported in reaction kettle, at 70 DEG C, with 160r/ The rotating speed of min stirs 30min, obtains material one;
C, plants essential oil is added into material one, after mixing, imports in mulser, stirring, emulsification obtain material two;
D, solution one, material two and organic extractant are mixed, imports in batch mixer, 15min is stirred at 50 DEG C, it is cooling To room temperature, you can obtain finished product.
The preparation method of the modified sodium alginate of step b is:Sodium alginate is added in phosphate buffer and is stirred 1h, Mixed solvent is added, reacts 2h at 80 DEG C, sodium cyanoborohydride is added and is stirred to react 40min, reuses methanol progress Precipitation reaction, sediment is soluble in water, progress dialysis are freeze-dried, you can to obtain modified sodium alginate.
Mixed solvent is by n-hexylamine and methanol in mass ratio 2:9 mix.
The plants essential oil of step c is Salvia japonica essential oil, Herba Origani Vulgaris quintessence oil and clove oil in mass ratio 3:5:9 mix.
The preparation method of the organic extractant of step d is:By garlic and ginger mixed grinding at powder, 6 times of weight are added Deionized water, at 90 DEG C heat extraction, filtering removal filter residue, you can obtain organic extractant.
Embodiment 2
A kind of apple fresh-keeping agent includes the raw material of following parts by weight:22 parts of chitosan, 23 parts of modified sodium alginate, sodium citrate 15 parts of 15 parts, 15 parts of plants essential oil, 14 parts of sucrose fatty ester, 9 parts of vitamin e1,12 parts of organic extractant and water.
A kind of preparation method of apple fresh-keeping agent, including following preparation process:
A, chitosan, vitamin E and water are mixed, 25min is stirred at 55 DEG C and obtains solution one after cooling;
B, modified sodium alginate, sodium citrate and sucrose fatty ester are mixed, is imported in reaction kettle, at 65 DEG C, with 120r/ The rotating speed of min stirs 30min, obtains material one;
C, plants essential oil is added into material one, after mixing, imports in mulser, stirring, emulsification obtain material two;
D, solution one, material two and organic extractant are mixed, imports in batch mixer, 10min is stirred at 50 DEG C, it is cooling To room temperature, you can obtain finished product.
The preparation method of the modified sodium alginate of step b is:Sodium alginate is added in phosphate buffer and is stirred 1h, Mixed solvent is added, reacts 2h at 70 DEG C, sodium cyanoborohydride is added and is stirred to react 25min, reuses methanol progress Precipitation reaction, sediment is soluble in water, progress dialysis are freeze-dried, you can to obtain modified sodium alginate.
Mixed solvent is by n-hexylamine and methanol in mass ratio 2:9 mix.
The plants essential oil of step c is Salvia japonica essential oil, Herba Origani Vulgaris quintessence oil and clove oil in mass ratio 3:5:9 mix.
The preparation method of the organic extractant of step d is:By garlic and ginger mixed grinding at powder, 6 times of weight are added Deionized water, at 80 DEG C heat extraction, filtering removal filter residue, you can obtain organic extractant.
Embodiment 3
A kind of apple fresh-keeping agent includes the raw material of following parts by weight:23 parts of chitosan, 25 parts of modified sodium alginate, sodium citrate 14 parts of 18 parts, 20 parts of plants essential oil, 14 parts of sucrose fatty ester, 4 parts of vitamin E2,12 parts of organic extractant and water.
A kind of preparation method of apple fresh-keeping agent, including following preparation process:
A, chitosan, vitamin E and water are mixed, 25min is stirred at 60 DEG C and obtains solution one after cooling;
B, modified sodium alginate, sodium citrate and sucrose fatty ester are mixed, is imported in reaction kettle, at 70 DEG C, with 160r/ The rotating speed of min stirs 40min, obtains material one;
C, plants essential oil is added into material one, after mixing, imports in mulser, stirring, emulsification obtain material two;
D, solution one, material two and organic extractant are mixed, imports in batch mixer, 15min is stirred at 55 DEG C, it is cooling To room temperature, you can obtain finished product.
The preparation method of the modified sodium alginate of step b is:Sodium alginate is added in phosphate buffer and is stirred 2h, Mixed solvent is added, reacts 3h at 80 DEG C, sodium cyanoborohydride is added and is stirred to react 40min, reuses methanol progress Precipitation reaction, sediment is soluble in water, progress dialysis are freeze-dried, you can to obtain modified sodium alginate.
Mixed solvent is by n-hexylamine and methanol in mass ratio 2:9 mix.
The plants essential oil of step c is Salvia japonica essential oil, Herba Origani Vulgaris quintessence oil and clove oil in mass ratio 3:5:9 mix.
The preparation method of the organic extractant of step d is:By garlic and ginger mixed grinding at powder, 8 times of weight are added Deionized water, at 90 DEG C heat extraction, filtering removal filter residue, you can obtain organic extractant.
Finished product prepared by above example is detected, following detection data is obtained:
Table one:
Project Embodiment 1 Embodiment 2 Embodiment 3
After 30 days, apple state Surface is unchanged, and internal unchanged, eating mouth feel is normal Surface is unchanged, and internal unchanged, eating mouth feel is normal Surface is unchanged, and internal unchanged, eating mouth feel is normal
After 50 days, apple state Surface is unchanged, and internal unchanged, eating mouth feel is normal Surface is unchanged, and internal unchanged, eating mouth feel is normal Surface is unchanged, and internal unchanged, eating mouth feel is normal
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to the foregoing embodiments Invention is explained in detail, for those skilled in the art, still can be to foregoing embodiments institute The technical solution of record is modified or equivalent replacement of some of the technical features.It is all the present invention spirit and Within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention.

Claims (8)

1. a kind of apple fresh-keeping agent, which is characterized in that include the raw material of following parts by weight:22-29 parts of chitosan, modified alginic acid 18-26 parts of sodium, 13-19 parts of sodium citrate, 15-22 parts of plants essential oil, 14-23 parts of sucrose fatty ester, 7-25 parts of vitamin e1, 12-17 parts of 12-18 parts of organic extractant and water.
2. a kind of apple fresh-keeping agent according to claim 1, which is characterized in that the antistaling agent includes following parts by weight Raw material:22-26 parts of chitosan, 23-26 parts of modified sodium alginate, 15-19 parts of sodium citrate, 15-20 parts of plants essential oil, Sucrose Fatty Acid Ester 12-15 parts of 14-21 parts of fat acid esters, 9-25 parts of vitamin e1,12-16 parts of organic extractant and water.
3. a kind of apple fresh-keeping agent according to claim 1, which is characterized in that the antistaling agent includes following parts by weight Raw material:23 parts of chitosan, 25 parts of modified sodium alginate, 18 parts of sodium citrate, 20 parts of plants essential oil, 14 parts of sucrose fatty ester, 14 parts of 4 parts of vitamin E2,12 parts of organic extractant and water.
4. a kind of preparation method of apple fresh-keeping agent of claim 1-3 any one of them, which is characterized in that including following preparation Step:
A, chitosan, vitamin E and water are mixed, 20-25min is stirred at 55-60 DEG C and obtains solution one after cooling;
B, modified sodium alginate, sodium citrate and sucrose fatty ester are mixed, is imported in reaction kettle, at 65-70 DEG C, with The rotating speed of 120-160r/min stirs 30-40min, obtains material one;
C, plants essential oil is added into material one, after mixing, imports in mulser, stirring, emulsification obtain material two;
D, solution one, material two and organic extractant are mixed, imports in batch mixer, 10- is stirred at 50-55 DEG C 15min, after being cooled to room temperature, you can obtain finished product.
5. a kind of preparation method of apple fresh-keeping agent according to claim 4, which is characterized in that the modification of the step b The preparation method of sodium alginate is:Sodium alginate is added in phosphate buffer and is stirred 1-2h, adds mixed solvent, 2-3h is reacted at 70-80 DEG C, sodium cyanoborohydride is added and is stirred to react 25-40min, methanol is reused and carries out precipitation reaction, Sediment is soluble in water, and progress dialysis is freeze-dried, you can to obtain modified sodium alginate.
6. a kind of preparation method of apple fresh-keeping agent according to claim 5, which is characterized in that the mixed solvent is by just Hexylamine and methanol in mass ratio 2:9 mix.
7. a kind of preparation method of apple fresh-keeping agent according to claim 4, which is characterized in that the plant of the step c Essential oil is Salvia japonica essential oil, Herba Origani Vulgaris quintessence oil and clove oil in mass ratio 3:5:9 mix.
8. a kind of preparation method of apple fresh-keeping agent according to claim 4, which is characterized in that the step d's is organic The preparation method of extractant is:By garlic and ginger mixed grinding at powder, the deionized water of 6-8 times of weight is added, in 80-90 Extraction, filtering removal filter residue, you can obtain organic extractant are heated at DEG C.
CN201810424727.0A 2018-05-07 2018-05-07 A kind of apple fresh-keeping agent and preparation method thereof Withdrawn CN108617763A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810424727.0A CN108617763A (en) 2018-05-07 2018-05-07 A kind of apple fresh-keeping agent and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201810424727.0A CN108617763A (en) 2018-05-07 2018-05-07 A kind of apple fresh-keeping agent and preparation method thereof

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CN108617763A true CN108617763A (en) 2018-10-09

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110201749A (en) * 2019-05-24 2019-09-06 安徽雁飞粮油有限责任公司 A kind of wheat treatment process improving Flour colour stability
CN112970493A (en) * 2021-02-25 2021-06-18 陕西品物皆春生态科技有限公司 Humic acid-polyglutamic acid fruit mask and using method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110201749A (en) * 2019-05-24 2019-09-06 安徽雁飞粮油有限责任公司 A kind of wheat treatment process improving Flour colour stability
CN112970493A (en) * 2021-02-25 2021-06-18 陕西品物皆春生态科技有限公司 Humic acid-polyglutamic acid fruit mask and using method thereof
CN112970493B (en) * 2021-02-25 2024-01-26 陕西品物皆春生态科技有限公司 Humic acid-polyglutamic acid fruit mask and application method thereof

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Application publication date: 20181009